IE43613L - Making tertiary amines. - Google Patents
Making tertiary amines.Info
- Publication number
- IE43613L IE43613L IE761729A IE172976A IE43613L IE 43613 L IE43613 L IE 43613L IE 761729 A IE761729 A IE 761729A IE 172976 A IE172976 A IE 172976A IE 43613 L IE43613 L IE 43613L
- Authority
- IE
- Ireland
- Prior art keywords
- methylamines
- reaction
- tertiary amines
- amine
- making tertiary
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling
- B01J2219/00108—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling involving reactant vapours
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Tertiary aliphatic methylamines of the formula I, which have 1 to 2 long-chain alkyl or alkenyl radicals having 8 to 24 C atoms, are prepared by reacting the corresponding alcohols and/or aldehydes with primary or secondary methylamines in the liquid phase under virtually pressure-free conditions. In this process, a hydrogen/amine mixture, where the amine accounts for 1 to 20% by volume, is circulated. The reaction is carried out in the presence of a cobalt chromite or copper chromite catalyst. The water of reaction is removed from the circulating gas. The resulting amines can be used as intermediates. <IMAGE>
[GB1538138A]
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2535073A DE2535073C3 (en) | 1975-08-06 | 1975-08-06 | Process for the preparation of tertiary aliphatic amines |
Publications (2)
Publication Number | Publication Date |
---|---|
IE43613L true IE43613L (en) | 1977-02-06 |
IE43613B1 IE43613B1 (en) | 1981-04-08 |
Family
ID=5953342
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IE1729/76A IE43613B1 (en) | 1975-08-06 | 1976-08-05 | Process for the preparation of tertiary aliphatic amines |
Country Status (28)
Country | Link |
---|---|
JP (1) | JPS601297B2 (en) |
AR (1) | AR208045A1 (en) |
AT (1) | AT346823B (en) |
AU (1) | AU509878B2 (en) |
BE (1) | BE844974A (en) |
BR (1) | BR7605125A (en) |
CA (1) | CA1101889A (en) |
CH (1) | CH622237A5 (en) |
DD (1) | DD125657A5 (en) |
DE (1) | DE2535073C3 (en) |
DK (1) | DK145493C (en) |
ES (1) | ES450344A1 (en) |
FI (1) | FI62822C (en) |
FR (1) | FR2320287A1 (en) |
GB (1) | GB1538138A (en) |
HU (1) | HU178244B (en) |
IE (1) | IE43613B1 (en) |
IT (1) | IT1065117B (en) |
LU (1) | LU75536A1 (en) |
MX (1) | MX143899A (en) |
NL (1) | NL186765C (en) |
NO (1) | NO142709C (en) |
PL (1) | PL106214B1 (en) |
PT (1) | PT65443B (en) |
SE (1) | SE433207B (en) |
SU (1) | SU745359A3 (en) |
YU (1) | YU193476A (en) |
ZA (1) | ZA764757B (en) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2639648A1 (en) * | 1976-09-03 | 1978-03-16 | Basf Ag | Tert.-amines prepd. from prim. or sec. amines and alcohols - with a hydrogenation-dehydrogenation catalyst and stoichiometric amt. of alcohol |
DE2621449C3 (en) * | 1976-05-14 | 1988-07-07 | Basf Ag, 6700 Ludwigshafen | Process for the preparation of tertiary amines |
BE530219A (en) * | 1976-05-14 | |||
BE871092A (en) * | 1977-10-17 | 1979-04-09 | Shell Int Research | PROCESS FOR PREPARING AN AMINE |
DE2824908A1 (en) * | 1978-06-07 | 1979-12-20 | Basf Ag | METHOD FOR MANUFACTURING OMEGA, OMEGA'-BIS-DIALKYLAMINOALKANES |
JPS559019A (en) * | 1978-07-04 | 1980-01-22 | Lion Corp | Preparation of tertiary long-chain aliphatic methylamine |
FR2463120A1 (en) * | 1979-08-14 | 1981-02-20 | Ugine Kuhlmann | Di:methyl:ethylamine prepn. from ethanol and di:methylamine - in presence of copper and chromium oxide catalyst |
EP0024225B2 (en) * | 1979-08-14 | 1993-11-10 | P C U K Produits Chimiques Ugine Kuhlmann | Process for the preparation of dimethylethyl amine |
US4255357A (en) * | 1980-03-24 | 1981-03-10 | Pennwalt Corporation | Catalytic process for preparing ethyl amines |
