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セレンの定量分析方法
JP4351946B2
Japan
Description
translated from
工業排水試験方法(JIS K0102の67.1〜67.3),社団法人日本工業用水協会,1998年4月20日
Claims (3)
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translated from
- 試料に含まれるセレンの定量分析方法であって、
大気圧より大きい圧力の酸素雰囲気下において、吸収液が注入された耐圧容器内で試料を燃焼する工程と、
前記吸収液を回収し、過酸化物を添加した前記吸収液を加熱して前記吸収液に含まれる有機物を分解するとともにセレンを酸化させる工程と、
加熱分解した前記吸収液を放冷する工程と、
放冷した前記吸収液に還元剤を添加した混合溶液を煮沸し、前記セレンを還元する工程と、
煮沸還元した前記混合溶液を放冷する工程と、
放冷した前記混合溶液にマスキング剤を添加する工程と、
マスキング剤を添加した前記混合溶液に含まれる不純物を除去する工程と、
不純物を除去した前記混合溶液に含まれるセレンを測定する工程と、
を含むことを特徴とするセレンの定量分析方法。 - 前記混合溶液を煮沸還元する工程は、前記混合溶液を10分間以上煮沸し、前記セレンを還元することを特徴とする請求項1に記載のセレンの定量分析方法。
- 前記過酸化物が過マンガン酸カリウムであることを特徴とする請求項1又は2に記載のセレンの定量分析方法。