JP4493592B2 - PET bottle sterilization method and apparatus - Google Patents

Description

  The present invention relates to a method and apparatus for sterilizing PET bottles for beverages.

As a method of sterilizing a container such as a bottle applied to an aseptic filling machine, a method of sterilizing a container by spraying an aqueous solution of peracetic acid or hydrogen peroxide on the container as disclosed in, for example, Japanese Patent No. 2851373 is known. Yes. Japanese Patent Laid-Open No. 3-224469 discloses that hydrogen peroxide sprayed in a chamber is heated and vaporized, and then hydrogen peroxide is condensed in air to form a bactericide mist. A method for sterilization by contacting with a liquid is disclosed.
Japanese Patent No. 2851373 JP-A-3-224469

  As an aseptic filling system for PET bottles and the like, there is an in-line type system that consistently performs from bottle molding to filling of contents on the same line. In this system, a processing capacity of about 500 to 1000 bottles per minute is desired, and in order to achieve this, reduction of the time required for bottle sterilization is a problem. However, the conventional method of spraying hydrogen peroxide water uses high-concentration hydrogen peroxide, so the sterilization ability is sufficient, but hydrogen peroxide adsorbs and penetrates into the surface of the plastic container, The removal takes time and the sterilization process cannot be shortened.

An object of this invention is to provide the sterilization method which can sterilize various PET bottles rapidly and reliably, and an apparatus suitable for it.

  The present invention will be described below. In order to facilitate understanding of the present invention, reference numerals in the accompanying drawings are appended in parentheses, but the present invention is not limited to the illustrated embodiment.

The present invention is, in terms of its tip nozzle is inserted into the PET bottle to be positioned in the transition region of the diameter of the PET bottle, the entire PET bottle by blowing hot air into the PET bottle from the nozzle tip A preheating step of heating the entire PET bottle to a desired temperature by blowing hot air from the outside to the mouth of the PET bottle, which is difficult to rise in temperature, and condenses after vaporizing hydrogen peroxide droplets once A step of generating hydrogen peroxide mist, a sterilization step of introducing the hydrogen peroxide mist into the preheated PET bottle to sterilize the inner surface of the PET bottle, and PET having the inner surface sterilized Hot air is sent into the bottle, and the PET bottle is heated with the hot air to enhance the sterilization effect by the hydrogen peroxide mist, so that hydrogen peroxide penetrates into the PET bottle. A step of discharging the mist drifting in the PET bottle out of the PET bottle, and a step of cleaning the inside of the PET bottle by introducing a heated cleaning liquid into the PET bottle from which the mist has been discharged. A PET bottle sterilization method comprising:

  In addition, the nozzle is inserted into the PET bottle so that its tip is positioned in the transition region of the diameter of the PET bottle, and hot air is blown into the PET bottle from the tip of the nozzle to heat the entire PET bottle. In addition, a preheating step of heating the entire PET bottle to a desired temperature by blowing hot air from the outside to the mouth portion of the PET bottle, which is difficult to rise in temperature, and once the hydrogen peroxide droplets are vaporized, they are condensed. A step of generating hydrogen oxide mist, a step of introducing the hydrogen peroxide mist into the pre-heated PET bottle and sterilizing the inner surface of the PET bottle, and introducing the mist for a predetermined holding time. After placing, hot air is sent into the PET bottle, and the PET bottle is heated with the hot air to enhance the sterilization effect by hydrogen peroxide mist. A PET bottle which suppresses penetration into the bottle and discharges the mist drifting in the PET bottle to the outside of the PET bottle and introduces a heated cleaning liquid into the PET bottle from which the mist has been discharged. A PET bottle sterilization method comprising a step of cleaning the inside is adopted.

