EP1724022B1 - Stirring mill - Google Patents

Stirring mill Download PDF

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Publication number
EP1724022B1
EP1724022B1 EP05010815A EP05010815A EP1724022B1 EP 1724022 B1 EP1724022 B1 EP 1724022B1 EP 05010815 A EP05010815 A EP 05010815A EP 05010815 A EP05010815 A EP 05010815A EP 1724022 B1 EP1724022 B1 EP 1724022B1
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EP
European Patent Office
Prior art keywords
grinding
grinding chamber
mill according
agitator mill
chamber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Not-in-force
Application number
EP05010815A
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German (de)
French (fr)
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EP1724022A1 (en
Inventor
Norbert Dr.-Ing. Stehr
Philipp Schmitt
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Buehler AG
Original Assignee
Buehler AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to EP05010815A priority Critical patent/EP1724022B1/en
Application filed by Buehler AG filed Critical Buehler AG
Priority to AT05010815T priority patent/ATE361146T1/en
Priority to DE502005000670T priority patent/DE502005000670D1/en
Priority to ES05010815T priority patent/ES2285603T3/en
Priority to US11/171,319 priority patent/US7216822B2/en
Priority to JP2006138920A priority patent/JP5010853B2/en
Priority to KR1020060044818A priority patent/KR101245478B1/en
Priority to CNB2006100826375A priority patent/CN100544892C/en
Publication of EP1724022A1 publication Critical patent/EP1724022A1/en
Application granted granted Critical
Publication of EP1724022B1 publication Critical patent/EP1724022B1/en
Not-in-force legal-status Critical Current
Anticipated expiration legal-status Critical

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/16Mills in which a fixed container houses stirring means tumbling the charge
    • B02C17/166Mills in which a fixed container houses stirring means tumbling the charge of the annular gap type
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/16Mills in which a fixed container houses stirring means tumbling the charge
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/04Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with unperforated container
    • B02C17/08Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with unperforated container with containers performing a planetary movement

