EP1985390B1 - Outils dotés d'une région de travail thermo-mécaniquement modifiée et procédés pour la formation de tels outils - Google Patents

Outils dotés d'une région de travail thermo-mécaniquement modifiée et procédés pour la formation de tels outils Download PDF

Info

Publication number
EP1985390B1
EP1985390B1 EP08251055A EP08251055A EP1985390B1 EP 1985390 B1 EP1985390 B1 EP 1985390B1 EP 08251055 A EP08251055 A EP 08251055A EP 08251055 A EP08251055 A EP 08251055A EP 1985390 B1 EP1985390 B1 EP 1985390B1
Authority
EP
European Patent Office
Prior art keywords
tool
tip
bands
region
carbide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
EP08251055A
Other languages
German (de)
English (en)
Other versions
EP1985390A1 (fr
Inventor
Christon L. Shepard
James M. Loffler
Ronald R. Laparre
Alan L. Shaffer
Shrinidhi Chandrasekharan
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dayton Progress Corp
Original Assignee
Dayton Progress Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US12/047,532 external-priority patent/US9132567B2/en
Application filed by Dayton Progress Corp filed Critical Dayton Progress Corp
Priority to SI200830276T priority Critical patent/SI1985390T1/sl
Priority to PL08251055T priority patent/PL1985390T3/pl
Priority to EP20110165001 priority patent/EP2359951A1/fr
Publication of EP1985390A1 publication Critical patent/EP1985390A1/fr
Application granted granted Critical
Publication of EP1985390B1 publication Critical patent/EP1985390B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21KMAKING FORGED OR PRESSED METAL PRODUCTS, e.g. HORSE-SHOES, RIVETS, BOLTS OR WHEELS
    • B21K5/00Making tools or tool parts, e.g. pliers
    • B21K5/20Making working faces of dies, either recessed or outstanding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21DWORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21D37/00Tools as parts of machines covered by this subclass
    • B21D37/20Making tools by operations not covered by a single other subclass
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21DWORKING OR PROCESSING OF SHEET METAL OR METAL TUBES, RODS OR PROFILES WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21D37/00Tools as parts of machines covered by this subclass
    • B21D37/20Making tools by operations not covered by a single other subclass
    • B21D37/205Making cutting tools
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • B21J5/06Methods for forging, hammering, or pressing; Special equipment or accessories therefor for performing particular operations
    • B21J5/08Upsetting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/17Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces by forging
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D6/00Heat treatment of ferrous alloys
    • C21D6/02Hardening by precipitation
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D7/00Modifying the physical properties of iron or steel by deformation
    • C21D7/13Modifying the physical properties of iron or steel by deformation by hot working
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0068Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for particular articles not mentioned below
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/18Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for knives, scythes, scissors, or like hand cutting tools
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/22Ferrous alloys, e.g. steel alloys containing chromium with molybdenum or tungsten
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/24Ferrous alloys, e.g. steel alloys containing chromium with vanadium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/17Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces by forging
    • B22F2003/175Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces by forging by hot forging, below sintering temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F5/00Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product
    • B22F2005/002Tools other than cutting tools

