JP2003160836A - Drawable high-strength steel thin-sheet with burring property superior in shape freezability, and manufacturing method therefor - Google Patents

Drawable high-strength steel thin-sheet with burring property superior in shape freezability, and manufacturing method therefor

Info

Publication number
JP2003160836A
JP2003160836A JP2001360084A JP2001360084A JP2003160836A JP 2003160836 A JP2003160836 A JP 2003160836A JP 2001360084 A JP2001360084 A JP 2001360084A JP 2001360084 A JP2001360084 A JP 2001360084A JP 2003160836 A JP2003160836 A JP 2003160836A
Authority
JP
Japan
Prior art keywords
steel sheet
burring
steel
rolling
shape fixability
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2001360084A
Other languages
Japanese (ja)
Other versions
JP4028719B2 (en
Inventor
Tatsuo Yokoi
龍雄 横井
Teruki Hayashida
輝樹 林田
Natsuko Sugiura
夏子 杉浦
Takaaki Nakamura
隆彰 中村
Takehiro Nakamoto
武広 中本
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Corp
Original Assignee
Nippon Steel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to JP2001360084A priority Critical patent/JP4028719B2/en
Application filed by Nippon Steel Corp filed Critical Nippon Steel Corp
Priority to AT02800781T priority patent/ATE383452T1/en
Priority to US10/491,928 priority patent/US7503984B2/en
Priority to DE60224557.5T priority patent/DE60224557T4/en
Priority to PCT/JP2002/010386 priority patent/WO2003031669A1/en
Priority to CA2462260A priority patent/CA2462260C/en
Priority to ES02800781T priority patent/ES2297047T5/en
Priority to CNB028243153A priority patent/CN100347325C/en
Priority to DE60224557A priority patent/DE60224557D1/en
Priority to KR1020047005067A priority patent/KR100627429B1/en
Priority to TW091123026A priority patent/TWI236503B/en
Priority to EP02800781.3A priority patent/EP1444374B9/en
Publication of JP2003160836A publication Critical patent/JP2003160836A/en
Application granted granted Critical
Publication of JP4028719B2 publication Critical patent/JP4028719B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Abstract

<P>PROBLEM TO BE SOLVED: To provide a drawable high-strength steel thin-sheet with a burring property superior in shape freezability, and a manufacturing method therefor. <P>SOLUTION: The steel sheet comprises 0.01-0.1% C, 0.03% or less S, 0.005% or less N, 0.05-0.5% Ti in such a range as to satisfy Ti-48/12C-48/14N-48/32 S≥0%, and the balance Fe with unavoidable impurities, having 3 or more of an average random intensity ratio of X-rays for grains orientated in ä100}<011> to ä223}<110> on the sheet face in at least 1/2 thickness of the sheet, having 3.5 or less of an average random intensity ratio of X-rays for grains with three orientations of ä554}<225>, ä111}<112>, and ä111}<110>, having 1-3.5 of arithmetic average roughness Ra on at least one of both surfaces, and having the composition with a lubricating effect coated thereon. The manufacturing method therefor is also disclosed. <P>COPYRIGHT: (C)2003,JPO

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】本発明は、形状凍結性に優れ
る絞り可能なバーリング性高強度薄鋼板およびその製造
方法に関するものであり、特に、絞り成形に不利な集合
組織を有する鋼板においても良好な絞り性を得ることが
できる。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a burring high-strength thin steel sheet which is excellent in shape fixability and is capable of being drawn, and is particularly suitable for a steel sheet having a texture which is disadvantageous for drawing. The drawability can be obtained.

【0002】[0002]

【従来の技術】近年、自動車の燃費向上などのために軽
量化を目的として、Al合金等の軽金属や高強度鋼板の
自動車部材への適用が進められている。ただし、Al合
金等の軽金属は比強度が高いという利点があるものの鋼
に比較して著しく高価であるためその適用は特殊な用途
に限られている。従ってより広い範囲で自動車の軽量化
を推進するためには安価な高強度鋼板の適用が強く求め
られている。
2. Description of the Related Art In recent years, application of light metals such as Al alloys and high-strength steel sheets to automobile members has been promoted for the purpose of weight reduction in order to improve fuel efficiency of automobiles. However, although light metals such as Al alloys have the advantage of high specific strength, they are significantly more expensive than steel, so their application is limited to special applications. Therefore, in order to promote the weight reduction of automobiles in a wider range, it is strongly required to apply inexpensive high strength steel sheets.

【0003】しかしながら、高強度鋼板に曲げ変形を加
えると、加工後の形状はその高強度ゆえに、加工冶具の
形状から離れて加工前の形状の方向にもどりやすくな
る。加工を与えても元の形状の方向にもどろうとする現
象はスプリング・バックと呼ばれている。このスプリン
グ・バックが発生すると、狙いとする加工部品の形状が
得られない。従って、従来の自動車の車体では、主とし
て440MPa以下の高強度鋼板に限って使用されてき
た。自動車車体にとっては、490MPa以上の高強度
鋼板を使用して車体の軽量化を進めていく必要があるに
もかかわらず、スプリング・バックが少なく形状凍結性
の良い高強度鋼板が存在しないのが実状である。付け加
えるまでもなく、440MPa以下の高強度鋼板や軟鋼
板の加工後の形状凍結性を高めることは、自動車や家電
製品などの製品の形状精度を高める上で極めて重要であ
ることはいうまでもない。
However, when bending deformation is applied to a high-strength steel sheet, the shape after processing tends to return to the shape before processing apart from the shape of the processing jig because of its high strength. The phenomenon of returning to the direction of the original shape after processing is called spring back. When this spring back occurs, it is not possible to obtain the desired shape of the processed part. Therefore, in the conventional car body, it has been mainly used only for the high strength steel plate of 440 MPa or less. For automobile bodies, although it is necessary to use high-strength steel sheets of 490 MPa or higher to reduce the weight of the vehicle body, the reality is that there are no high-strength steel sheets with few spring backs and good shape fixability. Is. Needless to say, it is needless to say that improving the shape fixability of a high-strength steel plate or mild steel plate of 440 MPa or less after processing is extremely important for improving the shape accuracy of products such as automobiles and home appliances. .

【0004】特開平10−72644号公報には、圧延
面に平行な面における{200}集合組織の集積度が
1.5以上であることを特徴とするスプリング・バック
量(本発明での寸法精度)が小さいオーステナイト系ス
テンレス冷延鋼板が開示されている。しかし、フェライ
ト系鋼板のスプリングバック現象や壁そり現象を低減す
る技術については何ら記載されていない。
In Japanese Unexamined Patent Publication No. 10-72644, the amount of spring back (dimensions in the present invention is characterized in that the degree of accumulation of {200} texture in a plane parallel to the rolling surface is 1.5 or more. An austenitic stainless cold-rolled steel sheet with low accuracy is disclosed. However, it does not describe any technique for reducing the springback phenomenon and wall warpage phenomenon of ferritic steel sheets.

【0005】また、フェライト系ステンレス鋼のスプリ
ングバック量を小さくする技術として、特開2001−
32050号公報に板厚中央部の集合組織において板面
に平行な{100}面の反射X線強度比を2以上とする
発明が開示されている。しかし、この発明は壁そりの低
減に関しては何ら記載がなく、{100}<011>〜
{223}<110>方位群および壁そり低減のために
重要な方位である{112}<110>についても何ら
規定がない。
Further, as a technique for reducing the springback amount of ferritic stainless steel, Japanese Patent Laid-Open No. 2001-2001
Japanese Patent No. 325050 discloses an invention in which the reflected X-ray intensity ratio of the {100} plane parallel to the plate surface is 2 or more in the texture in the central part of the plate thickness. However, the present invention has no description about reduction of wall warpage, and {100} <011> ~
There is no regulation on {223} <110> direction group and {112} <110> which is an important direction for reducing wall warpage.

【0006】また、WO00/06791号にて形状凍
結性の向上を目的として、{100}面と{111}面
の比が1以上であるフェライト系薄鋼板を開示したが、
この発明には本発明のように{100}<011>〜
{223}<110>方位群、並びに{554}<22
5>、{111}<112>および{111}<110
>のX線ランダム強度比の値については記載されていな
いと同時に絞り性を向上させる技術については何ら開示
されていない。
Further, in WO00 / 06791, a ferrite thin steel sheet having a ratio of {100} plane to {111} plane of 1 or more was disclosed for the purpose of improving shape fixability.
In the present invention, like the present invention, {100} <011> ~
{223} <110> direction group, and {554} <22
5>, {111} <112> and {111} <110
The value of the X-ray random intensity ratio of> is not described, and at the same time, the technique for improving the drawability is not disclosed.

【0007】また、特開2001−64750号公報に
て、スプリングバック量を小さくする技術として板面に
平行な{100}面の反射X線強度比が3以上である冷
延鋼板を開示したが、この発明は板厚最表面での{10
0}面反射X線強度比を規定することを特徴としてお
り、本発明での規定である板厚1/2tでの{100}
<011>〜{223}<110>方位群の平均X線強
度比とはX線の測定位置が異なる。また{554}<2
25>、{111}<112>および{111}<11
0>方位についても何ら記載されていないと同時に絞り
性を向上させる技術については何ら開示されていない。
Further, Japanese Patent Laid-Open No. 2001-64750 discloses a cold rolled steel sheet having a reflected X-ray intensity ratio of 3 or more on the {100} plane parallel to the sheet surface as a technique for reducing the amount of springback. , The present invention is the thickest surface {10
0} surface reflection X-ray intensity ratio is specified, and {100} at a plate thickness of 1 / 2t, which is the specification in the present invention.
The X-ray measurement position is different from the average X-ray intensity ratio of the <011> to {223} <110> orientation groups. Also, {554} <2
25>, {111} <112> and {111} <11
No mention is made of 0> direction, and at the same time, there is no disclosure of a technique for improving drawability.

【0008】また、特開2000−297349号公報
には形状凍結性の良好な鋼板として、r値の面内異方性
Δrの絶対値が0.2以下である熱延鋼板が開示されて
いる。しかし、この発明は低降伏比化することによって
形状凍結性を向上させることを特徴としており、本発明
で述べているような思想に基づいた形状凍結性の向上を
目的とした集合組織制御に関しては、記載されていな
い。
Further, Japanese Unexamined Patent Publication No. 2000-297349 discloses a hot rolled steel sheet having an excellent in-plane anisotropy Δr of an r value of 0.2 or less as a steel sheet having a good shape fixability. . However, the present invention is characterized by improving the shape fixability by lowering the yield ratio, and regarding texture control for the purpose of improving the shape fixability based on the idea described in the present invention, ,Not listed.

【0009】[0009]

【発明が解決しようとする課題】そこで、本発明は、絞
り成形に不利な集合組織を有する鋼板においても良好な
絞り性を得るための形状凍結性に優れる絞り可能なバー
リング性高強度薄鋼板およびその製造方法を提供する。
すなわち、本発明は、絞り可能なバーリング性高強度薄
鋼板およびその鋼板を安価に安定して製造できる製造方
法を提供することを目的とするものである。
SUMMARY OF THE INVENTION Therefore, the present invention provides a burringable high strength thin steel sheet which is excellent in shape fixability so as to obtain good drawability even in a steel sheet having a texture which is disadvantageous for drawing and The manufacturing method is provided.
That is, an object of the present invention is to provide a burring high-strength thin steel sheet that can be drawn and a manufacturing method capable of stably manufacturing the steel sheet at low cost.

【0010】[0010]

【課題を解決するための手段】本発明者らは、現在通常
に採用されている製造設備により工業的規模で生産され
ている高強度薄鋼板の製造プロセスを念頭において、高
強度薄鋼板の形状凍結性と絞り性を両立すべく鋭意研究
を重ねた。その結果、少なくとも板厚の1/2厚におけ
る板面の{100}<011>〜{223}<110>
方位群のX線ランダム強度比の平均値が3以上かつ、
{554}<225>、{111}<112>および
{111}<110>の3方位のX線ランダム強度比の
平均値が3.5以下であり、少なくとも一方の鋼板表面
の算術平均粗さRaが1〜3.5である鋼板に潤滑効果
のある組成物が塗布されており、また、その鋼板の0〜
200℃における圧延方向およびその直角方向の摩擦係
数のうち少なくともその一つが0.05〜0.2である
ことが形状凍結性と絞り性の両立に非常に有効であるこ
とを新たに見出し、本発明をなしたものである。
The inventors of the present invention have taken into consideration the manufacturing process of the high-strength thin steel sheet that is produced on an industrial scale by the production equipment that is normally adopted at present, and the shape of the high-strength thin steel sheet. We have conducted intensive studies to achieve both freezing and squeezing properties. As a result, {100} <011> to {223} <110> of the plate surface at least ½ of the plate thickness
The average value of the X-ray random intensity ratio of the azimuth group is 3 or more, and
The average value of the X-ray random intensity ratio in the three directions of {554} <225>, {111} <112>, and {111} <110> is 3.5 or less, and the arithmetic mean roughness of at least one steel plate surface. A composition having a lubricating effect is applied to a steel plate having Ra of 1 to 3.5, and 0 to
It was newly found that at least one of the friction coefficients in the rolling direction at 200 ° C and in the direction perpendicular to the rolling direction is 0.05 to 0.2, which is very effective in achieving both shape fixability and drawability. It is an invention.

【0011】即ち、本発明の要旨は、以下の通りであ
る。 (1)質量%にて、 C =0.01〜0.1%、 S ≦0.03%、 N ≦0.005%、 Ti=0.05〜0.5% を含み、さらに Ti−48/12C−48/14N−48/32S≧0% を満たす範囲でTiを含有し、残部がFeおよび不可避
的不純物からなる鋼であって、少なくとも板厚の1/2
厚における板面の{100}<011>〜{223}<
110>方位群のX線ランダム強度比の平均値が3以上
かつ、{554}<225>、{111}<112>お
よび{111}<110>の3方位のX線ランダム強度
比の平均値が3.5以下であり、その表裏の表面のうち
少なくとも一方の算術平均粗さRaが1〜3.5である
鋼板に潤滑効果のある組成物が塗布されていることを特
徴とする形状凍結性に優れる絞り可能なバーリング性高
強度薄鋼板。
That is, the gist of the present invention is as follows. (1) In mass%, C = 0.01 to 0.1%, S ≦ 0.03%, N ≦ 0.005%, Ti = 0.05 to 0.5% are included, and Ti-48 is further included. / 12C-48 / 14N-48 / 32S ≧ 0% Ti is contained, and the balance is Fe and unavoidable impurities.
{100} <011> to {223} <of the plate surface in thickness
The average value of the X-ray random intensity ratios of the 110> orientation group is 3 or more and the average value of the X-ray random intensity ratios of the three orientations of {554} <225>, {111} <112> and {111} <110>. Is 3.5 or less, and a composition having a lubricating effect is applied to a steel sheet having an arithmetic average roughness Ra of 1 to 3.5 on at least one of the front and back surfaces of the shape freezing. High strength thin steel plate with excellent burring properties that can be drawn.

