FR3116817B1 - Pièce en CMC et procédé de fabrication d'une telle pièce - Google Patents

Pièce en CMC et procédé de fabrication d'une telle pièce Download PDF

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Publication number
FR3116817B1
FR3116817B1 FR2012373A FR2012373A FR3116817B1 FR 3116817 B1 FR3116817 B1 FR 3116817B1 FR 2012373 A FR2012373 A FR 2012373A FR 2012373 A FR2012373 A FR 2012373A FR 3116817 B1 FR3116817 B1 FR 3116817B1
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France
Prior art keywords
manufacturing
cmc
reinforcement
matrix
making
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Active
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FR2012373A
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English (en)
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FR3116817A1 (fr
Inventor
William Ros
Simon Lucien René Thibaud
Maxime Box
Christophe Hirondelle
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Safran Ceramics SA
IRT Saint Exupery
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Safran Ceramics SA
IRT Saint Exupery
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Application filed by Safran Ceramics SA, IRT Saint Exupery filed Critical Safran Ceramics SA
Priority to FR2012373A priority Critical patent/FR3116817B1/fr
Priority to CN202180082700.8A priority patent/CN116568654A/zh
Priority to US18/255,030 priority patent/US20240018054A1/en
Priority to PCT/FR2021/052054 priority patent/WO2022112696A1/fr
Priority to EP21823971.3A priority patent/EP4251588A1/fr
Publication of FR3116817A1 publication Critical patent/FR3116817A1/fr
Application granted granted Critical
Publication of FR3116817B1 publication Critical patent/FR3116817B1/fr
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/56Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
    • C04B35/565Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide
    • C04B35/573Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide obtained by reaction sintering or recrystallisation
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/56Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
    • C04B35/565Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/71Ceramic products containing macroscopic reinforcing agents
    • C04B35/78Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
    • C04B35/80Fibres, filaments, whiskers, platelets, or the like
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/42Non metallic elements added as constituents or additives, e.g. sulfur, phosphor, selenium or tellurium
    • C04B2235/428Silicon
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52Constituents or additives characterised by their shapes
    • C04B2235/5208Fibers
    • C04B2235/5216Inorganic
    • C04B2235/524Non-oxidic, e.g. borides, carbides, silicides or nitrides
    • C04B2235/5244Silicon carbide
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52Constituents or additives characterised by their shapes
    • C04B2235/5208Fibers
    • C04B2235/5252Fibers having a specific pre-form
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/602Making the green bodies or pre-forms by moulding
    • C04B2235/6028Shaping around a core which is removed later
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/616Liquid infiltration of green bodies or pre-forms
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6565Cooling rate
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/96Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
    • C04B2235/9607Thermal properties, e.g. thermal expansion coefficient
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F05INDEXING SCHEMES RELATING TO ENGINES OR PUMPS IN VARIOUS SUBCLASSES OF CLASSES F01-F04
    • F05DINDEXING SCHEME FOR ASPECTS RELATING TO NON-POSITIVE-DISPLACEMENT MACHINES OR ENGINES, GAS-TURBINES OR JET-PROPULSION PLANTS
    • F05D2300/00Materials; Properties thereof
    • F05D2300/60Properties or characteristics given to material by treatment or manufacturing
    • F05D2300/603Composites; e.g. fibre-reinforced
    • F05D2300/6033Ceramic matrix composites [CMC]
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02TCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO TRANSPORTATION
    • Y02T50/00Aeronautics or air transport
    • Y02T50/60Efficient propulsion technologies, e.g. for aircraft

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Turbine Rotor Nozzle Sealing (AREA)
  • Ceramic Products (AREA)
  • Prostheses (AREA)

Abstract

Procédé de fabrication d’une pièce en CMC, permettant de mieux contrôler l’étape de densification de la pièce, et pièce intermédiaire permettant de mettre en œuvre ce procédé, la pièce intermédiaire comprenant un renfort (10’), une matrice, comportant un matériau céramique, et au moins un insert (50a-50e), réalisé dans un matériau différent de celui du renfort (10’) et de la matrice, configuré pour favoriser la migration de silicium liquide au sein de la pièce intermédiaire au cours d’une étape de densification de la pièce intermédiaire. Fig. 5.
FR2012373A 2020-11-30 2020-11-30 Pièce en CMC et procédé de fabrication d'une telle pièce Active FR3116817B1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
FR2012373A FR3116817B1 (fr) 2020-11-30 2020-11-30 Pièce en CMC et procédé de fabrication d'une telle pièce
CN202180082700.8A CN116568654A (zh) 2020-11-30 2021-11-22 由cmc制成的部件和用于制造这种部件的方法
US18/255,030 US20240018054A1 (en) 2020-11-30 2021-11-22 Part made from cmc and method for manufacturing such a part
PCT/FR2021/052054 WO2022112696A1 (fr) 2020-11-30 2021-11-22 Piece en cmc et procede de fabrication d'une telle piece
EP21823971.3A EP4251588A1 (fr) 2020-11-30 2021-11-22 Piece en cmc et procede de fabrication d'une telle piece

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2012373A FR3116817B1 (fr) 2020-11-30 2020-11-30 Pièce en CMC et procédé de fabrication d'une telle pièce
FR2012373 2020-11-30

Publications (2)

Publication Number Publication Date
FR3116817A1 FR3116817A1 (fr) 2022-06-03
FR3116817B1 true FR3116817B1 (fr) 2023-09-01

Family

ID=75746714

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2012373A Active FR3116817B1 (fr) 2020-11-30 2020-11-30 Pièce en CMC et procédé de fabrication d'une telle pièce

Country Status (5)

Country Link
US (1) US20240018054A1 (fr)
EP (1) EP4251588A1 (fr)
CN (1) CN116568654A (fr)
FR (1) FR3116817B1 (fr)
WO (1) WO2022112696A1 (fr)

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5952100A (en) * 1997-05-21 1999-09-14 General Electric Company Silicon-doped boron nitride coated fibers in silicon melt infiltrated composites
US6274078B1 (en) * 1999-01-27 2001-08-14 General Electric Company Method of removing cores from ceramic matrix composite articles
EP3241815B1 (fr) * 2016-05-02 2019-11-13 Rolls-Royce High Temperature Composites Inc Réduction de nodules de surface dans des composites à matrice céramique infiltrée fondue
FR3062336B1 (fr) * 2017-02-02 2019-04-12 Safran Ceramics Procede de fabrication d'une piece en materiau composite
US10384981B2 (en) * 2017-06-14 2019-08-20 General Electric Company Methods of forming ceramic matrix composites using sacrificial fibers and related products
FR3071246B1 (fr) * 2017-09-21 2022-05-06 Safran Ceram Procede de fabrication d'une piece en cmc
US10995039B1 (en) * 2019-12-20 2021-05-04 General Electric Company Methods of forming ceramic matrix composites using sacrificial fibers and non-wetting coating

Also Published As

Publication number Publication date
EP4251588A1 (fr) 2023-10-04
US20240018054A1 (en) 2024-01-18
CN116568654A (zh) 2023-08-08
WO2022112696A1 (fr) 2022-06-02
FR3116817A1 (fr) 2022-06-03

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