Definitions

  • punches and dies represent types of metal forming tools used to pierce, perforate, and shape metallic and non-metallic workpieces.
  • Cutting tools and inserts represent types of metal forming tools used in machining applications to shape metallic and non-metallic workpieces.
  • Punches and dies are subjected to severe and repeated loading during their operational life. In particular, punches tend to fail during use from catastrophic breakage induced by the significant stresses at the working end of the tool or other mechanisms, such as wear.
  • UHSS's ultra-high strength steels
  • AHSS's advanced high-strength steels
  • TRIP transformation induced plasticity steels
  • MART martensitic steels
  • Punches are commonly constructed from various grades of tool steel.
  • Conventional tool steels contain metal carbides that develop from a reaction of carbon with alloying metals, such as chromium, vanadium, and tungsten, found in common steel formulations.
  • the metal carbide particles are initially present in bulk tool steel as clumps or aggregates.
  • the carbide morphology i.e. particle size and distribution, impacts the tool steel's material and mechanical properties, such as fracture toughness, impact resistance and wear resistance. These material and mechanical properties determine the ability of the tool steel to withstand the service conditions encountered by punches and dies in metalworking operations and serve as a guide in material selection for a particular application.
  • tool steel ingots or billets are typically hot worked above recrystallization temperature by hot rolling or forging process.
  • segregated metal carbides may align substantially in the direction of work to form what is commonly known as carbide banding.
  • Hot working of tool steel may also align regions enriched in certain segregated alloy components substantially in the direction of work to form what is commonly known as elemental or alloy banding.
  • FIGS. 1 and 1B The tendency of segregated metal carbides and alloy components to align along the working direction of hot rolled tool steel (i.e., in the rolling direction) in parallel, linear bands is illustrated in the optical micrographs of FIGS. 1 and 1B and a Scanning Electron Microscopy (SEM) micrograph of FIG. 1A .
  • SEM Scanning Electron Microscopy
  • the micrographs show images of polished and etched regions of a commercially available M2 tool steel grade bar stock in the hot rolled condition.
  • the carbide and alloy bands have a prominent appearance as apparent from FIGS. 1, 1A , and 1B .
  • the lighter bands visible in FIG. 1A represent higher alloy contents by weight percent and darker bands represent lower alloy contents by weight percent.
  • FIG. 1A is an optical micrograph of the banding in as-rolled commercial AISI M2 steel following heat treatment and triple tempering. The specimen was cut and polished and then etched with a 3% nital solution. Measurements of interband spacing, that is, measurements from mid-band on one band to mid-band on an adjacent band, indicate an average of approximately 135 ⁇ m with a standard deviation of the average of approximately 21 ⁇ m.
  • FIG. 2 is an optical micrograph of a powder metallurgical M4 tool steel grade bar stock, which exhibits similar alignment of the metal carbide and alloy bands substantially along the rolling direction as apparent in FIG. 1A .
  • the tool steel After hot rolling, the tool steel is fashioned into a blank that preserves the carbide and/or alloy banding.
  • the directionality of the metal carbides in the carbide bands and the segregated alloy components in the alloy bands increases the probability of brittle fracture and wear along that direction.
  • the carbide and alloy bands tend to coincide with the primary loading direction along which fracture may occur during subsequent use.
  • Methods of processing steel elements are known from EP-A-0587 489 which discloses twisting, US-A-5136905 which discloses forging/upsetting, and JP-A-56151125 which discloses forging.
  • a tool for use in a machine to modify a workpiece, the tool comprising a member formed from a tool steel, the member including a working surface adapted to contact the workpiece; a first region beneath the working surface, the tool steel in the first region having a microstructure containing a plurality of carbide bands or a plurality of alloy bands that are not unidirectionally aligned, wherein each of the plurality of carbide bands or each of the plurality of alloy bands has a positive angle of inclination over a portion of the first region and a negative angle of inclination over another portion of the first region, wherein the transition between the positive angle of inclination and the negative angle of inclination is continuous, and a second region including a microstructure containing another plurality of carbide bands or another plurality of alloy bands, the carbide bands or the alloy bands in the first region being compressed more tightly together than the carbide bands or the alloy bands in the second region such that the carbide bands or the alloy bands in the first region have an average density that is
  • the tool may comprise an elongate steel member including a longitudinal axis, a shank configured to be coupled with the machine, and a tip spaced along the longitudinal axis from the shank.
  • the tip includes the working surface and the first region in which the carbide and/or alloy bands are not substantially aligned with the longitudinal axis.
  • plurality of carbide bands or plurality of alloy bands of the second region are substantially aligned with the longitudinal axis.
  • the carbide bands or alloy bands in the first region have an interband spacing that is less than a second interband spacing of the carbide bands or alloy bands in the second region. The carbide or alloy bands are more tightly compressed in the first region compared to the second.
  • thermo-mechanically processing includes heating the tip to a processing temperature and, while the tip is at the processing temperature, applying
  • the steel in the elongate member or preform may comprise a tool steel commonly used to form tools for machining, metal cutting, powder compaction, metal engraving, pin stamping, and metal-forming applications.
  • the tool steel may have a carbide content ranging from about 5 percent to about 40 percent by weight.
  • the steel of the preform is mechanically processed at an elevated temperature by a thermo-mechanical treatment or process, such as conventional forging processes.
  • Suitable conventional forging processes include, but are not limited to, ring rolling, swaging, rotary forging, radial forging, hot and warm upsetting, and combinations of these forging processes.
  • Thermo-mechanical treatment generally involves the simultaneous application of heat and a deformation process to an alloy, in order to change its shape and refine the microstructure.
  • the thermo-mechanical process economically improves the resultant mechanical properties, such as impact resistance, fracture toughness, and wear resistance, of the steel.
  • the modified mechanical properties are achieved without altering the metallurgical composition of the steel.
  • FIG. 1 is an optical micrograph taken at a magnification of about 14x showing a polished and etched region of a commercially available M2 tool steel grade bar stock with carbide and/or alloy banding apparent along the rolling direction in accordance with the prior art.
  • FIG. 1A is an SEM micrograph at a magnification of about 130x showing a polished region of a commercially available S7 tool steel grade bar stock with alloy banding apparent along the rolling direction in accordance with the prior art.
  • FIG. 1B is an optical micrograph taken at a magnification of about 100X showing a polished and etched region of a commercially available M2 tool steel grade bar stock with carbide and/or alloy banding apparent along the rolling direction in accordance with the prior art.
  • FIG. 2 is an optical micrograph similar to FIG. 1 of a powder metallurgical M4 tool steel grade bar stock that also exhibits aligned carbide and/or alloy banding in the rolling direction in accordance with the prior art.
  • FIG. 3 is a plan view of a tool in accordance with a representative embodiment of the invention.
  • FIG. 3A is a schematic cross-sectional view diagrammatically illustrating the carbide and/or alloy banding in region, L, of the tool in FIG. 3 after modification by thermo-mechanical processing in accordance with an embodiment of the invention.
  • FIGS. 4A and 4B are side views of preforms or blanks that can be used to fabricate the tool of FIG. 3 .
  • FIGS. 4C and 4D are perspective views of preforms or blanks that can be used to fabricate the tool of FIGS. 5A and 5B , respectively.
  • FIGS. 5A and 5B are perspective views of embodiments of tools according one aspect of the invention.
  • FIB. 5C is a perspective view of one embodiment of a tool, following thermo-mechanically processing of a preform with subsequent machining.
  • FIGS. 6A and 6B show a representative sequence of operations for thermo-mechanically processing a hot-rolled steel blank by hot-upsetting in accordance with an embodiment of the invention.
  • FIGS. 6C and 6D show other tool embodiments following thermo-mechanically processing a hot-rolled steel blank of FIG. 4A by forging and hot-upsetting in accordance with an alternative embodiment of the invention.
  • FIG. 7 is an optical micrograph of an M2 grade tool steel preform that has been modified by a thermo-mechanical process in accordance with one aspect of the invention and that, in the processed section, exhibits carbide and/or alloy banding that is not substantially aligned in the rolling direction.
  • FIG. 7A is an optical micrograph taken of an area 7A of a specimen prepared similar to that shown in FIG. 7 taken at a magnification of about 100X showing a polished and etched region with carbide and/or alloy banding.
  • FIG. 7B is an optical micrograph taken of an area 7B of a specimen prepared similar to that shown in FIG. 7 taken at a magnification of about 100X showing a polished and etched region with carbide and/or alloy banding.
  • FIG. 8 is an optical micrograph of an as-rolled M2 grade tool steel preform after being subjected to two, discrete, hot-upsetting thermo-mechanical processes in accordance with an embodiment of the invention.
  • FIG. 9 is an optical micrograph of a powder metallurgical M4-grade tool steel grade preform after thermo-mechanical processing using a single hot-upsetting process in accordance with an embodiment of the invention.
  • FIG. 10 is an optical micrograph of a typical as-rolled bar stock specimen after a head-forging process to define a head for a tool in accordance with the prior art.
  • FIG. 10A is an optical micrograph taken at about 100X of an area 10A of FIG. 10 after a head-forging process to define a head for a tool in accordance with the prior art.
  • FIG. 11 is graphical representation of the influence of thermo-mechanical processing on tool service life in a metal-forming (i.e., piercing) application for a tool in accordance with an embodiment of the invention.
  • FIG. 12 is a graphical representation of the influence of processing method on wear rate in a metal-forming (i.e., piercing) application for a tool in accordance with an embodiment of the invention.
  • FIG. 13A is a schematic side view of a punch with a thermo-mechanically processed tip and working surface that was used in the metal-forming application to acquire the data shown in FIGS. 11 and 12 .
  • FIG. 13B is an electron micrograph of the cutting edge as indicated from the enclosed area 13B of FIG. 13A of a conventional punch formed from M2 grade tool steel in the as-rolled condition in accordance with the prior art and used to acquire the data for the conventional punch shown in FIGS. 11 and 12 .
  • FIG. 13C is an electron micrograph of the cutting edge as indicated from the enclosed area 13B of FIG. 13A of a punch that includes the thermo-mechanically processed tip and working surface in accordance with an embodiment of the invention and used to acquire the data for the punch shown in FIGS. 11 and 12 .
  • FIG. 14 is a graphical representation showing the influence of thermo-mechanical processing on tool life in a machining (i.e., broaching) application for a broach in accordance with an embodiment of the invention and a broach in accordance with the prior art.
  • FIGS. 15A and 15B are a side view and an end view, respectively, of a tool according to one embodiment of the invention having a broach configuration and used in the machining application to acquire the data of FIG. 14 .
  • FIGS. 15C and 15D are an optical micrograph of a working surface and an electron micrograph of encircled area 15D, 15F of FIG. 15A , respectively, of a broach that is formed from a conventional M4-grade powder metal tool steel in accordance with the prior art.
  • FIGS. 15E and 15F are an optical micrograph of a working surface and an electron micrograph of encircled area 15D, 15F of FIG. 15A , respectively, of a broach in accordance with an embodiment of the invention formed from M4-grade powder metal tool steel that has a working tip that has been thermo-mechanically processed.
  • a tool 10 is an elongate member that includes a barrel or shank 14, a head 12 disposed at one end of the shank 14, and a nose or body 16 with a tip 15 disposed at an opposite end of the shank 14 from the head 12.
  • a working surface 18 carried on the tip 15 joins a sidewall of the tip 15 along a cutting edge 20.
  • the cutting edge 20 and working surface 18 define the portion of the tool 10 that contacts the surface of a workpiece 25.
  • the workpiece 25 may comprise a material to be processed by the tool 10 in a metal-forming application, such as a thin metal sheet.
  • the shank 14 and body 16 of the elongate member When viewed along a longitudinal axis or centerline 22 of the tool 10, the shank 14 and body 16 of the elongate member have a suitable cross-sectional profile, such as, for example, a round, rectangular, square or oval cross-sectional profile.
  • the shank 14 and body 16 may have cross-sectional profiles of identical areas or the body 16 may have a smaller cross-sectional area to provide a relief region between the shank 14 and body 16.
  • the shank 14 and body 16 are symmetrically disposed about the centerline 22 and, in particular, may have a circular or round cross-sectional profile centered on and/or symmetrical about the centerline 22.
  • the head 12 of the tool 10 has a construction appropriate for being retained with a tool holding device used with a metalworking machine like a machine tool or a press (not shown).
  • the head 12 is a flange having a diameter greater than the diameter of the shank 14.
  • the tool 10 may alternatively include a ball-lock retainer, a wedge-lock retainer, a turret, or another type of retaining structure for coupling the shank 14 of tool 10 with a tool-retaining device.
  • the tool 10 which has the construction of a punch in the representative embodiment, typically forms a component of a die set for use in a stamping operation.
  • the die set further includes a die 26 containing an opening that receives a portion of the tip 15 of tool 10.
  • the die 26 and tool 10 cooperate, when pressed together, to form a shaped hole in a workpiece or to deform the workpiece 25 in some desired manner.
  • the tool 10 and the die 26 are removable from the metalworking machine with the tool 10 being temporarily attached by using a tool retention mechanism to the end of a ram.
  • the tool 10 moves generally in a direction towards the workpiece 25 and with a load normal to the point of contact between the working surface 18 and the workpiece 25.
  • the metalworking machine may be driven mechanically, hydraulically, pneumatically, or electrically to apply a load that forces the tool 10 into the workpiece 25.
  • the tip 15 of tool 10 is forced under the high load imparted by the metalworking machine through, or into, the thicknesses of the workpiece 25 and into the die opening.
  • the workpiece 25 is cut and/or deformed at, and about, the contact zone between the working surface 18 of tool 10 and the workpiece 25.
  • regions of the die 26 beneath one or more working surfaces of the die 26 may be formed from steel that has been thermo-mechanically processed in a manner consistent with the embodiments of the invention.
  • the workpiece 25 may comprise a powder housed in a recess of the die 26, instead of the representative sheet metal.
  • the tool 10 can be fabricated from various different classifications of steel including, but not limited to, tool steels like cold-work, hot-work, or high-speed tool steel grade materials, as well as stainless steels, specialty steels, and proprietary tool steel grades.
  • the tool 10 may also comprise a powder metallurgical steel grade or, in particular, a powder metallurgical tool steel.
  • Tool steel material grades are generally iron-carbon alloy systems with vanadium, tungsten, chromium and molybdenum that exhibit hardening and tempering behavior.
  • the carbon content may be within a range from about 0.35 wt.% to about 1.50 wt.%, with other carbon contents contemplated depending on the carbide particles desired for precipitation, if any.
  • the carbon content is within a range from about 0.85 wt.% to about 1.30 wt.%.
  • the tool steel may exhibit hardening with heat treatment and may be tempered to achieve desired mechanical properties.
  • Table 1 shows the nominal composition in weight percent of exemplary tool steel grades that may be used to fabricate the tool 10, the balance being iron (Fe).
  • the tip 15 of body 16 near the working surface 18 is subjected to a thermo-mechanical process that alters the morphology or microstructure of the material of the tool 10 by heating at least the tip 15 and applying a force to the tip 15.
  • the thermo-mechanical process modifies the constituent microstructure of the tip 15 in a region L, such that the service life of the tool 10 in machining and metal-forming applications is significantly prolonged, but does not modify the composition of the tool steel.
  • region L intersects the working surface 18 and, therefore, region L may be measured along the length of the tip 15 of body 16 relative to the working surface 18.
  • the structurally modified region L may extend a distance of between 0.125 inches (0.3175 centimeters) and 0.25 inches (0.635 centimeters) along the tip 15 from the working surface 18. In other specific embodiments, the structurally modified region L may extend a distance greater than about 0.001 inches (about 0.00254 centimeters) along the tip 15 from the working surface 18.
  • the extended service life may arise from a change in the directionality of the carbide and/or alloy banding in region L.
  • the thermo-mechanical process operates to misalign the carbide and/or alloy bands in region L such that adjacent bands are no longer aligned parallel to each other and with the centerline 22, as schematically shown in FIG. 3A .
  • the carbide and/or alloy bands 24 have non-linear alignment in region L.
  • an inclination angle, ⁇ 1 of at least one of the carbide and/or alloy bands 24 transitions from approximate alignment with the centerline 22 outside of the thermo-mechanically modified region, L, to significant misalignment or nonalignment with the centerline 22 inside region, L.
  • the inclination angle, ⁇ 1 of at least one of the carbide and/or alloy bands 24 has a positive slope relative to the centerline 22 over a portion of region, L, near the working surface 18 and a negative slope over another portion of region, L.
  • the transition between the positively-sloped and negatively-sloped portions of the bands 24 is smooth, as is the transition from the negatively-sloped portion of the bands 24 to portions of the bands 24 outside of region, L, which are approximately aligned with the centerline 22.
  • An inclination angle, ⁇ 2 of at least another of the carbide and/or alloy bands 24 may transition from approximate alignment with the centerline 22 outside of the thermo-mechanically modified region, L, to significant misalignment or nonalignment with the centerline 22 inside region, L.
  • the inclination angle, ⁇ 2 may differ from the inclination angle, ⁇ 1 , such that one of the carbide and/or alloy bands 24 appears to approach another of the carbide and/or alloy bands 24 in a converging manner.
  • one carbide and/or alloy band 24 may appear to diverge from another carbide and/or alloy band 24.
  • the carbide and/or alloy bands 24 may transition from approximate alignment with the centerline outside of the thermo-mechanically modified region, L, to an orientation such that the carbide and/or alloy bands 24 are not unidirectionally aligned.
  • adjacent pairs of the carbide and/or alloy bands 24 may appear to converge at some depths within region L while appearing to diverge from each other at other depths within region L so that the interband spacing varies with position along the centerline 22 in region L.
  • all of the carbide and/or alloy bands 24 may exhibit the same changes in inclination angle, ⁇ 1 , over the length of the thermo-mechanically modified region, L, so that the inter-band spacing is approximately constant.
  • This morphological modification producing the misaligned carbide and/or alloy bands locally in region, L may operate to improve the mechanical properties of the tool 10.
  • the resistance of the tool steel to brittle fracture is believed to be greatly improved by eliminating directionality in the carbide and/or alloy banding in the modified region, L.
  • Regions of the body 16 and shank 14 outside of the modified region, L are not modified by the thermo-mechanical process and, therefore, these regions will exhibit the directionality of the carbide and/or alloy bands characteristic of hot worked tool steel, like hot rolled tool steel.
  • the improvement in mechanical properties for tip 15 is independent of the tool retaining mechanism used in tool 10.
  • the tool 10 may be fabricated by shaping a preform or blank, such as the representative blank 30, with the thermo-mechanical treatment process.
  • Blank 30 has a tip 32 that is at least partially shaped by the thermo-mechanical process during the fabrication of the tool 10.
  • the tip 32 which has the shape of a truncated cone or a frustoconical shape, tapers along its length and terminates at a blunt end 33. Following the thermo-mechanical treatment process and any subsequent secondary processes, tip 32 defines the tip 15 of tool 10 and includes the working surface 18 ( FIG. 3 ). The remainder of the blank 30 defines the head 12, shank 14, and the remainder of the body 16 of tool 10.
  • the extended service life may be influenced by additional morphological modifications.
  • the carbide and/or alloy bands in region L are compressed more tightly together. That is, the distance between adjacent bands is less resulting in a higher density of bands in a given area than in other regions. The higher density of bands in region L may further operate to improve the mechanical properties of the tool 10.
  • the geometry or shape of the initial blank 30, before the application of the thermo-mechanical processing, will impact the resultant microstructure in region L of the tool 10, for example, like the tool 10 illustrated in FIG. 3 .
  • the geometry of the blank 30 may be selected based upon the type of thermo-mechanical process employed and the targeted final geometry for the tool 10.
  • the geometry of the blank 30 can comprise cylindrical rod stock, rectilinear bar stock, coil stock, or stock material having other, more complex shapes and cross-sectional profiles.