【0012】(2)前記(1)に記載の鋼板表面の0〜
200℃における摩擦係数が0.05〜0.2であるこ
とを特徴とする形状凍結性に優れる絞り可能なバーリン
グ性高強度薄鋼板。
(2) 0 to 0 on the surface of the steel sheet described in (1) above
A burring-type high-strength steel sheet capable of being drawn, which is excellent in shape fixability and has a coefficient of friction of 0.05 to 0.2 at 200 ° C.

【0013】(3)前記(1)または(2)に記載の鋼
が、さらに、質量%にて、 Nb=0.01〜0.5% を含み、さらに Ti+48/93Nb−48/12C−48/14N−
48/32S≧0% を満たす範囲でTiとNbを含有し、残部がFeおよび
不可避的不純物からなる鋼であることを特徴とする形状
凍結性に優れる絞り可能なバーリング性高強度薄鋼板。
(3) The steel according to (1) or (2) above further contains, in mass%, Nb = 0.01 to 0.5%, and further Ti + 48 / 93Nb-48 / 12C-48. / 14N-
A drawable burring high-strength thin steel sheet having excellent shape fixability, which is a steel containing Ti and Nb in a range satisfying 48 / 32S ≧ 0% and the balance being Fe and inevitable impurities.

【0014】(4)前記(1)ないし(3)のいずれか
1項に記載の鋼が、さらに、質量%にて、Si=0.0
1〜2%、 Mn=0.05〜3%、 P ≦0.1%、 Al=0.005〜1% を含有することを特徴とする形状凍結性に優れる絞り可
能なバーリング性高強度薄鋼板。
(4) The steel according to any one of the above items (1) to (3) further contains Si = 0.0% by mass.
1 to 2%, Mn = 0.05 to 3%, P ≤ 0.1%, Al = 0.005 to 1%, excellent shape fixability, squeezable burring property, high strength and thinness steel sheet.

【0015】(5)前記(1)ないし(4)のいずれか
1項に記載の鋼が、さらに、質量%にて、 B =0.0002〜0.002% を含有することを特徴とする形状凍結性に優れる絞り可
能なバーリング性高強度薄鋼板。
(5) The steel according to any one of (1) to (4) above is characterized by further containing B = 0.0002 to 0.002% in mass%. A burring, high-strength thin steel sheet with excellent shape-freezing properties that can be drawn.

【0016】(6)前記(1)ないし(5)のいずれか
1項に記載の鋼が、さらに、質量%にて、 Cu=0.2〜1.2% を含有することを特徴とする形状凍結性に優れる絞り可
能なバーリング性高強度薄鋼板。
(6) The steel according to any one of (1) to (5) above is characterized by further containing Cu = 0.2 to 1.2% in mass%. A burring, high-strength thin steel sheet with excellent shape-freezing properties that can be drawn.

【0017】(7)前記(1)ないし(6)のいずれか
1項に記載の鋼が、さらに、質量%にて、 Ni=0.1〜0.6% を含有することを特徴とする形状凍結性に優れる絞り可
能なバーリング性高強度薄鋼板。
(7) The steel according to any one of (1) to (6) above is characterized by further containing, in mass%, Ni = 0.1 to 0.6%. A burring, high-strength thin steel sheet with excellent shape-freezing properties that can be drawn.

【0018】(8)前記(1)ないし(7)のいずれか
1項に記載の鋼が、さらに、質量%にて、 Ca=0.0005〜0.002%、REM=0.00
05〜0.02% の一種または二種を含有することを特徴とする形状凍結
性に優れる絞り可能なバーリング性高強度薄鋼板。
(8) The steel according to any one of the above (1) to (7) further contains, in mass%, Ca = 0.005 to 0.002% and REM = 0.00.
A burring burring high-strength thin steel sheet having excellent shape-freezing properties, characterized by containing 05 to 0.02% of one or two kinds.

【0019】(9)前記(1)ないし(8)のいずれか
1項に記載の鋼が、さらに、質量%にて、 Mo=0.05〜1%、 V =0.02〜0.2%、 Cr=0.01〜1%、 Zr=0.02〜0.2% の一種または二種以上を含有することを特徴とする形状
凍結性に優れる絞り可能なバーリング性高強度薄鋼板。
(9) The steel according to any one of the above (1) to (8), further in mass%, Mo = 0.05 to 1%, V = 0.02 to 0.2. %, Cr = 0.01 to 1%, Zr = 0.02 to 0.2%, and a burring high strength steel sheet having excellent shape fixability capable of being drawn.

【0020】(10)前記(1)ないし(9)のいずれ
か1項に記載の絞り可能なバーリング性高強度薄鋼板に
亜鉛めっきを施されていることを特徴とするの形状凍結
性に優れる絞り可能なバーリング性高強度薄鋼板。
(10) Excellent shape fixability, which is characterized in that the drawable burring high-strength steel sheet according to any one of (1) to (9) is galvanized. High strength thin steel plate with burring property that can be drawn.

【0021】(11)前記(1)ないし(9)のいずれ
か1項に記載の成分を有する薄鋼板を得るための熱間圧
延する際に、該成分を有する鋼片を粗圧延後にAr3 変
態点温度+100℃以下の温度域で鋼板厚の合計圧下率
25%以上の仕上圧延をし、その後冷却して巻き取った
後、潤滑効果のある組成物を塗布することを特徴とす
る、形状凍結性に優れる絞り可能なバーリング性高強度
薄鋼板の製造方法。
(11) During hot rolling to obtain a thin steel sheet having the composition described in any one of (1) to (9), a steel piece having the composition is subjected to Ar3 transformation after rough rolling. Shape freezing, characterized in that finish rolling with a total reduction of steel plate thickness of 25% or more in a temperature range of point temperature + 100 ° C or less, then cooling and winding, and then applying a composition having a lubricating effect. A method for producing a burring high-strength thin steel sheet which is excellent in drawability and which can be drawn.

【0022】(12)前記熱間圧延に際し、粗圧延後の
仕上圧延において潤滑圧延を施すことを特徴とする前記
(11)に記載の形状凍結性に優れる絞り可能なバーリ
ング性高強度薄鋼板の製造方法。
(12) In the hot rolling, lubrication rolling is performed in finish rolling after rough rolling, and the drawable burring high strength thin steel sheet excellent in shape fixability as described in (11) above. Production method.

【0023】(13)前記(11)または(12)に記
載の熱間圧延に際し、粗圧延終了後、デスケーリングを
行うことを特徴とする形状凍結性に優れる絞り可能なバ
ーリング性高強度薄鋼板の製造方法。
(13) In the hot rolling as set forth in (11) or (12) above, descaling is performed after the rough rolling is finished, and descaling is performed. Manufacturing method.

【0024】[0024]

【0025】(14)前記(1)ないし(9)のいずれ
か1項に記載の成分を有する薄鋼板を得るために該成分
を有する鋼片を熱間圧延、続く酸洗、鋼板厚圧下率80
%未満の冷間圧延後、回復温度以上Ac3 変態点温度+
100℃以下の温度域で5〜150秒間保持し、冷却す
る工程の熱処理をした後、潤滑効果のある組成物を塗布
することを特徴とする形状凍結性に優れる絞り可能なバ
ーリング性高強度薄鋼板の製造方法。
(14) In order to obtain a thin steel sheet having the composition described in any one of (1) to (9) above, a billet having the composition is hot-rolled, followed by pickling, and a steel plate thickness reduction rate. 80
After cold rolling of less than%, recovery temperature above Ac3 transformation point temperature +
Holding at a temperature range of 100 ° C. or lower for 5 to 150 seconds, and performing a heat treatment in a cooling step, and then applying a composition having a lubricating effect. Steel plate manufacturing method.

【0026】(15)前記(11)ないし(13)のい
ずれか1項に記載の製造方法に際し、熱間圧延後に亜鉛
めっき浴中に浸積させて鋼板表面を亜鉛めっきした後、
潤滑効果のある組成物を塗布することを特徴とする形状
凍結性に優れる絞り可能なバーリング性高強度薄鋼板の
製造方法。
(15) In the manufacturing method according to any one of (11) to (13), after hot rolling, the steel sheet surface is galvanized by being immersed in a galvanizing bath,
A method for producing a burring high-strength steel sheet capable of being drawn, which is excellent in shape fixability, characterized by applying a composition having a lubricating effect.

【0027】(16)前記(14)に記載の製造方法に
際し、熱処理終了後、亜鉛めっき浴中に浸積させて鋼板
表面を亜鉛めっきした後、潤滑効果のある組成物を塗布
することを特徴とする形状凍結性に優れる絞り可能なバ
ーリング性高強度薄鋼板の製造方法。
(16) In the manufacturing method described in (14) above, after the heat treatment is finished, the surface of the steel sheet is galvanized by being immersed in a galvanizing bath, and then a composition having a lubricating effect is applied. A method for producing a burring high-strength thin steel sheet which is excellent in shape fixability and which can be drawn.

【0028】(17)前記(15)または(16)に記
載の製造方法に際し、亜鉛めっき浴中に浸積して亜鉛め
っき後、合金化処理した後、潤滑効果のある組成物を塗
布することを特徴とする形状凍結性に優れる絞り可能な
バーリング性高強度薄鋼板の製造方法。
(17) In the production method according to (15) or (16), the composition having a lubricating effect is applied after dipping in a zinc plating bath for galvanizing and then alloying treatment. A method for producing a burring high strength steel sheet capable of being drawn, which is excellent in shape fixability.

【0029】[0029]

【発明の実施の形態】まず、前記(1)または(2)に
係わる本発明の詳細を説明する。優れた形状凍結性を得
るためには、1/2厚における板面の{100}<01
1>〜{223}<110>方位群のX線ランダム強度
比の平均値のは3以上でなくてはならない。これが3未
満であると形状凍結性が劣悪となる。
BEST MODE FOR CARRYING OUT THE INVENTION First, the details of the present invention relating to (1) or (2) above will be described. In order to obtain excellent shape fixability, {100} <01 of the plate surface at 1/2 thickness
The average value of the X-ray random intensity ratio of the 1> to {223} <110> orientation groups must be 3 or more. If this is less than 3, the shape fixability will be poor.

【0030】ここで、{100}<011>〜{22
3}<110>方位群のX線ランダム強度比の平均値と
は、この方位群に含まれる主な方位、{100}<01
1>、{116}<110>、{114}<110>、
{113}<110>、{112}<110>、{33
5}<110>および{223}<110>のX線回折
強度を{110}極点図に基づきベクトル法により計算
した3次元集合組織、または{110}、{100}、
{211}、{310}極点図のうち複数の極点図(望
ましくは3つ以上)を用いて級数展開法で計算した3次
元集合組織から求めた。
Here, {100} <011> to {22
3} The average value of the X-ray random intensity ratio of the <110> direction group is the main direction included in this direction group, {100} <01.
1>, {116} <110>, {114} <110>,
{113} <110>, {112} <110>, {33
5} <110> and {223} <110> X-ray diffraction intensities calculated by the vector method based on the {110} pole figure, or {110}, {100},
It was determined from a three-dimensional texture calculated by the series expansion method using a plurality of pole figures (preferably three or more) of the {211} and {310} pole figures.

【0031】例えば、後者の方法における上記各結晶方
位のX線ランダム強度比は、3次元集合組織のφ2=4
5゜断面における(001)[1−10]、(116)
[1−10]、(114)[1−10]、(113)
[1−10]、(112)[1−10]、(335)
[1−10]、(223)[1−10]の強度をそのま
ま用ればよい。ただし、{100}<011>〜{22
3}<110>方位群のX線ランダム強度比の平均値と
は、上記の各方位の相加平均である。上記全ての方位の
強度を得ることができない場合には、{100}<01
1>、{116}<110>、{114}<110>、
{112}<110>、{223}<110>の各方位
の相加平均で代替してもよい。
For example, the X-ray random intensity ratio of each crystal orientation in the latter method is φ2 = 4 for a three-dimensional texture.
(001) [1-10], (116) at 5 ° cross section
[1-10], (114) [1-10], (113)
[1-10], (112) [1-10], (335)
The strengths of [1-10] and (223) [1-10] may be used as they are. However, {100} <011> to {22
3} The average value of the X-ray random intensity ratio of the <110> orientation group is the arithmetic average of the above orientations. If it is not possible to obtain the intensities in all of the above directions, {100} <01
1>, {116} <110>, {114} <110>,
You may substitute by the arithmetic mean of each direction of {112} <110> and {223} <110>.

【0032】さらに{554}<225>、{111}
<112>および{111}<110>の3方位のX線
ランダム強度比の平均値は3.5以下でなくてはならな
い。これが3.5超であると{100}<011>〜
{223}<110>方位群のX線ランダム強度比の平
均値が適正であっても良好な形状凍結性は得ることがで
きない。{554}<225>、{111}<112>
および{111}<110>の3方位のX線ランダム強
度比の平均値とは、上記の方法と同様に計算した3次元
集合組織から求めればよい。
Further, {554} <225>, {111}
The average value of the X-ray random intensity ratios in the three directions of <112> and {111} <110> must be 3.5 or less. If this exceeds 3.5, {100} <011> ~
Even if the average value of the X-ray random intensity ratio of the {223} <110> orientation group is appropriate, good shape fixability cannot be obtained. {554} <225>, {111} <112>
And the average value of the X-ray random intensity ratios in the three directions of {111} <110> may be obtained from the three-dimensional texture calculated in the same manner as the above method.

【0033】これら本発明の範囲はより望ましくは、
{100}<011>〜{223}<110>方位群の
X線ランダム強度比の平均値が4以上、{554}<2
25>、{111}<112>および{111}<11
0>のX線ランダム強度比の相加平均値が2.5未満で
ある。以上述べた結晶方位のX線強度が曲げ加工時の形
状凍結性に対して重要であることの理由は必ずしも明ら
かではないが、曲げ変形時の結晶のすべり挙動と関係が
あるものと推測される。
More preferably, the scope of the present invention is
The average value of the X-ray random intensity ratio of the {100} <011> to {223} <110> orientation groups is 4 or more, {554} <2.
25>, {111} <112> and {111} <11
The arithmetic mean value of the X-ray random intensity ratio of 0> is less than 2.5. The reason why the X-ray intensity of the crystal orientation described above is important for shape fixability during bending is not necessarily clear, but it is presumed that it is related to the slip behavior of the crystal during bending deformation. .

