EP2310116B1 - Vorrichtung zum kontinuierlichen mischen von ausgespeichertem erdgas mit sauerstoff zu einem brenngas für eine erwärmung des unter druck stehenden erdgases vor oder nach seiner entspannung - Google Patents
Vorrichtung zum kontinuierlichen mischen von ausgespeichertem erdgas mit sauerstoff zu einem brenngas für eine erwärmung des unter druck stehenden erdgases vor oder nach seiner entspannung Download PDFInfo
- Publication number
- EP2310116B1 EP2310116B1 EP20090775871 EP09775871A EP2310116B1 EP 2310116 B1 EP2310116 B1 EP 2310116B1 EP 20090775871 EP20090775871 EP 20090775871 EP 09775871 A EP09775871 A EP 09775871A EP 2310116 B1 EP2310116 B1 EP 2310116B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- mixing
- oxygen
- natural gas
- container
- mixing chamber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Not-in-force
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/10—Mixing gases with gases
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/45—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
- B01F25/452—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces
- B01F25/4524—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces the components being pressed through foam-like inserts or through a bed of loose bodies, e.g. balls
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
- B01F25/45—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads
- B01F25/452—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces
- B01F25/4524—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces the components being pressed through foam-like inserts or through a bed of loose bodies, e.g. balls
- B01F25/45241—Mixers in which the materials to be mixed are pressed together through orifices or interstitial spaces, e.g. between beads characterised by elements provided with orifices or interstitial spaces the components being pressed through foam-like inserts or through a bed of loose bodies, e.g. balls through a bed of balls
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23K—FEEDING FUEL TO COMBUSTION APPARATUS
- F23K5/00—Feeding or distributing other fuel to combustion apparatus
- F23K5/002—Gaseous fuel
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23K—FEEDING FUEL TO COMBUSTION APPARATUS
- F23K2400/00—Pretreatment and supply of gaseous fuel
- F23K2400/20—Supply line arrangements
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/4238—With cleaner, lubrication added to fluid or liquid sealing at valve interface
- Y10T137/4245—Cleaning or steam sterilizing
- Y10T137/4259—With separate material addition
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/8593—Systems
- Y10T137/86348—Tank with internally extending flow guide, pipe or conduit
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/8593—Systems
- Y10T137/86348—Tank with internally extending flow guide, pipe or conduit
- Y10T137/86372—Inlet internally extending
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/8593—Systems
- Y10T137/87571—Multiple inlet with single outlet
Definitions
- the invention relates to an apparatus for the continuous mixing of stored natural gas with oxygen to a fuel gas for heating the pressurized natural gas before or after its expansion, with a closed mixing vessel with connections for a natural gas supply, an oxygen introduction and a fuel gas discharge.
- Natural gas is to be preheated prior to pressure reduction during the withdrawal, eg from underground storage tanks, in order to compensate for the Joule-Thomson effect. It is known to continuously burn a portion of the Aus Grandestromes in a so-called "inline reactor" under controlled supply of oxygen. In this process, temperatures of up to 400 ° C are achieved by catalytic conversion of oxygen with natural gas directly in the gas stream taken from the memory. The heat is used by direct mixing of the hot combustion gases in the cold gas stream for continuous heating. This procedure is in the EP 0 920 578 B1 described.
- a mixing device upstream of a catalytic combustion device wherein the natural gas is arranged in the center of the mixing zone. Downstream of the natural gas supply is a Mixed insert of corrugated material used. A bed of ceramic grain material is arranged as a thermal barrier in front of the catalyst.
- the invention has for its object to provide a device that ensures a safe dosage of oxygen in continuously flowing natural gas.
- the mixing section provided in the known "in-line heating", that is to say within a natural gas line, is now designed as a closed mixing container. Its function is to supply a cold natural gas stream, which is introduced into the mixing vessel, high pressure oxygen in the gaseous state at a temperature of about 5 to 30 ° C via the oxygen inlet and the natural gas within the mixing chamber of the container via the manifold at a High pressure of eg To mix 70 to 170 bar.
- the mixing chamber is complete and the manifold at least partially filled with a self-ignition complicating bed of ceramic grain material.
- the bed of ceramic grain material ensures an increase in operational safety; because it offers an inert behavior, so it does not participate in a reaction with one of the gases to be mixed. It shows a very low and therefore advantageous thermal conductivity, so that the released in a possible ignition within the mixing container heat can not damage the container wall.
- the material also has the advantageous property of a high melting point, whereby, with a possible ignition, no formation of channels by melting is possible.
- Part of a safety device of the device are also equipments of the mixing chamber of the container with temperature sensors.
