FR2381006A1 - Procede de production du 1,1,1,2tetrafluoroethane - Google Patents
Procede de production du 1,1,1,2tetrafluoroethaneInfo
- Publication number
- FR2381006A1 FR2381006A1 FR7804638A FR7804638A FR2381006A1 FR 2381006 A1 FR2381006 A1 FR 2381006A1 FR 7804638 A FR7804638 A FR 7804638A FR 7804638 A FR7804638 A FR 7804638A FR 2381006 A1 FR2381006 A1 FR 2381006A1
- Authority
- FR
- France
- Prior art keywords
- chromium oxide
- fluoroethane
- prodn
- ethane
- halo
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 title abstract 2
- 239000003054 catalyst Substances 0.000 title abstract 2
- 229910000423 chromium oxide Inorganic materials 0.000 title abstract 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 title 1
- VHPYNVZYZFYVII-UHFFFAOYSA-N fluoroethane Chemical compound [CH2]CF VHPYNVZYZFYVII-UHFFFAOYSA-N 0.000 title 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 title 1
- 229910021563 chromium fluoride Inorganic materials 0.000 abstract 1
- 239000002826 coolant Substances 0.000 abstract 1
- 230000008014 freezing Effects 0.000 abstract 1
- 238000007710 freezing Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000003380 propellant Substances 0.000 abstract 1
- FTBATIJJKIIOTP-UHFFFAOYSA-K trifluorochromium Chemical compound F[Cr](F)F FTBATIJJKIIOTP-UHFFFAOYSA-K 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/395—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to a chemical modification of at least one compound
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
L'invention concerne l'industrie des composés organiques halogénés. Elle a pour objet un procédé pour produire le 1,1,1,2-tétrafluoroéthane, suivant lequel on fait réagir en phase vapeur, à une température élevée, un halogénoéthane de formule CX3 CH2 Y, où X représente le brome, chlore ou le fluor et Y représente le brome ou le chlore, avec du fluorure d'hydrogène en présence d'un catalyseur qui est de l'oxyde de chrome ou qui est au moins pour partie du fluorure de chrome basique. Ce procédé est préféré pour la production du 1,1,1,2-tétrafluoroethane de haute pureté.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB6687/77A GB1589924A (en) | 1977-02-17 | 1977-02-17 | Manufacture of 1,1,1,2-tetrafluoroethane halogenated compounds |
GB3972177 | 1977-09-23 |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2381006A1 true FR2381006A1 (fr) | 1978-09-15 |
Family
ID=26240883
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7804638A Withdrawn FR2381006A1 (fr) | 1977-02-17 | 1978-02-17 | Procede de production du 1,1,1,2tetrafluoroethane |
Country Status (11)
Country | Link |
---|---|
JP (1) | JPS53105404A (fr) |
AR (1) | AR216937A1 (fr) |
AU (1) | AU518050B2 (fr) |
BR (1) | BR7800944A (fr) |
CA (1) | CA1119202A (fr) |
DE (1) | DE2806865A1 (fr) |
ES (1) | ES467081A1 (fr) |
FR (1) | FR2381006A1 (fr) |
GR (1) | GR65299B (fr) |
IT (1) | IT1095355B (fr) |
NL (1) | NL7801741A (fr) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2433500A1 (fr) * | 1978-08-14 | 1980-03-14 | Daikin Ind Ltd | Procede de preparation du tetrafluorethane |
EP0328127A1 (fr) * | 1988-02-12 | 1989-08-16 | E.I. Du Pont De Nemours And Company | Procédé de fluoration en phase gazeuse |