Definitions

  • the invention relates to a stirred mill according to the preamble of claim 1.
  • both the inner grinding chamber and the outer grinding chamber are smooth-walled without perforations and are free of stirring tools.
  • the gap width, ie the radial extent of the outer grinding chamber is significantly greater than that of the inner grinding chamber. This is intended to achieve that the grinding and dispersion of the flowable, slurried grind takes place predominantly by shear effects in such a way that the local stress intensity of the grind over the entire Mahlweg is substantially constant. Due to the smooth-walled configuration of the cylindrical boundary walls of the outer grinding chamber and the inner grinding chamber, a flow is generated in which the auxiliary grinding bodies are moved in layers relative to one another.
  • the shear gradient and thus the local stress intensity is constant in the outer grinding chamber on the one hand and in the inner grinding chamber on the other hand above the respective Mahlraumiere. Since the gap width of the inner grinding chamber is smaller than the gap width of the outer grinding chamber, the shear gradient in the outer grinding chamber and in the inner grinding chamber can be made the same size; it is then constant over virtually the entire grinding space. It has turned out to be problematical that, with a high grinding auxiliary body filling level, it is difficult to start up the agitator mill. Because of the problems with starting up the agitator mill, it is operated with a reduced grinding aid filling, which in turn leads to an unfavorably wide grinding stock particle size distribution.
  • the invention has for its object to design a stirred mill of the generic type so that the startup of the stirred mill easier and during operation a narrow grinding material particle size distribution is achieved.
  • the agitator mill can be operated with a high Mahltostage filling level, ie the Mahltostage filling need not be reduced. This in turn leads to a particularly intensive grinding while avoiding a grinding stock pass, since Mahlosterrorism be transported back in sufficient amount by the Mahlos stresses-return channels.
  • inventively desired effects are still particularly favorably influenced by the development according to claim 2, wherein the development according to claim 3 continues to be supportive.
  • the inner stator is provided in the region of the outflow channel according to claim 12 with a wear protection, which is particularly advantageous if the gap width of the outflow channel to the separating device, ie radially inwardly, not enlarged, so if the flow area is reduced with a corresponding acceleration of the Mahlgut Mahlosêt flow.
  • the agitator mill shown in Fig. 1 has in the usual way a stand 1, to which a cylindrical grinding container 2 can be attached.
  • an electric drive motor 3 is housed, which is provided with a V-belt pulley 4, of which via V-belt 5 with a drive shaft 6 rotatably connected V-belt pulley 7 is rotationally driven.
  • the grinding container 2 consists of a cylindrical inner wall 9 surrounding a grinding chamber 8, which is surrounded by a substantially cylindrical outer jacket 10.
  • the lower wall of the grinding chamber 8 is formed by an annular bottom plate 12, which is fastened to the grinding container 2 by means of screws 13.
  • the grinding container 2 has an upper annular flange 14, by means of which it is attached to the underside of a support housing 15 by means of screws 16 which is mounted on the stator 1 of the agitator mill.
  • the grinding chamber 8 is closed by means of a lid 17.
  • the support housing 15 has a central bearing and seal housing 18 which is arranged coaxially to the central longitudinal axis 19 of the grinding container 2. This bearing and seal housing 18 is penetrated by the likewise coaxial to the axis 19 extending drive shaft 6, to which a stirrer 20 is mounted. In the grinding chamber 8 adjacent region of the bearing and seal housing 18 opens a regrind supply line 21 a.
  • annular bottom plate 12 a projecting into the grinding chamber 8 approximately cup-shaped, cylindrical inner stator 22 is attached, consisting of a grinding chamber 8 bounding, coaxial to the axis 19, cylindrical outer shell 23 and a likewise coaxial to the axis 19, cylindrical inner shell 24 exists. They limit between a cooling space 25.
  • the cooling space 25 is connected to a cooling space 26 in the bottom plate 12, the cooling water via a cooling water supply port 27 is supplied, which is discharged via a cooling water discharge port 28.
  • the cooling space 11 of the grinding container 2 is supplied with cooling water via a cooling water supply pipe 29, which is discharged via a cooling water discharge pipe 30.
  • a Mahlgut Mahltosève-separating device 32 is arranged, which is connected to a regrind discharge line 33. Between the separator 32 and the drain line 33, a grinding stock hopper 34 is provided.
  • the drain line 33 is provided in the region of the bottom plate 12 with a mounting bracket 35, which is releasably connected by means of screws 36 with the bottom plate 12 and the fixedly connected to this inner stator 22.
  • the separating device 32 is sealed relative to the annular end portion 31 of the inner stator 22 by means of a seal 37 and can be pulled out after loosening the screws 36 together with the drain line 33 and the collecting hopper 34 from the inner stator 22 down.
  • the separating device 32 can thus be pulled out of the grinding chamber 8, without the Mahlospian located in this 38 must be removed from the grinding chamber 8, since the filling of the grinding chamber 8 with these Mahlos stressesn 38 with non-driven agitator 20 does not reach to the front part 31.
  • the agitator 20 is cup-shaped in its basic structure, ie it has a substantially annular cylindrical rotor 39.
  • the rotor 39 has a cylindrical inner wall 41, which has a cylindrical outer wall 40 and a coaxial with it and coaxial with the axis 19.
  • the outer wall 40 and the inner wall 41 are smooth-walled and as closed surfaces trained, so have no openings.
  • a cooling space 42 is formed between the outer wall 40 and the inner wall 41 of the rotor 39.
  • the agitator 20 is provided with a cover-like termination part 43, to whose bottom side facing the rotor 39, a closure plate 44 is attached.
  • the termination part 43 and the end plate 44 are attached to the drive shaft 6.
  • a Mahlospian-return module 45 is arranged between the rotor 39 and the end plate 44 of the agitator 20, a Mahlospian-return module 45 is arranged.