【0034】X線回折に供する試料を得るために、板幅
の1/4Wもしくは3/4W位置より30mmφに切り
取った試片に三山仕上の研削を行い、次いで化学研磨ま
たは電解研磨によって歪みを除去して作製する。なお、
{hkl}<uvw>で表される結晶方位とは、板面の
法線方向が<hkl>に平行で、圧延方向が<uvw>
と平行であることを示している。X線による結晶方位の
測定は、例えば新版カリティX線回折要論(1986年
発行、松村源太郎訳、株式会社アグネ)274〜296
頁に記載の方法に従う。
In order to obtain a sample to be subjected to X-ray diffraction, a test piece cut to 30 mmφ from a position of 1/4 W or 3/4 W of the plate width is ground with three peaks, and then strain is removed by chemical polishing or electrolytic polishing. To produce. In addition,
The crystal orientation represented by {hkl} <uvw> means that the normal direction of the plate surface is parallel to <hkl> and the rolling direction is <uvw>.
It is shown to be parallel to. The crystal orientation measurement by X-ray can be performed, for example, by the new edition of the Kariti X-ray diffraction theory (published in 1986, translated by Gentaro Matsumura, Agne Co., Ltd.) 274-296
Follow the method described on page.

【0035】次に本発明において絞り性を確保する上で
重要な鋼板表面の状態について説明する。本発明におい
て、潤滑効果のある組成物が塗布されている以前の鋼板
表裏の表面のうち、少なくとも一方の算術平均粗さRa
が1以上3.5以下とする。この算術平均粗さRaが1
未満であると後に塗布される潤滑効果のある組成物を鋼
板表面に保持することが困難になる。一方、算術平均粗
さRaが3.5超であると潤滑効果のある組成物が塗布
されても十分な潤滑効果が得られない。従って、鋼板表
裏の表面のうち、少なくとも一方の算術平均粗さRaが
1〜3.5とする。望ましくは1〜3である。ここで、
算術平均粗さRaとはJIS B0601−1994に
記載されている算術平均粗さRaのことである。
Next, the state of the steel sheet surface, which is important for ensuring the drawability in the present invention, will be described. In the present invention, the arithmetic mean roughness Ra of at least one of the front and back surfaces of the steel sheet before being coated with the composition having a lubricating effect
Is 1 or more and 3.5 or less. This arithmetic average roughness Ra is 1
If the amount is less than the range, it becomes difficult to retain the composition having a lubricating effect applied later on the surface of the steel sheet. On the other hand, if the arithmetic average roughness Ra exceeds 3.5, a sufficient lubricating effect cannot be obtained even if a composition having a lubricating effect is applied. Therefore, at least one of the front and back surfaces of the steel sheet has an arithmetic average roughness Ra of 1 to 3.5. It is preferably 1 to 3. here,
The arithmetic average roughness Ra is the arithmetic average roughness Ra described in JIS B0601-1994.

【0036】さらに、潤滑効果のある組成物が塗布され
た後の鋼板の0〜200℃における圧延方向およびその
直角方向の摩擦係数のうち少なくともその一つは0.0
5以上0.2以下とする。摩擦係数が0.05未満であ
るとプレス成形時に形状凍結性を向上させるためにしわ
押さえ力(BHF:Blank Holding Fo
rce)を増加させても鋼板が保持できずに流れ込んで
しまい形状凍結性が劣化する。
Furthermore, at least one of the coefficient of friction in the rolling direction at 0 to 200 ° C. and the direction perpendicular thereto of the steel sheet after the composition having the lubricating effect is applied is 0.0.
It is set to 5 or more and 0.2 or less. If the coefficient of friction is less than 0.05, the crease holding force (BHF: Blank Holding Fo) is increased in order to improve shape fixability during press molding.
(rce) is increased, the steel sheet cannot be held and flows in, deteriorating the shape fixability.

【0037】一方、摩擦係数が0.2超ではしわ押さえ
力(BHF:Blank Holding Forc
e)を実用的範囲で低減しても鋼板の流れ込みが低下す
るため絞り加工性が低下する恐れがある。従って、摩擦
係数は少なくともその一つは0.05〜0.2とする。
On the other hand, when the coefficient of friction exceeds 0.2, the wrinkle holding force (BHF: Blank Holding Force) is increased.
Even if e) is reduced within a practical range, the flowability of the steel sheet is reduced, and therefore drawability may be reduced. Therefore, at least one of the friction coefficients is 0.05 to 0.2.

【0038】また、摩擦係数を限定している温度域であ
るが、0℃未満では霜等が付着し正当な評価が不可能に
なる。200℃超では鋼板表面に塗布した潤滑効果のあ
る組成物が不安定となる恐れがある。従って、摩擦係数
を限定している温度域は0〜200℃とする。
In the temperature range in which the coefficient of friction is limited, frost or the like adheres at temperatures below 0 ° C., making proper evaluation impossible. If it exceeds 200 ° C, the composition having a lubricating effect applied to the surface of the steel sheet may become unstable. Therefore, the temperature range limiting the friction coefficient is set to 0 to 200 ° C.

【0039】ここで、摩擦係数とは評価対象とする鋼板
表面に潤滑効果のある組成物を塗布した後、表面のビッ
カース硬さがHv600以上を有する2枚の平板の間に
挟み、面圧が1.5〜2kgf/mm2 となるように鋼
板表面に対して垂直の力(F)を与えたうえで、鋼板を
引き抜く。その際、Fに対する引き抜き力fの割合(f
/F)を摩擦係数と定義する。
Here, the friction coefficient means that after a composition having a lubricating effect is applied to the surface of a steel sheet to be evaluated, it is sandwiched between two flat plates having a Vickers hardness of Hv600 or more, and the surface pressure is A vertical force (F) is applied to the surface of the steel sheet so as to be 1.5 to 2 kgf / mm 2, and then the steel sheet is pulled out. At that time, the ratio of the pulling force f to F (f
/ F) is defined as the friction coefficient.

【0040】次に、鋼板の絞り性指標は、鋼板を円形に
加工した後、円筒ポンチで絞り成形を行った際に、絞り
抜け可能な最大径(D)を円筒ポンチ直径(d)で除し
た値(D/d)と定義する。この測定において、鋼板の
円形加工サイズは、300〜400φの種々の直径と
し、円筒ポンチ径は175φ、底面の肩部は10R、ダ
イス面の肩部は15Rの金型を用いて評価する。
Next, the drawability index of the steel sheet is obtained by dividing the maximum diameter (D) that can be drawn out by the cylindrical punch diameter (d) when the steel sheet is processed into a circular shape and then drawn using a cylindrical punch. Defined value (D / d). In this measurement, the circular processing size of the steel sheet is various diameters of 300 to 400φ, the diameter of the cylindrical punch is 175φ, the bottom shoulder portion is 10R, and the die surface shoulder portion is 15R.

【0041】次に本発明における鋼板のミクロ組織につ
いて説明する。鋼板のミクロ組織は、優れたバーリング
加工性(穴拡げ性)を確保するためにフェライト単相が
望ましい。ただし、必要に応じ一部ベイナイトを含むこ
とを許容するものである。なお、良好なバーリング加工
性を確保するためには、ベイナイトの体積分率は10%
以下が望ましい。ただし、不可避的なマルテンサイト、
残留オーステナイトおよびパーライトを含むことを許容
するものである。さらに、残留オーステナイト等の結晶
構造がbccでないものを含む場合は、それ以外の組織
の体積分率で換算したX線ランダム強度比が本発明の範
囲内であれば差し支えなく、本発明の効果が得られる。
なお、ここで言うフェライトとはベイニティックフェラ
イトおよびアシュキュラーフェライト組織も含む。ま
た、良好な疲労特性を確保するためには、粗大な炭化物
を含むパーライトの体積分率は5%以下が望ましい。ま
た、良好なバーリング性(穴拡げ性)を確保するために
は、残留オーステナイトおよびマルテンサイトを合わせ
た体積分率は5%未満が望ましい。
Next, the microstructure of the steel sheet according to the present invention will be described. The microstructure of the steel sheet is preferably a ferrite single phase in order to ensure excellent burring workability (hole expandability). However, some bainite may be included if necessary. In order to ensure good burring workability, the volume fraction of bainite is 10%.
The following is desirable. However, inevitable martensite,
It is allowed to contain residual austenite and perlite. Further, in the case where the crystal structure such as retained austenite is not bcc, the X-ray random intensity ratio converted by the volume fraction of the other structures may be within the range of the present invention, and the effect of the present invention can be obtained. can get.
The term "ferrite" used herein includes bainitic ferrite and ashular ferrite structures. Further, in order to secure good fatigue characteristics, it is desirable that the volume fraction of pearlite containing coarse carbides be 5% or less. Further, in order to secure good burring property (hole expandability), it is desirable that the volume fraction of residual austenite and martensite is less than 5%.

【0042】ここで、フェライト、ベイナイト、残留オ
ーステナイト、パーライト、マルテンサイトの体積分率
とは鋼板板幅の1/4Wもしくは3/4W位置より切出
した試料を圧延方向断面に研磨し、ナイタール試薬を用
いてエッチングし、光学顕微鏡を用い200〜500倍
の倍率で観察された板厚の1/4tにおけるミクロ組織
の面積分率で定義される。
Here, the volume fraction of ferrite, bainite, retained austenite, pearlite, and martensite means that a sample cut out from a position of 1/4 W or 3/4 W of the width of a steel plate is ground to a section in the rolling direction, and a Nital reagent is used. It is defined as the area fraction of the microstructure at 1/4 t of the plate thickness, which was etched and used under an optical microscope at a magnification of 200 to 500 times.

【0043】続いて、本発明の化学成分の限定理由につ
いて説明する。Cは、0.1%超含有していると加工性
および溶接性が劣化するので、0.1%以下とする。ま
た0.01%未満であると強度が低下するので0.01
%以上とする。
Next, the reasons for limiting the chemical components of the present invention will be explained. If the content of C exceeds 0.1%, the workability and weldability deteriorate, so the content is made 0.1% or less. If it is less than 0.01%, the strength will decrease, so 0.01
% Or more.

【0044】Sは、多すぎると熱間圧延時の割れを引き
起こすので極力低減させるべきであるが、0.03%以
下ならば許容できる範囲である。
If S is too large, it causes cracking during hot rolling, so it should be reduced as much as possible, but if it is 0.03% or less, it is within the allowable range.

【0045】Nは、Cよりも高温にてTiおよびNbと
析出物を形成し、Cを固定するのに有効なTiおよびN
bを減少させる。従って極力低減させるべきであるが、
0.005%以下ならば許容できる範囲である。
N forms a precipitate with Ti and Nb at a temperature higher than that of C and is effective for fixing C.
b is reduced. Therefore, it should be reduced as much as possible,
If it is 0.005% or less, it is in an allowable range.

【0046】Tiは、本発明における最も重要な元素の
一つである。すなわち、Tiは析出強化により鋼板の強
度上昇に寄与する。ただし、0.05%未満ではこの効
果が不十分であり、0.5%超含有してもその効果が飽
和するだけでなく合金コストの上昇を招く。従って、T
iの含有量は0.05%以上、0.5%以下とする。さ
らに、バーリング加工性を劣化させるセメンタイト等の
炭化物の原因となるCを析出固定し、バーリング加工性
の向上に寄与するためにはTi−48/12C−48/
14N−48/32S≧0%の条件を満たすことが必要
である。ここで、SおよびNはCよりも比較的高温域で
Tiと析出物を形成するのでTi≧48/12Cを確保
するためには必然的にTi−48/12C−48/14
N−48/32S≧0%の条件を満たすことが必要であ
る。
Ti is one of the most important elements in the present invention. That is, Ti contributes to the strength increase of the steel sheet by precipitation strengthening. However, if it is less than 0.05%, this effect is insufficient, and if it exceeds 0.5%, not only the effect is saturated but also the alloy cost is increased. Therefore, T
The content of i is 0.05% or more and 0.5% or less. Further, in order to contribute to the improvement of the burring workability by precipitating and fixing C, which causes carbides such as cementite, which deteriorates the burring workability, and contributing to the improvement of the burring workability, Ti-48 / 12C-48 /
It is necessary to satisfy the condition of 14N-48 / 32S ≧ 0%. Here, since S and N form precipitates with Ti in a relatively high temperature range than C, in order to secure Ti ≧ 48 / 12C, Ti-48 / 12C-48 / 14 is inevitable.
It is necessary to satisfy the condition of N-48 / 32S ≧ 0%.

【0047】Nbは、Tiと同様に析出強化により鋼板
の強度上昇に寄与する。また、結晶粒を細粒化してバー
リング加工性を改善する効果もある。ただし、0.01
%未満ではこの効果が不十分であり、0.5%超含有し
てもその効果が飽和するだけでなく合金コストの上昇を
招く。従って、Nbの含有量は0.01%以上、0.5
%以下とする。さらに、バーリング加工性を劣化させる
セメンタイト等の炭化物の原因となるCを析出固定し、
バーリング加工性の向上に寄与するためにはTi+48
/93Nb−48/12C−48/14N−48/32
S≧0%の条件を満たすことが必要である。ここで、N
bはTiよりも比較的低温で炭化物を形成するためTi
+48/93Nb≧48/12Cを確保するためには必
然的にTi+48/93Nb−48/12C−48/1
4N−48/32S≧0%の条件を満たすことが必要で
ある。
Nb, like Ti, contributes to the strength increase of the steel sheet by precipitation strengthening. It also has the effect of improving the burring workability by refining the crystal grains. However, 0.01
If it is less than 0.5%, this effect is insufficient, and if it exceeds 0.5%, not only the effect is saturated but also the alloy cost rises. Therefore, the content of Nb is 0.01% or more, 0.5
% Or less. Furthermore, C, which causes carbides such as cementite, which deteriorates burring workability, is precipitated and fixed,
To contribute to the improvement of burring workability, Ti + 48
/ 93Nb-48 / 12C-48 / 14N-48 / 32
It is necessary to satisfy the condition of S ≧ 0%. Where N
Since b forms carbides at a relatively lower temperature than Ti, Ti
In order to secure + 48 / 93Nb ≧ 48 / 12C, Ti + 48 / 93Nb-48 / 12C-48 / 1 is inevitable.
It is necessary to satisfy the condition of 4N-48 / 32S ≧ 0%.