EP0357328A1 (fr) * | 1988-09-01 | 1990-03-07 | E.I. Du Pont De Nemours And Company | Procédé de purification de 2,2-dichloro-1,1,1-trifluoro-éthane |
EP0417680A1 (fr) * | 1989-09-13 | 1991-03-20 | Hoechst Aktiengesellschaft | Procédé pour la fabrication de 1,1,1,2-tétrafluoroéthane |
EP0507458A2 (fr) * | 1991-04-04 | 1992-10-07 | Imperial Chemical Industries Plc | Procédé pour l'épuration de 1,1,1,2-tétrafluoroéthane |
EP0582494A1 (fr) * | 1992-08-05 | 1994-02-09 | Elf Atochem S.A. | Procédé de purification du 1,1,1,2-tetrafluoroéthane |
EP0612709A1 (fr) * | 1993-02-24 | 1994-08-31 | Elf Atochem S.A. | Purification du pentafluoroethane |
US5463151A (en) * | 1989-07-12 | 1995-10-31 | Ausimont S.R.L. | Process for preparing 1,1,1,2-tetrafluoroethane |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2501062A1 (fr) * | 1980-12-29 | 1982-09-10 | Ugine Kuhlmann | Catalyseurs de fluoruration en phase gazeuse de derives chlores aliphatiques, a base de microbilles d'oxyde de chrome, et procedes de fluoruration utilisant ces catalyseurs |
DE3323374A1 (de) * | 1983-06-29 | 1985-01-10 | Hoechst Ag, 6230 Frankfurt | Katalysatoren fuer fluorierungs- und/oder dismutierungsreaktionen von halogenkohlenwasserstoffen und verfahren zu ihrer herstellung |
GB8717595D0 (en) * | 1987-07-24 | 1987-09-03 | Ici Plc | Chemical process |
JPH0685878B2 (ja) * | 1988-04-13 | 1994-11-02 | ダイキン工業株式会社 | クロム系フッ素化触媒の賦活方法 |
JP3233310B2 (ja) * | 1990-03-13 | 2001-11-26 | ダイキン工業株式会社 | 1,1,1,2−テトラフルオロエタンの製造方法 |
ZA923274B (en) * | 1991-05-06 | 1993-11-08 | Du Pont | Process for the manufacture of pentafluoroethane |
WO1992019576A1 (fr) * | 1991-05-06 | 1992-11-12 | E.I. Du Pont De Nemours And Company | Procede d'elaboration du pentafluoroethane |
KR960016683B1 (en) * | 1993-12-09 | 1996-12-20 | Korea Inst Sci & Tech | Method of producing fluorization catalyst for preparing 1,1,1,2-tetrafluoroethane |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2999885A (en) * | 1959-09-17 | 1961-09-12 | Du Pont | Purification of fluorocarbons |
FR1369782A (fr) * | 1962-09-26 | 1964-08-14 | Allied Chem | Fluoruration d'hydrocarbures halogénés à l'aide d'acide fluorhydrique sur un catalyseur d'oxyde de chrome |
FR1492823A (fr) * | 1965-01-01 | 1967-08-25 | Ici Ltd | Procédé de purification du 2, 2, 2-trifluoro-1-chloro-1-bromoéthane |
FR2000688A1 (fr) * | 1968-01-24 | 1969-09-12 | Du Pont | |
FR2051409A5 (fr) * | 1969-06-27 | 1971-04-02 | Ici Ltd | |
JPS5450376A (en) * | 1977-09-27 | 1979-04-20 | Sharp Corp | Signal counter |
-
1978
- 1978-02-08 AU AU33118/78A patent/AU518050B2/en not_active Expired
- 1978-02-13 GR GR55436A patent/GR65299B/el unknown
- 1978-02-13 IT IT20257/78A patent/IT1095355B/it active
- 1978-02-16 BR BR7800944A patent/BR7800944A/pt unknown
- 1978-02-16 NL NL7801741A patent/NL7801741A/xx not_active Application Discontinuation
- 1978-02-16 AR AR271120A patent/AR216937A1/es active
- 1978-02-17 ES ES467081A patent/ES467081A1/es not_active Expired
- 1978-02-17 CA CA000297242A patent/CA1119202A/fr not_active Expired
- 1978-02-17 FR FR7804638A patent/FR2381006A1/fr not_active Withdrawn
- 1978-02-17 JP JP1669178A patent/JPS53105404A/ja active Pending