  • the rotor 39, the return module 45 and the end plate 44 are detachably connected together by tie rods 46.
  • an outer grinding chamber 8a is formed.
  • an inner grinding chamber 8b is limited.
  • this inner grinding chamber 8b protrude on the outer surface 23 of the inner stator 22 mounted, designed as a pin-shaped tools 49 surveys in which - as is apparent in particular from Fig. 4 - are arranged helically over the circumference and the length of the outer shell 23.
  • adjacent tools 49 in the circumferential direction of the inner stator 22 overlap one another in the direction of the central longitudinal axis 19 arranged so that in one revolution of the rotor 39 whose inner wall 41 is completely swept by the tools 49.
  • the grinding chamber 8 is thus divided into a cylindrical outer grinding chamber 8a on the one hand and a cylindrical annular grinding chamber 8b on the other hand, connected by a constantly widening from outside to inside deflection space 50 in the vicinity of the bottom plate 12 are.
  • the cylindrical separator 32 consists of a stack of annular disks 51, between each of which a separating gap 52 is left free, the width of which is generally smaller than the diameter of the smallest grinding auxiliary body 38 used; However, the width can also be greater, since the separation of the Mahlos stresses 38 takes place before reaching the separator 32.
  • the stack of annular discs 51 is the end side, ie at the end plate 44 facing side, completed by a closure plate 53.
  • the separator 32 is disposed within the return module 45.
  • the return channels 54 extend in the direction of the axis 19 almost over the full height of the return module 45, wherein its axial height e is greater than the axial height f of the separator 32.
  • Die Return channels 54 extend in this embodiment except via the separator 32 in the direction of the axis 19 still obliquely upward from the upper end of the inner grinding chamber 8b and inside to the separator 32 leading, so tapering in the direction of the end plate 44 towards frustoconical Outflow channel 59.
  • the return channels 54 are also open to the outflow channel 59, as Fig. 2 reveals.
  • the outflow channel 59 is therefore not spatially limited upwards. Rather, it is open in the direction of the central longitudinal axis 19 towards the internal grinding chamber 8b and thus permeable to the exit of the grinding auxiliary bodies 38, while the millbase flows through the outflow channel 59 in the direction of the separating device 32.
  • the material to be ground flows through the grinding chamber 8 corresponding to the flow direction arrows 60 coming from the grinding material supply line 21 through a Mahlgut feed chamber 61 between the end portion 43 of the agitator 20 on the one hand and the lid 17 and the adjacent region of the inner wall 9 on the other hand, the grinding material feed Area 57, the outer grinding chamber 8a down, by the steadily widening deflection space 50 radially inwardly and from there through the inner grinding chamber 8b after on the way up to the outflow channel 59 and from there to the separator 32.
  • the material to be ground is milled in rotationally driven agitator 20 in cooperation with the auxiliary grinding bodies 38.
  • the ground material leaves the interior grinding chamber 8 b through the separating device 32, from where it flows through the grinding stock discharge line 33.
  • FIGS. 6 and 7 differs from that of FIGS. 2 to 5 essentially in that between the end plate 44 and the rotor 39 except a Mahltospian feedback module 45 'still a jam device 62 is provided as part of the agitator 20'.
  • a jam device 62 is provided as part of the agitator 20'.
  • the inner grinding chamber 8b does not open at its upper end directly into the return channels 54 ', but instead feeds the grinding material.
  • Mahltosêt mixture is forced by the jam device 62 obliquely upwards and inwards in the direction of the separator 32 '.
  • the gap width j of the outflow channel 59 ' is constant.
  • the separating device 32 'does not extend over the full area above the end portion 31. Rather, a closed ring portion as wear protection 63 is provided between the end portion 31 and the separator 32', which is formed integrally with the separator 32 '. Before him or on him the outflow channel ends 59 ', so that from the outflow channel 59' exiting and deflected in an axis-parallel motion Mahltosève 38, the separator 32 'do not hit.
  • the embodiment according to FIG. 8 differs from that according to FIGS. 6 and 7 only in that the grinding aid return channels 54 "have a minimum required height e" for trouble-free operation at low grinding stock throughputs. Otherwise, the Mahlosterrorism feedback module 45 "includes here to the jam means 62, wherein in this embodiment, as in the two aforementioned embodiments, the return channels 54" are bounded on their upper side by the end plate 44. The axial height k is the same in the return modules 45 'and 45 ".
  • FIG. 9 corresponds to that of FIG. 6 with the difference that no wear protection 63 is provided and that on the other hand the outflow channels 59 '' extend towards the grinding aid separator 32, ie the gap width j '' of the outflow channel 59 '' increases inwards to such an extent that the total cross-sectional area of this channel 59 '' In any case, it does not become smaller in the direction of the separating device 32 so that there is no acceleration of the grinding stock auxiliary body flow in the outflow channel 59 '' to the separating device 32. For this reason, the separating device 32 can extend to the front part 31, since the auxiliary grinding bodies 38 do not hit the separator 32.
  • FIG. 10 substantially corresponds to that of FIG. 9, wherein the Mahlosève feedback module 45 "" is not brought up to the separator 32.
  • the inlet openings 55 “" of the grinding auxiliary body return channels 54 “” thus have a clear radial distance from the separating device 32.
  • this annular space 64 a plurality of scrapers 65 are provided, which are attached to the end plate 44 and rotate with the agitator 20 "".
  • the exemplary embodiment according to FIGS. 11 to 13 has a grinding aid body return module 45 ""'which bears against an intermediate ring 66 toward the accumulation device 62.
  • the module 45 “"' is thus down to the grinding chamber 8, ie to an end face 67, open.
  • the axial height e ""' is constant from the respective inlet opening 55 ""' to the outlet opening 56 ""'and is significantly smaller than the height f' of the separating device 32 '.