【0048】Siは、固溶強化元素として強度上昇に有
効である。所望の強度を得るためには、0.01%以上
含有する必要がある。しかし、2%超含有すると加工性
が劣化する。そこで、Siの含有量は0.01%以上、
2%以下とする。
Si is effective as a solid solution strengthening element for increasing strength. To obtain the desired strength, it is necessary to contain 0.01% or more. However, if the content exceeds 2%, the workability deteriorates. Therefore, the Si content is 0.01% or more,
2% or less.

【0049】Mnは、固溶強化元素として強度上昇に有
効である。所望の強度を得るためには、0.05%以上
必要である。また、Mn以外にSによる熱間割れの発生
を抑制するTiなどの元素が十分に添加されない場合に
は、質量%で、Mn/S≧20となるMn量を添加する
ことが望ましい。一方、3%超添加するとスラブ割れを
生ずるため、3%以下とする。
Mn is effective as a solid solution strengthening element for increasing strength. In order to obtain the desired strength, 0.05% or more is necessary. When elements other than Mn, such as Ti, which suppress the occurrence of hot cracking due to S, are not sufficiently added, it is desirable to add the amount of Mn such that Mn / S ≧ 20 in mass%. On the other hand, if added in excess of 3%, slab cracking will occur, so the content should be 3% or less.

【0050】Pは、不純物であり低いほど望ましく、
0.1%超含有すると加工性や溶接性に悪影響を及ぼす
とともに疲労特性も低下させるので、0.1%以下とす
る。
P is an impurity and is preferably as low as possible.
If the content exceeds 0.1%, the workability and weldability are adversely affected and the fatigue properties are deteriorated, so the content is made 0.1% or less.

【0051】Alは、溶鋼脱酸のために0.005%以
上添加する必要があるが、コストの上昇を招くため、そ
の上限を1%とする。また、あまり多量に添加すると、
非金属介在物を増大させ伸びを劣化させるので、望まし
くは0.5%以下とする。
Although Al needs to be added in an amount of 0.005% or more for deoxidation of molten steel, it causes an increase in cost, so the upper limit is made 1%. Also, if you add too much,
Since non-metallic inclusions increase and elongation deteriorates, it is preferably 0.5% or less.

【0052】Bは、固溶C量の減少が原因と考えられる
Pによる粒界脆化を抑制することによって疲労限を上昇
させる効果があるので必要に応じ添加する。ただし、
0.0002%未満ではその効果を得るために不十分で
あり、0.002%超添加するとスラブ割れが起こる。
よって、Bの添加は、0.0002%以上、0.002
%以下とする。
B has the effect of increasing the fatigue limit by suppressing the grain boundary embrittlement due to P, which is considered to be caused by the decrease in the amount of solid solution C, so it is added as necessary. However,
If it is less than 0.0002%, it is insufficient to obtain the effect, and if it exceeds 0.002%, slab cracking occurs.
Therefore, the addition of B is 0.0002% or more and 0.002%.
% Or less.

【0053】Cuは、固溶状態で疲労特性を改善する効
果があるので必要に応じ添加する。ただし、0.2%未
満では、その効果は少なく、1.2%を超えて含有する
と巻取り中に析出して加工性を著しく劣化させる恐れが
ある。そこで、Cuの含有量は0.2〜1.2%の範囲
とする。
Cu has an effect of improving fatigue characteristics in a solid solution state, so Cu is added if necessary. However, if it is less than 0.2%, its effect is small, and if it exceeds 1.2%, it may be precipitated during winding and remarkably deteriorate the workability. Therefore, the Cu content is set in the range of 0.2 to 1.2%.

【0054】Niは、Cu含有による熱間脆性防止のた
めに必要に応じ添加する。ただし、0.1%未満ではそ
の効果が少なく、0.6%を超えて添加してもその効果
が飽和するので、0.1〜0.6%とする。
Ni is added as necessary to prevent hot embrittlement due to the inclusion of Cu. However, if less than 0.1%, the effect is small, and even if added over 0.6%, the effect is saturated, so 0.1 to 0.6% is set.

【0055】CaおよびREMは、破壊の起点となった
り、加工性を劣化させる非金属介在物の形態を変化させ
て無害化する元素である。ただし、0.0005%未満
添加してもその効果がなく、Caならば0.002%
超、REMならば0.02%超添加してもその効果が飽
和するのでCa=0.0005〜0.002%、REM
=0.0005〜0.02%添加することが望ましい。
[0056] Ca and REM are elements that change the form of non-metallic inclusions that become the starting point of fracture or deteriorate workability and render them harmless. However, even if added less than 0.0005%, it has no effect. If Ca, 0.002%
If it is more than REM, the effect will be saturated even if more than 0.02% is added, so Ca = 0.0005 to 0.002%, REM
= 0.0005 to 0.02% is desirable.

【0056】さらに、強度を付与するために、Mo、
V、Cr、Zrの析出強化もしくは固溶強化元素の一種
または二種以上を添加してもよい。ただし、それぞれ、
0.05%、0.02%、0.01%、0.02%未満
ではその効果を得ることができない。また、それぞれ、
1%、0.2%、1%、0.2%を超え添加してもその
効果は飽和する。
Further, in order to impart strength, Mo,
One or more of V, Cr and Zr precipitation strengthening or solid solution strengthening elements may be added. However,
If less than 0.05%, 0.02%, 0.01%, 0.02%, the effect cannot be obtained. Also, respectively
Even if added over 1%, 0.2%, 1%, 0.2%, the effect is saturated.

【0057】なお、これらを主成分とする鋼にSn、C
o、Zn、W、Mgを合計で1%以下含有しても構わな
い。しかしながら、Snは熱間圧延時に疵が発生する恐
れがあるので0.05%以下が望ましい。
In addition, Sn, C
The total content of o, Zn, W, and Mg may be 1% or less. However, Sn may be flawed during hot rolling, so 0.05% or less is preferable.

【0058】次に、本発明の製造方法の限定理由につい
て、以下に詳細に述べる。本発明は、鋳造後、熱間圧延
後冷却ままもしくは熱間圧延後、熱間圧延後冷却・酸洗
し冷延した後に熱処理、あるいは熱延鋼板もしくは冷延
鋼板を溶融めっきラインにて熱処理を施したまま、更に
はこれらの鋼板に別途表面処理を施すことによっても得
られる。
Next, the reasons for limiting the manufacturing method of the present invention will be described in detail below. The present invention, after casting, after hot rolling after cooling or after hot rolling, after hot rolling after cooling, pickling and cold rolling, heat treatment, or heat treatment of hot rolled steel sheet or cold rolled steel sheet in a hot dip line It can be obtained as it is, or by subjecting these steel plates to a separate surface treatment.

【0059】本発明において熱間圧延に先行する製造方
法は特に限定するものではない。すなわち、高炉や電炉
等による溶製に引き続き各種の2次製錬で目的の成分含
有量になるように成分調整を行い、次いで通常の連続鋳
造、インゴット法による鋳造の他、薄スラブ鋳造などの
方法で鋳造すればよい。原料にはスクラップを使用して
も構わない。連続鋳造よって得たスラブの場合には高温
鋳片のまま熱間圧延機に直送してもよいし、室温まで冷
却後に加熱炉にて再加熱した後に熱間圧延してもよい。
The production method prior to hot rolling in the present invention is not particularly limited. That is, after the smelting in a blast furnace, an electric furnace, etc., the components are adjusted in various secondary smelting so that the target component content is obtained, and then, in addition to ordinary continuous casting, ingot casting, thin slab casting, etc. It may be cast by the method. Scrap may be used as a raw material. In the case of a slab obtained by continuous casting, it may be directly sent to a hot rolling mill as it is as a high temperature slab, or may be reheated in a heating furnace after being cooled to room temperature and then hot rolled.

【0060】再加熱温度については特に制限はないが、
1400℃以上であると、スケールオフ量が多量になり
歩留まりが低下するので、再加熱温度は1400℃未満
が望ましい。また、1000℃未満の加熱はスケジュー
ル上操業効率を著しく損なうため、再加熱温度は100
0℃以上が望ましい。さらには、1100℃未満での加
熱はTiおよび/またはNbを含む析出物がスラブ中で
再溶解せず粗大化し析出強化能を失うばかりでなくバー
リング加工性にとって望ましいサイズと分布のTiおよ
び/またはNbを含む析出物が析出しなくなるので、再
加熱温度は1100℃以上が望ましい。
The reheating temperature is not particularly limited,
If it is 1400 ° C or higher, the scale-off amount increases and the yield decreases, so the reheating temperature is preferably lower than 1400 ° C. In addition, since heating below 1000 ° C. significantly impairs operating efficiency on schedule, the reheating temperature is 100
0 ° C or higher is desirable. Further, heating below 1100 ° C. not only causes precipitates containing Ti and / or Nb to coarsen without redissolving in the slab and loses precipitation strengthening ability, but also has Ti and / or Ti and / or a size and distribution desirable for burring workability. Since the precipitate containing Nb does not precipitate, the reheating temperature is preferably 1100 ° C or higher.

【0061】熱間圧延工程は、粗圧延を終了後、仕上げ
圧延を行うが、粗圧延終了後にデスケーリングを行う場
合は、鋼板表面での高圧水の衝突圧P(MPa)×流量
L(リットル/cm2 )≧0.0025の条件を満たす
ことが望ましい。
In the hot rolling step, finish rolling is carried out after the rough rolling is completed. When descaling is carried out after the rough rolling is completed, the collision pressure P (MPa) of the high-pressure water on the surface of the steel sheet x the flow rate L (liter). / Cm 2 ) ≧ 0.0025 is preferable.

【0062】鋼板表面での高圧水の衝突圧Pは以下のよ
うに記述される(「鉄と鋼」1991 vol.77
No.9 p1450参照)。 P(MPa)=5.64×P0 ×V/H2 ただし、 P0 (MPa):液圧力 V(リットル/min):ノズル流液量 H(cm):鋼板表面とノズル間の距離
The collision pressure P of high-pressure water on the surface of the steel sheet is described as follows ("Iron and Steel" 1991 vol.77).
No. 9 p1450). P (MPa) = 5.64 × P 0 × V / H 2 where P 0 (MPa): Liquid pressure V (liter / min): Nozzle flow rate H (cm): Distance between steel plate surface and nozzle

【0063】流量Lは以下のように記述される。 L(リットル/cm2 )=V/(W×v) ただし、 V(リットル/min):ノズル流液量 W(cm):ノズル当たり噴射液が鋼板表面に当たって
いる幅 v(cm/min):通板速度
The flow rate L is described as follows. L (liter / cm 2 ) = V / (W × v) However, V (liter / min): Nozzle flow amount W (cm): Width v (cm / min) where the jet liquid hits the steel plate surface per nozzle: Plate passing speed

【0064】衝突圧P×流量Lの上限は本発明の効果を
得るためには特に定める必要はないが、ノズル流液量を
増加させるとノズルの摩耗が激しくなる等の不都合が生
じるため、0.02以下とすることが望ましい。
The upper limit of the collision pressure P.times.the flow rate L does not have to be specified in order to obtain the effect of the present invention. However, if the flow rate of the nozzle liquid is increased, the wear of the nozzle becomes severe, and the like. It is desirable to set it to 0.02 or less.

【0065】さらに、仕上げ圧延後の鋼板の最大高さR
yが15μm(15μmRy,l2.5mm,ln1
2.5mm)以下であることが望ましい。これは、例え
ば金属材料疲労設計便覧、日本材料学会編、84ページ
に記載されている通り熱延または酸洗ままの鋼板の疲労
強度は鋼板表面の最大高さRyと相関があることから明
らかである。また、その後の仕上げ圧延はデスケーリン
グ後に再びスケールが生成してしまうのを防ぐために5
秒以内に行うのが望ましい。
Further, the maximum height R of the steel sheet after finish rolling
y is 15 μm (15 μm Ry, l2.5 mm, ln1
2.5 mm) or less is desirable. This is clear, for example, from the fact that the fatigue strength of a hot rolled or pickled steel sheet correlates with the maximum height Ry of the steel sheet surface as described in Metal Material Fatigue Design Handbook, edited by Japan Society of Materials, page 84. is there. In addition, the finish rolling after that is performed in order to prevent the scale from being generated again after the descaling.
It is desirable to do it within seconds.

【0066】さらに潤滑効果のある組成物が塗布し、摩
擦係数を低減させる効果を得るためには、仕上げ圧延後
の鋼板の算術平均粗さRaは3.5以下が望ましい。た
だし、熱間圧延後または酸洗後にスキンパス圧延もしく
は冷間圧延を施す場合はこの限りでない。
Further, in order to obtain the effect of reducing the friction coefficient by applying a composition having a lubricating effect, the arithmetic mean roughness Ra of the steel sheet after finish rolling is preferably 3.5 or less. However, this does not apply when skin pass rolling or cold rolling is performed after hot rolling or pickling.

【0067】また、粗圧延後または、それに続くデスケ
ーリング後にシートバーを接合し、連続的に仕上げ圧延
をしてもよい。その際に粗バーを一旦コイル状に巻き、
必要に応じて保温機能を有するカバーに格納し、再度巻
き戻してから接合を行ってもよい。
Further, after the rough rolling or the subsequent descaling, the sheet bars may be joined and continuously subjected to finish rolling. At that time, wind the coarse bar once in a coil,
If necessary, the sheets may be stored in a cover having a heat retaining function, rewound, and then joined.

【0068】仕上げ圧延は、熱延鋼板として最終製品に
する場合においては、その仕上げ圧延後半にAr3 変
態点温度+100℃以下の温度域で合計圧下率25%以
上の圧延を行う必要がある。ここでAr3 変態点温度
とは、例えば以下の計算式により鋼成分との関係で簡易
的に示される。すなわち、 Ar3 =910−310×%C+25×%Si−80
×%Mn
In the final rolling, when the final product is a hot-rolled steel sheet, it is necessary to perform rolling with a total reduction of 25% or more in the temperature range of Ar3 transformation point temperature + 100 ° C. or lower in the latter half of the finish rolling. Here, the Ar3 transformation point temperature is simply shown in relation to the steel composition, for example, by the following calculation formula. That is, Ar3 = 910-310 ×% C + 25 ×% Si-80
×% Mn

【0069】Ar3 変態点温度+100℃以下の温度
域での合計圧下率25%未満であると圧延されたオース
テナイトの集合組織が十分に発達しないために、この
後、如何様な冷却を施したとしても本発明の効果が得ら
れない。よりシャープな集合組織を得るためにはAr3
変態点温度+100℃以下の温度域での合計圧下率を
35%以上とすることが望ましい。
If the total rolling reduction in the temperature range of Ar3 transformation point temperature + 100 ° C. or less is less than 25%, the texture of the rolled austenite does not sufficiently develop. Therefore, no matter what kind of cooling is performed thereafter, However, the effect of the present invention cannot be obtained. Ar3 for a sharper texture
It is desirable that the total rolling reduction in the temperature range of the transformation point temperature + 100 ° C. or less is 35% or more.

