ES8304131A1 - "un procedimiento para la preparacion de cafeina purificada". - Google Patents
"un procedimiento para la preparacion de cafeina purificada".Info
- Publication number
- ES8304131A1 ES8304131A1 ES511377A ES511377A ES8304131A1 ES 8304131 A1 ES8304131 A1 ES 8304131A1 ES 511377 A ES511377 A ES 511377A ES 511377 A ES511377 A ES 511377A ES 8304131 A1 ES8304131 A1 ES 8304131A1
- Authority
- ES
- Spain
- Prior art keywords
- caffeine
- purification
- alkaline solution
- aqueous alkaline
- recrystallisation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- RYYVLZVUVIJVGH-UHFFFAOYSA-N caffeine Chemical compound CN1C(=O)N(C)C(=O)C2=C1N=CN2C RYYVLZVUVIJVGH-UHFFFAOYSA-N 0.000 title abstract 12
- LPHGQDQBBGAPDZ-UHFFFAOYSA-N Isocaffeine Natural products CN1C(=O)N(C)C(=O)C2=C1N(C)C=N2 LPHGQDQBBGAPDZ-UHFFFAOYSA-N 0.000 title abstract 6
- 229960001948 caffeine Drugs 0.000 title abstract 6
- VJEONQKOZGKCAK-UHFFFAOYSA-N caffeine Natural products CN1C(=O)N(C)C(=O)C2=C1C=CN2C VJEONQKOZGKCAK-UHFFFAOYSA-N 0.000 title abstract 6
- 238000000746 purification Methods 0.000 title abstract 2
- 239000012670 alkaline solution Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 239000003638 chemical reducing agent Substances 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000001953 recrystallisation Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D473/00—Heterocyclic compounds containing purine ring systems
- C07D473/02—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6
- C07D473/04—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms
- C07D473/06—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms with radicals containing only hydrogen and carbon atoms, attached in position 1 or 3
- C07D473/12—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms with radicals containing only hydrogen and carbon atoms, attached in position 1 or 3 with methyl radicals in positions 1, 3, and 7, e.g. caffeine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US25410081A | 1981-04-14 | 1981-04-14 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES511377A0 ES511377A0 (es) | 1983-02-16 |
| ES8304131A1 true ES8304131A1 (es) | 1983-02-16 |
Family
ID=22962929
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES511377A Expired ES8304131A1 (es) | 1981-04-14 | 1982-04-13 | "un procedimiento para la preparacion de cafeina purificada". |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP0062776B1 (https=) |
| JP (1) | JPS57179184A (https=) |
| DE (1) | DE3263721D1 (https=) |
| ES (1) | ES8304131A1 (https=) |
| FI (1) | FI69466C (https=) |
| MX (1) | MX7061E (https=) |
| PH (1) | PH18582A (https=) |
| PL (1) | PL135880B1 (https=) |
| PT (1) | PT74740B (https=) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019063465A1 (en) * | 2017-09-29 | 2019-04-04 | Nestec S.A. | PROCESS FOR PRODUCING CAFFEINE |
| CN115228134A (zh) * | 2022-09-05 | 2022-10-25 | 青海大学 | 一种从茶叶中提取咖啡因的方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH114904A (de) * | 1924-05-16 | 1926-05-17 | Kuendig Jun & Cie F | Verfahren zur Herstellung von koffeinfreiem Kaffee. |
| US2508545A (en) * | 1948-07-20 | 1950-05-23 | Gen Foods Corp | Process of recovering caffein |
| GB854703A (en) * | 1956-04-20 | 1960-11-23 | Hag Ag | Process for removing caffeine from coffee extracts |
| US3321142A (en) * | 1964-10-17 | 1967-05-23 | Dresden Arzneimittel | Method for the production of an abrasion-resistant discoloration-free caffeine granulate |
-
1982
- 1982-03-18 DE DE8282102211T patent/DE3263721D1/de not_active Expired
- 1982-03-18 EP EP19820102211 patent/EP0062776B1/en not_active Expired
- 1982-03-19 FI FI820971A patent/FI69466C/fi not_active IP Right Cessation
- 1982-03-29 PH PH27069A patent/PH18582A/en unknown
- 1982-03-31 PL PL23573582A patent/PL135880B1/pl unknown
- 1982-04-12 PT PT7474082A patent/PT74740B/pt unknown
- 1982-04-13 MX MX1002882U patent/MX7061E/es unknown
- 1982-04-13 ES ES511377A patent/ES8304131A1/es not_active Expired
- 1982-04-14 JP JP6228282A patent/JPS57179184A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| PL235735A1 (https=) | 1982-11-22 |
| DE3263721D1 (en) | 1985-06-27 |
| PL135880B1 (en) | 1985-12-31 |
| FI69466B (fi) | 1985-10-31 |
| ES511377A0 (es) | 1983-02-16 |
| JPS6318948B2 (https=) | 1988-04-20 |
| EP0062776B1 (en) | 1985-05-22 |
| FI820971L (fi) | 1982-10-15 |
| MX7061E (es) | 1987-04-10 |
| EP0062776A1 (en) | 1982-10-20 |
| JPS57179184A (en) | 1982-11-04 |
| PT74740A (en) | 1982-05-01 |
| PT74740B (en) | 1983-11-14 |
| FI69466C (fi) | 1986-02-10 |
| PH18582A (en) | 1985-08-12 |
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