- 1978-02-17 DE DE19782806865 patent/DE2806865A1/de not_active Withdrawn
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2999885A (en) * | 1959-09-17 | 1961-09-12 | Du Pont | Purification of fluorocarbons |
FR1369782A (fr) * | 1962-09-26 | 1964-08-14 | Allied Chem | Fluoruration d'hydrocarbures halogénés à l'aide d'acide fluorhydrique sur un catalyseur d'oxyde de chrome |
FR1492823A (fr) * | 1965-01-01 | 1967-08-25 | Ici Ltd | Procédé de purification du 2, 2, 2-trifluoro-1-chloro-1-bromoéthane |
FR2000688A1 (fr) * | 1968-01-24 | 1969-09-12 | Du Pont | |
FR2051409A5 (fr) * | 1969-06-27 | 1971-04-02 | Ici Ltd | |
GB1307224A (en) * | 1969-06-27 | 1973-02-14 | Ici Ltd | Chromium oxide catalyst |
JPS5450376A (en) * | 1977-09-27 | 1979-04-20 | Sharp Corp | Signal counter |
Non-Patent Citations (1)
Title |
---|
CA1976 * |
Cited By (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2433500A1 (fr) * | 1978-08-14 | 1980-03-14 | Daikin Ind Ltd | Procede de preparation du tetrafluorethane |
EP0328127A1 (fr) * | 1988-02-12 | 1989-08-16 | E.I. Du Pont De Nemours And Company | Procédé de fluoration en phase gazeuse |
EP0357328A1 (fr) * | 1988-09-01 | 1990-03-07 | E.I. Du Pont De Nemours And Company | Procédé de purification de 2,2-dichloro-1,1,1-trifluoro-éthane |
US5463151A (en) * | 1989-07-12 | 1995-10-31 | Ausimont S.R.L. | Process for preparing 1,1,1,2-tetrafluoroethane |
US6037508A (en) * | 1989-07-12 | 2000-03-14 | Ausimont S.P.A. | Process for preparing 1,1,1,2-tetrafluoroethane |
US5880316A (en) * | 1989-07-12 | 1999-03-09 | Ausimont S.P.A. | Process for preparing 1,1,1,2-tetrafluoroethane |
US5608125A (en) * | 1989-07-12 | 1997-03-04 | Ausimont S.P.A. | Process for preparing 1,1,1,2-tetrafluoroethane |
EP0417680A1 (fr) * | 1989-09-13 | 1991-03-20 | Hoechst Aktiengesellschaft | Procédé pour la fabrication de 1,1,1,2-tétrafluoroéthane |
EP0507458A2 (fr) * | 1991-04-04 | 1992-10-07 | Imperial Chemical Industries Plc | Procédé pour l'épuration de 1,1,1,2-tétrafluoroéthane |
EP0507458A3 (en) * | 1991-04-04 | 1993-08-11 | Imperial Chemical Industries Plc | Process for the purification of 1,1,1,2-tetrafluoroethane |
EP0582494A1 (fr) * | 1992-08-05 | 1994-02-09 | Elf Atochem S.A. | Procédé de purification du 1,1,1,2-tetrafluoroéthane |
FR2694556A1 (fr) * | 1992-08-05 | 1994-02-11 | Atochem Elf Sa | Procédé de purification du 1,1,1,2-tétrafluoroéthane. |
US5453551A (en) * | 1993-02-24 | 1995-09-26 | Elf Atochem S.A. | Purification of pentafluoroethane |
FR2701943A1 (fr) * | 1993-02-24 | 1994-09-02 | Atochem Elf Sa | Purification du pentafluoroéthane. |
EP0612709A1 (fr) * | 1993-02-24 | 1994-08-31 | Elf Atochem S.A. | Purification du pentafluoroethane |
Also Published As
Publication number | Publication date |
---|---|
ES467081A1 (es) | 1979-08-16 |
AU3311878A (en) | 1979-08-16 |
AR216937A1 (es) | 1980-02-15 |
DE2806865A1 (de) | 1978-10-05 |
BR7800944A (pt) | 1978-10-31 |
IT7820257A0 (it) | 1978-02-13 |
NL7801741A (nl) | 1978-08-21 |
JPS53105404A (en) | 1978-09-13 |
IT1095355B (it) | 1985-08-10 |
CA1119202A (fr) | 1982-03-02 |
AU518050B2 (en) | 1981-09-10 |
GR65299B (en) | 1980-08-01 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |