EP2150510A1 - Keramischer werkstoff - Google Patents
Keramischer werkstoffInfo
- Publication number
- EP2150510A1 EP2150510A1 EP08736574A EP08736574A EP2150510A1 EP 2150510 A1 EP2150510 A1 EP 2150510A1 EP 08736574 A EP08736574 A EP 08736574A EP 08736574 A EP08736574 A EP 08736574A EP 2150510 A1 EP2150510 A1 EP 2150510A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- ceramic material
- material according
- production
- strontium aluminate
- ceramic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
- C04B35/111—Fine ceramics
- C04B35/117—Composites
- C04B35/119—Composites with zirconium oxide
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
- C04B35/645—Pressure sintering
- C04B35/6455—Hot isostatic pressing
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- C—CHEMISTRY; METALLURGY
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3206—Magnesium oxides or oxide-forming salts thereof
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3213—Strontium oxides or oxide-forming salts thereof
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
- C04B2235/3222—Aluminates other than alumino-silicates, e.g. spinel (MgAl2O4)
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- C—CHEMISTRY; METALLURGY
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
- C04B2235/3225—Yttrium oxide or oxide-forming salts thereof
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3232—Titanium oxides or titanates, e.g. rutile or anatase
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3241—Chromium oxides, chromates, or oxide-forming salts thereof
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/612—Machining
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- C—CHEMISTRY; METALLURGY
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering
- C04B2235/661—Multi-step sintering
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering
- C04B2235/661—Multi-step sintering
- C04B2235/662—Annealing after sintering
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- C—CHEMISTRY; METALLURGY
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/77—Density
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/78—Grain sizes and shapes, product microstructures, e.g. acicular grains, equiaxed grains, platelet-structures
- C04B2235/785—Submicron sized grains, i.e. from 0,1 to 1 micron
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/80—Phases present in the sintered or melt-cast ceramic products other than the main phase
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/80—Phases present in the sintered or melt-cast ceramic products other than the main phase
- C04B2235/87—Grain boundary phases intentionally being absent
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
Definitions
- the invention relates to a ceramic material.
- Ceramic materials offer a variety of applications. Their composition can be tailored by specific addition of certain elements and / or their compounds to the intended use.
- Aluminum oxide and zirconium oxide, for example, are ceramic materials which are processed individually or in combination with one another inter alia to cutting tools, catalyst supports or prostheses.
- Hardness, aging resistance, water wetting behavior, and high thermal conductivity are properties known of alumina sintered compacts, high strength, and high fracture toughness, that is, damage tolerance, are properties known from zirconia sintered compacts.
- an aluminum oxide material in the following composition in the sintered body is suitable as a material, in particular for use in the field of medical technology, for example for the production of orthoses and endoprostheses, such as hip joint and knee joint implants.
- Alumina in appropriate addition to 100 wt .-%.
- Dominant structural component of such a combination of materials is the aluminum oxide. Therefore, the property-determining characteristics such as hardness, Young's modulus and thermal conductivity close to the properties of pure alumina.
- the constituents zirconium oxide and optionally strontium aluminate are incorporated in the aluminum oxide matrix.
- the raw materials are preferably used in high purity. Due to the high purity of the raw materials, grain boundary phases are formed only to an extremely small extent.
- the strontium aluminate forms characteristic platelet-shaped crystallites, platelets, which contribute significantly to the increase in strength.
- the constituents zirconium oxide and strontium aluminate contribute to increasing the fracture toughness, which is about 60% higher than with pure aluminum oxide.
- the strength is increased almost by a factor of 2
- the damage tolerance that is, the property of the component, even with a possible damage still retain a high residual strength.
- the crack path is surprisingly deflected, so that additional energy is absorbed in the crack propagation.
- a peculiarity of the material according to the invention is to be considered that the two mechanisms mutually reinforce, so that the effective increase in the fracture toughness is even greater than would be expected by simple addition of the individual mechanisms.
- Al 2 O 3 The content of Al 2 O 3 supplements from 72.65 wt .-% to 74.54 wt .-%. Commodity related contaminants ( ⁇ 0.05% by weight) are possible but not listed separately because of their minority.
- the production of sintered molded articles from the material according to the invention takes place by means of conventional ceramic technology.
- the properties of the sintered body from the material according to the invention can still be reinforced by inclusions. It is thus possible to mix whiskers and / or fibers into the material before forming a sintered body or incorporating reticulated structures or fabrics into the green state material.
- the whiskers, fibers or nets or webs must be made of a material that does not interact with the ceramic material in such a way that deterioration of its properties occurs. In addition, the material must not change during sintering in such a way that the material is damaged.
