IN2015DN01079A - - Google Patents
Info
- Publication number
- IN2015DN01079A IN2015DN01079A IN1079DEN2015A IN2015DN01079A IN 2015DN01079 A IN2015DN01079 A IN 2015DN01079A IN 1079DEN2015 A IN1079DEN2015 A IN 1079DEN2015A IN 2015DN01079 A IN2015DN01079 A IN 2015DN01079A
- Authority
- IN
- India
- Prior art keywords
- moieties
- compound
- acid
- ammoalkylenephosphomc
- aldehyde
- Prior art date
Links
- 150000001875 compounds Chemical class 0.000 abstract 3
- 229910004856 P—O—P Inorganic materials 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- 150000001299 aldehydes Chemical class 0.000 abstract 2
- 150000002576 ketones Chemical class 0.000 abstract 2
- 230000003647 oxidation Effects 0.000 abstract 2
- 238000007254 oxidation reaction Methods 0.000 abstract 2
- 125000004437 phosphorous atom Chemical group 0.000 abstract 2
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical class OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 abstract 1
- 239000003377 acid catalyst Substances 0.000 abstract 1
- 150000008064 anhydrides Chemical group 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000003786 synthesis reaction Methods 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
- A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/6527—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having nitrogen and oxygen atoms as the only ring hetero atoms
- C07F9/6533—Six-membered rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
- C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
- C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
- C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
- C07F9/3839—Polyphosphonic acids
- C07F9/3873—Polyphosphonic acids containing nitrogen substituent, e.g. N.....H or N-hydrocarbon group which can be substituted by halogen or nitro(so), N.....O, N.....S, N.....C(=X)- (X =O, S), N.....N, N...C(=X)...N (X =O, S)
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
- C07F9/572—Five-membered rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
- C07F9/572—Five-membered rings
- C07F9/5728—Five-membered rings condensed with carbocyclic rings or carbocyclic ring systems
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/645—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having two nitrogen atoms as the only ring hetero atoms
- C07F9/6503—Five-membered rings
- C07F9/6506—Five-membered rings having the nitrogen atoms in positions 1 and 3
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/6527—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having nitrogen and oxygen atoms as the only ring hetero atoms
- C07F9/653—Five-membered rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Molecular Biology (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
The present invention is related to a method for the synthesis of an ammoalkylenephosphomc acid or its phosphonate esters comprising the following steps: a) forming, in the presence of an aldehyde or ketone and an acid catalyst, a reaction mixture by mixing a compound comprising at least one HNR'R 2 moiety or a salt thereof, with a compound having one or more P-O-P anhydride moieties, said moieties comprising one P atom at the oxidation state (+IP) and one P atom at the oxidation state (+IP) or (+V), wherein the ratio of moles of aldehyde or ketone to N-H moieties is 1 or more and wherein the ratio of N-H moieties to P-O-P an - hydride moieties is 0.3 or more and, b) recovering the resulting ammoalkylenephosphomc acid comprising compound or its pilosphonate esters.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12176753 | 2012-07-17 | ||