  In addition, the nozzle is inserted into the PET bottle so that its tip is positioned in the transition region of the diameter of the PET bottle, and hot air is blown into the PET bottle from the tip of the nozzle to heat the entire PET bottle. In addition, a preheating step of heating the entire PET bottle to a desired temperature by blowing hot air from the outside to the mouth portion of the PET bottle, which is difficult to rise in temperature, and once the hydrogen peroxide droplets are vaporized, they are condensed. A step of generating hydrogen oxide mist, a sterilization step of sterilizing the inner surface of the PET bottle by introducing the mist of hydrogen peroxide into the preheated PET bottle, and a PET bottle having the inner surface sterilized Hot air is sent into the inside, and the PET bottle is heated with the hot air to enhance the sterilization effect by the hydrogen peroxide mist, thereby suppressing the penetration of hydrogen peroxide into the PET bottle. Then, a step of discharging the mist drifting in the PET bottle to the outside of the PET bottle, and a predetermined waiting time after discharging the mist, introducing a cleaning solution heated in the PET bottle to introduce the PET bottle A PET bottle sterilization method comprising a step of cleaning the inside is adopted.

  Since the hydrogen peroxide mist is generated by once vaporizing hydrogen peroxide droplets and condensing, it has a high concentration and can be sterilized efficiently. After the mist is introduced, the sterilizing effect is improved by heating the PET bottle, and at the same time, the permeation of hydrogen peroxide into the PET bottle is suppressed and the hydrogen peroxide easily floats on the surface of the PET bottle. In addition, by discharging the mist drifting in the interior space of the PET bottle, excess hydrogen peroxide is prevented from adhering to the inner surface of the PET bottle from the viewpoint of the sterilization effect, and the hydrogen peroxide to the PET bottle is Can be more effectively suppressed. Then, by washing the PET bottle after discharging the mist, the hydrogen peroxide adsorbed and permeated into the PET bottle can be washed away to reduce the residual concentration of hydrogen peroxide to the minimum.

  The sterilization method of the present invention may include a step of preheating the PET bottle prior to the introduction of the mist. By performing preheating, a high sterilization effect can be exhibited from the beginning of the mist introduction, and sterilization can be performed efficiently in a short time. The penetration of hydrogen peroxide into the PET bottle can be more effectively suppressed.

  In the preliminary heating step, in addition to heating the entire PET bottle, the mouth portion (1a) of the PET bottle may be separately heated. Alternatively, in the preliminary heating step, hot air may be sent into the PET bottle to heat the entire PET bottle, and the mouth (1a) of the PET bottle may be separately heated. Since the mouth is less likely to rise in temperature compared to other parts, the effect of the preheating can be more effectively brought out by heating this part separately. The supply of hot air into the PET bottle is preferably performed from a nozzle inserted in the PET bottle. The mouth can be heated by, for example, a method of blowing hot air from the outside of the mouth.

  In the sterilization method of the present invention, a predetermined holding time may be provided after the introduction of the mist and before the discharge of the mist is started. By providing the holding time, the mist can be brought into uniform contact with the inner surface of the PET bottle and can be sterilized reliably. The holding time can also be used as the transportation time of the PET bottle from the step of introducing mist to the step of discharging mist.

  A predetermined waiting time may be provided after the discharge of the mist and before the cleaning of the PET bottle is started. If it does in this way, hydrogen peroxide can be made to float on the surface of a PET bottle reliably, and the cleaning effect can be improved. The waiting time can also be used as the transportation time of the PET bottle from the step of discharging the mist to the step of cleaning.

  In the sterilization method of the present invention, hot air may be sent to the PET bottle into which the mist has been introduced to heat the PET bottle and discharge the mist. In this way, it is possible to efficiently discharge the mist and heat the PET bottle.

  In the washing step, a heated washing solution may be introduced into the PET bottle. If the cleaning liquid is heated, the heat can promote the permeation of hydrogen peroxide to the surface of the PET bottle, and a high cleaning effect can be obtained.

