GB764340A - Process for the preparation of derivatives of aliphatic sulphonic acids or their salts - Google Patents

Process for the preparation of derivatives of aliphatic sulphonic acids or their salts

Info

Publication number
GB764340A
GB764340A GB22734/54A GB2273454A GB764340A GB 764340 A GB764340 A GB 764340A GB 22734/54 A GB22734/54 A GB 22734/54A GB 2273454 A GB2273454 A GB 2273454A GB 764340 A GB764340 A GB 764340A
Authority
GB
United Kingdom
Prior art keywords
acids
sulphonic acid
acid
propane
sodium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB22734/54A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Boehme Fettchemie GmbH
Original Assignee
Boehme Fettchemie GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Boehme Fettchemie GmbH filed Critical Boehme Fettchemie GmbH
Publication of GB764340A publication Critical patent/GB764340A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D295/00Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/16Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms acylated on ring nitrogen atoms
    • C07D295/20Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms acylated on ring nitrogen atoms by radicals derived from carbonic acid, or sulfur or nitrogen analogues thereof
    • C07D295/21Radicals derived from sulfur analogues of carbonic acid
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/32Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of salts of sulfonic acids
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C329/00Thiocarbonic acids; Halides, esters or anhydrides thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C333/00Derivatives of thiocarbamic acids, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
    • C07C333/14Dithiocarbamic acids; Derivatives thereof
    • C07C333/18Esters of dithiocarbamic acids
    • C07C333/20Esters of dithiocarbamic acids having nitrogen atoms of dithiocarbamate groups bound to hydrogen atoms or to acyclic carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C335/00Thioureas, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C335/30Isothioureas
    • C07C335/32Isothioureas having sulfur atoms of isothiourea groups bound to acyclic carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D213/00Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/06Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom
    • C07D213/16Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom containing only one pyridine ring
    • C07D213/20Quaternary compounds thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D277/00Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings
    • C07D277/60Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings condensed with carbocyclic rings or ring systems
    • C07D277/62Benzothiazoles
    • C07D277/68Benzothiazoles with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached in position 2
    • C07D277/70Sulfur atoms
    • C07D277/74Sulfur atoms substituted by carbon atoms

Abstract

Derivatives of aliphatic sulphonic acids or their salts are obtained by reacting together a compound which contains a reactive hydrogen atom or a reactive replaceable metal atom or an atom convertible to a higher state of valency and which can be alkylated and a cyclic anhydride of an organic sulphonic acid (a sultone), if necessary in the presence of acid-neutralizing means, the reaction being carried out in the presence of water or an aqueous organic solvent. As sultones there may be used 1,3-propane sultone, 1,4-butanesultone, isobutane sultone, tolylsultone, and 1,8-naphthsultone. The other reactant may comprise hydroxy, carboxy, amino, imino, amido, imide or mercapto compounds of inorganic, aliphatic, cycloaliphatic, aromatic or heterocyclic nature or salts thereof, thiol-acids, dithio-acids, xanthogenic acids, dithiocarbamic acids, trithiocarbamic acids, trithiocarbonic acids and sulphinic acids, tetiary amines, thio-ethers and phosphines. Examples disclose the preparation of the sodium salt of 2,4,6-trichlorophenoxypropaneo -sulphonic acid, sodium phenylthiopropane-o -sulphonate, the disodium salt of thiocarbonylbis-thiopropane-o -sulphonic acid, sodium N,N-diethylthiocarbamic acid - propyl - ester - o - sulphonate, the sulphobetaine of isothiourea-S-propane-o -sulphonic acid, the sulphobetaine of isothiourea - S - butane - o - sulphonic acid, sodium mercaptobenzthiazole-S-propane-o -sulphonate, the betaine of pyridine-N-propane-o -sulphonic acid, 3-chloropropane-1-sulphonic acid, the sodium salt of piperazine-N,n1-bisdithiocarbonic acid - n - propylester - o - sulphonic acid, and the sodium salt of N,N-diethanoldithiocarbamic acid n-propyl ester sulphonic acid.
GB22734/54A 1953-08-05 1954-08-05 Process for the preparation of derivatives of aliphatic sulphonic acids or their salts Expired GB764340A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE764340X 1953-08-05