| PCT/EP2013/065121 WO2014012987A1 (en) | 2012-07-17 | 2013-07-17 | Method for the synthesis of aminoalkylenephosphonic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IN2015DN01079A true IN2015DN01079A (en) | 2015-06-26 |
Family
ID=49003748
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IN1079DEN2015 IN2015DN01079A (en) | 2012-07-17 | 2013-07-17 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US10280189B2 (en) |
| EP (1) | EP2875036A1 (en) |
| CN (1) | CN104812766B (en) |
| BR (1) | BR112015000990B1 (en) |
| IN (1) | IN2015DN01079A (en) |
| RU (1) | RU2694047C2 (en) |
| WO (1) | WO2014012987A1 (en) |
Family Cites Families (69)
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| CH275435A (en) | 1949-06-30 | 1951-05-31 | Cilag Ag | Process for producing a phosphonic acid. |
| NL285361A (en) | 1961-11-13 | 1900-01-01 | ||
| US3400148A (en) | 1965-09-23 | 1968-09-03 | Procter & Gamble | Phosphonate compounds |
| GB1142294A (en) | 1966-02-08 | 1969-02-05 | Albright & Wilson Mfg Ltd | Improvements in production of amino alkylene phosphonic acids |
| GB1230121A (en) | 1967-01-27 | 1971-04-28 | ||
| US3455675A (en) | 1968-06-25 | 1969-07-15 | Monsanto Co | Aminophosphonate herbicides |
| DE2013371B1 (en) | 1970-03-20 | 1971-11-04 | Joh A , Benckiser GmbH, Chemische Fabrik, 6700 Ludwigshafen | Process for the production of amino methylenephosphonic acids |
| DE2132511C3 (en) | 1971-06-30 | 1974-06-27 | Joh. A. Benckiser Gmbh, 6700 Ludwigshafen | Process for the preparation of aminomethylene phosphonic acids |
| DE2017974A1 (en) | 1970-04-15 | 1971-11-04 | Joh. A. Benckiser Gmbh Chemische Fabrik, 6700 Ludwigshafen | Process for the preparation of aminoalkylenephosphonic acids |
| US3799758A (en) | 1971-08-09 | 1974-03-26 | Monsanto Co | N-phosphonomethyl-glycine phytotoxicant compositions |
| US3969398A (en) | 1974-05-01 | 1976-07-13 | Monsanto Company | Process for producing N-phosphonomethyl glycine |
| HU173170B (en) | 1974-06-27 | 1979-03-28 | Chinoin Gyogyszer Es Vegyeszet | Process for producing n-phosphonomethyl-glycine |
| US3927080A (en) | 1974-09-03 | 1975-12-16 | Monsanto Co | Process for producing N-phosphonomethyl glycine |
| IL48619A (en) | 1974-12-11 | 1978-04-30 | Monsanto Co | Process for the production of n-(phosphonomethyl)-glycine compounds |
| DD123192A1 (en) | 1975-01-16 | 1976-12-05 | ||
| CH647528A5 (en) | 1978-10-27 | 1985-01-31 | Bcap Biolog Chem Act Pat | PROCESS FOR THE PREPARATION OF N-phosphonomethylglycine. |
| US4211547A (en) | 1978-12-22 | 1980-07-08 | Monsanto Company | N-Phosphonomethyliminodiacetonitrile and certain derivatives thereof |
| DE3016289A1 (en) | 1980-04-28 | 1981-10-29 | Henkel KGaA, 4000 Düsseldorf | METHOD FOR PRODUCING OMEGA-AMINO-1-HYDROXYALKYLIDEN-1,1-BIS-PHOSPHONIC ACIDS |
| JPS5775990A (en) | 1980-10-27 | 1982-05-12 | Mitsubishi Gas Chem Co Inc | Preparation of n,n,n',n'-tetra(phosphonomethyl) diaminoalkane |
| US4422982A (en) | 1982-06-30 | 1983-12-27 | Stauffer Chemical Company | Method for preparation of N-phosphonomethylglycine |
| US4400330A (en) | 1982-07-29 | 1983-08-23 | Stauffer Chemical Company | Method for preparation of N-phosphonomethylglycine |
| US4654429A (en) | 1983-12-02 | 1987-03-31 | Monsanto Company | Process for the preparation of a glyphosate product |
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| US4724103A (en) | 1984-02-27 | 1988-02-09 | Monsanto Company | Process for preparing N,N-diacetic acid aminomethylenephosphonic acid |
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| US4804499A (en) | 1985-09-23 | 1989-02-14 | Monsanto Company | Process for the preparation of N-substituted aminomethylphosphonic acids |
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| HU200780B (en) | 1988-02-08 | 1990-08-28 | Nitrokemia Ipartelepek | Process for producing n-phosphonomethyl iminodiacetic acid from double salt of iminodiacetic acid |