  In the sterilization apparatus of the present invention, the nozzle is inserted into the PET bottle so that the tip thereof is located in the transition region of the diameter of the PET bottle, and then hot air is blown into the PET bottle from the tip of the nozzle. A preheating means for heating the whole PET bottle to a desired temperature by blowing hot air from another nozzle to the outside of the mouth of the PET bottle, which is difficult to rise in temperature, and a drop of hydrogen peroxide Means for condensing and generating hydrogen peroxide mist once vaporized, means for introducing the hydrogen peroxide mist into the preheated PET bottle, and sterilizing the PET bottle inner surface, Hot air is sent into a PET bottle whose inner surface is sterilized, and the PET bottle is heated with the hot air to enhance the sterilization effect by hydrogen peroxide mist. Means for suppressing penetration into the bottle and discharging the mist drifting in the PET bottle to the outside of the PET bottle, and introducing a heated cleaning liquid into the PET bottle from which the mist has been discharged Means for cleaning the inside of the bottle.

  In the PET bottle sterilization apparatus, the preliminary heating means, the sterilization means, the discharge means, and the cleaning means are sequentially arranged along a continuous turning path formed by a plurality of turntables, Pre-heating by blowing hot air to the bottle moving, sterilization by hydrogen peroxide mist generated after vaporizing hydrogen peroxide droplets, discharging hydrogen peroxide mist by blowing hot air and hydrogen peroxide You may make it perform washing | cleaning in order.

  According to these apparatuses, the mist of hydrogen peroxide is introduced into the PET bottle, and the mist is discharged from the PET bottle while heating the PET bottle into which the mist has been introduced. Since the inside of the bottle can be washed, the sterilization method of the present invention can be realized.

  The sterilization apparatus of the present invention may include means for preheating the PET bottle prior to the introduction of the mist. As the preheating means, there may be provided means for sending hot air into the PET bottle to heat the whole PET bottle and means for heating the mouth of the PET bottle from the outside. As the means for washing, a means for introducing a heated washing solution into the PET bottle may be provided. The supply of hot air into the PET bottle is preferably performed from a nozzle inserted in the PET bottle.

  As described above, according to the sterilization method and apparatus of the present invention, the penetration of hydrogen peroxide into the PET bottle while heating the PET bottle introduced with the hydrogen peroxide mist to enhance the sterilization effect by the mist. In addition, the excess hydrogen peroxide mist drifting in the PET bottle is forcibly discharged to prevent hydrogen peroxide from penetrating into the PET bottle more effectively. Since the bottle is washed and the hydrogen peroxide absorbed and permeated into the PET bottle is washed away, it is possible to reliably sterilize the inner surface of the PET bottle in a short time while minimizing the residual concentration of hydrogen peroxide. it can.

  FIG. 1: has shown the outline | summary of the disinfection procedure of the bottle for drinks concerning one Embodiment of this invention. In this sterilization method, first, as shown in FIG. 1 (a), the nozzle 2 is inserted into the inside of the mouth 1a of the PET bottle 1, hot air is sent from the nozzle 2 and the bottle 1 is preheated. . At the same time, nozzles 3 and 3 are installed on the outer periphery of the mouth portion 1a of the bottle 1, and hot air is blown from the nozzles 3 to the mouth portion 1a to further heat the mouth portion 1a. This is because the mouth 1a may not be sufficiently heated by only the hot air from the nozzle 2. When the mouth 1a can be sufficiently heated only by hot air from the nozzle 2, the nozzle 3 may be omitted. The reason why the nozzle 2 is inserted into the bottle 1 is to reliably send hot air into the bottle 1. The insertion amount of the nozzle 2 may be appropriately changed according to the flow rate of hot air, the diameter of the mouth portion 1a, etc., but as shown in FIG. 2, the bottle provided between the mouth portion 1a and the body portion 1c of the bottle 1 The tip of the nozzle 2 may be positioned in the diameter transition region 1b. The transition region 1b can be defined as a range in which the bottle diameter expands to, for example, 70% of the maximum diameter from the lower end of the mouth 1a. The preheating is desirably performed so that the inner surface of the bottle 1 is 40 ° C. or higher.

