JP2007246364A - Lightweight foamed tile and method of producing the same - Google Patents

Lightweight foamed tile and method of producing the same Download PDF

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JP2007246364A
JP2007246364A JP2006074842A JP2006074842A JP2007246364A JP 2007246364 A JP2007246364 A JP 2007246364A JP 2006074842 A JP2006074842 A JP 2006074842A JP 2006074842 A JP2006074842 A JP 2006074842A JP 2007246364 A JP2007246364 A JP 2007246364A
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tile
producing
raw material
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concave
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Nobuyoshi Suzuki
信義 鈴木
Masatoshi Kato
正俊 加藤
Ariyoshi Kaita
有佳 貝田
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Inax Corp
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Inax Corp
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a lightweight foamed tile and a method of producing the same by which a difference in height between a recessed part and a projecting part of the uneven surface is made large. <P>SOLUTION: In the method of producing the lightweight foamed tile carried out by forming a tile raw material to form recessed and projecting parts on the surface, drying the formed body and firing, a foaming agent is previously blended in the tile raw material. It is preferable that the average value of the distance from the deepest part of the recessed part to the topmost part of the adjacent projecting part of the uneven surface is 1-50 mm and the average value of the difference in height between the deepest part of the recessed part and the topmost of the adjacent projecting part is 0.5-20 mm. <P>COPYRIGHT: (C)2007,JPO&INPIT

Description

本発明は、炭化珪素(SiC)などの発泡剤をタイル原料に配合し、焼成時に発泡させて軽量化させるようにした軽量発泡タイルと、その製造方法に関する。   The present invention relates to a lightweight foam tile in which a foaming agent such as silicon carbide (SiC) is blended in a tile raw material and foamed during firing to reduce the weight, and a method for manufacturing the same.

炭化珪素(SiC)などの発泡剤をタイル原料に配合し、焼成時に発泡させて軽量化させるようにした軽量発泡タイルの製造方法は既に公知である(例えば特開昭61−191577号)。   A method for producing a lightweight foam tile in which a foaming agent such as silicon carbide (SiC) is blended with a tile raw material and foamed during firing to reduce the weight is already known (for example, Japanese Patent Laid-Open No. 61-191577).

また、タイルを製造する場合に、成形体の表面を凹凸模様付きのローラで押圧して成形体の表面に凹凸模様を形成し、タイル表面に凹凸意匠を与えることも周知である(例えば特開平8−72046号の第0003段落)。
特開昭61−191577号 特開平8−72046号
In addition, when manufacturing a tile, it is also well known to form a concavo-convex pattern on the surface of the molded body by pressing the surface of the molded body with a roller with a concavo-convex pattern (for example, Japanese Patent Laid-Open No. 8-72046, paragraph 0003).
JP 61-191577 JP-A-8-72046

特開平8−72046号によると、タイル表面に凹凸模様が形成され、それなりの意匠性が与えられる。この模様はローラによって転圧されて形成されるものであるが、焼成時に凸部が焼き締まってその高さを減じ、凹凸の高低差が小さくなることがある。   According to Japanese Patent Laid-Open No. 8-72046, a concavo-convex pattern is formed on the tile surface, and a certain design property is given. This pattern is formed by rolling with a roller, but the convex portion may be baked down during firing to reduce its height, and the height difference of the unevenness may be reduced.

本発明は、上記従来の問題点を解決し、表面の凹凸の凹部と凸部との高低差を大きくすることができる軽量発泡タイル及びその製造方法を提供することを目的とする。   An object of the present invention is to solve the above-mentioned conventional problems, and to provide a lightweight foam tile that can increase the difference in height between the concave and convex portions on the surface and the manufacturing method thereof.

請求項1の軽量発泡タイルの製造方法は、表面に凹凸が形成されるようにタイル原料を成形し、成形体を乾燥後、焼成するタイルの製造方法において、該タイル原料に発泡剤を配合しておくことを特徴とするものである。   The method for manufacturing a lightweight foam tile according to claim 1 is a method for manufacturing a tile in which a tile raw material is molded so that irregularities are formed on the surface, and the molded body is dried and then fired. It is characterized by keeping.