  • the determination of preform geometry may be developed based on past experience, tooling requirements, and process limitations. For example, a minimum upset ratio of about 2:1 may be specified from process limitations to provide a microstructure that provides a perceivable improvement in the mechanical properties. The improvement in mechanical properties is believed to increase with increasing upset ratio.
  • the blank 30 with a frustoconical tip 32 may be particularly suitable for use as a preform in a hot upsetting process to impart the desired mechanical properties to the tool steel comprising tool 10.
  • the frustoconical tip 32 of the blank 30 may be formed by machining in a lathe, shaped by swaging, etc. Machining may remove some of the material along the exterior during formation of the tip 32. The removed material may contain less carbide than, for example, the remaining material forming the tip 32.
  • the tip 32 is expanded radially by the thermo-mechanical process relative to the centerline 22 as is more fully described with reference to FIGS. 6A-6C below.
  • the extended service life of tool 10 may be influenced by additional morphological modifications. For example, removing a portion of the relatively lower carbide containing material prior to thermo-mechanical processing may provide greater carbide content at and/or near the working surface 18 following thermo-mechanical processing.
  • thermo-mechanical treatments include, but are not limited to, forging processes such as radial forging, ring rolling, rotary forging, swaging, thixoforming, ausforming, and warm/hot upsetting.
  • forging processes such as radial forging, ring rolling, rotary forging, swaging, thixoforming, ausforming, and warm/hot upsetting.
  • upset forging also referred to simply as upsetting
  • single or multiple upsetting may be used to shape the blank 30.
  • the blank 30 may be heat treated, finish machined, and ground to supply any required tooling geometry as found in conventional tools.
  • a blank 34 having a "bullet-shaped" tip 36 may be shaped by thermo-mechanical treatment into tool 10.
  • Tip 36 tapers with a curvature along its length and terminates at a blunt end 37.
  • the microstructural morphology of the tool steel comprising blank 34 initially includes carbide and/or alloy bands similar to those shown in the optical micrograph of FIG. 1 .
  • tip 36 defines the tip 15 of the tool 10, for example, like the tool 10 depicted in FIG. 3 , and includes the working surface 18.
  • the remainder of the blank 34 defines the head 12, shank 14, and the remainder of the body 16 of the tool 10.
  • the blank 38 having a smaller diameter tip 40 than tip 32 ( FIG. 4A ) and tip 36 ( FIG. 4B ) may be shaped by thermo-mechanical treatment into a tool 43, such as shown in FIG. 5A .
  • the tip 40 shown in FIG. 4C , tapers along its length and has a smaller diameter than the remainder of the blank 38.
  • the tip 40 defines a tip 42 of the tool 43 having a working surface 44 shown in FIG. 5A .
  • a blank having a relatively small tip compared to the remaining portion of the blank may be utilized such that the upset ratio is maximized.
  • FIG. 4D illustrates another exemplary embodiment of a blank 46 utilized to thermo-mechanically form a tool having a relatively small tip, such as a tool 48 shown in FIG. 5B .
  • the blank 46 has a tapered rectangular tip 50. Following thermo-mechanical treatment, the tip 50 defines, for example, a tip 54 of tool 48 shown in FIG. 5B .
  • the tip 54 has a rectangular shaped working surface 56. While various embodiments of blanks 30, 34, 38, 46 are illustrated and described above, blanks are not limited to those shown.
  • the tip 15, 42, 54 of the tool 10, 43, 48 may be any shape. Furthermore, the shape may be determined by the metal-forming or machining application.
  • a tip 62 of a blank 60 which is similar to blank 30 ( FIG. 4A ), is subjected to a single-stage thermo-mechanical process that modifies the microstructure of tip 62.
  • the blank 60 initially contains a microstructure with carbide and/or alloy bands aligned approximately along the centerline 22 of blank 60.
  • the tip 62 of the blank 60 is machined by, for example, lathe turning into a truncated conical shape, as best shown in FIG. 6A , having an included angle ⁇ 1 .
  • the tip 62 is subjected to a hot-upsetting thermo-mechanical process that deforms the tip 62 into a more cylindrical shape, as best shown in FIG. 6B .
  • a larger included angle ⁇ 1 may be a result of the thermo-mechanical process.
  • the hot-upsetting thermo-mechanical process deforms the tip 62 such that tip 62 no longer has an included angle or the included angle may approach 180° (for example, the tip 62 may have a substantially cylindrical appearance as shown in FIG. 6B ).
  • the processing temperature range can vary depending on parameters such as the specific thermo-mechanical process, the part size, the part material, etc.
  • the processing temperature may be above the lower transformation temperature, i.e., the AC 1 temperature, at which the structure of the constituent tool steel begins to change from ferrite and carbide to austenite when being heated.
  • the hot-upsetting thermo-mechanical process alters the microstructure in the tip 62 such that the carbide and/or alloy bands deviate from the alignment parallel to the centerline 22 that is characteristic of the material before the thermo-mechanical process is performed. After processing, all or a portion of tip 62 defines the tip 15 ( FIG. 3 ) containing the modified carbide and/or alloy bands.
  • blank 60 (shown in FIG. 6B ) may be machined or hot forged, after the single stage thermo-mechanical process, to form a blank 70 having a tip 72 with a truncated conical shape.
  • the initial included angle ⁇ 2 in FIG. 6C of the tip 72 may differ from the included angle ⁇ 1 of the tip 62 of blank 60.
  • the initial included angle ⁇ 2 of tip 72 may be about 20° and the initial included angle ⁇ 1 of tip 62 may be about 16°.
  • the tip 72 is subjected to a second hot-upsetting thermo-mechanical process that deforms the tip 72 into a more cylindrical shape, as best shown in FIG. 6D .
  • the second hot-upsetting thermo-mechanical process reduces the included angle ⁇ of the tip 72.
  • the processing temperature range can vary depending on parameters such as the specific thermo-mechanical process, the part size, the part material, etc.
  • the second hot-upsetting thermo-mechanical processes further modifies the microstructure in the tip 72, which may act to further increase the deviation of the carbide and/or alloy bands from alignment along the centerline 22.
  • the application of multiple thermo-mechanical processes may modify the microstructure of the tip 72 to further enhance the improvement in mechanical properties.
  • all or a portion of tip 72 defines the tip 15 ( FIG. 3 ) containing the modified carbide and/or alloy bands.
  • a secondary process may be used to further modify the tip 15 ( FIG. 3 ) of the tool 10 to shape the tip 15 for a particular application or to impart additional improvements in tool life.
  • a tip 74 may be machined from the tip 42 shown in FIG. 5A .
  • the tip 74 may include a concave cutout 76 adapted to provide shearing action when forcibly engaged with a workpiece. While the blanks illustrated herein are depicted as generally cylindrically shaped, the blanks are not limited to generally cylindrical shapes, as other shapes will suffice or may be required depending on, for example, the final application, the workpiece, or even available bar stock.
  • Exemplary secondary processes include thermal spraying or cladding the working surface of the tool 10 with one or more wear resistant materials.
  • Other secondary process may include applying a coating on the working surface of the tool 10 by a conventional coating techniques including, but not limited to, physical vapor deposition (PVD), chemical vapor deposition (CVD), or salt bath coatings.
  • PVD physical vapor deposition
  • CVD chemical vapor deposition
  • Other surface modification techniques may include ion implantation, laser or plasma surface hardening techniques, nitriding, or carburizing. These exemplary surface modification techniques may be used to modify a surface layer at the working surface of the tool.
  • Additional secondary processes, such as edge honing are contemplated by the invention for use in modifying the working surface of the tool 10.
  • various different secondary processes may be used in any combination for further modifying tip 15.
  • the tool 10 may have other punch constructions that differ from the construction of the representative embodiments.
  • tool 10 may be configured as a blade, a heel punch, a pedestal punch, a round punch, etc.
  • tool 10 is depicted as having a construction consistent with a punch in the representative embodiment, a person having ordinary skill will understand that the tool 10 may have other constructions.
  • tool 10 in the form of punch or stripper may be applied in metal stamping and forming operations like piercing and perforating, fine blanking, forming, and extrusions or coining.
  • the tool 10 may also have the construction of a cutting tool, such as a rotary broach, a non-rotary broach, a tap, a reamer, a drill, a milling cutter, etc.
  • Tool 10 may be used in casting and molding applications, such as conventional die casting, high pressure die casting, and injection molding.
  • Tool 10 may also be utilized in powder compaction applications used in pharmaceutical processes, nutraceutical processes, battery manufacture, cosmetics, confectionary and food and beverage industries, and in the manufacture of household products and nuclear fuels, tableting, explosives, ammunition, ceramics, and other products.
  • Tool 10 may also be used in automation and part fixturing applications, such as locating or part-touching details.
  • tool 10 may be made by machining a thermo-mechanically processed end of an existing tool to define a tip 15 arranged along the centerline 22 with the shank 14, such as the tip 74 depicted in FIG. 5C .
  • the tip 15 contains a region L having a microstructure with carbide and/or alloy bands that are not substantially aligned with the centerline 22 of the tip 15.
  • the tip 15 may be further modified by additional thermo-mechanical processing to further modify the alignment of the carbide bands relative to the centerline 22 of the tip 15.
  • tool 10 may be made by machining an end of an existing tool to define tip 15 arranged along the centerline 22 with the shank 14.
  • the tip 15 contains carbide and/or alloy bands that are aligned with the rolling direction.
  • the tip 15 is thermo-mechanically processed to modify an alignment of the carbide and/or alloy bands relative to the centerline 22 of the tip 15.
  • a conical blank or preform for a punch was prepared with a geometry as shown in FIG. 4A .
  • the blank had an overall length of about 4.25 inches and a diameter of about 0.51 inches.
  • the tip had a length dimension of about 0.7 inches with an included angle of about 16° such that the tip tapered to a blunt end having a diameter of about 0.070 inches.
  • the conical blank was composed of a hot-rolled M2-type tool steel.
  • the tip of the conical blank was thermo-mechanically processed using a single hot-upsetting type of thermo-mechanical process. Specifically, a fifty-ton horizontal hot-upsetting machine was used for themio-mechanically processing the preform.
  • the conical preform was locally heated at the tip using an induction heater to a targeted processing temperature before the tip was hot-upset forged from the conical shape to a cylindrical shape.
  • the processing temperature of the tip was in a temperature range of about 1652°F (about 900°C) to about 1742°F (about 950°C).
  • the processed cylindrical bars were then used to conventionally manufacture a tool having the shape of a punch. Care was taken during tool manufacture to make sure that the tool working edge, i.e. tool edge and working surface that contacts the workpiece during use, was in the processed section.