The preheated bottle 1 is conveyed to a mist supply process. In the mist supply step, the mist of the disinfectant is supplied from the nozzle 4 to the inside of the bottle 1. The mist of the disinfectant is generated by, for example, a mist generator 33 shown in FIG. The generator 33 includes a bactericidal agent supply unit 35 that supplies an aqueous solution of hydrogen peroxide (H ₂ O ₂ ) as a bactericidal agent in the form of drops, and a hydrogen peroxide aqueous solution supplied from the bactericide supplying unit 35. And a vaporizing section 36 that vaporizes by heating to a boiling point or higher. The disinfectant supply unit 35 is provided with a spray 35a. The spray 35a is provided with a bactericidal agent supply port 35b and a compressed air supply port 35c, and these supply ports 35b and 35c are connected to a hydrogen peroxide supply source or a spray compressed air supply source (not shown).

  The aqueous solution of hydrogen peroxide and compressed air supplied from the supply ports 35b and 35c are mixed inside the two-fluid spray 35a, so that the vaporizer 36 is connected to the spray 35a and the nozzle 35d connected via the extension pipe 35e. An aqueous solution of hydrogen peroxide is sprayed into the vaporizing tube 37. The vaporizing pipe 37 is, for example, an outer cylinder 37a made of asbestos ribbon, an inner cylinder 37b made of a sanitary pipe forming the inner wall of the vaporizing pipe 37, and a heater as heating means provided between the outer cylinder 37a and the inner cylinder 37b. 37c. The nozzle 4 described above is connected to the discharge port 37 d at the lower end of the vaporizing tube 37.

  Drop-like hydrogen peroxide supplied to the inside of the vaporizing tube 37 is vaporized by the heat of the heater 37c. The vaporized hydrogen peroxide is liquefied again by the temperature drop until it is led to the vicinity of the bottle 1 through the nozzle 4. As a result, hydrogen peroxide mist finer than the hydrogen peroxide droplets generated by the two-fluid spray 35a is generated. By introducing the mist hydrogen peroxide into the inside of the bottle 1, the inner surface of the bottle 1 comes into contact with the hydrogen peroxide and is sterilized. It should be noted that the amount of hydrogen peroxide mist attached to one bottle having a capacity of 500 ml is preferably in the range of 5 μl to 100 μl in terms of a 35 wt% hydrogen peroxide solution. That is, the amount of mist is set so that hydrogen peroxide equivalent to when hydrogen peroxide solution containing 35% by weight of hydrogen peroxide is supplied into the bottle in the range of 5 μl to 100 μl adheres to the bottle 1. Is preferred. The blowing time of mist is preferably in the range of 0.1 second to 1 second with respect to one bottle. The concentration of hydrogen peroxide contained in the generated mist is preferably 35% by weight or more. The bactericidal agent is not limited to hydrogen peroxide, and various chemicals having a bactericidal action can be used.

  After supplying the mist, the bottle 1 is conveyed to the hot air supply process. During conveyance, the bottle 1 is held for a predetermined time with the bactericide mist introduced therein. In the hot air supply process, the nozzle 5 is inserted into the bottle 1, and hot air is sent from the nozzle 5. The bottle 1 is heated from the inner surface by hot air, the sterilizing effect by the sterilizing agent mist is enhanced, and the permeation of hydrogen peroxide into the bottle 1 is suppressed, so that the hydrogen peroxide easily floats on the inner surface of the bottle 1. Furthermore, the mist drifting inside the bottle 1 is discharged out of the bottle 1 by hot air. At this point, since the sterilization is sufficiently performed by the sterilizing agent mist attached to the inner surface of the bottle 1, the sterilizing effect is not impaired even if the mist drifting in the inner space of the bottle 1 is discharged. By discharging the mist at an early stage, there is an advantage that excessive permeation of hydrogen peroxide into the inner surface of the bottle 1 can be suppressed and cleaning in the subsequent process can be completed in a short time.