- Sinterform body which are made of the material according to the invention, surprisingly combine the respective best properties of competing ceramic materials alumina and zirconia for implant applications in itself: hardness, aging resistance, water wetting behavior and high thermal conductivity are properties of sintered form bodies of alumina High strength and high fracture toughness, that is damage tolerance, are properties known from zirconia sintered compacts.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Composite Materials (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Materials For Medical Uses (AREA)
- Prostheses (AREA)
Abstract
Description
Claims
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102007020473.8A DE102007020473B4 (de) | 2007-04-27 | 2007-04-27 | Keramischer Werkstoff, seine Verwendung und Sinterformkörper |
PCT/EP2008/055056 WO2008132158A1 (de) | 2007-04-27 | 2008-04-25 | Keramischer werkstoff |
Publications (1)
Publication Number | Publication Date |
---|---|
EP2150510A1 true EP2150510A1 (de) | 2010-02-10 |
Family
ID=39494673
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP08736574A Withdrawn EP2150510A1 (de) | 2007-04-27 | 2008-04-25 | Keramischer werkstoff |
Country Status (7)
Country | Link |
---|---|
US (1) | US8932970B2 (de) |
EP (1) | EP2150510A1 (de) |
JP (2) | JP5641928B2 (de) |
KR (1) | KR101556719B1 (de) |
CN (1) | CN101730672A (de) |
DE (1) | DE102007020473B4 (de) |
WO (1) | WO2008132158A1 (de) |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2448880B1 (de) * | 2009-06-30 | 2019-06-05 | Aktiebolaget SKF | Zirkon-aluminium-keramisches rollelement und verfahren zu dessen herstellung |
WO2011083022A1 (de) * | 2009-12-16 | 2011-07-14 | Ceramtec Gmbh | Keramischer verbundwerkstoff, bestehend aus den hauptbestandteilen aluminiumoxid und zirkonoxid |
KR101747870B1 (ko) | 2009-12-16 | 2017-06-15 | 세람테크 게엠베하 | 주성분으로서의 알루미늄 옥사이드 및 지르코늄 옥사이드, 및 분산질상으로 구성되는 세라믹 복합 재료 |
DE102010032174B4 (de) | 2010-07-23 | 2015-10-15 | Ibu-Tec Advanced Materials Ag | Verfahren zur Herstellung von stäbchenverstärkten Keramiken, Keramikwerkstoff und seine Verwendung, Pulverwerkstoff, Granulat, sowie vorgesinterter Körper |
US9783459B2 (en) * | 2012-08-20 | 2017-10-10 | Ceramtec Gmbh | Zirconium oxide-based composite material |
FR2996843B1 (fr) * | 2012-10-15 | 2020-01-03 | Saint-Gobain Centre De Recherches Et D'etudes Europeen | Produit d'oxyde de chrome. |
RU2016121145A (ru) * | 2013-11-01 | 2017-12-06 | Баладжи Индастриал Продактс Лтд. | Износостойкий состав для изготовления износостойкого элемента, применяемого для изготовления измельчающего валка или футеровки размольного стола вертикальной валковой мельницы, и способы их изготовления |
CN104529402A (zh) * | 2014-12-20 | 2015-04-22 | 佛山铭乾科技有限公司 | 一种陶瓷浴盆 |
US20180221538A1 (en) | 2015-07-28 | 2018-08-09 | Ceramtec Gmbh | Metallic and/ or ceramic components with at least one osseointegrative and osteoinductive surface (multi)layer structure |
CN108975933A (zh) * | 2018-09-18 | 2018-12-11 | 广东蓝狮医疗科技有限公司 | 一种石墨增强耐磨损氧化铝-氧化锆复合陶瓷及其制备方法 |
DE102019201097A1 (de) * | 2019-01-29 | 2020-07-30 | Thyssenkrupp Ag | Verschleißschutzelement für eine Zerkleinerungsvorrichtung |
CN118026654B (zh) * | 2024-04-11 | 2024-06-25 | 北京国械堂科技发展有限责任公司 | 一种氧化铝基生物陶瓷材料及其制备方法 |
Family Cites Families (26)
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US4155124A (en) * | 1975-01-31 | 1979-05-22 | Kyoto Ceramic Co., Ltd. | Burnt ceramic bone implant |
US4316964A (en) * | 1980-07-14 | 1982-02-23 | Rockwell International Corporation | Al2 O3 /ZrO2 ceramic |
JPS61117153A (ja) * | 1984-11-09 | 1986-06-04 | 鳴海製陶株式会社 | アルミナ焼結体の製造法 |
JPS62260766A (ja) * | 1986-05-08 | 1987-11-13 | 東レ株式会社 | アルミナ焼結体 |
US4657877A (en) * | 1986-05-21 | 1987-04-14 | The United States Of America As Represented By The United States Department Of Energy | Silicon carbide whisker-zirconia reinforced mullite and alumina ceramics |
US5389450A (en) * | 1987-06-12 | 1995-02-14 | Lanxide Technology Company, Lp | Composite materials and methods for making the same |
DE3881113T2 (de) * | 1987-07-22 | 1993-12-02 | Champion Spark Plug Co | Aluminiumoxid-Zirkonoxid-Keramik. |