  • the tip was sectioned longitudinally approximately along the centerline using a diamond saw, ground, and polished using standard metallographic sample preparation techniques.
  • the polished sample was etched using a 3% nital solution (i.e., 3 vol.% nitric acid and the rest methanol), rinsed and dried.
  • FIG. 7 represents an optical micrograph of the etched sample taken with a stereoscope at a 14X magnification.
  • the optical micrograph in FIG. 7 has been converted to a grayscale image.
  • some of the optical micrographs herein have been embellished with lines intended to guide the eye. However, the addition of the guide lines has not altered the information contained in the original image.
  • the microstructure in the unprocessed section shows unidirectional carbide and/or alloy banding similar to FIG. 1 .
  • the carbide and/or alloy banding in the processed section has been modified to realign the carbide and/or alloy bands so that the carbide and/or alloy bands are not aligned with the centerline of the preform, which is believed to lead to an improvement in mechanical properties.
  • the modification of the carbide and/or alloy bands is apparent from a comparison between the processed and unprocessed sections in FIG. 7 .
  • a tool prepared in accordance with Example 1 was heat treated and triple tempered. Following this preparation, the tool was cut and one of the cut specimens was polished and then etched with a 3% nital solution. Optical micrographs at about 100X, as shown in FIGS. 7A and 7B , of the specimen were taken in areas similar to those shown in FIG. 7 (as indicated by enclosed areas 7A and 7B, respectively). The working surface of the tip of a tool made from this processed blank is on the terminal face of the processed region and the tip has a centerline substantially as indicated in FIG. 7 .
  • FIG. 7A a magnified view of a processed section of the tool is provided.
  • the carbide/alloy banding is not substantially aligned with the longitudinal axis of the tool (represented by centerline, C L , in FIG. 7 ).
  • measurements of interband spacing in FIG. 7A indicate an average interband spacing of approximately 87 ⁇ m with a standard deviation of the average of approximately 13 ⁇ m.
  • FIG. 7B is another magnified view of an area different from the area depicted in FIG. 7A of the processed section of the tool as illustrated in FIG. 7 .
  • Interband spacing measurements of carbide/alloy banding of FIG. 7B indicate an average interband spacing of approximately 68 ⁇ m with a standard deviation of the average of about 12 ⁇ m.
  • measurements of interband spacing of an unprocessed section of the tool indicate spacing similar to that provided in the description of FIG. 1A .
  • the unprocessed section of the tool therefore, appears unchanged from the as-rolled condition.
  • the processed sections are characterized by about a 150% to 200% decrease in interband spacing compared to the as-rolled or unprocessed section within the same tool.
  • the interband spacing in the processed section is less than the interband spacing in the unprocessed section.
  • the interband spacing may gradually increase along a radial line from the outer peripheral surface to a radial midpoint and then decrease from the radial midpoint to the center of the tool.
  • Another gradient in the interband spacing may be observed along a direction parallel to, and positioned radially from, the longitudinal axis through the processed section into the unprocessed section. For example, starting at a working surface, the interband spacing may initially decrease through the processed section and then increase as the unprocessed section is approached. It is expected that similar interband spacing would be observed for tools made via powder metallurgy.
  • FIG. 8 shows an optical micrograph of an as-rolled bar stock specimen or preform after being subjected to two, discrete hot upsetting thermo-mechanical processes.
  • the microstructure in the unprocessed section shows unidirectional carbide and/or alloy banding similar to FIG. 1 .
  • the carbide and/or alloy banding in the processed section has been modified to realign the carbide and/or alloy bands so that the carbide and/or alloy bands are not aligned with the centerline of the preform, which is believed to lead to an improvement in mechanical properties.
  • the modification of the carbide and/or alloy bands is apparent from a comparison between the processed and unprocessed sections in FIG. 8 . It is also believed that two, discrete hot upsetting thermo-mechanical processes decrease the interband spacing compared to the tool prepared according to Example 1 by, for example, at least 50%.
  • the working surface of the tip of a tool made from this processed blank is on the terminal face of the processed region and the tip has a centerline substantially as indicated in FIG. 8 .
  • FIG. 9 shows an optical micrograph of a powder metallurgical M4-grade tool steel as-rolled bar stock specimen or preform after thermo-mechanical processing using a single hot-upsetting process.
  • the microstructure in the unprocessed section shows unidirectional carbide and/or alloy banding similar to FIG. 2 .
  • the carbide and/or alloy banding in the processed section has been modified to realign the carbide and/or alloy bands so that the carbide and/or alloy bands are not aligned with the centerline of the preform, which is believed to lead to an improvement in mechanical properties.
  • the modification of the carbide and/or alloy bands is apparent from a comparison between the processed and unprocessed sections in FIG. 9 .
  • the working surface of the tip of a tool made from this processed blank is on the terminal face of the processed region and the tip has a centerline substantially as indicated in FIG. 9 .
  • FIG. 10 shows a micrograph of a typical as-rolled bar stock blank after head-forging or head-upsetting to form a head in accordance with the prior art.
  • head forging the head is deformed such that an overall dimension is expanded.
  • a 0.5 inch diameter steel preform may be head forged such that the head has a diameter of 0.625 inches.
  • the head formed by head-forging is used to couple the resultant tool with a tool retaining device of a metalworking machine.
  • the head of the tool having a microstructure or alloy banding shown in FIG. 10 does not contact the workpiece or otherwise perform any operation on the workpiece.
  • the hot forging process is one way to produce the head of the tool but not all tools require a shaped head.
  • the microstructure in the head-forged section shows unidirectional carbide and/or alloy banding generally parallel to the centerline of the specimen and the rolling direction similar to the aligned carbide and/or alloy bands visible in FIG. 1 .
  • the carbide and/or alloy banding in the head-forged section is modified by the head-forging to have a more widely spaced pattern with larger separations between adjacent carbide and/or alloy bands.
  • an interband spacing between adjacent bands is greater in the head-forged section than in the unprocessed section.
  • Measurements of the interband spacing in the head-forged region shown in FIG. 10A indicate an average interband spacing in this area of approximately 162 ⁇ m with a standard deviation of the average of approximately 5 ⁇ m.
  • a cylindrical-shaped head deforms into a larger diameter cylinder with the carbide and/or alloy bands being displaced radially. Since the final diameter of the head-forged section is larger than the initial diameter of the preform, the carbide and/or alloy bands may spread apart in proportion to the overall radial expansion.
  • Punches were formed from the preforms of Examples 1 and 2 with the working surface and underlying portion of the body formed from the thermo-mechanically modified M2 grade tool steel.
  • the punches were used to pierce 0.5 inch diameter holes in workpieces comprising 0.125 inch thick re-rolled 125,000 psi yield strength rail steel.
  • Two parameters, the number of cycles or parts/hits and the burr height were used as benchmark in this piercing application.
  • the punches were held using a ball-lock tool retention mechanism.
  • the punch made from the thermo-mechanically modified preform of Example 1 exhibited a tool service life improvement of about 3.1 times in comparison with a comparable punch manufactured from conventional as-rolled M2 grade tool steel.
  • the conventional M2-grade steel punch lasted for 8,000 hits while the modified M2-grade steel punch made from the preform of Example 1 lasted 24,800 hits and the modified M2-grade steel punch made from the preform of Example 2 lasted about 34,000 hits.
  • thermo-mechanically processed punches As shown in FIGS. 12 and 13A-C , similar improvements in wear resistance and edge retention are also evident for the thermo-mechanically processed punches in comparison with the conventional punch.
  • the thermo-mechanically processed M2-grade tool steel punches exhibited a slower rate of wear, as indicated by the smaller slope, and better edge retention than the conventional M2 tools as is graphically illustrated in FIG. 12 .
  • This slower rate of wear may be favored in high precision applications, wherein such thermo-mechanically processed tools may significantly improve the consistency of the metalworking operation over the entire tool service life in comparison with conventional punches.
  • the edge of the conventional M2-grade tool steel punch (shown in the electron micrograph of FIG. 13B ) experienced severe adhesive and abrasive wear typical in the metal-forming application, while the edge of the processed M2 tool (shown in the electron micrograph of FIG. 13C ) experienced minor abrasive wear by comparison.
  • the punches were evaluated at end of the service life of each respective tool.
  • a conical blank or preform was prepared with a geometry as shown in FIG. 4A .
  • the blank had an overall length of about 5.3 inches and a diameter of about 0.76 inches.
  • the tip had a length dimension of about 0.74 inches with an included angle of about 24° such that the tip tapered to a blunt end having a diameter of about 0.105 inches.
  • the conical blank was composed of a hot-rolled powder metal M4-type tool steel.
  • the tip of the conical blank was thermo-mechanically processed using a single hot-upsetting type of thermo-mechanical process as described above in Example 1.
  • the preform was formed into a broach with the working end containing the thermo-mechanically processed material. The construction of the broach is shown in FIG. 15A with the cross-sectional configuration shown in FIG. 15B .
  • the broach was used to make 0.883 inch diameter spline shapes in workpieces comprising cold drawn 85,000 psi yield strength steel with the working end contacting the workpieces.
  • Tool life a conventionally accepted standard for the machining process, was used to benchmark a broach fabricated according to an embodiment described herein against a conventional broach. During use, each broach was held using a whistle notch tool retention mechanism.
  • the broach with the thermo-mechanically processed working tip (labeled "PM-M4[Single Upset]" and characterized by the modified carbide and/or alloy banding) exhibited an improvement in tool service life of about 1.75 times that of a conventional broach formed from as-rolled M4-grade powder metal tool steel that has aligned carbide and/or alloy bands as shown in FIG. 2 .
  • the conventional broach lasted for about 2,835 cycles and the thermo-mechanically processed broach lasted for about 4,953 cycles.
  • the conventional broach also exhibited significantly higher regions of catastrophic failure and poor edge retention in comparison with the broach with the thermo-mechanically processed working tip.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Forging (AREA)

Claims (26)

  1. Outil (10, 43, 48) pour utilisation dans une machine permettant de modifier une pièce à travailler, l'outil comprenant un membre formé à partir d'un acier à outils, le membre comprenant une surface de travail (18, 44, 56) adaptée pour entrer en contact avec la pièce à travailler; une première région en dessous la surface de travail (18, 44, 56), l'acier à outils dans la première région ayant un microstructure comportant une pluralité de bandes de carbure ou une pluralité de bandes d'alliage qui ne sont pas alignées unidirectionnellement, dans lequel chacune de la pluralité des bandes de carbure ou chacune de la pluralité des bandes d'alliage possède un angle d'inclinaison positif sur une portion de la première région et un angle d'inclinaison négatif sur une autre portion de la première région, dans lequel la transition entre l'angle d'inclinaison positif et l'angle d'inclinaison négatif est continue, et une deuxième région comportant une microstructure qui contient une autre pluralité de bandes de carbure ou une autre pluralité de bandes d'alliage, les bandes de carbure ou les bandes d'alliage dans la première région étant comprimées plus étroitement ensemble que les bandes de carbure ou les bandes d'alliage dans la deuxième région, de sorte que les bandes de carbure ou les bandes d'alliage dans la première région ont une densité moyenne plus élevée que la densité moyenne les bandes de carbure ou les bandes d'alliage dans la deuxième région.
  2. Outil de la revendication 1, dans lequel la surface de travail (18, 44, 56) possède une surface normale, et les bandes de carbure ou les bandes d'alliage sont alignées dans une direction qui n'est pas parallèle à la surface normale.
  3. Outil de la revendication 1 ou de la revendication 2, dans lequel le membre est allongé, ledit membre allongé comprenant un axe longitudinal (22), un corps (14) configuré pour être couplé avec la machine, et une pointe (15, 42, 54, 74) espacée le long de l'axe longitudinal (22) du corps (14), ladite pointe (15, 42, 54, 74) comprenant la surface de travail (18, 44, 56) et la première région à proximité, les bandes de carbure ou les bandes d'alliage dans la première région non sensiblement alignées avec l'axe longitudinal (22), et la deuxième région étant juxtaposée avec la première région et entre la première région et la tige (14).
  4. Outil de la revendication 3, dans lequel les bandes de carbure ou les bandes d'alliage de la deuxième région sont substantiellement alignées avec l'axe longitudinal (22).
  5. Outil de la revendication 4, dans lequel chacune des bandes de carbure ou des bandes d'alliage dans la première région est continue avec l'une des bandes de carbure ou des bandes d'alliage respective dans la deuxième région.
  6. Outil de la revendication 3, dans lequel les bandes de carbure ou les bandes d'alliage dans la première région coupent la surface de travail (18, 44, 56, 74).
  7. Outil de la revendication 6, dans lequel les bandes de carbure ou les bandes d'alliage dans la première région coupent la surface de travail (18, 44, 56) à un angle non-perpendiculaire relatif à un plan de la surface de travail (18, 44, 56).
  8. Outil de la revendication 6, dans lequel la première région s'étend de la surface de travail (18, 44, 56) jusque dans la pointe (15, 42, 54, 74) à une profondeur relative à la surface de travail (18, 44, 56) d'environ 0,3175 centimètres (environ 0,125 pouces) à environ 0,635 centimètres (environ 0,25 pouces).
  9. Outil de la revendication 6, dans lequel la première région s'étend de la surface de travail (18, 44, 56) jusque dans la pointe à une profondeur relative à la surface de travail (18, 44, 56) d'au moins environ 0,00254 centimètres (environ 0,001 pouces).
  10. Outil de la revendication 3, dans lequel la première région est enfouie dans la pointe (15, 42, 54, 74) sous la surface de travail (18, 44, 56).
  11. Outil de la revendication 3, dans lequel la tige (14) comporte une structure de rétention d'outil configurée pour coupler le membre allongé avec un porteur d'outil de machine.
  12. Outil de la revendication 3, dans lequel l'axe longitudinal (22) coupe la surface de travail (18, 44, 56).
  13. Outil de la revendication 1, dans lequel des bandes de carbure adjacentes ou des bandes d'alliage adjacentes dans la première région sont espacées séparément par un espace interbande, et ledit espace interbande augmente le long d'une ligne radiale depuis la surface périphérique externe de l'outil (10, 43, 48) à un point médian radial entre la surface périphérique externe et l'axe longitudinal, et ensuite diminue du point médian radial au centre de l'outil (10, 43, 48).
  14. Outil de l'un quelconque des revendications précédentes, dans lequel l'acier à outils est formé à partir d'un matériel de poudre métallique.
  15. Procédé pour fabriquer un outil, ledit procédé comprenant :
    la fabrication d'une préforme d'acier à outils (30, 34, 38, 60, 70) ayant une tige et une pointe (32, 36, 40, 54, 62, 72) arrangé le long d'un axe longitudinal (22), l'acier à outils de la pointe (32, 36, 40, 54, 62, 72) ayant un microstructure avec une pluralité de bandes de carbure ou une pluralité de bandes d'alliage ayant une première densité ;
    le traitement thermomécanique de la pointe (32, 36, 40, 54, 62, 72) de la préforme (30, 34, 38, 60, 70) pour définir une première région dans la pointe (32, 36, 40, 54, 62, 72) de sorte que les bandes de carbure ou les bandes d'alliage dans la première région ne sont pas unidirectionnellement alignées et que chacune des bandes de carbure ou chacune des bandes d'alliage dans la première région a un angle d'inclinaison positif sur une première portion de la première région et un angle d'inclinaison négatif sur une deuxième portion de la première région, dans lequel la transition entre l'angle d'inclinaison positif et l'angle d'inclinaison négatif est continue et la distance entre les bandes de carbure ou les bandes d'alliage est réduite résultant en une deuxième densité plus élevé que la première densité, et dans lequel le traitement thermomécanique inclut le chauffage de la pointe (32, 36, 40, 54, 62, 72) à une température de traitement et, pendant que la pointe (32, 36, 40, 54, 62, 72) est à température de traitement, une force est exercée sur la pointe (32, 36, 40, 54, 62, 72) pour déformer la première région ;; et
    la transformation de la préforme en outil (10, 43, 48) avec la première région de la pointe définissant une surface de travail (18, 44, 56) de l'outil (10, 43, 48).
  16. Procédé de la revendication 15, dans lequel les bandes de carbure ou les bandes d'alliage, dans la première région sont comprimées plus étroitement ensemble qu'une autre pluralité de bandes de carbure ou qu'une autre pluralité de bandes d'alliage dans une deuxième région juxtaposée à la première région.
  17. Procédé de la revendication 15, dans lequel la fabrication de la préforme comprend en outre :
    la formation de la pointe (32, 36, 40, 54, 62, 72) avec un profil en coupe vu le long de l'axe longitudinal qui est plus petit en surface qu'un profil en coupe du corps.
  18. Procédé de la revendication 17, dans lequel le traitement thermomécanique de la pointe (32, 36, 40, 54, 62, 72) comprend en outre :
    l'augmentation de l'aire du profil en coupe de la pointe (32, 36, 40, 54, 62, 72) lorsque la pointe (32, 36, 40, 54, 62, 72) est traitée thermomécaniquement.
  19. Procédé de la revendication 17, dans lequel la pointe (32, 36, 40, 62, 72) a une forme tronconique ou de projectile avec un angle inclus, et le traitement thermomécanique de la pointe (32, 36, 40, 62, 72) comprend en outre :
    l'augmentation de l'angle du cône de la pointe (32, 36, 40, 62, 72) lorsque la pointe (32, 36, 40, 62, 72) est traité thermomécaniquement.
  20. Procédé de la revendication 15, dans lequel la pointe (32, 36, 40, 54, 62, 72) est traitée thermomécaniquement par un procédé de forgeage.
  21. Procédé de la revendication 20, dans lequel le procédé de forgeage est sélectionnée parmi un groupe qui consiste en du travail de forgeage radial, du roulage d'anneau, du travail de forge rotatif, de la retreinte, du thixoformage, de l'écrouissage, du refoulement à chaud/froid et des combinaisons de ceux-ci.
  22. Procédé de la revendication 15, dans lequel les bandes de carbure ou les bandes d'alliage dans la pointe (32, 36, 40, 54, 62, 72) de la préforme (30, 34, 38, 60, 70) sont alignées sensiblement avec l'axe longitudinal (22) de la pointe (32, 36, 40, 54, 62, 72) avant que la pointe (32, 36, 40, 54, 62, 72) ne soit traitée thermomécaniquement.
  23. Procédé de la revendication 15, dans lequel la transformation de la préforme (30, 34, 38, 60, 70) en l'outil (10, 43, 48) comprend en outre :
    la modification de la tige (14) pour inclure une structure de rétention d'outil.
  24. Procédé de la revendication 15, dans lequel le traitement thermomécanique de la pointe (62) de la préforme (60) comprend en outre :
    le traitement thermomécanique de la pointe (62) avec un premier processus thermomécanique pour définir la première région dans l'acier à outils ;
    la modification de la forme de la pointe (62) de la préforme (60) ; et
    le traitement thermomécaniquement la pointe (62) avec un deuxième processus thermomécanique pour désaligner encore plus une orientation des bandes de carbure ou des bandes d'alliage dans la première région relative à l'axe longitudinal de la pointe.
  25. Procédé de la revendication 24, dans lequel la modification de la pointe comprend en outre :
    l'usinage ou le forgeage la pointe (62) de la préforme (60).
  26. Procédé de la revendication 15, dans lequel la température de traitement est supérieure à la température inférieure de transformation de l'acier à outils.
EP08251055A 2007-03-23 2008-03-25 Outils dotés d'une région de travail thermo-mécaniquement modifiée et procédés pour la formation de tels outils Active EP1985390B1 (fr)