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| ES2225764T3 (en) | 2001-01-12 | 2005-03-16 | Basf Aktiengesellschaft | PROCEDURE FOR OBTAINING N-PHOSPHONE-METHYLIMINODYACETIC ACID. |
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| EP1681294A1 (en) | 2005-01-17 | 2006-07-19 | Solutia Europe N.V./S.A. | Process for the manufacture of aminopolyalkylene-phosphonic acid compounds |
| EP1681295A1 (en) | 2005-01-17 | 2006-07-19 | Solutia Europe N.V./S.A. | Process for the manufacture of aminoakylenephosphonic acid compounds in the presence of a heterogeneous catalyst |
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| JP2007022956A (en) | 2005-07-15 | 2007-02-01 | Mitsubishi Gas Chem Co Inc | Method for producing high purity aminomethylene phosphonic acid |
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| CL2008003539A1 (en) | 2007-11-28 | 2009-07-03 | Process for the production of p4o6 that comprises mixing o2 or a mixture of o2 plus an inert gas and phosphorus where the product obtained is kept within a reaction unit at a temperature between 1600 and 2000 k for at least 1 second. | |
| EP2112156A1 (en) | 2008-04-25 | 2009-10-28 | Thermphos International B.V. | Method for the Manufacture of Aminoalkylene Phosphonic Acid |
| PL2297169T3 (en) | 2008-04-25 | 2015-06-30 | Monsanto Technology Llc | Method for the manufacture of aminoalkylene phosphonic acid |
| KR101361345B1 (en) | 2008-11-12 | 2014-02-10 | 스트라이트마르크 홀딩 아게 | Process for the manufacture of p4o6 with high yield |
| CN102448975A (en) * | 2009-05-28 | 2012-05-09 | 施里特马克控股公司 | Process for preparing aminoalkylene phosphonic acids |
| CN102448974A (en) | 2009-05-28 | 2012-05-09 | 施里特马克控股公司 | Process for preparing phosphonoalkyliminodiacetic acid |
| US8779135B2 (en) | 2009-10-02 | 2014-07-15 | Straitmark Holding Ag | Method for the manufacture of aminohydroxy diphosphonic acids |
| CN102639546B (en) | 2009-10-27 | 2015-03-25 | 施里特马克控股公司 | Process for the preparation of phosphonoalkyliminodiacetic acids |
| CN104620073B (en) | 2012-06-13 | 2016-08-17 | 皇家飞利浦有限公司 | Determine the spread speed of surface wave |
| BR112015000966B1 (en) | 2012-07-17 | 2020-04-28 | Monsanto Technology Llc | method for the synthesis of n- (phosphonomethyl) glycine or one of its derivatives selected from the group consisting of its salts, its phosphonate esters and its phosphonate ester salts |
| CN104812765B (en) | 2012-07-17 | 2017-06-06 | 斯特雷特马克控股股份公司 | Process for the synthesis of α-aminoalkylene phosphonic acids |
| BR112015000988A2 (en) | 2012-07-17 | 2017-06-27 | Straitmark Holding Ag | method for the synthesis of n-phosphonomethyliminodiacetic acid or derivatives thereof |
-
2013
- 2013-07-17 US US14/415,686 patent/US10280189B2/en active Active
- 2013-07-17 WO PCT/EP2013/065121 patent/WO2014012987A1/en active Application Filing
- 2013-07-17 IN IN1079DEN2015 patent/IN2015DN01079A/en unknown
- 2013-07-17 EP EP13750855.2A patent/EP2875036A1/en not_active Withdrawn
- 2013-07-17 BR BR112015000990A patent/BR112015000990B1/en active IP Right Grant
- 2013-07-17 RU RU2015103306A patent/RU2694047C2/en active
- 2013-07-17 CN CN201380037546.8A patent/CN104812766B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| RU2694047C2 (en) | 2019-07-09 |
| BR112015000990A2 (en) | 2017-06-27 |
| US10280189B2 (en) | 2019-05-07 |
| CN104812766A (en) | 2015-07-29 |
| CN104812766B (en) | 2017-06-06 |
| US20150225431A1 (en) | 2015-08-13 |
| BR112015000990B1 (en) | 2020-04-28 |
| WO2014012987A1 (en) | 2014-01-23 |
| EP2875036A1 (en) | 2015-05-27 |
| RU2015103306A (en) | 2016-09-10 |
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