US5002911A (en) * | 1989-04-07 | 1991-03-26 | Cerametec, Inc. | Ceramics with high toughness, strength and hardness |
US5009822A (en) * | 1989-07-17 | 1991-04-23 | University Of Florida | Alumina-or alumina/zirconia-silicon carbide whisker ceramic composites and methods of manufacture |
DE4116008A1 (de) * | 1991-05-16 | 1992-11-19 | Feldmuehle Ag Stora | Sinterformkoerper und seine verwendung |
US5830816A (en) * | 1990-08-06 | 1998-11-03 | Cerasiv Gmbh Innovatives Keramik-Engineering | Sintered molding |
ATE109441T1 (de) * | 1990-08-06 | 1994-08-15 | Cerasiv Gmbh | Sinterformkörper und seine verwendung. |
FR2677641B1 (fr) * | 1991-06-17 | 1994-01-28 | Propulsion Ste Europeenne | Procede d'elaboration de pieces en materiau composite a matrice alumine. |
US6452957B1 (en) * | 1997-10-31 | 2002-09-17 | Ceramtec Ag Innovative Ceramic Engineering | Sintered shaped body reinforced with platelets |
US20020010070A1 (en) * | 2000-04-25 | 2002-01-24 | Bernard Cales | Zirconia-toughened alumina biocomponent having high resistance to low temperature degradation and method for preparing same |
US6986940B1 (en) * | 2000-07-27 | 2006-01-17 | General Electric Company | Fiber reinforced composite article, fiber member, and method for making |
EP1228774B1 (de) * | 2000-08-07 | 2005-04-20 | Matsushita Electric Works, Ltd. | Künstliches gelenk aus einer zirkonium-aluminiumverbundkeramik |
EP1188729A3 (de) * | 2000-09-13 | 2004-03-31 | CeramTec AG Innovative Ceramic Engineering | Verbundwerkstoff mit plateletverstärkter Aluminiumoxidkeramik-Matrix |
US6617013B2 (en) * | 2001-05-10 | 2003-09-09 | Siemens Westinghouse Power Corporation | Ceramic matrix composite having improved interlaminar strength |
JP4589642B2 (ja) * | 2003-08-28 | 2010-12-01 | 京セラ株式会社 | アルミナ・ジルコニア系セラミックス及びその製法 |
US7148167B2 (en) * | 2003-08-28 | 2006-12-12 | Kyocera Corporation | Alumina/zirconia ceramics and method of producing the same |
JP4570348B2 (ja) * | 2003-10-30 | 2010-10-27 | 京セラ株式会社 | 生体部材の製造方法及び生体部材ならびにそれを用いた人工関節 |
US7820577B2 (en) * | 2003-10-30 | 2010-10-26 | Kyocera Corporation | Biomedical member and method for producing the same |
IL164054A (en) * | 2004-09-13 | 2010-06-16 | Cohen Michael | Alumina ceramic products |
EP1845072B1 (de) * | 2005-01-27 | 2016-09-28 | Kyocera Corporation | Mischkeramik und herstellungsverfahren dafür |
US7300621B2 (en) * | 2005-03-16 | 2007-11-27 | Siemens Power Generation, Inc. | Method of making a ceramic matrix composite utilizing partially stabilized fibers |
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2007
- 2007-04-27 DE DE102007020473.8A patent/DE102007020473B4/de not_active Revoked
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2008
- 2008-04-25 CN CN200880013764A patent/CN101730672A/zh active Pending
- 2008-04-25 US US12/597,547 patent/US8932970B2/en not_active Expired - Fee Related
- 2008-04-25 WO PCT/EP2008/055056 patent/WO2008132158A1/de active Application Filing
- 2008-04-25 EP EP08736574A patent/EP2150510A1/de not_active Withdrawn
- 2008-04-25 JP JP2010504705A patent/JP5641928B2/ja not_active Expired - Fee Related
- 2008-04-25 KR KR1020097024454A patent/KR101556719B1/ko active IP Right Grant
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2014
- 2014-06-23 JP JP2014128511A patent/JP2014210706A/ja not_active Withdrawn
Non-Patent Citations (2)
Title |
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G.M. INSLEY ET AL: "Next Generation Ceramics Based on Zirconia Toughened Alumina for Hip Joint Prostheses", KEY ENGINEERING MATERIALS, vol. 254-256, 1 January 2004 (2004-01-01), pages 675 - 678, XP055470965, DOI: 10.4028/www.scientific.net/KEM.254-256.675 * |
See also references of WO2008132158A1 * |
Also Published As
Publication number | Publication date |
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JP2014210706A (ja) | 2014-11-13 |
CN101730672A (zh) | 2010-06-09 |
KR20100017312A (ko) | 2010-02-16 |
WO2008132158A1 (de) | 2008-11-06 |
JP5641928B2 (ja) | 2014-12-17 |
KR101556719B1 (ko) | 2015-10-02 |
US20100152018A1 (en) | 2010-06-17 |
JP2010524833A (ja) | 2010-07-22 |
US8932970B2 (en) | 2015-01-13 |
DE102007020473A1 (de) | 2008-10-30 |
DE102007020473B4 (de) | 2016-03-03 |
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