  The holding time after the introduction of the bactericide mist until the start of hot air blowing is preferably in the range of 1.0 to 10 seconds. The hot air may be blown in a range in which all of the mist drifting inside the bottle 1 can be discharged, and about 1 second is sufficient for the time. When the temperature of the hot air is equal to or higher than the heat resistance temperature (for example, 60 ° C.) of the bottle 1, if the hot air blowing time is too long, the bottle 1 may be heated beyond the heat resistance temperature and may be deformed. It is desirable to insert the nozzle 5 up to the bottle diameter transition region 1b as in the preheating step.

  After the supply of hot air, the bottle 1 is conveyed to the cleaning process. During conveyance, the bottle 1 is held in a heated state for a predetermined time. And the bottle 1 is reversed up and down at the end of conveyance. In the cleaning process, the nozzle 6 is inserted into the bottle 1 and aseptic water heated from the nozzle 6 is fed as a cleaning liquid. Thereby, the hydrogen peroxide adhering to the inner surface of the bottle 1 is washed away. It is desirable to insert the nozzle 6 to a position overlapping the transition region 1b inside the bottle 1 as in the preheating process and the hot air supply process.

  The standby time until the start of the supply of sterile water after the supply of hot air is stopped is preferably in the range of 0.1 to 10 seconds. Sterile water may be at room temperature, but heating is preferable because it improves cleaning efficiency. The temperature of the cleaning liquid is preferably in the range of 40 ° C to 80 ° C. Since the permeation of hydrogen peroxide into the bottle 1 is suppressed in the hot air supply step described above, cleaning with sterile water can be completed in a short time. For example, a 500 ml bottle can be completed in about 3 seconds.

  FIG. 4 shows an example of an aseptic filling system using the sterilization method described above. The aseptic filling system has an aseptic chamber 10. Prior to filling the bottle 1 with the beverage, the inside of the sterile chamber 10 is subjected to a predetermined sterilization treatment. Thereafter, aseptic air filtered by a filter is constantly supplied into the chamber 10, and the inside of the chamber 10 is maintained at a positive pressure (a state higher than the atmospheric pressure).

  The aseptic chamber 10 is provided with an inlet 11 and an outlet 12 for the bottle 1. A bottle molded by a bottle molding machine (not shown) is transported along the transport line 13, taken into the chamber 10 from the introduction port 11, and further supplied to the outer surface sterilizer 15 via the turntable 14. The outer surface sterilizer 15 sterilizes the outer surface of the bottle 1 by bringing a mist of a disinfectant (hydrogen peroxide) into contact with the outer surface of the bottle 1 conveyed by the turntable 15a. A preheating zone 15b is provided in a part of the turning path of the turntable 15a. In the zone 15b, the nozzle 2 of FIG. 1A is inserted into the bottle 1, and hot air is sent into the bottle 1 while the nozzle 2 moves in synchronization with the bottle 1 to preheat the bottle 1. . If necessary, the zone 15b is also provided with a nozzle 3 for heating the mouth 1a.

  The bottle 1 whose outer surface is sterilized by the outer surface sterilizer 15 is then transferred to the turntable 16 a of the inner surface sterilizer 16. A holding zone 16b is provided in a part of the turning path of the turntable 16a, and the bottle 1 is held for a predetermined time by passing through the zone 16b. The bottle 1 that has passed through the holding zone 16b is guided to the internal sterilization zone 16c. A nozzle 4 (see FIG. 1B) for supplying hydrogen peroxide mist is provided in the internal sterilization zone 16c, and hydrogen peroxide mist is supplied from the nozzle 4 to the inside of the bottle 1. The bottle 1 that has passed through the internal sterilization zone 16 c is transferred to the turntable 17 a of the hot air supply machine 17.

  A holding zone 17b and a hot air blowing zone 17c are provided on the turning path of the turntable 17a. By passing through the holding zone 17b, the bottle 1 is held for a predetermined time while hydrogen peroxide mist is blown into the bottle 1. In the hot air blowing zone 17 c, the nozzle 5 of FIG. 1C is inserted into the bottle 1, and the hot air is sent into the bottle 1 while the nozzle 5 moves in synchronization with the bottle 1 to heat the bottle 1. The hydrogen peroxide mist inside is discharged.