Priority Applications (3)

Application Number Priority Date Filing Date Title
SI200830276T SI1985390T1 (sl) 2007-03-23 2008-03-25 Orodja s termo-mehansko spremenjenim delovnim območjem in postopki oblikovanja takih orodij
PL08251055T PL1985390T3 (pl) 2007-03-23 2008-03-25 Narzędzia z termo-mechanicznie modyfikowanym obszarem roboczym i sposoby formowania takich narzędzi
EP20110165001 EP2359951A1 (fr) 2007-03-23 2008-03-25 Outils dotés d'une région de travail thermo-mécaniquement modifiée et procédés pour la formation de tels outils

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US89672907P 2007-03-23 2007-03-23
US12/047,532 US9132567B2 (en) 2007-03-23 2008-03-13 Tools with a thermo-mechanically modified working region and methods of forming such tools

Publications (2)

Publication Number Publication Date
EP1985390A1 EP1985390A1 (fr) 2008-10-29
EP1985390B1 true EP1985390B1 (fr) 2011-05-11

Family

ID=39743311

Family Applications (1)

Application Number Title Priority Date Filing Date
EP08251055A Active EP1985390B1 (fr) 2007-03-23 2008-03-25 Outils dotés d'une région de travail thermo-mécaniquement modifiée et procédés pour la formation de tels outils

Country Status (2)

