FR2334687A1 - Procede de preparation d'hexamethyldisilazane avec emploi de cette substance comme solvant et separation par distillation de l'hexamethyldisilazane forme - Google Patents
Procede de preparation d'hexamethyldisilazane avec emploi de cette substance comme solvant et separation par distillation de l'hexamethyldisilazane formeInfo
- Publication number
- FR2334687A1 FR2334687A1 FR7635495A FR7635495A FR2334687A1 FR 2334687 A1 FR2334687 A1 FR 2334687A1 FR 7635495 A FR7635495 A FR 7635495A FR 7635495 A FR7635495 A FR 7635495A FR 2334687 A1 FR2334687 A1 FR 2334687A1
- Authority
- FR
- France
- Prior art keywords
- prodn
- solvent
- disilazane
- hexamethyl
- prod
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- FFUAGWLWBBFQJT-UHFFFAOYSA-N hexamethyldisilazane Chemical compound C[Si](C)(C)N[Si](C)(C)C FFUAGWLWBBFQJT-UHFFFAOYSA-N 0.000 title abstract 4
- 239000002904 solvent Substances 0.000 title abstract 2
- ZXZSEQFNAKXEAN-UHFFFAOYSA-N N.C[Si](C)(C)Cl Chemical compound N.C[Si](C)(C)Cl ZXZSEQFNAKXEAN-UHFFFAOYSA-N 0.000 title 1
- 238000011084 recovery Methods 0.000 title 1
- IJOOHPMOJXWVHK-UHFFFAOYSA-N chlorotrimethylsilane Chemical compound C[Si](C)(C)Cl IJOOHPMOJXWVHK-UHFFFAOYSA-N 0.000 abstract 4
- 238000004821 distillation Methods 0.000 abstract 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 abstract 2
- 235000019270 ammonium chloride Nutrition 0.000 abstract 2
- 238000004508 fractional distillation Methods 0.000 abstract 1
- 238000000859 sublimation Methods 0.000 abstract 1
- 230000008022 sublimation Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/10—Compounds having one or more C—Si linkages containing nitrogen having a Si-N linkage
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/0834—Compounds having one or more O-Si linkage
- C07F7/0838—Compounds with one or more Si-O-Si sequences
- C07F7/0872—Preparation and treatment thereof
- C07F7/0874—Reactions involving a bond of the Si-O-Si linkage
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB5068075A GB1516899A (en) | 1975-12-10 | 1975-12-10 | Process for the manufacture of hexamethyldisilazane |
| DE19762645792 DE2645792C2 (de) | 1975-12-10 | 1976-10-09 | Verfahren zur Gewinnung von Hexamethyldisilazan |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2334687A1 true FR2334687A1 (fr) | 1977-07-08 |
| FR2334687B1 FR2334687B1 (cs) | 1978-12-22 |
Family
ID=25770996
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7635495A Granted FR2334687A1 (fr) | 1975-12-10 | 1976-11-25 | Procede de preparation d'hexamethyldisilazane avec emploi de cette substance comme solvant et separation par distillation de l'hexamethyldisilazane forme |
Country Status (3)
| Country | Link |
|---|---|
| FR (1) | FR2334687A1 (cs) |
| IT (1) | IT1069982B (cs) |
| NL (1) | NL162655C (cs) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2416233A1 (fr) * | 1978-02-03 | 1979-08-31 | Goldschmidt Ag Th | Procede de production d'hexamethyldisilasane |
| CN114507253A (zh) * | 2022-01-20 | 2022-05-17 | 杭州四马化工科技有限公司 | 一种硅氮烷的连续化生产工艺 |
-
1976
- 1976-11-25 FR FR7635495A patent/FR2334687A1/fr active Granted
- 1976-12-07 IT IT5250676A patent/IT1069982B/it active
- 1976-12-09 NL NL7613725A patent/NL162655C/xx not_active IP Right Cessation
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2416233A1 (fr) * | 1978-02-03 | 1979-08-31 | Goldschmidt Ag Th | Procede de production d'hexamethyldisilasane |
| CN114507253A (zh) * | 2022-01-20 | 2022-05-17 | 杭州四马化工科技有限公司 | 一种硅氮烷的连续化生产工艺 |
Also Published As
| Publication number | Publication date |
|---|---|
| NL162655B (nl) | 1980-01-15 |
| FR2334687B1 (cs) | 1978-12-22 |
| NL162655C (nl) | 1980-06-16 |
| IT1069982B (it) | 1985-03-25 |
| NL7613725A (nl) | 1977-06-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |