ES2568303A1 - Device for the development of simultaneous chemical reactions in parallel with independent temperature control and global pressure control (Machine-translation by Google Translate, not legally binding) - Google Patents

Device for the development of simultaneous chemical reactions in parallel with independent temperature control and global pressure control (Machine-translation by Google Translate, not legally binding) Download PDF

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Publication number
ES2568303A1
ES2568303A1 ES201431575A ES201431575A ES2568303A1 ES 2568303 A1 ES2568303 A1 ES 2568303A1 ES 201431575 A ES201431575 A ES 201431575A ES 201431575 A ES201431575 A ES 201431575A ES 2568303 A1 ES2568303 A1 ES 2568303A1
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Spain
Prior art keywords
support
elements
dome
possibility
fifteen
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Granted
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ES201431575A
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Spanish (es)
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ES2568303B1 (en
Inventor
Jorge BOU SERRA
Sergi ALDEA ROSELLÓ
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Universitat Politecnica de Catalunya UPC
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Universitat Politecnica de Catalunya UPC
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Priority to ES201431575A priority Critical patent/ES2568303B1/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2445Stationary reactors without moving elements inside placed in parallel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L99/00Subject matter not provided for in other groups of this subclass

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Clinical Laboratory Science (AREA)
  • Control Of Fluid Pressure (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The objective of the applicant is the design of the invention that provides an alternative to processes that require chemical reactions on a small scale, for unique reactions or providing the possibility of performing reactions in parallel simultaneously, with the possibility of independently controlling the temperature of each reaction, with the possibility of controlling the global pressure of the reactive medium, with the possibility of controlling the vacuum pressure of the reactive medium, with the possibility of carrying out the reactions at different pressures, with the possibility of controlling the possible entry of desired gases to the reactive medium and to carry out the reactions in atmospheres of variable composition, and with the possibility of controlling the operating time of all the elements, and introducing the necessary elements so that said functions are carried out correctly and safely. (Machine-translation by Google Translate, not legally binding)

Claims (1)