【0070】また、合計圧下率25%以上の圧延を行う
温度域の下限は特に限定しないが、Ar3 変態点温度
未満であると圧延中に析出したフェライトに加工組織が
残留して延性が低下してしまい加工性が劣化するため、
合計圧下率25%以上の圧延を行う温度域の下限はAr
3 変態点温度以上が望ましい。
The lower limit of the temperature range for rolling at a total reduction of 25% or more is not particularly limited, but if it is lower than the Ar3 transformation point temperature, the ferrite precipitated during rolling retains the work structure and the ductility decreases. Processability deteriorates,
The lower limit of the temperature range for rolling at a total reduction of 25% or more is Ar.
3 A transformation temperature or higher is desirable.

【0071】本発明ではAr3 変態点温度+100℃
以下の温度域での合計圧下率の上限を特に限定しない
が、この圧下率合計が97.5%を越えると、圧延荷重
が増大し圧延機の剛性を過剰に高める必要があり、経済
上のデメリットを生じるために、望ましくは97.5%
以下とする。
In the present invention, Ar3 transformation point temperature + 100 ° C.
The upper limit of the total rolling reduction in the following temperature range is not particularly limited, but if the total rolling reduction exceeds 97.5%, the rolling load increases and the rigidity of the rolling mill needs to be excessively increased, which is economically disadvantageous. 97.5% is desirable in order to cause disadvantages
Below.

【0072】ここで、Ar3 変態点温度+100℃以
下の温度域での熱間圧延時の熱間圧延ロールと鋼板との
摩擦が大きい場合には、鋼板表面近傍における板面に
{110}面を主とする結晶方位が発達し、形状凍結性
が劣化するために熱間圧延ロールと鋼板との摩擦を低減
するために必要に応じて潤滑を施す。
Here, when the friction between the hot rolling roll and the steel sheet during hot rolling in the temperature range of Ar3 transformation point temperature + 100 ° C. or less is large, the {110} plane is formed on the sheet surface in the vicinity of the steel sheet surface. Since the main crystal orientation develops and the shape fixability deteriorates, lubrication is applied as necessary to reduce the friction between the hot rolling roll and the steel sheet.

【0073】本発明において熱間圧延ロールと鋼板との
摩擦係数の上限は特に限定しないが、0.2超では{1
10}面を主とする結晶方位の発達が顕著になり形状凍
結性が劣化するので、Ar3 変態点温度+100℃以
下の温度域での熱間圧延時における少なくとも1パスに
ついて熱間圧延ロールと鋼板との摩擦係数を0.2以下
とすることが望ましい。さらに望ましくは、Ar3 変
態点温度+100℃以下の温度域での熱間圧延時におけ
る全パスについて熱間圧延ロールと鋼板との摩擦係数を
0.15以下とする。ここで熱間圧延ロールと鋼板との
摩擦係数とは、先進率、圧延荷重、圧延トルク等の値よ
り圧延理論に基づいて計算により求めた値である。
In the present invention, the upper limit of the friction coefficient between the hot rolling roll and the steel sheet is not particularly limited, but if it exceeds 0.2, {1
Since the crystal orientation mainly in the 10} plane becomes remarkable and the shape fixability deteriorates, at least one pass during hot rolling in the temperature range of Ar3 transformation point temperature + 100 ° C or less, the hot rolling roll and the steel sheet It is desirable that the coefficient of friction with is 0.2 or less. More preferably, the coefficient of friction between the hot rolling roll and the steel sheet is 0.15 or less for all passes during hot rolling in the temperature range of Ar3 transformation point temperature + 100 ° C. or less. Here, the friction coefficient between the hot rolling roll and the steel sheet is a value obtained by calculation based on the theory of rolling from the values of the advance rate, rolling load, rolling torque and the like.

【0074】仕上げ圧延の最終パス温度(FT)につい
ては特に限定しないが、仕上げ圧延の最終パス温度(F
T)はAr3 変態点温度以上で終了することが望まし
い。これは、熱間圧延中に圧延温度がAr3 変態点温
度未満であると圧延前もしくは圧延中に析出したフェラ
イトに加工組織が残留して延性が低下してしまい加工性
が劣化するためである。
The final pass temperature (FT) of finish rolling is not particularly limited, but the final pass temperature (F) of finish rolling is
It is desirable that T) ends at the Ar3 transformation temperature or higher. This is because if the rolling temperature is lower than the Ar3 transformation point temperature during hot rolling, the work structure remains in the ferrite precipitated before or during rolling, and the ductility decreases and the workability deteriorates.

【0075】一方、仕上げ温度の上限については特に上
限を設けないがAr3 変態点温度+100℃超ではA
r3 変態点温度+100℃以下の温度域で合計圧下率
25%以上の圧延を行うことが事実上不可能であるので
仕上げ温度の上限はAr3変態点温度+100℃以下が
望ましい。
On the other hand, there is no particular upper limit on the finishing temperature, but if the Ar3 transformation point temperature exceeds 100 ° C.
Since it is practically impossible to carry out rolling with a total reduction of 25% or more in a temperature range of r3 transformation point temperature + 100 ° C. or less, the upper limit of finishing temperature is preferably Ar3 transformation point temperature + 100 ° C. or less.

【0076】本発明において仕上圧延を終了した後、所
定の巻取温度(CT)にて巻取るまでの工程については
特に定めないが、バーリング性をそれほど劣化させずに
延性との両立を目指す場合は、Ar3 変態点からAr1
変態点までの温度域(フェライトとオーステナイトの
二相域)で1〜20秒間滞留させてもよい。ここでの滞
留は、二相域でフェライト変態を促進させるために行う
が、1秒未満では、二相域におけるフェライト変態が不
十分なため、十分な延性が得られず、20秒超では、T
iおよび/またはNbを含む析出物のサイズが粗大化し
析出強化による強度上昇に寄与しなくなる恐れがある。
また、1〜20秒間の滞留をさせる温度域はフェライト
変態を容易に促進させるためにはAr1 変態点以上8
60℃以下が望ましい。さらに、1〜20秒間の滞留時
間は生産性を極端に低下させないためには1〜10秒間
とすることが望ましい。
In the present invention, the steps from the completion of finish rolling to the winding at a predetermined winding temperature (CT) are not particularly specified, but when aiming at compatibility with ductility without deteriorating the burring property so much. From the Ar3 transformation point to Ar1
It may be allowed to stay for 1 to 20 seconds in the temperature range up to the transformation point (two-phase range of ferrite and austenite). The residence here is performed in order to accelerate the ferrite transformation in the two-phase region, but if it is less than 1 second, sufficient ductility cannot be obtained because the ferrite transformation in the two-phase region is insufficient, and if it exceeds 20 seconds, T
The size of the precipitate containing i and / or Nb may become coarse and may not contribute to the strength increase due to precipitation strengthening.
In addition, the temperature range in which the steel is retained for 1 to 20 seconds is 8 or higher than the Ar1 transformation point in order to facilitate the ferrite transformation easily.
60 ° C or lower is desirable. Further, the residence time of 1 to 20 seconds is preferably 1 to 10 seconds in order not to extremely reduce the productivity.

【0077】また、これらの条件を満たすためには、仕
上げ圧延終了後20℃/s以上の冷却速度で当該温度域
に迅速に到達させることが必要である。冷却速度の上限
は特に定めないが、冷却設備の能力上300℃/s以下
が妥当な冷却速度である。さらに、あまりにもこの冷却
速度が早いと冷却終了温度を制御できずオーバーシュー
トしてAr1 変態点以下まで過冷却されてしまう可能
性があり、延性改善の効果が失われるので、ここでの冷
却速度は150℃/s以下が望ましい。
In order to satisfy these conditions, it is necessary to quickly reach the temperature range at a cooling rate of 20 ° C./s or more after finishing rolling. Although the upper limit of the cooling rate is not specified, 300 ° C./s or less is a reasonable cooling rate in view of the capacity of the cooling equipment. Furthermore, if this cooling rate is too fast, the cooling end temperature cannot be controlled, and there is a possibility of overshooting and overcooling to below the Ar1 transformation point, and the effect of improving ductility will be lost. Is preferably 150 ° C./s or less.

【0078】次に、その温度域から所定の巻取温度(C
T)まで冷却するが、その冷却速度は本発明の効果を得
るためには特に定める必要はない。ただし、冷却速度が
あまりに遅いとTiおよび/またはNbを含む析出物の
サイズが粗大化し析出強化による強度上昇に寄与しなく
なる恐れがあるので、冷却速度の下限は20℃/s以上
が望ましい。また、巻取温度までの冷却速度の上限は特
に定めることなく本発明の効果を得ることができるが、
熱ひずみによる板そりが懸念されることから、300℃
/s以下とすることが望ましい。
Next, a predetermined winding temperature (C
Although it is cooled to T), the cooling rate is not particularly required to obtain the effects of the present invention. However, if the cooling rate is too slow, the size of precipitates containing Ti and / or Nb may become coarse and may not contribute to the increase in strength due to precipitation strengthening. Therefore, the lower limit of the cooling rate is preferably 20 ° C./s or more. Further, although the upper limit of the cooling rate up to the winding temperature can obtain the effect of the present invention without particularly defining,
Since there is concern about plate warpage due to thermal strain, 300 ° C
It is desirable to be below / s.

【0079】本発明において巻取温度(CT)について
は特に定めないが、その上限はAr3 変態点温度+1
00℃以下の温度域で合計圧下率25%以上の圧延で得
られたオーステナイトの集合組織を遺伝させるためには
下記に示す巻取温度T0 以下で巻き取ることが望まし
い。このT0 は、オーステナイトとオーステナイトと
同一成分のフェライトが同一の自由エネルギーを持つ温
度として熱力学的に定義される温度で、C以外の成分の
影響も考慮して、下記の式を用いて簡易的に計算するこ
とができる。 T0 =−650.4×%C+B ここで、Bは下記のように決定される。 B=−50.6×Mneq+894.3 また、ここで、Mneqとは、下記に示す含有元素の質
量%より決定される。 Mneq=%Mn+0.24×%Ni+0.13×%S
i+0.38×%Mo+0.55×%Cr+0.16×
%Cu−0.50×%Al−0.45×%Co+0.9
0×%V なお、T0 に及ぼす本発明に規定された上記以外の成
分の質量%の影響はそれほど大きくないのでここでは無
視できる。
In the present invention, the coiling temperature (CT) is not particularly specified, but the upper limit is the Ar3 transformation point temperature + 1.
In order to inherit the texture of austenite obtained by rolling at a total rolling reduction of 25% or more in a temperature range of 00 ° C. or less, it is desirable to wind at a winding temperature T 0 or less shown below. This T 0 is a temperature that is thermodynamically defined as a temperature at which austenite and ferrite having the same component as austenite have the same free energy, and in consideration of the effects of components other than C, the following formula is used. Can be calculated. T 0 = −650.4 ×% C + B where B is determined as follows. B = −50.6 × Mneq + 894.3 Further, here, Mneq is determined by the mass% of the contained elements shown below. Mneq =% Mn + 0.24 ×% Ni + 0.13 ×% S
i + 0.38 ×% Mo + 0.55 ×% Cr + 0.16 ×
% Cu-0.50x% Al-0.45x% Co + 0.9
0 ×% V Note that the influence of the mass% of the components other than the above specified in the present invention on T 0 is not so large and can be ignored here.

【0080】一方、巻取温度(CT)の下限は、350
℃以下では十分なTiおよび/またはNbを含む析出物
が生じなくなり、鋼中に固溶Cが残留して加工性を低下
させる恐れがあるので、350℃超で巻き取ることが望
ましい。さらに、巻取り後の冷却速度は特に限定しない
が、Cuを1%以上添加した場合、巻取温度(CT)が
450℃超であると巻取り後にCuが析出して加工性が
劣化するばかりでなく、疲労特性向上に有効な固溶状態
のCuが失われる恐れがあるので、巻取温度(CT)が
450℃超の場合、巻取り後の冷却速度は200℃まで
を30℃/s以上とすることが望ましい。
On the other hand, the lower limit of the winding temperature (CT) is 350.
Precipitates containing sufficient Ti and / or Nb will not be generated at a temperature of not higher than 0 ° C, and solid solution C may remain in the steel to lower the workability. Further, although the cooling rate after winding is not particularly limited, when Cu is added in an amount of 1% or more, if the winding temperature (CT) is higher than 450 ° C., Cu precipitates after winding and workability deteriorates. However, since Cu in a solid solution state that is effective in improving fatigue characteristics may be lost, when the coiling temperature (CT) is higher than 450 ° C, the cooling rate after coiling is 30 ° C / s up to 200 ° C. It is desirable to set the above.

【0081】熱間圧延工程終了後は必要に応じて酸洗
し、その後インラインまたはオフラインで圧下率10%
以下のスキンパスまたは圧下率40%程度までの冷間圧
延を施しても構わない。ただし、この場合、潤滑効果の
ある組成物を塗布し、摩擦係数を低減させる効果を得る
ためには、スキンパス後の鋼板表裏の表面のうち、少な
くとも一方の算術平均粗さRaが1〜3.5であるよう
にスキンパス圧下率を制御する。
After completion of the hot rolling process, pickling is carried out if necessary, and then in-line or off-line reduction of 10%.
The following skin pass or cold rolling up to a rolling reduction of about 40% may be performed. However, in this case, in order to apply a composition having a lubricating effect and obtain the effect of reducing the friction coefficient, at least one of the surfaces of the front and back surfaces of the steel sheet after the skin pass has an arithmetic average roughness Ra of 1 to 3. The skin pass reduction is controlled to be 5.

【0082】次に、冷延鋼板として最終製品にする場合
であるが、熱間での仕上げ圧延条件は特に限定しない。
ただし、より良好な形状凍結性を得るためには、Ar3
変態点温度+100℃以下の温度域での合計圧下率が2
5%以上であることが望ましい。また、仕上げ圧延の最
終パス温度(FT)はAr3 変態点温度未満で終了して
も差し支えないが、その場合は、圧延前もしくは圧延中
に析出したフェライトに強い加工組織が残留するため、
続く巻取処理または加熱処理により回復、再結晶させる
ことが望ましい。
Next, there is a case where a cold rolled steel sheet is used as a final product, but hot finish rolling conditions are not particularly limited.
However, in order to obtain better shape fixability, Ar3
The total rolling reduction in the temperature range below the transformation point temperature + 100 ° C is 2
It is preferably 5% or more. Also, the final pass temperature (FT) of finish rolling may be completed below the Ar3 transformation point temperature, but in that case, since a strong work structure remains in ferrite precipitated before or during rolling,
It is desirable to recover and recrystallize by the subsequent winding treatment or heat treatment.