Publications (1)

Publication Number Publication Date
GB764340A true GB764340A (en) 1956-12-28

Family

ID=6672851

Family Applications (1)

Application Number Title Priority Date Filing Date
GB22734/54A Expired GB764340A (en) 1953-08-05 1954-08-05 Process for the preparation of derivatives of aliphatic sulphonic acids or their salts

Country Status (1)

Country Link
GB (1) GB764340A (en)

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3084163A (en) * 1958-04-29 1963-04-02 Dehydag Gmbh Heterocyclic thioalkane sulfonic acids and methods for their production
US3151123A (en) * 1962-06-19 1964-09-29 Keystone Chemurgic Corp Acid-soluble chlorophyllins and their production
US3231580A (en) * 1961-06-30 1966-01-25 Hans S Mannheimer Substituted imidazolines
US3244724A (en) * 1961-01-25 1966-04-05 Armour & Co Sulfoalkylated imidazolines
US3280179A (en) * 1961-03-16 1966-10-18 Textilana Corp Processes for producing acyclic surfactant sulfobetaines
US3474135A (en) * 1964-01-16 1969-10-21 Bayer Ag N-(omega-aminoalkylene)-aminoalkyl sulfonic acids
US3547985A (en) * 1965-03-06 1970-12-15 Bayer Ag Unsaturated sulphonic acid betaines
WO2004113391A3 (en) * 2003-06-23 2005-04-14 Neurochem Int Ltd Improved pharmaceutical drug candidates and methods for preparation thereof
US7253306B2 (en) 2003-06-23 2007-08-07 Neurochem (International) Limited Pharmaceutical drug candidates and methods for preparation thereof
CN111910222A (en) * 2020-08-21 2020-11-10 九江德福科技股份有限公司 Electrolytic copper foil additive with brightening and leveling functions and application thereof
CN115093353A (en) * 2022-07-06 2022-09-23 武汉天立表面技术有限公司 Preparation method and application of OPX

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3084163A (en) * 1958-04-29 1963-04-02 Dehydag Gmbh Heterocyclic thioalkane sulfonic acids and methods for their production
US3244724A (en) * 1961-01-25 1966-04-05 Armour & Co Sulfoalkylated imidazolines
US3280179A (en) * 1961-03-16 1966-10-18 Textilana Corp Processes for producing acyclic surfactant sulfobetaines
US3231580A (en) * 1961-06-30 1966-01-25 Hans S Mannheimer Substituted imidazolines
US3151123A (en) * 1962-06-19 1964-09-29 Keystone Chemurgic Corp Acid-soluble chlorophyllins and their production
US3474135A (en) * 1964-01-16 1969-10-21 Bayer Ag N-(omega-aminoalkylene)-aminoalkyl sulfonic acids
US3547985A (en) * 1965-03-06 1970-12-15 Bayer Ag Unsaturated sulphonic acid betaines
WO2004113391A3 (en) * 2003-06-23 2005-04-14 Neurochem Int Ltd Improved pharmaceutical drug candidates and methods for preparation thereof
JP2007516940A (en) * 2003-06-23 2007-06-28 ニューロケム (インターナショナル) リミテッド Improved drug candidates and methods for their preparation
US7253306B2 (en) 2003-06-23 2007-08-07 Neurochem (International) Limited Pharmaceutical drug candidates and methods for preparation thereof
AU2004249530B2 (en) * 2003-06-23 2011-08-18 Kiacta Sarl Improved pharmaceutical drug candidates and methods for preparation thereof
CN111910222A (en) * 2020-08-21 2020-11-10 九江德福科技股份有限公司 Electrolytic copper foil additive with brightening and leveling functions and application thereof
CN111910222B (en) * 2020-08-21 2022-08-23 九江德福科技股份有限公司 Electrolytic copper foil additive with brightening and leveling functions and application thereof
CN115093353A (en) * 2022-07-06 2022-09-23 武汉天立表面技术有限公司 Preparation method and application of OPX

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