Country Link
EP (1) EP1985390B1 (fr)
PL (1) PL1985390T3 (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8968495B2 (en) 2007-03-23 2015-03-03 Dayton Progress Corporation Methods of thermo-mechanically processing tool steel and tools made from thermo-mechanically processed tool steels
US9132567B2 (en) 2007-03-23 2015-09-15 Dayton Progress Corporation Tools with a thermo-mechanically modified working region and methods of forming such tools
WO2009102848A1 (fr) * 2008-02-15 2009-08-20 Dayton Progress Corporation Procédés de traitement thermomécanique d'acier à outils et outils faits en aciers à outils traités de façon thermomécanique

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB848594A (en) * 1958-06-19 1960-09-21 Charles Henry Clews Improvements in or relating to press tool punches
US3290936A (en) * 1962-09-05 1966-12-13 Metaltronics Inc Metal processing
AT304999B (de) * 1970-10-15 1973-02-12 Boehler & Co Ag Geb Verfahren zur Herstellung von geschmiedetem oder gewalztem Stabstahl aus ledeburitischen Werkzeugstählen
JPS56151125A (en) * 1980-04-25 1981-11-24 Miyagawa Kinzoku Kogyo Kk Blanking tool
US5136905A (en) * 1991-02-07 1992-08-11 Joyce I. Stack Device and method for forming a gasket hole
FR2695331B1 (fr) * 1992-09-08 1994-10-28 Jacques Ory Procédé et machine pour fabriquer une barre à trous torsadée trempée, en particulier pour la fabrication ultérieure de forets en acier rapide.

Also Published As

Publication number Publication date
EP1985390A1 (fr) 2008-10-29
PL1985390T3 (pl) 2011-09-30

Similar Documents

Publication Publication Date Title
US9132567B2 (en) Tools with a thermo-mechanically modified working region and methods of forming such tools
US9481023B2 (en) Methods of thermo-mechanically processing tool steel and tools made from thermo-mechanically processed tool steels
EP2090383B1 (fr) Procédés d'acier d'outil à traitement thermomécanique et outil fabriqué à partir d'aciers d'outils traités thermo-mécaniquement
DE19630115C2 (de) Verfahren zum Herstellen eines Kegelrades sowie kombinierte Pressenvorrichtung
US20150093592A1 (en) Integrated Die Trim And Method
Kasak et al. Powder-metallurgy tool steels
KR20070118198A (ko) 공구
US7297177B2 (en) Cold work steel
EP1985390B1 (fr) Outils dotés d'une région de travail thermo-mécaniquement modifiée et procédés pour la formation de tels outils
Pinnow et al. P/M tool steels
EP0227001B1 (fr) Procédé de fabrication d'outils
US20110247467A1 (en) Heavy-duty punch technology
EP3414072B1 (fr) Procédé et dispositif de fabrication de pièces en acier trempé
WO2021171759A1 (fr) Matrice de cisaillement et procédé de moulage à la presse
DE102023104087A1 (de) Verfahren zum Härten und Richten hochlegierter Werkzeugstähle
Van Tyne Forging of carbon and alloy steels
Carnes et al. TOOL STEEL SELECTION.
EP0430922A2 (fr) Matrice d'extrusion métallique et procédé de sa fabrication

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MT NL NO PL PT RO SE SI SK TR

AX Request for extension of the european patent

Extension state: AL BA MK RS

17P Request for examination filed

Effective date: 20090428

17Q First examination report despatched

Effective date: 20090604

AKX Designation fees paid

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MT NL NO PL PT RO SE SI SK TR

RIC1 Information provided on ipc code assigned before grant

Ipc: B22F 3/17 20060101ALI20100917BHEP

Ipc: B21J 5/08 20060101ALI20100917BHEP

Ipc: B21D 37/20 20060101ALI20100917BHEP

Ipc: C21D 9/18 20060101ALI20100917BHEP

Ipc: C21D 9/00 20060101ALI20100917BHEP

Ipc: C21D 7/13 20060101ALI20100917BHEP

Ipc: C21D 6/02 20060101ALI20100917BHEP

Ipc: B21K 5/20 20060101AFI20100917BHEP

Ipc: C22C 38/22 20060101ALI20100917BHEP

Ipc: C22C 38/24 20060101ALI20100917BHEP

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MT NL NO PL PT RO SE SI SK TR

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

REG Reference to a national code

Ref country code: CH

Ref legal event code: EP

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

REG Reference to a national code

Ref country code: CH

Ref legal event code: NV

Representative=s name: ING. MARCO ZARDI C/O M. ZARDI & CO. S.A.

REG Reference to a national code

Ref country code: DE

Ref legal event code: R096

Ref document number: 602008006795

Country of ref document: DE

Effective date: 20110622

REG Reference to a national code

Ref country code: PT

Ref legal event code: SC4A

Free format text: AVAILABILITY OF NATIONAL TRANSLATION

Effective date: 20110718

REG Reference to a national code

Ref country code: SE

Ref legal event code: TRGR

REG Reference to a national code

Ref country code: NL

Ref legal event code: T3

REG Reference to a national code

Ref country code: PL

Ref legal event code: T3

REG Reference to a national code

Ref country code: ES

Ref legal event code: FG2A

Ref document number: 2366163

Country of ref document: ES

Kind code of ref document: T3

Effective date: 20111017

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: NO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110811

Ref country code: HR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110608

Ref country code: LT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110511

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LV

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110511

Ref country code: BE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110511

Ref country code: CY

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110511

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110812

Ref country code: IS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110911

Ref country code: FI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110511

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: EE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110511

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: DK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110511

Ref country code: SK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110511

Ref country code: RO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110511

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

26N No opposition filed

Effective date: 20120214

REG Reference to a national code

Ref country code: DE

Ref legal event code: R097

Ref document number: 602008006795

Country of ref document: DE

Effective date: 20120214

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MC

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120331

REG Reference to a national code

Ref country code: IE

Ref legal event code: MM4A

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120325

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: BG

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110811

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110511

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: HR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20110511

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LU

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20120325

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: HU

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20080325

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 9

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 10

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: PL

Payment date: 20161220

Year of fee payment: 10

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: NL

Payment date: 20170309

Year of fee payment: 10

Ref country code: FR

Payment date: 20170222

Year of fee payment: 10

Ref country code: SE

Payment date: 20170307

Year of fee payment: 10

Ref country code: CH

Payment date: 20170124

Year of fee payment: 10

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: PT

Payment date: 20170224

Year of fee payment: 10

Ref country code: AT

Payment date: 20170223

Year of fee payment: 10

Ref country code: SI

Payment date: 20170320

Year of fee payment: 10

Ref country code: CZ

Payment date: 20170315

Year of fee payment: 10

Ref country code: GB

Payment date: 20170223

Year of fee payment: 10

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: ES

Payment date: 20170308

Year of fee payment: 10

Ref country code: TR

Payment date: 20170228

Year of fee payment: 10

Ref country code: IT

Payment date: 20170310

Year of fee payment: 10

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: PT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180925

Ref country code: SE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180326

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

REG Reference to a national code

Ref country code: NL

Ref legal event code: MM

Effective date: 20180401

REG Reference to a national code

Ref country code: AT

Ref legal event code: MM01

Ref document number: 508816

Country of ref document: AT

Kind code of ref document: T

Effective date: 20180325

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20180325

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: CZ

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180325

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: NL

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180401

REG Reference to a national code

Ref country code: SI

Ref legal event code: KO00

Effective date: 20181108

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: AT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180325

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180325

Ref country code: IT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180325

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180331

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180331

Ref country code: SI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180326

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180331

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: PL

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180325

REG Reference to a national code

Ref country code: ES

Ref legal event code: FD2A

Effective date: 20190911

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: ES

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180326

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: TR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20180325

P01 Opt-out of the competence of the unified patent court (upc) registered

Effective date: 20230531

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20240625

Year of fee payment: 17