請求項2の軽量発泡タイルの製造方法は、請求項1において、成形に際し成形体の表面にローラ又は金型の凹凸面を押し付けることにより前記凹凸を形成することを特徴とするものである。   According to a second aspect of the present invention, there is provided a method for producing a lightweight foam tile according to the first aspect, wherein the irregularities are formed by pressing an irregular surface of a roller or a mold against the surface of the molded body during molding.

請求項3の軽量発泡タイルの製造方法は、請求項1又は2において、製造されたタイルにあっては、凹凸の凹部の最深部から隣接する凸部の最頂部までの距離の平均値が1〜50mmであり、該凹部の最深部と、隣接する凸部の最頂部との高低差の平均値が0.5〜20mmであることを特徴とするものである。   In the method for manufacturing a lightweight foam tile according to claim 3, in the tile according to claim 1 or 2, the average value of the distance from the deepest part of the concave and convex concave parts to the top of the adjacent convex part is 1 The average value of the height difference between the deepest part of the concave part and the top part of the adjacent convex part is 0.5 to 20 mm.

請求項4の軽量発泡タイルの製造方法は、請求項1ないし3のいずれか1項において、前記タイルの嵩比重が1.10〜1.90であることを特徴とするものである。   A method for producing a lightweight foam tile according to a fourth aspect is characterized in that, in any one of the first to third aspects, the bulk specific gravity of the tile is 1.10 to 1.90.

発泡剤を配分して原料を成形し焼成して発泡軽量タイルを製造する場合、焼成工程において発泡剤からガスが発生する。このガスは、成形体(被焼成体)内を主として外側に移動する。   When a foamed light weight tile is manufactured by allocating a foaming agent to form a raw material and firing it, gas is generated from the foaming agent in the firing process. This gas moves mainly inside the molded body (sintered body) to the outside.

請求項1の軽量発泡タイルの製造方法によると、成形体の表面に凹凸が形成されており、成形体(被焼成物)内の凹部で発生したガスは凹部より外側に位置する凸部まで上昇し、凸部の膨張が凹部の膨張よりも大きくなる。この結果、凸部の焼成収縮(焼き締まり)が抑制され、表面に高低差の大きい凹凸が形成されたタイルが製造される。   According to the method for manufacturing a lightweight foam tile according to claim 1, irregularities are formed on the surface of the molded body, and the gas generated in the recesses in the molded body (fired article) rises to the convex portions located outside the concave portions. Then, the expansion of the convex portion is larger than the expansion of the concave portion. As a result, firing shrinkage (baking tightening) of the protrusions is suppressed, and a tile having unevenness with a large difference in height is produced on the surface.

請求項2の通り、この成形体の表面にローラ又は金型の凹凸面の押し付けにより凹凸を形成しておくと、凹凸の凸部はローラ又は金型で比較的軽度に押されて比較的低密度となっているため、焼成時の収縮率は大きいが、発泡剤により生じたガスが外側方向に向かうため、より外側に位置し、低所より低密度である凸部である部分に集まり、膨張し易くなる。一方、凹凸の凹部は、ローラ又は金型で比較的強く押されて比較的高密度となっているので、凸部に比べて膨張が小さくなる。この結果、タイル表面の凸部の膨張が凹部に比べて大きくなり、表面の凹凸の高低差が大きくなる。   If unevenness is formed on the surface of the molded body by pressing the uneven surface of the roller or mold as in claim 2, the uneven protrusion is relatively lightly pressed by the roller or mold and relatively low. Because of the density, the shrinkage rate during firing is large, but because the gas generated by the foaming agent goes outward, it is located on the outer side and gathers at the part that is a convex part that is lower in density than the low part, It becomes easy to expand. On the other hand, since the concave and convex portions are relatively strongly pressed by a roller or a mold and have a relatively high density, expansion is smaller than that of the convex portion. As a result, the expansion of the convex portion on the tile surface is larger than that of the concave portion, and the difference in level of the concave and convex portions on the surface is increased.