【0083】続く酸洗後の冷間圧延の合計圧下率は80
%未満とする。これは、冷間圧延の合計圧下率は80%
以上であると一般的な冷間圧延−再結晶集合組織である
板面に平行な結晶面の{111}面や{554}面のX
線回折積分面強度比が高くなるためである。また、望ま
しくは70%以下である。冷間圧延率の下限は特に定め
ることなく本発明の効果を得ることができるが、結晶方
位の強度を適当な範囲に制御するためには3%以上とす
ることが望ましい。
The total reduction ratio of the cold rolling after the subsequent pickling was 80.
Less than%. This is because the total reduction ratio of cold rolling is 80%.
As described above, the X-axis of the {111} plane or the {554} plane of the crystal plane parallel to the plate surface which is a general cold rolling-recrystallization texture
This is because the line diffraction integrated surface intensity ratio becomes high. Further, it is preferably 70% or less. The effect of the present invention can be obtained without particularly defining the lower limit of the cold rolling rate, but it is preferably 3% or more in order to control the strength of the crystal orientation within an appropriate range.

【0084】この様に冷間圧延された鋼板の熱処理は連
続焼鈍工程を前提としている。まず、回復温度以上Ac
3 変態点温度+100℃以下の温度域で5〜150秒
間行う。ここでAc3 変態点温度とは、例えば、レス
リー鉄鋼材科学(1985年発行、熊井浩 野田龍彦
訳、丸善株式会社)273頁に記載の計算式により鋼成
分との関係で示される。この熱処理温度(ST)が回復
温度未満の場合には加工組織が残留し延性を著しく劣化
させるので、熱処理温度(ST)は回復温度以上とす
る。さらに良好な延性を得るためには、再結晶温度以上
が望ましい。また、熱処理温度(ST)がAc3 変態
点温度+100℃超では、再結晶によって生成したフェ
ライトがオーステナイトへ変態し、オーステナイトの粒
成長によっての集合組織がランダム化され、最終的に得
られる集合組織もランダム化されてしまうので熱処理温
度(ST)はAc3 変態点温度+100℃以下とす
る。
The heat treatment of the cold rolled steel sheet is premised on the continuous annealing step. First, the recovery temperature or higher Ac
3 Perform for 5 to 150 seconds in the temperature range of the transformation point temperature + 100 ° C. or less. Here, the Ac3 transformation point temperature is shown in relation to the steel composition by a calculation formula described on page 273, for example, Leslie Steel Science (issued in 1985, translated by Hiroshi Kumai, translated by Tatsuhiko Noda, Maruzen Co., Ltd.). When the heat treatment temperature (ST) is lower than the recovery temperature, the worked structure remains and ductility is significantly deteriorated. Therefore, the heat treatment temperature (ST) is set to the recovery temperature or higher. In order to obtain even better ductility, the recrystallization temperature or higher is desirable. Further, when the heat treatment temperature (ST) exceeds the Ac3 transformation point temperature + 100 ° C, the ferrite produced by recrystallization transforms to austenite, the texture by austenite grain growth is randomized, and the finally obtained texture is also obtained. Since it is randomized, the heat treatment temperature (ST) is set to Ac3 transformation point temperature + 100 ° C. or less.

【0085】一方、この温度域での保持時間(Tim
e)は、5秒未満では、TiおよびNbの炭窒化物が完
全に再固溶するのに不十分であり、一方、150秒超の
熱処理を行ってもその効果が飽和するばかりでなく生産
性を低下させるので、保持時間(Time)は5〜15
0秒間とする。
On the other hand, the holding time (Tim in this temperature range
With respect to e), if it is less than 5 seconds, carbonitrides of Ti and Nb are insufficient for complete solid solution again. On the other hand, even if the heat treatment is performed for more than 150 seconds, the effect is not only saturated but also produced. Retention time (Time) of 5 to 15
0 seconds.

【0086】その後の冷却条件については特に限定しな
いが、20℃/s以上の冷却速度で350℃超前記T0
温度以下の温度域まで冷却することが望ましい。これ
は、冷却速度が20℃/s未満では、Tiおよび/また
はNbを含む析出物のサイズが粗大化し析出強化による
強度上昇に寄与しなくなる恐れがあるためである。ま
た、冷却終了温度は、350℃以下では十分なTiおよ
び/またはNbを含む析出物が生じなくなり、鋼中に固
溶Cが残留して加工性を低下させる恐れがあるので、3
50℃超が望ましい。また、冷却工程の終了温度は、2
00℃超では時効性が劣化する恐れがあるので200℃
以下とすることが望ましい。また、下限には、水冷もし
くはミストで冷却する場合コイルが長時間水濡れの状態
にあると錆による外観不良が懸念されるため、50℃以
上が望ましい。
The cooling conditions thereafter are not particularly limited, but the T 0 above 350 ° C. at a cooling rate of 20 ° C./s or more is used.
It is desirable to cool to a temperature range below the temperature. This is because if the cooling rate is less than 20 ° C./s, the size of the precipitate containing Ti and / or Nb may become coarse and may not contribute to the strength increase due to precipitation strengthening. If the cooling end temperature is 350 ° C. or lower, sufficient precipitates containing Ti and / or Nb will not be generated, and solid solution C may remain in the steel to reduce workability.
More than 50 ° C is desirable. Also, the end temperature of the cooling process is 2
If the temperature exceeds 00 ° C, aging may deteriorate, so 200 ° C
The following is desirable. In addition, the lower limit is preferably 50 ° C. or higher because when the coil is water-cooled or when it is cooled with a mist, if the coil is wet with water for a long period of time, there is a fear of appearance failure due to rust.

【0087】さらにその後、必要に応じてスキンパス圧
延を実施する。ただし、この場合、潤滑効果のある組成
物を塗布し、摩擦係数を低減させる効果を得るために
は、スキンパス後の鋼板表裏の表面のうち、少なくとも
一方の算術平均粗さRaが1〜3.5であるようにスキ
ンパス圧下率を制御する。
After that, if necessary, skin pass rolling is carried out. However, in this case, in order to apply a composition having a lubricating effect and obtain the effect of reducing the friction coefficient, at least one of the surfaces of the front and back surfaces of the steel sheet after the skin pass has an arithmetic average roughness Ra of 1 to 3. The skin pass reduction is controlled to be 5.

【0088】酸洗後の熱延鋼板、もしくは上記の再結晶
熱処理終了後の冷延鋼板に亜鉛めっきを施すためには、
亜鉛めっき浴中に浸積し、必要に応じて合金化処理して
もよい。
In order to galvanize the hot-rolled steel sheet after pickling or the cold-rolled steel sheet after completion of the above recrystallization heat treatment,
It may be immersed in a galvanizing bath and may be alloyed if necessary.

【0089】最後に絞り性を確保するために上記の製造
工程の後に潤滑効果のある組成物を塗布する。塗布する
方法は望ましい塗布厚さを得られれば特に限定しない
が、静電塗布、ロールコータによる方法が一般的に用い
られる。
Finally, in order to secure the drawability, a composition having a lubricating effect is applied after the above manufacturing process. The coating method is not particularly limited as long as a desired coating thickness can be obtained, but an electrostatic coating method or a roll coater method is generally used.

【0090】[0090]

【実施例】以下に、実施例により本発明をさらに説明す
る。表1に示す化学成分を有するA〜Lの鋼は、転炉に
て溶製して、連続鋳造後、表2に示す加熱温度で再加熱
し、粗圧延に続く仕上げ圧延で1.2〜5.5mmの板
厚にした後に巻き取った。ただし、表中の化学組成につ
いての表示は質量%である。なお、表2に示すようにい
くらかについて潤滑圧延を行った。また、鋼Lについて
は粗圧延後に衝突圧2.7MPa、流量0.001リッ
トル/cm2の条件でデスケーリングを施した。さら
に、表2に示すように一部については熱間圧延工程後、
酸洗、冷延、熱処理を行った。板厚は0.7〜2.3m
mである。一方、上記鋼板のうち鋼Gおよび鋼A−8に
ついては、亜鉛めっきを施した。
EXAMPLES The present invention will be further described below with reference to examples. Steels A to L having the chemical components shown in Table 1 were melted in a converter, continuously cast, then reheated at the heating temperature shown in Table 2, and 1.2 to 12 in rough rolling followed by finish rolling. It was rolled up after the plate had a thickness of 5.5 mm. However, the chemical composition shown in the table is% by mass. In addition, some lubrication rolling was performed as shown in Table 2. Further, the steel L was subjected to descaling under conditions of a collision pressure of 2.7 MPa and a flow rate of 0.001 liter / cm 2 after rough rolling. Furthermore, as shown in Table 2, after a hot rolling process,
Pickling, cold rolling, and heat treatment were performed. Board thickness is 0.7 to 2.3 m
m. On the other hand, among the above steel sheets, Steel G and Steel A-8 were galvanized.

【0091】製造条件の詳細を表2に示す。ここで、
「SRT」はスラブ加熱温度、「FT」は最終パス仕上
げ圧延温度、「圧延率」とはAr3 変態点温度+10
0℃以下の温度域での圧下率の合計を示す。ただし、後
に冷延工程にて圧延を行う場合はこのような制限の限り
ではないので「−」とした。また、「潤滑」はAr3変
態点温度+100℃以下の温度域での潤滑の有無を示し
た。さらに「CT」とは巻取温度を示している。ただ
し、冷延鋼板の場合は製造の条件として特に限定する必
要がないので「−」とした。次に、「冷延率」とは合計
冷間圧延率、「ST」とは、熱処理温度、「Time」
は熱処理時間である。
Details of the manufacturing conditions are shown in Table 2. here,
"SRT" is the slab heating temperature, "FT" is the final pass finish rolling temperature, and "rolling rate" is the Ar3 transformation point temperature +10.
The total reduction rate in the temperature range of 0 ° C or lower is shown. However, when rolling is performed later in the cold rolling process, such limitation is not applied, and thus "-" is set. Further, "lubrication" indicates the presence or absence of lubrication in the temperature range of Ar3 transformation point temperature + 100 ° C or lower. Furthermore, "CT" indicates the winding temperature. However, in the case of a cold-rolled steel sheet, it is not necessary to specifically limit the manufacturing conditions, so "-" is set. Next, "cold rolling rate" is the total cold rolling rate, "ST" is the heat treatment temperature, "Time".
Is the heat treatment time.

【0092】また、上記製造プロセスを経た後、静電塗
布装置またはロールコータにて潤滑効果のある組成物を
塗布した。
After passing through the above manufacturing process, a composition having a lubricating effect was applied by an electrostatic coating device or a roll coater.

【0093】このようにして得られた熱延板の引張試験
は、供試材を、まず、JIS Z2201記載の5号試
験片に加工し、JIS Z 2241記載の試験方法に
従って行った。表2に降伏強度(σY )、引張強度
(σB )、破断伸び(El)を示す。一方、バーリン
グ加工性(穴拡げ性)については日本鉄鋼連盟規格JF
S T 1001−1996記載の穴拡げ試験方法に従
って評価した。表2に穴拡げ率(λ)を示す。
The tensile test of the hot-rolled sheet thus obtained was carried out by first processing the test material into a No. 5 test piece described in JIS Z2201 and performing the test method described in JIS Z2241. Table 2 shows the yield strength (σ Y ), the tensile strength (σ B ), and the breaking elongation (El). On the other hand, regarding burring workability (hole expandability), the Japan Iron and Steel Federation Standard JF
Evaluation was performed according to the hole expansion test method described in ST 1001-1996. Table 2 shows the hole expansion ratio (λ).

【0094】ここで、フェライト、ベイナイト、残留オ
ーステナイト、パーライト、マルテンサイトの体積分率
とは鋼板板幅の1/4Wもしくは3/4W位置より切出
した試料を圧延方向断面に研磨、エッチングし、光学顕
微鏡を用い200〜500倍の倍率で観察された板厚の
1/4tにおけるミクロ組織の面積分率で定義される。
Here, the volume fraction of ferrite, bainite, retained austenite, pearlite, and martensite means that a sample cut from a position of 1/4 W or 3/4 W of the steel plate width is polished and etched in a cross section in the rolling direction, It is defined as the area fraction of the microstructure at 1/4 t of the plate thickness observed under a microscope at a magnification of 200 to 500 times.

【0095】さらに、板幅の1/4Wもしくは3/4W
位置より30mmφに切り取った試片より30mmφに
切り取った試片に三山仕上の研削を行い、次いで化学研
磨または電解研磨によって歪みを除去して作製し、新版
カリティX線回折要論(1986年発行、松村源太郎
訳、株式会社アグネ)274〜296頁に記載の方法に
従ってX線回折強度の測定を行った。
Furthermore, 1/4 W or 3/4 W of the plate width
The specimen cut to 30 mmφ from the position was ground to 3 mm on the specimen cut to 30 mmφ, and then the strain was removed by chemical polishing or electrolytic polishing to prepare a new edition of the Kariti X-ray diffraction theory (issued in 1986, The X-ray diffraction intensity was measured according to the method described in Gentaro Matsumura, Agne Co., Ltd. pp. 274-296.

【0096】ここで、{100}<011>〜{22
3}<110>方位群のX線ランダム強度比の平均値と
は、この方位群に含まれる主な方位、{100}<01
1>、{116}<110>、{114}<110>、
{113}<110>、{112}<110>、{33
5}<110>および{223}<110>のX線回折
強度を{110}極点図に基づきベクトル法により計算
した3次元集合組織、または{110}、{100}、
{211}、{310}極点図のうち複数の極点図(望
ましくは3つ以上)を用いて級数展開法で計算した3次
元集合組織から求めた。
Here, {100} <011> to {22
3} The average value of the X-ray random intensity ratio of the <110> direction group is the main direction included in this direction group, {100} <01.
1>, {116} <110>, {114} <110>,
{113} <110>, {112} <110>, {33
5} <110> and {223} <110> X-ray diffraction intensities calculated by the vector method based on the {110} pole figure, or {110}, {100},
It was determined from a three-dimensional texture calculated by the series expansion method using a plurality of pole figures (preferably three or more) of the {211} and {310} pole figures.