- the mixing container is advantageously designed as a stationary container, which has at the bottom the connection for the natural gas supply line and at the top the connection for the fuel gas discharge.
- the advantageous working principle of the device allows a cold mixing of oxygen and natural gas at high pressures, taking into account a certain concentration centrally in a equipped with the ceramic bed and with safety monitoring by probe standing container.
- the introduced in the container bed with insulating and inert effect is, especially in standing containers, safe to discharge and wear-resistant by its high density at small defined cavities. This prevents the propagation of flames within the container should auto-ignition occur.
- the container inner wall is temperature-monitored.
- the container is, the bed remains constant during operation obtained and always has small cavities, because then, if particles of the ceramic grain material would be torn by the sharp flow, immediately slipping takes place.
- the ceramic grain material of the bed is a high-density alumina in spherical form with a homogeneous particle size distribution of 1.5 to 3 mm.
- the safety against ignition during the mixing of the fuel gas from natural gas and oxygen within the container serving measure provides that the mixing zone on the inflow side has a flow velocity in the mixing zone increasing, concentric cross-sectional constriction.
- the flow velocity of the incoming natural gas is increased by the concentric cross-sectional constriction, which can also be referred to as built-in reduction, in the area before the actual mixing zone in the container so that the turbulence caused in the natural gas flow optimum mixing with the incoming oxygen in the mixing tube surrounding area ,
- the range of ignitability of the natural gas-oxygen mixture, So the fuel gas is thus very fast drive through.
- the inert ceramic fill prevents flame development.
- the distributor tube has outlet slots in its tube wall, which runs parallel to the surrounding walls of the mixing container.
- the outlet slots are dimensioned so that particles of the bulk ceramic grain material present in the distributor tube can not be torn through the outlet slots by the oxygen flowing in the distributor tube or can be pressed from the outside into the distributor tube.
- the exit slits produce the effect of a screen while at the same time having an advantageous effect on the mixing effect of the oxygen flowing out of the distributor tube into the mixing zone through the exit slits.
- the mixing container is advantageously designed double-walled in the region of the mixing zone of the mixing chamber, wherein an insulating material is arranged between the outer mixing container wall and the inner mixing chamber wall.
- the inner mixing chamber wall may e.g. consist of a stainless steel sheet, which is welded circumferentially with the outer mixing tank wall, wherein in the space a lining with ceramic wool to protect the mixing chamber wall against thermal influences is arranged.
- three circumferentially evenly distributed, fast-responding temperature sensor with protective tube are welded. This makes it possible to monitor the temperature increase during a possible ignition of the natural gas-oxygen mixture permanently and safety-oriented.
- the temperature sensors are integrated in a safety device.
- the safety device has with particular advantage a connected to the oxygen inlet nitrogen purge. Upon reaching a temperature rise detected in the mixing tank by the temperature sensors, the oxygen addition by the safety device is immediately stopped and a purging process with nitrogen is introduced into the oxygen introduction port.
- a redundant measuring and control device is integrated in the oxygen inlet and in the natural gas supply.
- the safety device limits this oxygen concentration, wherein the monitoring is performed by the measuring and control device.
- two different series-connected measuring methods of flow measurement, differential pressure measurement on a diaphragm and ultrasonic measurement are used, the values of which are processed in the safety device. As a result, on the one hand given a redundancy and on the other hand there is a possibility of comparison.
- the preselected parameters of the mixing process are, determined by experiments, under the auto-ignition of the fuel gas mixed from natural gas and oxygen, wherein the state in the process is permanently monitored by the safety-related measurement technique.
- Fig. 1 shows a view of an apparatus for continuously mixing stored natural gas with oxygen to a fuel gas for heating the pressurized natural gas before or after its relaxation.
- the mixing section 1 is formed, which ends in the fuel gas discharge line 10 with flange 15.
- the mixing container 2 forming the mixing section 1 is a standing container with legs 5, at the lower ends of which base plates 6 are located, which serve to anchor the mixing container 2 on a standing surface.
- Legs 5 and bottom plates 6 form a stand for the mixing container 2, the bottom flows over the flange 3 and the natural gas supply 8 natural gas, and is entered into the via the oxygen inlet 9 with the flange 4 oxygen, which mixes in the mixing tank with the natural gas becomes.
- the gas mixture forms a fuel gas which is discharged via the fuel gas discharge line 10 with the flange 15 from the mixing container 2.
- temperature sensor 7 At the periphery of the mixing container 2, distributed evenly around the circumference, temperature sensor 7 is attached.