  The bottle 1 that has passed through the hot air blowing zone 17 c is transferred to the turntable 19 a of the washing machine 19 through the turntable 18. A holding reversal zone 18a is provided between the hot air blowing zone 17c and the delivery point of the bottle 1 from the turntable 18 to the washing machine 19. As the bottle 1 passes through the holding reversal zone 18a, a predetermined waiting time is ensured between the blowing of hot air and the start of cleaning. Further, the bottle 1 is inverted up and down while passing through the holding inversion zone 18a.

  The nozzle 1 shown in FIG. 1D is inserted into the bottle 1 transferred to the turntable 19 a of the washing machine 19, and the aseptic water heated inside the bottle 1 while moving in synchronization with the bottle 1. Is sent to clean the inside of the bottle 1.

  The bottle 1 washed by the washing machine 19 is subsequently transferred to the turntable 21a of the filling machine 21 via the transfer turntable group 20. While the bottle 1 is conveyed along the turntable 21a, the bottle 1 is filled with a beverage. The bottle 1 filled with the beverage is guided to the lid closing machine 22. The capping machine 22 seals the bottle 1 by screwing a cap (not shown) into the mouth 1 a of the bottle 1. The cap tightener 22 is supplied with a sterilized cap through a cap sterilizer 24 from a cap feeder 23 installed outside the aseptic chamber 10. The bottle 1 sealed by the lid fastening machine 22 is carried out from the discharge port 12 to the outside of the aseptic chamber 10 by the transport line 25.

  In addition, this invention is not limited to the above embodiment, It can implement with a various form. The discharging of the mist from the bottle 1 and the heating of the bottle 1 may be performed by different means. For example, air may be sucked from the inside of the bottle 1 to discharge mist, and the bottle 1 may be heated by radiant heat from a heat source installed outside thereof. A hot air jet outlet may be provided at a position facing the inner surface of the mouth of the nozzle 2 so that the mouth 1a can be heated separately from the body 1c and the like. The present invention is not limited to PET bottles 1 for beverages, but can be used for sterilization of various PET containers. Preheating may be omitted. The hot air supply may be started immediately after the supply of the disinfectant mist is stopped. After removing mist by supplying hot air, cleaning may be started immediately.

  The sterilization treatment was carried out on the PET bottle (polyethylene terephthalate bottle) having a capacity of 500 ml while changing the detailed conditions according to the following procedure.

1. The bottle was preheated by supplying hot air of 0.1 m ^{3 /} min from a nozzle with an inner diameter of 10 mm into the bottle. The temperature of the hot air was set to 105 ° C. to 125 ° C. in the vicinity of the tip of the nozzle, and the insertion amount of the nozzle into the bottle was set to 30 mm. At the same time, hot air at 85 ° C. was blown from the nozzle with an inner diameter of 50 mm toward the mouth of the bottle at a flow rate of 0.1 m ³ per minute. Note that the number of nozzles for heating the mouth was two for one bottle. The hot air blowing time from each nozzle was set to 3 seconds. The temperature in the bottle after completion of the hot air blowing reached 50 ° C.

  2. After stopping the hot air blowing, the bottle was left for 1 second, and then hydrogen peroxide mist was blown into the bottle for 0.6 seconds. The amount of hydrogen peroxide attached to the inner surface of the bottle was 15 to 40 μl in terms of a 35 wt% hydrogen peroxide solution.

  3. After completion of the mist blowing, the bottle was left for 0.5 to 3.5 seconds. Thereafter, a nozzle was inserted into the bottle and hot air was blown in for 1 second. The inner diameter of the nozzle, the amount of insertion, the temperature and flow rate of hot air are the same as in preheating.

  4). After blowing hot air, the bottle was left for 1 to 3.5 seconds. Thereafter, the bottle was inverted, a nozzle with an inner diameter of 6 mm was inserted into the bottle, and aseptic water heated to 70 ° C. was sent in for 3 seconds to wash the inside of the bottle. The flow rate of sterile water was 8.5 liters per minute.