【0097】例えば、後者の方法における上記各結晶方
位のX線ランダム強度比は、3次元集合組織のφ2=4
5゜断面における(001)[1−10]、(116)
[1−10]、(114)[1−10]、(113)
[1−10]、(112)[1−10]、(335)
[1−10]、(223)[1−10]の強度をそのま
ま用ればよい。ただし、{100}<011>〜{22
3}<110>方位群のX線ランダム強度比の平均値と
は、上記の各方位の相加平均である。上記全ての方位の
強度を得ることができない場合には、{100}<01
1>、{116}<110>、{114}<110>、
{112}<110>、{223}<110>の各方位
の相加平均で代替してもよい。
For example, the X-ray random intensity ratio of each crystal orientation in the latter method is φ2 = 4 of the three-dimensional texture.
(001) [1-10], (116) at 5 ° cross section
[1-10], (114) [1-10], (113)
[1-10], (112) [1-10], (335)
The strengths of [1-10] and (223) [1-10] may be used as they are. However, {100} <011> to {22
3} The average value of the X-ray random intensity ratio of the <110> orientation group is the arithmetic average of the above orientations. If it is not possible to obtain the intensities in all of the above directions, {100} <01
1>, {116} <110>, {114} <110>,
You may substitute by the arithmetic mean of each direction of {112} <110> and {223} <110>.

【0098】次に{554}<225>、{111}<
112>および{111}<110>の3方位のX線ラ
ンダム強度比の平均値とは、上記の方法と同様に計算し
た3次元集合組織から求めればよい
Next, {554} <225> and {111} <
The average value of the X-ray random intensity ratios in the three directions of 112> and {111} <110> may be obtained from the three-dimensional texture calculated in the same manner as the above method.

【0099】表2においてX線ランダム強度比のうち
「強度比1」とは、{100}<011>〜{223}
<110>方位群のX線ランダム強度比の平均値、「強
度比2」とは{554}<225>、{111}<11
2>および{111}<110>の3方位のX線ランダ
ム強度比の平均値である。
In Table 2, "intensity ratio 1" of the X-ray random intensity ratio means {100} <011> to {223}.
The average value of the X-ray random intensity ratio of the <110> orientation group, “intensity ratio 2” is {554} <225>, {111} <11.
2 is an average value of X-ray random intensity ratios in 3 directions of 2> and {111} <110>.

【0100】次に、上記鋼板の形状凍結性を調査するた
めに板幅の1/4Wもしくは3/4W位置から圧延方向
が長辺になるように50mm幅,270mm長さの試験
片を作成し、ポンチ幅78mm,ポンチ肩R5,ダイ肩
R5の金型を用いてハット曲げ試験を行った。曲げ試験
を行った試験片は三次元形状測定装置にて板幅中心部の
形状を測定し、図1に示した様に、左右の点間の長さ
からポンチ幅を引いた値を寸法精度、点と点の接線
と点と点の接線の交点の角度から90# を引いた値
の左右での平均値をスプリング・バック量、点と点
間の曲率の逆数を左右で平均化した値を壁そり量として
形状凍結性を評価した。
Next, in order to investigate the shape fixability of the steel sheet, a test piece having a width of 50 mm and a length of 270 mm was prepared from the position of 1/4 W or 3/4 W of the sheet width so that the rolling direction was the long side. , A punch width of 78 mm, a punch shoulder R5 and a die shoulder R5 were used to perform a hat bending test. For the test piece that underwent the bending test, the shape of the center of the plate width was measured with a three-dimensional shape measuring device, and as shown in Fig. 1, the value obtained by subtracting the punch width from the length between the left and right points was used for dimensional accuracy. , Spring-back amount is the average value on the left and right of the value obtained by subtracting 90 # from the intersection angle between the tangents of the points and the tangent of the points, and the reciprocal of the curvature between the points is averaged on the left and right. The shape freezing property was evaluated using the amount of wall warpage.

【0101】ところでスプリングバック量や壁そり量は
BHF(しわ押さえ力)によっても変化する。本発明の
効果はいずれのBHFで評価を行ってもその傾向は変わ
らないが、生産現場で実部品をプレスする際にはあまり
高いBHFはかけられないことから、今回はBHF29
kNで各鋼種のハット曲げ試験を行った。上記曲げ試験
によって得られた寸法精度、壁そり量をもとに形状凍結
性は最終的には寸法精度(△d)で判断することができ
る。寸法精度は鋼板の強度上昇とともに劣化することが
よく知られているために、ここでは表2に示す結果、Δ
d/σB を指標とした。
By the way, the amount of springback and the amount of wall warp also change depending on BHF (wrinkle holding force). The tendency of the effect of the present invention does not change regardless of which BHF is evaluated, but since BHF that is too high cannot be applied when pressing actual parts at the production site, this time BHF29
A hat bending test of each steel type was performed at kN. The shape fixability can be finally judged by the dimensional accuracy (Δd) based on the dimensional accuracy and the wall warp amount obtained by the bending test. It is well known that the dimensional accuracy deteriorates as the strength of the steel sheet increases.
d / σ B was used as an index.

【0102】また、算術平均粗さRaついては、レーザ
ーを用いた非接触型の測定装置を用いJIS B060
1−1994に記載されている方法にて求めた。
Regarding the arithmetic mean roughness Ra, JIS B060 is used by using a non-contact type measuring device using a laser.
It was determined by the method described in 1-1994.

【0103】さらに摩擦係数は図2に示すように、表面
のビッカース硬さがHv600以上を有する2枚の平板
の間に挟み、面圧が1.5〜2kgf/mm2 となるよ
うに鋼板表面に対して垂直の力(F)を与えたうえで、
鋼板を引き抜く。その際のFに対する引き抜き力fの割
合(f/F)として求めた。
Further, as shown in FIG. 2, the coefficient of friction is sandwiched between two flat plates having a Vickers hardness of Hv600 or more on the surface of the steel plate so that the surface pressure becomes 1.5 to 2 kgf / mm 2. After applying a vertical force (F) to
Pull out the steel plate. It was determined as a ratio (f / F) of the pulling force f to F at that time.

【0104】最後に、鋼板の絞り性指標は、鋼板を円形
に加工した後、円筒ポンチで絞り成形を行った際に、絞
り抜け可能な最大径(D)を円筒ポンチ直径(d)で除
した値(D/d)とした。この測定において、鋼板の円
形加工サイズは、300〜400φの種々の直径とし、
円筒ポンチ径は175φ、底面の肩部は10R、ダイス
面の肩部は15R、シワ押さえ力は、鋼Bは10kN、
鋼J、は100kN、鋼A、鋼C、鋼E、鋼F、鋼G、
鋼H、鋼I、鋼Kは120kNとした。
Finally, the drawability index of the steel plate is obtained by dividing the maximum diameter (D) that can be drawn out by the cylindrical punch diameter (d) when the steel plate is processed into a circular shape and then drawn by a cylindrical punch. Value (D / d). In this measurement, the circular processing size of the steel plate is various diameters of 300 to 400φ,
Cylindrical punch diameter is 175φ, bottom shoulder is 10R, die surface shoulder is 15R, wrinkle holding force is 10kN for steel B,
Steel J is 100 kN, Steel A, Steel C, Steel E, Steel F, Steel G,
Steel H, steel I, and steel K were 120 kN.

【0105】本発明範囲内の摩擦係数である鋼板は、本
発明範囲よりも高い摩擦係数を持つ鋼板に比べ絞り指標
値(D/d)値が高く、いずれも1.91以上であるこ
とがわかる。
Steel sheets having a coefficient of friction within the range of the present invention have a higher reduction index value (D / d) than steel sheets having a coefficient of friction higher than the range of the present invention, and are both 1.91 or more. Recognize.

【0106】本発明に沿うものは、鋼A−1、A−3、
A−4、A−8、A−10、C、E、G、H、I、J、
Lの12鋼であり、所定の量の鋼成分を含有し、少なく
とも板厚の1/2厚における板面の{100}<011
>〜{223}<110>方位群のX線ランダム強度比
の平均値が3以上かつ、{554}<225>、{11
1}<112>および{111}<110>の3方位の
X線ランダム強度比の平均値が3.5以下であり、その
表裏の表面のうち少なくとも一方の算術平均粗さRaが
1以上3.5以下である鋼板に潤滑効果のある組成物が
塗布されていることを特徴とし、かつ0〜200℃にお
ける圧延方向およびその直角方向の摩擦係数のうち少な
くともその一つが0.05以上0.2以下であることを
特徴とする、形状凍結性に優れる絞り可能なバーリング
性高強度薄鋼板が得られており、従って、本発明記載の
方法によって評価した従来鋼の形状凍結性指標を上回っ
ている。
According to the present invention, steels A-1, A-3,
A-4, A-8, A-10, C, E, G, H, I, J,
L steel 12 containing a predetermined amount of steel component, and {100} <011 of the plate surface at least at ½ of the plate thickness.
> To {223} <110> the average value of the X-ray random intensity ratio of the orientation group is 3 or more, and {554} <225>, {11
The average value of the X-ray random intensity ratios in the three directions of 1} <112> and {111} <110> is 3.5 or less, and the arithmetic average roughness Ra of at least one of the front and back surfaces is 1 or more 3 A steel sheet having a hardness of 0.5 or less is coated with a composition having a lubricating effect, and at least one of friction coefficients in a rolling direction and a direction perpendicular to the rolling direction at 0 to 200 ° C. is 0.05 or more and 0. A drawable burring high-strength steel sheet excellent in shape fixability, which is characterized by being 2 or less, is obtained, and therefore exceeds the shape fixability index of the conventional steel evaluated by the method according to the present invention. There is.

【0107】上記以外の鋼は、以下の理由によって本発
明の範囲外である。すなわち、鋼A−2は、仕上圧延終
了温度(FT)およびAr3 変態点温度+100℃以
下の温度域での合計圧下率が本発明請求項11の範囲外
であるので、請求項1記載の目的とする集合組織が得ら
れず十分な形状凍結性(Δd/σB)が得られていな
い。鋼A−5は、潤滑効果のある組成物の塗布がなされ
ていないので、請求項2記載の目的とする摩擦係数が得
られず十分な絞り性(D/d)が得られていない。鋼A
−6は、算術平均粗さRaが本発明請求項1の範囲外で
あるので、請求項2記載の目的とする摩擦係数が得られ
ず十分な絞り性(D/d)が得られていない。鋼A−7
は、熱処理温度(ST)が本発明請求項14の範囲外で
あるので、請求項1記載の目的とする集合組織が得られ
ず十分な形状凍結性(Δd/σB )が得られていな
い。鋼A−9は、冷延率が本発明請求項14の範囲外で
あるので、請求項1記載の目的とする集合組織が得られ
ず十分な形状凍結性(Δd/σB )が得られていな
い。
Steels other than the above are out of the scope of the present invention for the following reasons. That is, since the steel A-2 has a total reduction ratio in the temperature range of the finish rolling end temperature (FT) and the Ar3 transformation point temperature + 100 ° C or less, it is outside the scope of claim 11 of the present invention. And the shape fixability (Δd / σ B ) is not sufficiently obtained. Steel A-5 was not coated with a composition having a lubricating effect, so that the target friction coefficient of claim 2 was not obtained and sufficient drawability (D / d) was not obtained. Steel A
In No. 6, since the arithmetic average roughness Ra is outside the scope of claim 1 of the present invention, the desired friction coefficient of claim 2 is not obtained and sufficient drawability (D / d) is not obtained. . Steel A-7
Since the heat treatment temperature (ST) is outside the scope of claim 14 of the present invention, the target texture of claim 1 is not obtained and sufficient shape fixability (Δd / σ B ) is not obtained. . Steel A-9 has a cold rolling ratio outside the scope of claim 14 of the present invention, and therefore the desired texture of claim 1 is not obtained and sufficient shape fixability (Δd / σ B ) is obtained. Not not.

【0108】鋼Bは、Cの含有量が本発明請求項1の範
囲外であるので十分な強度(σB)が得られていない。
鋼Dは、Tiの含有量が本発明請求項1の範囲外である
ので十分な強度(σB )および形状凍結性(Δd/σB
)が得られていない。鋼Fは、Cの含有量が本発明請
求項1の範囲外であるので十分な穴拡げ率(λ)が得ら
れていない。鋼Iは、Sの含有量が本発明請求項1の範
囲外であるので十分な穴拡げ率(λ)および伸び(E
l)が得られていない。鋼Kは、Nの含有量が本発明請
求項1の範囲外であるので十分な穴拡げ率(λ)および
伸び(El)が得られていない。
Steel B does not have sufficient strength (σ B ) because the content of C is outside the scope of claim 1 of the present invention.
Steel D has a Ti content outside the scope of claim 1 of the present invention, and therefore has sufficient strength (σ B ) and shape fixability (Δd / σ B).
) Has not been obtained. Steel F has a C content outside the scope of claim 1 of the present invention, so a sufficient hole expansion ratio (λ) is not obtained. In Steel I, since the content of S is outside the scope of claim 1 of the present invention, a sufficient hole expansion ratio (λ) and elongation (E) are obtained.
l) has not been obtained. Steel K does not have a sufficient hole expansion ratio (λ) and elongation (El) because the N content is outside the scope of claim 1 of the present invention.

【0109】[0109]

【表1】 [Table 1]

【0110】[0110]

【表2】 [Table 2]

【0111】[0111]

【発明の効果】以上詳述したように、本発明は、形状凍
結性に優れる絞り可能なバーリング性高強度薄鋼板およ
びその製造方法に関するものであり、これらの高強度薄
鋼板を用いることにより、絞り成形に不利な集合組織を
有する鋼板においても良好な絞り性を得ることができる
ため、形状凍結性と絞り性の両立が期待できるため、本
発明は、工業的価値が高い発明であると言える。
As described in detail above, the present invention relates to a drawable burring high strength steel sheet which is excellent in shape fixability and a manufacturing method thereof. By using these high strength steel sheets, Since it is possible to obtain good drawability even in a steel sheet having a texture that is disadvantageous to draw forming, compatibility of shape fixability and drawability can be expected, so the present invention can be said to be an invention of high industrial value. .

【図面の簡単な説明】[Brief description of drawings]

【図1】曲げ試験を行ったサンプルの断面形状の概念図
である。
FIG. 1 is a conceptual diagram of a cross-sectional shape of a sample that has been subjected to a bending test.

【図2】摩擦係数測定器具を説明する図である。FIG. 2 is a diagram illustrating a friction coefficient measuring instrument.