請求項3,5の通り、凹部の最深部と隣接する凸部との最頂部との高低差の平均値を1〜50mmとし、両者の水平距離の平均値を0.5〜20mmとすることにより、凹部と凸部との高低差が強調されたものとなる。なお最深部と隣接する凸部の最頂部との高低差とは最深部と隣接する凸部の最頂部からの最深部を含む平面までの垂線の長さをいう。   As in claims 3 and 5, the average value of the height difference between the deepest part of the concave part and the top part of the adjacent convex part is 1 to 50 mm, and the average value of both horizontal distances is 0.5 to 20 mm. Thus, the height difference between the concave portion and the convex portion is emphasized. The height difference between the deepest portion and the topmost portion of the adjacent convex portion refers to the length of a perpendicular line from the topmost portion of the convex portion adjacent to the deepest portion to the plane including the deepest portion.

請求項4の通り、比重が1.10〜1.90程度となるように適度に発泡させる場合、表面の凹部と凸部との高低差が強調された軽量発泡タイルが得られる。   As described in claim 4, when the foam is appropriately foamed so that the specific gravity is about 1.10 to 1.90, a lightweight foam tile in which the height difference between the concave and convex portions on the surface is emphasized is obtained.

以下、本発明についてさらに詳細に説明する。   Hereinafter, the present invention will be described in more detail.

本発明では、発泡剤を含むタイル原料を成形し、成形体を乾燥後、焼成して軽量発泡タイルを製造する方法において、成形に際し、好ましくは金型又はローラの押し付けにより成形体表面に凹凸を形成する。   In the present invention, in a method for producing a lightweight foamed tile by molding a tile raw material containing a foaming agent, drying the molded body, and firing it, the surface of the molded body is preferably uneven by pressing with a mold or a roller. Form.

このタイル原料としては、粘土40〜60重量部、ガラス10〜25重量部、長石25〜50重量部、発泡剤としてSiC0.01〜5重量部(合計で100重量部)が好適である。粘土としては、モンモリロナイト、カメリナイト、蛙目粘土、木節粘土などを用いることができるが、これに限定されない。ガラスとしては、窓ガラス、瓶ガラス、ブラウン管ガラスなどが好適である。なお、原料に、骨材としてシャモット、陶石、アルミナ、ジルコン等の耐火性原料を30wt%以下好ましくは10〜20%や、顔料を加えてもよい。   As the tile raw material, 40 to 60 parts by weight of clay, 10 to 25 parts by weight of glass, 25 to 50 parts by weight of feldspar, and 0.01 to 5 parts by weight of SiC (100 parts by weight in total) as the foaming agent are suitable. Examples of the clay include, but are not limited to, montmorillonite, camelinite, glazed clay, and kibushi clay. As the glass, window glass, bottle glass, CRT glass and the like are suitable. In addition, you may add a refractory raw material, such as chamotte, porcelain stone, an alumina, a zircon, 30 wt% or less, preferably 10-20%, and a pigment as an aggregate to a raw material.

発泡剤としては、炭化珪素に限らず、窒化珪素、窒化ボロン等の加熱によりガスを生じるものであればよい。この原料を湿式ボールミル等によって十分に細磨混合した後、好ましくは押出成形機で押出成形し、次いで好ましくは押出成形物の表面に凹凸模様付きローラを押し当て、成形物の表面に凹凸模様を形成する。この凹凸は、凹部と隣接する凸部との高低差が平均して1〜50mm特に5〜20mm程度であることが望ましい。また、凹凸の凹部から隣接する凸部の最頂部までの距離は、平均すると0.5〜20mm特に1〜5mm程度が好ましい。   The foaming agent is not limited to silicon carbide, and any foaming agent may be used as long as it generates gas by heating silicon nitride, boron nitride, or the like. This raw material is sufficiently finely mixed by a wet ball mill or the like, and then preferably extrusion-molded by an extruder, and then preferably presses a roller with a concavo-convex pattern on the surface of the extruded product to form a concavo-convex pattern on the surface of the molded product. Form. As for this unevenness | corrugation, it is desirable that the height difference of a convex part adjacent to a recessed part is 1-50 mm on the average, especially about 5-20 mm. In addition, the average distance from the concave and convex concave portions to the topmost portion of the adjacent convex portions is preferably about 0.5 to 20 mm, particularly about 1 to 5 mm.

この成形物を所定寸法に切断した後、乾燥し、次いで焼成する。この焼成にはローラーハースキルンやトンネル窯を用いることができるが、好ましくはトンネル窯を用いる。   The molded product is cut to a predetermined size, dried, and then fired. A roller hearth kiln or a tunnel kiln can be used for this firing, but a tunnel kiln is preferably used.

焼成温度は1100〜1300℃が好ましく、焼成時間は36〜48時間程度が好ましい。   The firing temperature is preferably 1100 to 1300 ° C., and the firing time is preferably about 36 to 48 hours.

タイルの寸法は1辺が50〜200mm程度の大きさであることが望ましい。   The size of the tile is desirably about 50 to 200 mm on one side.

上記の焼成により、嵩比重が1.10〜1.90程度の凹凸模様付きタイルが製造される。この凹凸模様は、ローラの転写模様に起因したものであるが、焼成に際し内部で発生したガスが凸部に集まり、凸部の焼成収縮が防止ないし抑制される結果、凹凸の高低差が強調されたものとなる。   By the above firing, a tile with a concavo-convex pattern having a bulk specific gravity of about 1.10 to 1.90 is produced. This uneven pattern is caused by the transfer pattern of the roller, but the gas generated inside during baking gathers at the convex part, and as a result of preventing or suppressing the firing shrinkage of the convex part, the uneven height difference is emphasized. It will be.

なお、本発明では、上記の原料を乾式プレス成形して成形体とし、これを焼成して発泡タイルを製造してもよい。この場合、金型に凹凸を形成しておくことにより、成形体の表面に凹凸を形成する。この凹凸の程度は上記と同様でよい。   In the present invention, the above-mentioned raw materials may be dry press-molded to form a molded body, which may be fired to produce a foam tile. In this case, unevenness is formed on the surface of the molded body by forming unevenness on the mold. The degree of the unevenness may be the same as described above.

実施例1
表1の通り、粘土44.9重量部、ガラス20重量部、長石35重量部、SiC0.1重量部をタイル原料として用いた。
Example 1
As shown in Table 1, 44.9 parts by weight of clay, 20 parts by weight of glass, 35 parts by weight of feldspar, and 0.1 parts by weight of SiC were used as tile raw materials.

この原料を湿式ボールミルで24時間、細磨、混合した後、フィルタープレスした。次いで混練した後、真空押出成形機によって幅50mm、厚さ11.5mmに連続的に押出成形し、次いで凹凸模様付きローラを押し当てて表面に凹凸を転写した。この成形体の表面における凹凸の凹部の最深部と隣接する凸部の最頂部との高低差は平均して1.8mmであり、両者間の距離は平均して7.0mmであった。これを長さ200mmにカットして成形体とした。乾燥後、トンネル窯にて1200℃×40時間焼成した。その結果、図1(a)、(b)に示すタイルが得られた。このタイル表面の凹凸は表1に示すものとなった。   This raw material was finely ground and mixed in a wet ball mill for 24 hours, and then subjected to filter press. Next, after kneading, the film was continuously extruded to a width of 50 mm and a thickness of 11.5 mm using a vacuum extrusion molding machine, and then a concavo-convex patterned roller was pressed to transfer the concavo-convex to the surface. The height difference between the deepest portion of the concave and convex portions of the concave and convex portions on the surface of this molded body and the top portion of the adjacent convex portion was 1.8 mm on average, and the distance between both was 7.0 mm on average. This was cut into a length of 200 mm to obtain a molded body. After drying, it was fired at 1200 ° C. for 40 hours in a tunnel kiln. As a result, the tiles shown in FIGS. 1A and 1B were obtained. The irregularities on the tile surface were as shown in Table 1.

なお、タイルの嵩比重は1.10であった。   The bulk specific gravity of the tile was 1.10.

実施例2
配合を表1の通りとしたこと以外は同様にしてタイルを製造した。このタイルの表面には、表1に示した凹凸模様が形成されていた。タイルの嵩比重は1.55であった。
Example 2
Tiles were produced in the same manner except that the formulation was as shown in Table 1. The uneven pattern shown in Table 1 was formed on the surface of the tile. The bulk specific gravity of the tile was 1.55.

比較例1
実施例1において、表1に示す配合とし、発泡剤を添加しないようにしたこと以外は同様にしてタイルを製造した。このタイルの表面には、表1に示す凹凸模様が形成されていた。タイルの嵩比重は2.10であった。
Comparative Example 1
A tile was produced in the same manner as in Example 1 except that the formulation shown in Table 1 was used and no foaming agent was added. The uneven pattern shown in Table 1 was formed on the surface of the tile. The bulk specific gravity of the tile was 2.10.

表1に示すこれらの結果の通り、SiCを混入していない比較例1とSiCを混入した実施例1及び実施例2との差は、厚みに対して8.2%及び4.2%であり、発泡剤を添加することにより、より顕著な凹凸を付与することができた。   As these results shown in Table 1, the difference between Comparative Example 1 in which no SiC was mixed and Example 1 and Example 2 in which SiC was mixed was 8.2% and 4.2% with respect to the thickness. Yes, by adding a foaming agent, more remarkable unevenness could be imparted.

Figure 2007246364
Figure 2007246364

表1より、本発明によると表面の凹凸の高低差が強調された軽量タイルが製造される。   From Table 1, according to the present invention, a lightweight tile in which the height difference of the surface irregularities is emphasized is manufactured.

実施例で製造したタイルの断面図と斜視図である。It is sectional drawing and the perspective view of the tile manufactured in the Example.

符号の説明Explanation of symbols

1 タイル   1 tile

Claims (4)

表面に凹凸が形成されるようにタイル原料を成形し、成形体を乾燥後、焼成するタイルの製造方法において、
該タイル原料に発泡剤を配合しておくことを特徴とする軽量発泡タイルの製造方法。
In the tile manufacturing method in which the tile raw material is molded so that irregularities are formed on the surface, and the molded body is dried and then fired,
A method for producing a lightweight foam tile, wherein a foaming agent is blended in the tile raw material.
請求項1において、成形に際し成形体の表面にローラ又は金型の凹凸面を押し付けることにより前記凹凸を形成することを特徴とするタイルの製造方法。   The method for manufacturing a tile according to claim 1, wherein the unevenness is formed by pressing an uneven surface of a roller or a mold against the surface of the molded body during molding. 請求項1又は2において、製造されたタイルにあっては、凹凸の凹部の最深部から隣接する凸部の最頂部までの水平距離の平均値が1〜50mmであり、該凹部の最深部と、隣接する凸部の最頂部との高低差の平均値が0.5〜20mmであることを特徴とする軽量発泡タイルの製造方法。   In the tile according to claim 1 or 2, in the manufactured tile, an average value of a horizontal distance from the deepest part of the concave and convex concave part to the topmost part of the adjacent convex part is 1 to 50 mm, and the deepest part of the concave part and The method for producing a lightweight foam tile, characterized in that the average value of the height difference from the top of the adjacent convex portions is 0.5 to 20 mm. 請求項1ないし3のいずれか1項において、前記タイルの嵩比重が1.10〜1.90であることを特徴とする軽量発泡タイルの製造方法。   The method for producing a lightweight foam tile according to any one of claims 1 to 3, wherein the tile has a bulk specific gravity of 1.10 to 1.90.
JP2006074842A 2006-03-17 2006-03-17 Lightweight foamed tile and method of producing the same Pending JP2007246364A (en)

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JP2011148676A (en) * 2009-12-22 2011-08-04 Lixil Corp Raw material for foamed lightweight tile, foamed lightweight tile and method for producing the same

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JPS5192818A (en) * 1975-02-12 1976-08-14
JPH042675A (en) * 1990-04-17 1992-01-07 Inax Corp Foamed flooring material for interior use and production thereof
JPH07133169A (en) * 1993-11-05 1995-05-23 Inax Corp Ceramic building material
JPH10273358A (en) * 1997-01-28 1998-10-13 Inax Corp Production of pottery product
JPH1129353A (en) * 1997-07-09 1999-02-02 Inax Corp Production of glazed foamed light weight tile
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* Cited by examiner, † Cited by third party
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JP2011148676A (en) * 2009-12-22 2011-08-04 Lixil Corp Raw material for foamed lightweight tile, foamed lightweight tile and method for producing the same

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