REIVINDICACIONES 1) Un dispositivo para el desarrollo de reacciones químicas simultáneas en paralelo con control de temperatura independiente y control de presión global que comprende un cuerpo capaz de aportar el medio de reacción constituido 5 por un soporte (2) y una cúpula (5), y una carcasa (9) que soporta el cuerpo anterior y alberga los componentes del dispositivo y la interfaz. 1) A device for the development of simultaneous chemical reactions in parallel with independent temperature control and global pressure control comprising a body capable of providing the reaction medium constituted by a support (2) and a dome (5), and a housing (9) that supports the anterior body and houses the components of the device and the interface. 2) El dispositivo según la reivindicación 1), caracterizado porque el soporte dispone de una (25) a cincuenta (26) inserciones donde colocar las vasijas o tubos de ensayo, donde se insertarán los elementos calefactores y los 10 aislantes, además dicho soporte dispone de conductos de comunicación para salida de gases que pueden ser situados en el centro o en cualquier de las partes del elemento de tal manera que comuniquen la parte superior con la inferior, además dicho soporte dispone de rebabas en sus bordes con la finalidad de mantener en su superficie cualquier derrame. 15 2) The device according to claim one) , characterized in that the support has one (25) to fifty (26) inserts where to place the test vessels or tubes, where the heating elements and the 10 insulators will be inserted, in addition said support has communication conduits for gas outlet that they can be located in the center or in any of the parts of the element in such a way that they communicate the upper part with the lower part, in addition said support has burrs at its edges in order to keep any spillage on its surface. fifteen 3) El dispositivo según la reivindicación 1), caracterizado porque la cúpula tiene una forma tal que le permita ser insertada encima del soporte y guiada por las rebabas aportando así estanqueidad al sistema interior conseguido por la unión de estos dos elementos siendo el grosor de este elemento entre 1 milímetro y 5 milímetros. 20 3) The device according to claim one) , characterized in that the dome has a shape that allows it to be inserted on top of the support and guided by the burrs, thus providing tightness to the interior system achieved by the union of these two elements, the thickness of this element being between 1 millimeter and 5 millimeters. twenty 4) El dispositivo según la reivindicación 1) , caracterizado porque dispone de una junta intermedia en contacto entre el soporte y la cúpula. 4) The device according to claim 1), characterized in that it has an intermediate joint in contact between the support and the dome. 5) El dispositivo según la reivindicación 2) , caracterizado por disponer de elementos calefactores capaces de ser insertados en las inserciones que pueden ser resistencias de forma helicoidal , tubular, en formato envolvente o 25 de bloque, con o sin algún elemento disipador, dichos calefactores también pueden ser de camisa hidráulica o radiación, siendo en cualquiera de los casos el número de calefactores a implementar igual o menor al número de inserciones en el soporte . 5) The device according to claim 2), characterized by having heating elements capable of being inserted in the inserts that can be helical, tubular, block or block-shaped resistors, with or without some dissipating element, said heaters they can also be of hydraulic jacket or radiation, being in any case the number of heaters to be implemented equal to or less than the number of inserts in the support. 6) El soporte según la reivindicación 2), se constituye también por un elemento 30 aislante entre el elemento calefactor (3) y el soporte (2). 6) The support according to claim 2) is also constituted by an insulating element 30 between the heating element (3) and the support (2). 7) El dispositivo según la reivindicación 1), caracterizado porque el soporte (2) y la cúpula (5) quedan aisladas térmicamente mediante un elemento aislante (4) del resto del dispositivo. 7) The device according to claim one) , characterized in that the support (2) and the dome (5) are thermally insulated by an insulating element (4) from the rest of the device. 8) El dispositivo según la reivindicación 1), caracterizado porque la carcasa 35 consta de un conjunto de elementos estructurales capaces de realizar la 8) The device according to claim one) , characterized in that the housing 35 consists of a set of structural elements capable of carrying out the función de habitáculo para elementos del dispositivo y con el objetivo además de soportar físicamente el sistema reactivo formado por el soporte y cúpula y sus elementos de todas las reivindicaciones anteriores. cabin function for elements of the device and with the objective in addition to physically supporting the reactive system formed by the support and dome and its elements of all the preceding claims. 9) El dispositivo según la reivindicación 8), caracterizado porque la carcasa dispone de un sistema de conexiones hembra en relación a la conexión macho 5 de las resistencias calefactoras, la distribución de éstas se da de manera que con la posible variación de soportes con diferentes inserciones dentro de una relación de dimensiones con todos los elementos, estas puedan seguir realizando su función y abastecer de energía a los elementos relacionados como los calefactores. 10 9) The device according to claim 8) , characterized in that the housing has a female connection system in relation to the male connection 5 of the heating resistors, the distribution of these is given so that with the possible variation of supports with different inserts within a relationship of dimensions with all the elements, these can continue to perform their function and supply energy to related elements such as heaters. 10 10) El dispositivo según la reivindicación 9), caracterizado por disponer de un sistema de refrigeración. 10) The device according to claim 9), characterized by having a cooling system. 11) El dispositivo según reivindicación 10), caracterizado por disponer de un sistema de alimentación de energía con transformador de potencia e intensidad. 15 11) The device according to claim 10) , characterized by having a power supply system with power and intensity transformer. fifteen 12) El dispositivo según la reivindicación 11), caracterizado por tener un sistema capaz de regular la temperatura de cada uno de los elementos calefactores independientemente según la señal interpretada por cada uno de los sensores independientes de cada inserción. 12) The device according to claim eleven) , characterized by having a system capable of regulating the temperature of each of the heating elements independently according to the signal interpreted by each of the independent sensors of each insert. 13) El dispositivo según la reivindicación 12), caracterizado por tener un sistema 20 capaz de regular la presión global dentro de la cúpula según la señal interpretada por el sensor situado en el interior de dicha cúpula. 13) The device according to claim 12) , characterized by having a system 20 capable of regulating the overall pressure inside the dome according to the signal interpreted by the sensor located inside said dome. 14) El dispositivo según la reivindicación 13), caracterizado porque dispone de una válvula capaz de regular la presión global dentro del habitáculo soporte-cúpula y tiene la opción además de introducir un gas en la atmósfera que se crea en 25 su interior. 14) The device according to claim 13) , characterized in that it has a valve capable of regulating the overall pressure inside the support-dome cabin and has the option in addition to introducing a gas into the atmosphere that is created inside. 15) El dispositivo según la reivindicación 13), caracterizado por tener un sistema capaz de regular la temperatura del interior de la carcasa mediante la refrigeración por aire o por intercambiador hidráulico, según la señal interpretada por un sensor de temperatura insertado en dicha carcasa. 30 15) The device according to claim 13) , characterized by having a system capable of regulating the temperature inside the housing by air cooling or by hydraulic exchanger, according to the signal interpreted by a temperature sensor inserted in said housing. 30 16) El dispositivo según las reivindicaciones 12) 13) 15), 13) 15) y 15), caracterizado por tener un sistema electrónico tipo microprocesador o regulador capaz de tomar decisiones en función de las señales recibidas y las de consigna establecidas por el usuario. 16) The device according to the claims 12) 13) fifteen) , 13) fifteen) Y fifteen) , characterized by having an electronic microprocessor or regulator system capable of making decisions based on the signals received and the setpoints established by the user. 17) El dispositivo según la reivindicación 16), caracterizado por tener una salida de 35 información en formato digital o analógico para ser direccionada a un sistema informático periférico. 17) The device according to claim 16) , characterized by having an output of information in digital or analog format to be addressed to a peripheral computer system. 18) El dispositivo según la reivindicación 16), caracterizado por disponer de un control temporal mediante temporizador capaz de controlar el tiempo de funcionamiento de cada uno de los elementos calefactores y de control de presión. 18) The device according to claim 16) , characterized by having a temporary timer control capable of controlling the operating time of each of the heating and pressure control elements.
ES201431575A 2014-10-28 2014-10-28 Device for the development of simultaneous chemical reactions in parallel with independent temperature control and global pressure control Active ES2568303B1 (en)

