FI88047B - Pao tvenne elektrondonorer baserad katalysator foer polymerisation av olefiner - Google Patents
Pao tvenne elektrondonorer baserad katalysator foer polymerisation av olefiner Download PDFInfo
- Publication number
- FI88047B FI88047B FI912262A FI912262A FI88047B FI 88047 B FI88047 B FI 88047B FI 912262 A FI912262 A FI 912262A FI 912262 A FI912262 A FI 912262A FI 88047 B FI88047 B FI 88047B
- Authority
- FI
- Finland
- Prior art keywords
- procatalyst composition
- composition according
- phthalic acid
- acid ester
- catalyst
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Claims (12)
1. För polymerisation av olefiner avsedd prokatalysator-komposition, som framställts genom att förena MgCl2, en lag-re alkohol, en titanförening och en ftalsyraester, kanne- 5 tecknad av att den lägre alkoholen och ftalsyraestern trans - esteritierats, varvid ftalsyraesterns alkoxigrupp har ät-minstone 5 kolatomer.
2. Prokatalysatorkomposition enligt patentkravet 1, kanne- 10 tecknad av att alkoxigruppen hos den använda ftalsyraestern har ätminstone 8 och företrädesvis ätminstone 10 kolatomer.
3. Prokatalysatorkomposition enligt patentkravet l eller 2, kannetecknad av att den använda estern är propylhexyl- 15 ftalat (PrHP), dioktylftaiat (DOP), diisodekylftaiat (DIDP) och/eller ditridekylftaiat (DTDP).
4. Prokatalysatorkomposition enligt patentkravet 1, 2 eller 3, kannetecknad av att transesterifieringen utförs vid 20 en temperatur, som är mellan 110°C och 150°C, företrädesvis mellan 130°C och 140°C.
5. Prokatalysatorkomposition enligt nägot av de föregäende patentkraven 1, 2 eller 3, kannetecknad av att transesteri- :.*35 fieringen utförs i ett lösningsmedel, vars kokpunkt översti- :/.: ger transesterifieringstemperaturen, exempelvis i nonan el- *:·*: ler dekan.
6. Prokatalysatorkomposition enligt nägot av de föregäende .-.30 patentkraven, kannetecknad av att den använda lägre alkoho- Ien är etanol.
: ·· 7. Prokatalysatorkomposition enligt nägot av de föregäende patentkraven, kannetecknad av att titanföreningen är TiCl4.
8. Prokatalysatorkomposition enligt nägot av de föregäende patentkraven, kannetecknad av att den innehäller högst 2,5 vikt-% Ti, företrädesvis högst ca. 2,0 vikt-% Ti. Il : '·?5 23 88047
9. Prokatalysatorkomposition enligt nägot av de föregäende patentkraven, kännetecknad av att dess molförhällande donor/ Mg är mellan 0,03 och 0,04 och/eller dess donorhalt är mel-lan 4 och 6 vikt-%. 5
10. Prokatalysatorkomposition enligt nägot av de föregäende patentkraven, kännetecknad av att ftalsyraesterns alkoxi-grupp har ätminstone 8 kolatomer och att prokatalysatorkom-positionens aktivitet vid användning av trietylaluminium som 10 kokatalyt och cyklohexylmetyldimetoxisilan som yttre donor är ätminstone 800 kg PP/g Ti.
11. Prokatalysatorkomposition enligt nägot av de föregäende patentkraven, kännetecknad av att den framställts genom 15 a) att omsätta en addukt av MgCl2 och den lägre alkoholen med en titanförening, b) att omsätta produkten frän steget a) med en ftalsyraester vid förhällanden, där ftalsyraestern och den lägre alkoholen transesterifieras, 20 c) att tvätta produkten, och d) att eventuellt omsätta slutprodukten ur steget c) med en titanförening (mao. den andra behandlingen).
12. Användning av en prokatalysatorkomposition enligt nägot . -25 av de föregäende patentkraven för polymerisation av propen sä, att polymerisationen utförs i närvaro av en organometal-lisk kokatalysator som ett trialkylaluminium och företrädes-:T: vis en yttre donor säsom cyklohexylmetyldimetoxisilan.
Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FI912262A FI88047C (sv) | 1991-05-09 | 1991-05-09 | På tvenne elektrondonorer baserad katalysator för polymerisation av ol efiner |
CA002102816A CA2102816C (en) | 1991-05-09 | 1992-03-23 | A procatalyst for polymerization of olefins containing a trans-esterification product of a lower alcohol and a phthalic acid ester |
PCT/FI1992/000081 WO1992019653A1 (en) | 1991-05-09 | 1992-03-23 | A procatalyst for polymerization of olefins containing a trans-esterification product of a lower alcohol and a phthalic acid ester |
EP92907260A EP0591224B1 (en) | 1991-05-09 | 1992-03-23 | A procatalyst for polymerization of olefins containing a trans-esterification product of a lower alcohol and a phthalic acid ester |
JP50687792A JP3226538B2 (ja) | 1991-05-09 | 1992-03-23 | 二種の電子供与体に基づく重合触媒 |
DE69224435T DE69224435T2 (de) | 1991-05-09 | 1992-03-23 | Prokatalysator zur polymerisation von olefinen, der das umesterungsprodukt eines niederen alkohols und eines phthalsäureesters enthält |
NO1993933962A NO933962D0 (no) | 1991-05-09 | 1993-11-02 | Prokatalysator for polymerisasjon av olefiner inneholdeneet transforestringsprodukt av en lavere alkohol og en ftalsyreester |
US08/425,258 US6303532B1 (en) | 1991-05-09 | 1995-04-18 | Olefin polymerization catalyst containing a transesterification product of a lower alcohol and a phthalic acid ester |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FI912262 | 1991-05-09 | ||
FI912262A FI88047C (sv) | 1991-05-09 | 1991-05-09 | På tvenne elektrondonorer baserad katalysator för polymerisation av ol efiner |
Publications (3)
Publication Number | Publication Date |
---|---|
FI912262A0 FI912262A0 (fi) | 1991-05-09 |
FI88047B true FI88047B (fi) | 1992-12-15 |
FI88047C FI88047C (sv) | 1993-03-25 |
Family
ID=8532488
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FI912262A FI88047C (sv) | 1991-05-09 | 1991-05-09 | På tvenne elektrondonorer baserad katalysator för polymerisation av ol efiner |
Country Status (8)
Country | Link |
---|---|
US (1) | US6303532B1 (sv) |
EP (1) | EP0591224B1 (sv) |
JP (1) | JP3226538B2 (sv) |
CA (1) | CA2102816C (sv) |
DE (1) | DE69224435T2 (sv) |
FI (1) | FI88047C (sv) |
NO (1) | NO933962D0 (sv) |
WO (1) | WO1992019653A1 (sv) |
Cited By (4)
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Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT1209255B (it) * | 1980-08-13 | 1989-07-16 | Montedison Spa | Catalizzatori per la polimerizzazione di olefine. |
US4442276A (en) * | 1982-02-12 | 1984-04-10 | Mitsui Petrochemical Industries, Ltd. | Process for polymerizing or copolymerizing olefins |
DE3540699A1 (de) * | 1985-11-16 | 1987-05-27 | Basf Ag | Verfahren zum herstellen von homo- und copolymerisaten des propylens mittels eines ziegler-natta-katalysatorsystems |
FI80055C (sv) * | 1986-06-09 | 1990-04-10 | Neste Oy | Förfarande för framställning av katalytkomponenter för polymerisation av olefiner |
FI86548C (sv) * | 1990-11-07 | 1992-09-10 | Neste Oy | Förbättrad stereoselektiv katalysator för polymerisation av olefiner |
US5234879A (en) * | 1990-12-19 | 1993-08-10 | Neste Oy | Method for the modification of catalysts intended for the polymerization of olefins |
-
1991
- 1991-05-09 FI FI912262A patent/FI88047C/sv active
-
1992
- 1992-03-23 WO PCT/FI1992/000081 patent/WO1992019653A1/en active IP Right Grant
- 1992-03-23 EP EP92907260A patent/EP0591224B1/en not_active Expired - Lifetime
- 1992-03-23 JP JP50687792A patent/JP3226538B2/ja not_active Expired - Fee Related
- 1992-03-23 DE DE69224435T patent/DE69224435T2/de not_active Expired - Lifetime
- 1992-03-23 CA CA002102816A patent/CA2102816C/en not_active Expired - Fee Related
-
1993
- 1993-11-02 NO NO1993933962A patent/NO933962D0/no unknown
-
1995
- 1995-04-18 US US08/425,258 patent/US6303532B1/en not_active Expired - Lifetime
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7531478B2 (en) | 2001-12-19 | 2009-05-12 | Borealis Technology Oy | Production of supported olefin polymerisation catalysts |
EP2295478A2 (en) | 2007-05-22 | 2011-03-16 | Borealis Technology Oy | Polypropylene copolymer |
EP2202271A1 (en) | 2008-12-29 | 2010-06-30 | Borealis AG | Alpha-nucleated polypropylene for power cable insulation |
EP2787034A1 (en) | 2013-04-05 | 2014-10-08 | Borealis AG | High stiffness polypropylene compositions |
WO2014161621A1 (en) | 2013-04-05 | 2014-10-09 | Borealis Ag | High stiffness polypropylene compositions |
Also Published As
Publication number | Publication date |
---|---|
NO933962L (no) | 1993-11-02 |
DE69224435D1 (de) | 1998-03-19 |
FI88047C (sv) | 1993-03-25 |
NO933962D0 (no) | 1993-11-02 |
US6303532B1 (en) | 2001-10-16 |
JP3226538B2 (ja) | 2001-11-05 |
DE69224435T2 (de) | 1998-09-24 |
WO1992019653A1 (en) | 1992-11-12 |
JPH06511501A (ja) | 1994-12-22 |
CA2102816A1 (en) | 1992-11-10 |
EP0591224A1 (en) | 1994-04-13 |
EP0591224B1 (en) | 1998-02-11 |
FI912262A0 (fi) | 1991-05-09 |
CA2102816C (en) | 2003-12-09 |
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