フロントページの続き (51)Int.Cl.7 識別記号 FI テーマコート゛(参考) C22C 38/58 C22C 38/58 (72)発明者 杉浦 夏子 千葉県富津市新富20−1 新日本製鐵株式 会社技術開発本部内 (72)発明者 中村 隆彰 大分県大分市大字西ノ洲1番地 新日本製 鐵株式会社大分製鐵所内 (72)発明者 中本 武広 大分県大分市大字西ノ洲1番地 新日本製 鐵株式会社大分製鐵所内 Fターム(参考) 4E002 AD04 AD05 BC05 BC08 BD07 BD10 CB01 4K037 EA01 EA02 EA05 EA09 EA11 EA13 EA15 EA16 EA17 EA18 EA19 EA20 EA23 EA25 EA27 EA28 EA31 EA32 EA35 EA36 FB03 FB07 FB08 GA05 Continuation of front page (51) Int.Cl. 7 Identification code FI theme code (reference) C22C 38/58 C22C 38/58 (72) Inventor Natsuko Sugiura 20-1 Shintomi, Futtsu City, Chiba Nippon Steel Co., Ltd. (72) Inventor Takaaki Nakamura 1st Nishinosu, Oita-shi, Oita Prefecture Nippon Steel Co., Ltd. Oita Steel Co., Ltd. (72) Inventor Takehiro Nakamoto 1st Nishinosu, Oita-shi, Oita Nippon Steel Co., Ltd. Company Oita Steel Works F-term (reference) 4E002 AD04 AD05 BC05 BC08 BD07 BD10 CB01 4K037 EA01 EA02 EA05 EA09 EA11 EA13 EA15 EA16 EA17 EA18 EA19 EA20 EA23 EA25 EA03 FB03 GA08 EA03 FB08 EA03 FB03 EA35 FB03 EA03 FB03 EA35 FB03 EA35 FB03 EA35 FB08 EA03 FB08 EA03 FB03 EA35 FB03 EA03 FB08 EA03 FB03 FB05 EA36 FB08 EA35 FB03 FB03 FB07 FB07 FB08

Claims (17)

【特許請求の範囲】[Claims] 【請求項1】 質量%にて、 C :0.01〜0.1%、 S ≦0.03%、 N ≦0.005%、 Ti:0.05〜0.5% を含み、さらに Ti−48/12C−48/14N−48/32S≧0
% を満たす範囲でTiを含有し、残部がFe及び不可避的
不純物からなる鋼であって、少なくとも板厚の1/2厚
における板面の{100}<011>〜{223}<1
10>方位群のX線ランダム強度比の平均値が3以上か
つ、{554}<225>、{111}<112>およ
び{111}<110>の3方位のX線ランダム強度比
の平均値が3.5以下であり、少なくとも一方の鋼板表
面の算術平均粗さRaが1〜3.5である鋼板に潤滑効
果のある組成物が塗布されていることを特徴とする、形
状凍結性に優れる絞り可能なバーリング性高強度薄鋼
板。
1. In mass%, C: 0.01 to 0.1%, S ≤ 0.03%, N ≤ 0.005%, Ti: 0.05 to 0.5% are included, and Ti is further included. -48 / 12C-48 / 14N-48 / 32S ≧ 0
% Ti in a range of satisfying at least 1.0%, and the balance being Fe and unavoidable impurities, and having {100} <011> to {223} <1 of the plate surface at least at 1/2 the plate thickness.
10> The average value of the X-ray random intensity ratios of the orientation groups of 3 or more and the average value of the X-ray random intensity ratios of the three orientations of {554} <225>, {111} <112> and {111} <110>. Is 3.5 or less, and a composition having a lubricating effect is applied to a steel plate having an arithmetic average roughness Ra of at least one steel plate surface of 1 to 3.5. Excellent squeezable burring high strength steel sheet.
【請求項2】 請求項1に記載の鋼板表面の0〜200
℃における摩擦係数が0.05〜0.2であることを特
徴とする形状凍結性に優れる絞り可能なバーリング性高
強度薄鋼板。
2. The surface of the steel sheet according to claim 1, which is 0 to 200.
A burring-type high-strength thin steel sheet which is excellent in shape fixability and has a coefficient of friction of 0.05 to 0.2 at ℃.
【請求項3】 請求項1または2記載に記載の鋼が、さ
らに、質量%にて、 Nb=0.01〜0.5% を含み、さらに Ti+48/93Nb−48/12C−48/14N−
48/32S≧0% を満たす範囲でTiとNbを含有し、残部がFeおよび
不可避的不純物からなる鋼であることを特徴とする形状
凍結性に優れる絞り可能なバーリング性高強度薄鋼板。
3. The steel according to claim 1 or 2, further comprising, in mass%, Nb = 0.01 to 0.5%, and further Ti + 48 / 93Nb-48 / 12C-48 / 14N-.
A drawable burring high-strength thin steel sheet having excellent shape fixability, which is a steel containing Ti and Nb in a range satisfying 48 / 32S ≧ 0% and the balance being Fe and inevitable impurities.
【請求項4】 請求項1ないし3のいずれか1項に記載
の鋼が、さらに、質量%にて、 Si:0.01〜2%、 Mn:0.05〜3%、 P ≦0.1%、 Al:0.005〜1% を含有することを特徴とする形状凍結性に優れる絞り可
能なバーリング性高強度薄鋼板。
4. The steel according to claim 1, further comprising, in mass%, Si: 0.01 to 2%, Mn: 0.05 to 3%, and P ≤ 0. 1%, Al: 0.005 to 1% is contained, and a burringable high-strength thin steel sheet having excellent shape fixability and capable of being drawn.
【請求項5】 請求項1ないし4のいずれか1項に記載
の鋼が、さらに、質量%にて、 B :0.0002〜0.002% を含有することを特徴とする形状凍結性に優れる絞り可
能なバーリング性高強度薄鋼板。
5. The shape fixability according to claim 1, wherein the steel according to claim 1 further contains B: 0.0002 to 0.002% in mass%. Excellent squeezable burring high strength steel sheet.
【請求項6】 請求項1ないし5のいずれか1項に記載
の鋼が、さらに、質量%にて、 Cu:0.2〜1.2% を含有することを特徴とする形状凍結性に優れる絞り可
能なバーリング性高強度薄鋼板。
6. The shape fixability according to claim 1, wherein the steel according to claim 1 further contains Cu: 0.2 to 1.2% in mass%. Excellent squeezable burring high strength steel sheet.
【請求項7】 請求項1ないし6のいずれか1項に記載
の鋼が、さらに、質量%にて、 Ni:0.1〜0.6% を含有することを特徴とする形状凍結性に優れる絞り可
能なバーリング性高強度薄鋼板。
7. The shape fixability according to claim 1, wherein the steel according to any one of claims 1 to 6 further contains, in mass%, Ni: 0.1 to 0.6%. Excellent squeezable burring high strength steel sheet.
【請求項8】 請求項1ないし7のいずれか1項に記載
の鋼が、さらに、質量%にて、 Ca:0.0005〜0.002%、 REM:0.0005〜0.02% の一種または二種を含有することを特徴とする形状凍結
性に優れる絞り可能なバーリング性高強度薄鋼板。
8. The steel according to claim 1, further comprising, in mass%, Ca: 0.0005 to 0.002% and REM: 0.0005 to 0.02%. A burring high-strength thin steel sheet with excellent shape fixability, which contains one or two kinds.
【請求項9】 請求項1ないし8のいずれか1項に記載
の鋼が、さらに、質量%にて、 Mo:0.05〜1%、 V :0.02〜0.2%、 Cr:0.01〜1%、 Zr:0.02〜0.2% の一種または二種以上を含有することを特徴とする形状
凍結性に優れる絞り可能なバーリング性高強度薄鋼板。
9. The steel according to claim 1, further comprising, in mass%, Mo: 0.05 to 1%, V: 0.02 to 0.2%, Cr: 0.01 to 1%, Zr: 0.02 to 0.2%, and one or more of them are contained.
【請求項10】 請求項1ないし9のいずれか1項に記
載の絞り可能なバーリング性高強度薄鋼板に亜鉛めっき
を施されていることを特徴とする形状凍結性に優れる絞
り可能なバーリング性高強度薄鋼板。
10. A drawable burring property excellent in shape fixability, characterized in that the drawable burring high strength steel sheet according to claim 1 is galvanized. High strength thin steel sheet.
【請求項11】 請求項1ないし9のいずれか1項に記
載の成分を有する薄鋼板を得るための熱間圧延する際
に、該成分を有する鋼片を粗圧延後にAr3 変態点温度
+100℃以下の温度域で鋼板厚の合計圧下率25%以
上の仕上圧延をし、その後冷却して巻き取った後、潤滑
効果のある組成物を塗布することを特徴とする形状凍結
性に優れる絞り可能なバーリング性高強度薄鋼板の製造
方法。
11. When hot rolling to obtain a thin steel sheet having a component according to any one of claims 1 to 9, Ar3 transformation point temperature + 100 ° C. after rough rolling of a steel slab having the component. Finishing rolling with a total reduction of 25% or more of steel plate thickness in the following temperature range, then cooling and winding, and then applying a composition having a lubricating effect. For producing a high strength thin steel sheet with excellent burring property.
【請求項12】 前記熱間圧延に際し、粗圧延後の仕上
圧延において潤滑圧延を施すことを特徴とする請求項1
1に記載の形状凍結性に優れる絞り可能なバーリング性
高強度薄鋼板の製造方法。
12. The lubrication rolling is performed in the finishing rolling after the rough rolling during the hot rolling.
1. A method for producing a burring high-strength thin steel sheet capable of being drawn, which is excellent in shape fixability.
【請求項13】 請求項11または12に記載の熱間圧
延に際し、粗圧延終了後、デスケーリングを行うことを
特徴とする形状凍結性に優れる絞り可能なバーリング性
高強度薄鋼板の製造方法。
13. A method for producing a drawable burring high strength steel sheet having excellent shape fixability, which comprises descaling after rough rolling in the hot rolling according to claim 11 or 12.
【請求項14】 請求項1ないし9のいずれか1項に記
載の成分を有する薄鋼板を得るために、該成分を有する
鋼片を熱間圧延、続く酸洗、鋼板厚圧下率80%未満の
冷間圧延後、回復温度以上Ac3 変態点温度+100℃
以下の温度域で5〜150秒間保持し、冷却する工程の
熱処理をした後、潤滑効果のある組成物を塗布すること
を特徴とする形状凍結性に優れる絞り可能なバーリング
性高強度薄鋼板の製造方法。
14. In order to obtain a thin steel sheet having a component according to any one of claims 1 to 9, hot rolling of a slab having the component, subsequent pickling, and a steel plate thickness reduction of less than 80%. After cold rolling, recovery temperature is above Ac3 transformation point temperature + 100 ° C
A burring high-strength thin steel sheet having excellent shape fixability, which is characterized by applying a composition having a lubricating effect after performing heat treatment in a step of cooling for 5 to 150 seconds in the following temperature range. Production method.
【請求項15】 請求項11ないし13のいずれか1項
に記載の製造方法に際し、熱間圧延後に亜鉛めっき浴中
に浸積させて鋼板表面を亜鉛めっきした後、潤滑効果の
ある組成物を塗布することを特徴とする形状凍結性に優
れる絞り可能なバーリング性高強度薄鋼板の製造方法。
15. The method according to any one of claims 11 to 13, wherein after hot rolling, the surface of a steel sheet is galvanized by being immersed in a galvanizing bath, and then a composition having a lubricating effect is obtained. A method for producing a burring high-strength steel sheet capable of being drawn, which is excellent in shape fixability and is characterized by being applied.
【請求項16】 請求項14に記載の製造方法に際し、
熱処理終了後、亜鉛めっき浴中に浸積させて鋼板表面を
亜鉛めっきした後、潤滑効果のある組成物を塗布するこ
とを特徴とする形状凍結性に優れる絞り可能なバーリン
グ性高強度薄鋼板の製造方法。
16. In the manufacturing method according to claim 14,
After finishing the heat treatment, the steel sheet surface is dipped in a galvanizing bath to be galvanized, and then a composition having a lubricating effect is applied. Production method.
【請求項17】 請求項15または16に記載の製造方
法に際し、亜鉛めっき浴中に浸積して亜鉛めっき後、合
金化処理した後、潤滑効果のある組成物を塗布すること
を特徴とする形状凍結性に優れる絞り可能なバーリング
性高強度薄鋼板の製造方法。
17. The manufacturing method according to claim 15 or 16, wherein the composition having a lubricating effect is applied after dipping in a galvanizing bath for galvanizing and then alloying treatment. A method for producing a burring high-strength steel sheet capable of being drawn, which is excellent in shape fixability.
JP2001360084A 2001-10-04 2001-11-26 Squeezable burring high-strength thin steel sheet having excellent shape freezing property and manufacturing method thereof Expired - Fee Related JP4028719B2 (en)

Priority Applications (12)

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JP2001360084A JP4028719B2 (en) 2001-11-26 2001-11-26 Squeezable burring high-strength thin steel sheet having excellent shape freezing property and manufacturing method thereof
DE60224557A DE60224557D1 (en) 2001-10-04 2002-10-04 PULLABLE HIGH STRENGTH STEEL PLATE WITH OUTSTANDING FORMFIXING PROPERTY AND METHOD OF MANUFACTURING THEREOF
DE60224557.5T DE60224557T4 (en) 2001-10-04 2002-10-04 A tensile high strength thin steel sheet having excellent shape fixing property and manufacturing method therefor
PCT/JP2002/010386 WO2003031669A1 (en) 2001-10-04 2002-10-04 High-strength thin steel sheet drawable and excellent in shape fixation property and method of producing the same
CA2462260A CA2462260C (en) 2001-10-04 2002-10-04 High-strength thin steel sheet drawable and excellent in shape fixation property and method of producing the same
ES02800781T ES2297047T5 (en) 2001-10-04 2002-10-04 Thin steel sheet, high strength, which can be embedded and is excellent in the property of fixing the shapes, and method for its production
AT02800781T ATE383452T1 (en) 2001-10-04 2002-10-04 DRAWABLE HIGH STRENGTH THIN STEEL SHEET HAVING EXCELLENT FORM-FIXING PROPERTIES AND PRODUCTION PROCESS THEREOF
US10/491,928 US7503984B2 (en) 2001-10-04 2002-10-04 High-strength thin steel sheet drawable and excellent in shape fixation property and method of producing the same
KR1020047005067A KR100627429B1 (en) 2001-10-04 2002-10-04 High-strength thin steel sheet drawable and excellent in shape fixation property and method of producing the same
TW091123026A TWI236503B (en) 2001-10-04 2002-10-04 High-strength thin steel sheet drawable and excellent in shape fixation property and method of producing the same
EP02800781.3A EP1444374B9 (en) 2001-10-04 2002-10-04 High-strength thin steel sheet drawable and excellent in shape fixation property and method of producing the same
CNB028243153A CN100347325C (en) 2001-10-04 2002-10-04 High-strength thin steel sheet drawable and excellent in shape fixation property and method of producing the same

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