Priority Applications (1)

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ES201431575A ES2568303B1 (en) 2014-10-28 2014-10-28 Device for the development of simultaneous chemical reactions in parallel with independent temperature control and global pressure control

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ES201431575A ES2568303B1 (en) 2014-10-28 2014-10-28 Device for the development of simultaneous chemical reactions in parallel with independent temperature control and global pressure control

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ES2568303A1 true ES2568303A1 (en) 2016-04-28
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6051439A (en) * 1996-10-23 2000-04-18 Glaxo Wellcome Inc. Methods for parallel synthesis of organic compounds
WO2001005497A1 (en) * 1999-07-16 2001-01-25 General Electric Company Method and apparatus for rapid screening of multiphase reactions
WO2002081076A2 (en) * 2001-04-05 2002-10-17 Symyx Technologies, Inc. A combinatorial chemistry reactor system
US20050013748A1 (en) * 2003-07-18 2005-01-20 Boehringer Ingelheim Pharmaceuticals, Inc. Apparatus for automated synthesis

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6051439A (en) * 1996-10-23 2000-04-18 Glaxo Wellcome Inc. Methods for parallel synthesis of organic compounds
WO2001005497A1 (en) * 1999-07-16 2001-01-25 General Electric Company Method and apparatus for rapid screening of multiphase reactions
WO2002081076A2 (en) * 2001-04-05 2002-10-17 Symyx Technologies, Inc. A combinatorial chemistry reactor system
US20050013748A1 (en) * 2003-07-18 2005-01-20 Boehringer Ingelheim Pharmaceuticals, Inc. Apparatus for automated synthesis

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