- Fig. 2 shows a side view of the vertical container 2, which forms the mixing section 1, in a longitudinal section.
- the same components are designated by the same reference numerals as in Fig. 1 ,
- Fig. 2 indicates that in the interior of the mixing container 2, a mixing chamber 11 is formed, which is filled with a bed of ceramic grain material.
- the bed of ceramic grain material is indicated by microcircuits drawn.
- the manifold is also with the bed of ceramic grain material, here a high-density alumina in spherical form with a homogeneous grain size distribution of 1.5 to 3 mm filled, as indicated here.
- the inserts serve 30 and 31 in the inlets 8, 9 and the insert 32 in the outlet 10. At the same time carried by the inserts 30, 31 and 32, a homogenization of the flow in the manner of a multi-aperture.
- Fig. 2 illustrates further that the temperature sensor 7 with protective tube 15 in a region corresponding to the arrangement of the outlet slots 14 in the manifold 12, are arranged in the mixing vessel wall 16.
- the mixing container 2 is double-walled in the region of the mixing zone of the mixing chamber 11, an insulating material 18 being arranged between the outer mixing container wall 16 and the inner mixing chamber wall 17.
- the mixing zone formed in the interior of the mixing chamber has on the inflow side a concentric cross-sectional constriction 19 which increases the flow velocity in the mixing zone.
- the cross-sectional constriction 19 may be e.g. a formed from sheet metal funnel, which is placed in the lower end of the mixing vessel directly over the mouth of the natural gas feed line 8.
- Fig. 3 shows a side view of the entire device with mixing tank and its connections for a natural gas inlet 8 and for an oxygen inlet 9 with the respective upstream of these connections fittings a safety device, with nitrogen flushing system and with control valves for the introduction of oxygen.
- a check valve 20 is connected upstream and a shut-off valve 21, in front of, seen in the direction of the natural gas supply line, again a valve for measuring quantity 22 is arranged.
- the supply of natural gas takes place in the direction of arrow 23.
- a non-return valve 20 ' is again arranged on the inflow side, in front of which, seen in the inflow of the oxygen, a shut-off valve 21' and a device for measuring oxygen quantity 22 'sits.
- the latter fittings are components of the safety device of the device, which also includes the here only indicated nitrogen extinguishing system 24 with the outlet side existing fittings 25 and 26.
- Another device for oxygen quantity measurement is designated 22 ".
- a control valve for the introduction of oxygen, which controls the inflowing in the direction of arrow 27 oxygen in the amount is denoted by 28.
- valves are part of the safety device, which can control and control technology to work according to a program with which the measured values of the temperature, the pressure and the amount of oxygen and the natural gas introduced into the mixing chamber processed and the corresponding shut-off and control fittings 21st and 28 and 21 ', respectively.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Combustion & Propulsion (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Filling Or Discharging Of Gas Storage Vessels (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PL09775871T PL2310116T3 (pl) | 2008-08-04 | 2009-05-12 | Urządzenie do ciągłego mieszania wyprowadzanego gazu ziemnego z tlenem tworząc gaz palny dla ogrzewania będącego pod ciśnieniem gazu ziemnego przed albo po jego rozprężeniu |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE200810036269 DE102008036269A1 (de) | 2008-08-04 | 2008-08-04 | Vorrichtung zum kontinuierlichen Mischen von ausgespeichertem Erdgas mit Sauerstoff zu einem Brenngas für eine Erwärmung des unter Druck stehenden Erdgases vor oder nach seiner Entspannung |
PCT/DE2009/000666 WO2010015215A2 (de) | 2008-08-04 | 2009-05-12 | Vorrichtung zum kontinuierlichen mischen von ausgespeichertem erdgas mit sauerstoff zu einem brenngas für eine erwärmung des unter druck stehenden erdgases vor oder nach seiner entspannung |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2310116A2 EP2310116A2 (de) | 2011-04-20 |