JPS59106441A (en) * | 1982-12-09 | 1984-06-20 | New Japan Chem Co Ltd | Preparation of aliphatic tertiary amine |
JPS6115865A (en) * | 1984-06-29 | 1986-01-23 | Kao Corp | Production of tertiary amine |
DE3539266A1 (en) * | 1985-11-06 | 1987-05-07 | Basf Ag | METHOD FOR PRODUCING TRIALKYLAMINE |
DE3942793A1 (en) * | 1989-12-23 | 1991-06-27 | Hoechst Ag | METHOD FOR PRODUCING N, N-DIMETHYLAMINES |
JP2706595B2 (en) * | 1991-04-22 | 1998-01-28 | 花王株式会社 | Method for producing N-alkyl or alkenyl-N-methylamine |
JP5750367B2 (en) * | 2010-12-27 | 2015-07-22 | 花王株式会社 | Method for producing tertiary amine |
US8927772B2 (en) | 2010-12-27 | 2015-01-06 | Kao Corporation | Tertiary amine preparation process |
JP5879123B2 (en) * | 2011-12-27 | 2016-03-08 | 花王株式会社 | Method for producing tertiary amine |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE500692C (en) * | 1925-05-24 | 1930-09-05 | I G Farbenindustrie Akt Ges | Process for the production of pure iron |
US2597701A (en) * | 1948-12-06 | 1952-05-20 | Gen Aniline & Film Corp | Method of producing finely divided metals |
DE824198C (en) * | 1949-10-22 | 1951-12-10 | Basf Ag | Process for the production of iron powder |
DE833955C (en) * | 1950-01-03 | 1952-03-13 | Basf Ag | Production of coarse-grained metal powders |
US2612440A (en) * | 1950-05-03 | 1952-09-30 | Gen Aniline & Film Corp | Production of metal carbonyl powders of small size |
US2674528A (en) * | 1951-01-22 | 1954-04-06 | Gen Aniline & Film Corp | Production of metal carbonyl powders of small size |
DE936391C (en) * | 1954-01-06 | 1955-12-29 | Basf Ag | Process for the production of metal powders |
GB825740A (en) * | 1957-01-24 | 1959-12-23 | Gen Aniline & Film Corp | Production of finely divided metals |
DE1433361A1 (en) * | 1964-11-26 | 1968-12-12 | Friedenberg Serafima E | Process for the production of highly dispersed carbonyl iron powder |
-
1975
- 1975-08-06 DE DE2535073A patent/DE2535073C3/en not_active Expired
-
1976
- 1976-01-01 AR AR264239A patent/AR208045A1/en active
- 1976-07-30 NL NLAANVRAGE7608493,A patent/NL186765C/en not_active IP Right Cessation
- 1976-07-31 ES ES450344A patent/ES450344A1/en not_active Expired
- 1976-08-03 CH CH990876A patent/CH622237A5/en not_active IP Right Cessation
- 1976-08-04 HU HU76HO1920A patent/HU178244B/en unknown
- 1976-08-04 DD DD194209A patent/DD125657A5/xx unknown
- 1976-08-04 FI FI762223A patent/FI62822C/en not_active IP Right Cessation
- 1976-08-04 SE SE7608741A patent/SE433207B/en unknown
- 1976-08-04 IT IT26035/76A patent/IT1065117B/en active
- 1976-08-04 AT AT574976A patent/AT346823B/en not_active IP Right Cessation
- 1976-08-04 LU LU75536A patent/LU75536A1/xx unknown
- 1976-08-05 MX MX165794A patent/MX143899A/en unknown
- 1976-08-05 AU AU16582/76A patent/AU509878B2/en not_active Expired
- 1976-08-05 SU SU762388321A patent/SU745359A3/en active
- 1976-08-05 PL PL1976191645A patent/PL106214B1/en unknown
- 1976-08-05 JP JP51092851A patent/JPS601297B2/en not_active Expired
- 1976-08-05 YU YU01934/76A patent/YU193476A/en unknown
- 1976-08-05 CA CA258,464A patent/CA1101889A/en not_active Expired
- 1976-08-05 BR BR7605125A patent/BR7605125A/en unknown
- 1976-08-05 IE IE1729/76A patent/IE43613B1/en unknown
- 1976-08-05 DK DK353976A patent/DK145493C/en active
- 1976-08-05 NO NO762730A patent/NO142709C/en unknown
- 1976-08-05 PT PT65443A patent/PT65443B/en unknown
- 1976-08-06 ZA ZA764757A patent/ZA764757B/en unknown
- 1976-08-06 FR FR7624063A patent/FR2320287A1/en active Granted
- 1976-08-06 BE BE169632A patent/BE844974A/en not_active IP Right Cessation
- 1976-08-06 GB GB32873/76A patent/GB1538138A/en not_active Expired
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