  Moreover, some processes were abbreviate | omitted and sterilized.

For each sterilization condition, sterilize 5 bottles with 10 ³ , 10 ⁴ , or 10 ⁵ Bacillus subtilis spores, and aseptically dispense tryptic soy bouillon medium into the bottles, and culture and sterilize The presence or absence of sex was evaluated. From the test results under each sterilization condition, the number of surviving bacteria is calculated stochastically by the most probable number (MPN), and the logarithmic value of the number of adherent bacteria and the number of surviving bacteria is obtained by the following formula and sterilized. The effect was evaluated.
Bactericidal effect = log (number of adherent bacteria / number of surviving bacteria)

The list of test results is shown in the following table.

  The residue determination, sterilization determination, and comprehensive determination are each evaluated in four stages, and are indicated by ◎, ○, Δ, and X in order from the best.

  The following points can be confirmed from the above table.

  Condition 3 and condition 7 differ in the amount of hydrogen peroxide mist adhered and the presence or absence of preheating. In conditions 2 and 6, the residual concentration of hydrogen peroxide is the same, and the presence or absence of preheating is different. From these results, it can be seen that the sterilization effect is higher when hydrogen peroxide mist is supplied after preheating. However, if the holding time after mist spraying is lengthened, the bactericidal effect is improved to a practically sufficient level.

  Next, when the conditions 2 and 8 or the conditions 3 and 9 are compared, even if the residual amount of hydrogen peroxide or the amount of hydrogen peroxide mist adhered is the same, after introducing the hydrogen peroxide mist into the bottle, It can be seen that the bactericidal effect is impaired when the holding time until the start of feeding is short.

  Conditions 10 and 11 omit the blowing of hot air after the introduction of mist. Comparing condition 3 and condition 10, it can be seen that the residual concentration of hydrogen peroxide increases if hot air blowing is omitted even if the amount of hydrogen peroxide mist adhered is the same. Comparing condition 2 and condition 11, it can be seen that when the residual concentration of hydrogen peroxide mist is the same, the bactericidal effect is insufficient if hot air blowing is omitted.

  In order to see the effect of heating the bottle mouth part in the preheating step, the mouth part was not heated from the outside in Condition 3, and the mouth part of the bottle was heated from the outside in Condition 5. As is clear from these comparisons, the bactericidal effect increases if the mouth is heated separately.

The figure which shows the outline | summary of the disinfection procedure of the PET bottles for drinks concerning one Embodiment of this invention. The figure which shows the state which inserted the nozzle in the bottle made from PET. The figure which shows the apparatus for producing | generating the mist of a disinfectant. The top view of the aseptic filling system which concerns on one Embodiment of this invention.

1 bottle (PET container)
DESCRIPTION OF SYMBOLS 1a Nozzle part 2 Preheating nozzle 3 Nozzle heating nozzle 4 Mist supply nozzle 5 Mist discharge nozzle 6 Cleaning liquid supply nozzle 10 Aseptic chamber 15 External sterilizer 15b Preheating zone 16 Internal sterilizer 16c Internal sterilization zone 17 Hot air supply machine 19 Washing machine 21 Filling machine 22 Capping machine 23 Cap feeder 24 Cap sterilizer 35 Disinfectant supply part 35a Two-fluid spray

Claims (5)