EP2310116B1 true EP2310116B1 (de) | 2014-12-17 |
Family
ID=41501116
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP20090775871 Not-in-force EP2310116B1 (de) | 2008-08-04 | 2009-05-12 | Vorrichtung zum kontinuierlichen mischen von ausgespeichertem erdgas mit sauerstoff zu einem brenngas für eine erwärmung des unter druck stehenden erdgases vor oder nach seiner entspannung |
Country Status (10)
Country | Link |
---|---|
US (1) | US8607820B2 (pt) |
EP (1) | EP2310116B1 (pt) |
CA (1) | CA2734367C (pt) |
DE (1) | DE102008036269A1 (pt) |
DK (1) | DK2310116T3 (pt) |
ES (1) | ES2532465T3 (pt) |
PL (1) | PL2310116T3 (pt) |
PT (1) | PT2310116E (pt) |
RU (1) | RU2466776C2 (pt) |
WO (1) | WO2010015215A2 (pt) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2789164A1 (en) | 2010-02-02 | 2011-08-11 | Novacta Biosystems Limited | Lantibiotic salts |
RU2666423C1 (ru) * | 2017-11-30 | 2018-09-07 | Акционерное Общество "Российский Концерн По Производству Электрической И Тепловой Энергии На Атомных Станциях" (Ао "Концерн Росэнергоатом") | Устройство для смешивания и нагрева газовых сред |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3330773A (en) * | 1963-03-28 | 1967-07-11 | Du Pont | Process for preparing gaseous mixtures |
SU780868A2 (ru) * | 1979-04-19 | 1980-11-23 | Предприятие П/Я А-7372 | Смеситель |
US5003782A (en) * | 1990-07-06 | 1991-04-02 | Zoran Kucerija | Gas expander based power plant system |
DE4127883A1 (de) | 1991-08-22 | 1993-02-25 | Abb Patent Gmbh | Einrichtung zur waermeerzeugung durch katalytische verbrennung |
US5606858A (en) | 1993-07-22 | 1997-03-04 | Ormat Industries, Ltd. | Energy recovery, pressure reducing system and method for using the same |
DE19633674C2 (de) * | 1996-08-21 | 1998-07-16 | Hamburger Gaswerke Gmbh | In-Line Gasvorwärmung |
DE19847786A1 (de) * | 1998-10-16 | 2000-04-20 | Degussa | Vorrichtung und Verfahren zum Befüllen und Entleeren eines mit brennbarem sowie aggressivem Gas beaufschlagten Behälters |
KR100694903B1 (ko) * | 1998-12-01 | 2007-03-13 | 가부시키가이샤 에바라 세이사꾸쇼 | 폐기가스처리장치 |
FR2833863B1 (fr) | 2001-12-20 | 2004-08-20 | Air Liquide | Reacteur catalytique, installation et procede de reaction correspondants |
DE10200786B4 (de) * | 2002-01-11 | 2004-11-11 | Dockweiler Ag | Sicherheitsbehälter |
US7195026B2 (en) * | 2002-12-27 | 2007-03-27 | American Air Liquide, Inc. | Micro electromechanical systems for delivering high purity fluids in a chemical delivery system |
US7108838B2 (en) * | 2003-10-30 | 2006-09-19 | Conocophillips Company | Feed mixer for a partial oxidation reactor |
EP1865249B1 (en) * | 2006-06-07 | 2014-02-26 | 2Oc | A gas pressure reducer, and an energy generation and management system including a gas pressure reducer |
-
2008
- 2008-08-04 DE DE200810036269 patent/DE102008036269A1/de not_active Withdrawn
-
2009
- 2009-05-12 WO PCT/DE2009/000666 patent/WO2010015215A2/de active Application Filing
- 2009-05-12 RU RU2011103867/05A patent/RU2466776C2/ru not_active IP Right Cessation
- 2009-05-12 CA CA2734367A patent/CA2734367C/en not_active Expired - Fee Related
- 2009-05-12 US US12/737,590 patent/US8607820B2/en not_active Expired - Fee Related
- 2009-05-12 EP EP20090775871 patent/EP2310116B1/de not_active Not-in-force
- 2009-05-12 ES ES09775871.8T patent/ES2532465T3/es active Active
- 2009-05-12 PT PT09775871T patent/PT2310116E/pt unknown
- 2009-05-12 DK DK09775871T patent/DK2310116T3/da active
- 2009-05-12 PL PL09775871T patent/PL2310116T3/pl unknown
Also Published As
Publication number | Publication date |
---|---|
US20110132481A1 (en) | 2011-06-09 |
DE102008036269A1 (de) | 2010-02-11 |
WO2010015215A3 (de) | 2010-04-01 |
PT2310116E (pt) | 2015-03-04 |
CA2734367A1 (en) | 2010-02-11 |
WO2010015215A2 (de) | 2010-02-11 |
EP2310116A2 (de) | 2011-04-20 |
US8607820B2 (en) | 2013-12-17 |
CA2734367C (en) | 2016-02-02 |
PL2310116T3 (pl) | 2015-05-29 |
RU2011103867A (ru) | 2012-09-10 |
DK2310116T3 (da) | 2015-03-30 |
ES2532465T3 (es) | 2015-03-27 |
RU2466776C2 (ru) | 2012-11-20 |
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