After inserting the nozzle into the PET bottle so that its tip is located in the transition region of the diameter of the PET bottle, hot air is blown into the PET bottle from the tip of the nozzle to heat the entire PET bottle , A preheating step of heating the whole PET bottle to a desired temperature by blowing hot air from the outside to the mouth portion of the PET bottle, which is difficult to rise in temperature, and once hydrogen peroxide droplets are evaporated, the hydrogen peroxide is condensed and hydrogenated. A mist generation step, a sterilization step of sterilizing an inner surface of the PET bottle by introducing the hydrogen peroxide mist into the preheated PET bottle, and a PET bottle with the inner surface sterilized. Sending hot air, heating the PET bottle with the hot air to enhance the sterilization effect by hydrogen peroxide mist, suppressing the penetration of hydrogen peroxide into the PET bottle, It comprises a step of discharging the mist drifting in the ET bottle out of the PET bottle, and a step of cleaning the inside of the PET bottle by introducing a heated cleaning liquid into the PET bottle from which the mist has been discharged. A PET bottle sterilization method characterized by the above.   After inserting the nozzle into the PET bottle so that its tip is located in the transition region of the diameter of the PET bottle, hot air is blown into the PET bottle from the tip of the nozzle to heat the entire PET bottle, A preheating step of heating the entire PET bottle to a desired temperature by blowing hot air from the outside to the mouth of the PET bottle, where the temperature is difficult to rise, and once hydrogen peroxide droplets are evaporated, the hydrogen peroxide is condensed and hydrogenated. The mist is generated, the hydrogen peroxide mist is introduced into the preheated PET bottle, the inner surface of the PET bottle is sterilized, and the mist is introduced for a predetermined holding time. Then, hot air is sent into the PET bottle, and the PET bottle is heated with the hot air to enhance the sterilization effect by the hydrogen peroxide mist. The step of discharging the mist drifting in the PET bottle to the outside of the PET bottle, and introducing the heated cleaning liquid into the PET bottle from which the mist has been discharged. A method for sterilizing PET bottles comprising the step of washing   After inserting the nozzle into the PET bottle so that its tip is located in the transition region of the diameter of the PET bottle, hot air is blown into the PET bottle from the tip of the nozzle to heat the entire PET bottle, A preheating step of heating the whole PET bottle to a desired temperature by blowing hot air from the outside to the mouth portion of the PET bottle, which is difficult to rise in temperature, and once hydrogen peroxide droplets are evaporated, the hydrogen peroxide is condensed and hydrogenated. A mist generation step, a sterilization step of sterilizing an inner surface of the PET bottle by introducing the hydrogen peroxide mist into the preheated PET bottle, and a PET bottle with the inner surface sterilized. Sending hot air, heating the PET bottle with the hot air to enhance the sterilization effect by hydrogen peroxide mist, suppressing the penetration of hydrogen peroxide into the PET bottle, A step of discharging the mist drifting in the ET bottle outside the PET bottle, and a predetermined waiting time after discharging the mist, introducing a warmed cleaning solution into the PET bottle, A PET bottle sterilization method comprising the steps of:   After inserting the nozzle into the PET bottle so that its tip is located in the transition region of the diameter of the PET bottle, hot air is blown into the PET bottle from the tip of the nozzle to heat the entire PET bottle, Preheating means for heating the whole PET bottle to a desired temperature by blowing hot air from the other nozzle to the outside of the mouth of the PET bottle, which is difficult to rise in temperature, and once hydrogen peroxide droplets are evaporated Means for generating hydrogen peroxide mist, means for introducing the hydrogen peroxide mist into the pre-heated PET bottle and sterilizing the inner surface of the PET bottle, and PET made with the inner surface sterilized Hot air is sent into the bottle, and the PET bottle is heated with the hot air to enhance the sterilization effect by the hydrogen peroxide mist, so that hydrogen peroxide can penetrate into the PET bottle. And a means for discharging the mist drifting in the PET bottle to the outside of the PET bottle and a means for cleaning the inside of the PET bottle by introducing a heated cleaning liquid into the PET bottle from which the mist has been discharged. A PET bottle sterilizer characterized by comprising:   The preliminary heating means, the sterilizing means, the discharging means, and the cleaning means are sequentially arranged along a continuous swirling path formed by a plurality of turntables, and hot air is applied to the bottle moving on the swirling path. Preheating by blowing, sterilization by hydrogen peroxide mist generated after vaporizing hydrogen peroxide droplets once, discharging hydrogen peroxide mist by blowing hot air, and cleaning hydrogen peroxide in order The PET bottle sterilization apparatus according to claim 4.

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