Abstract

The radial gap width (g) of the outer grinding chamber (8a) is less than the gap width (h) of the inner grinding chamber (8b). The cross sectional surface area (Fa) of the outer grinding chamber is no greater than that (Fb) of the inner grinding chamber. Preferably Fb lies between 1.2 times Fa and 7 times Fa. The gap width of the outer grinding chamber is related to the diameter (i) of the largest grinding aid solids (38), which is preferably up to 1.5 mm. The gap width of the outer grinding chamber is preferably up to 5.0 mm.

Description

Die Erfindung betrifft eine Rührwerksmühle nach dem Oberbegriff des Anspruches 1.The invention relates to a stirred mill according to the preamble of claim 1.

Bei einer derartigen aus der EP 0 824 964 B1 (entsprechend US-PS 5,950,943) bekannten Rührwerksmühle ist sowohl der Innen-Mahlraum als auch der Außen-Mahlraum glattwandig ohne Durchbrechungen und frei von Rührwerkzeugen ausgebildet. Die Spaltweite, d. h. die radiale Erstreckung des Außen-Mahlraums ist deutlich größer als die des Innen-Mahlraums. Hierdurch soll erreicht werden, dass das Mahlen und Dispergieren des fließfähigen, aufgeschlämmten Mahlguts überwiegend durch Schereffekte in der Weise erfolgt, dass die örtliche Beanspruchungsintensität des Mahlguts über den gesamten Mahlweg im Wesentlichen konstant ist. Durch die glattwandige Ausgestaltung der zylindrischen Begrenzungswände von Außen-Mahlraum und Innen-Mahlraum wird eine Strömung erzeugt, in der die Mahlhilfskörper in Schichten relativ zueinander bewegt werden. Der Schergradient und damit die örtliche Beanspruchungsintensität ist im Außen-Mahlraum einerseits und im Innen-Mahlraum andererseits über der jeweiligen Mahlraumhöhe konstant. Da die Spaltweite des Innen-Mahlraums kleiner ist als die Spaltweite des Außen-Mahlraums, kann der Schergradient im Außen-Mahlraum und im Innen-Mahlraum gleich groß gemacht werden; er ist dann über praktisch den gesamten Mahlraum konstant. Als problematisch hat sich herausgestellt, dass bei hohem Mahlhilfskörper-Füllgrad das Anfahren der Rührwerksmühle schwierig ist. Wegen der Probleme beim Anfahren der Rührwerksmühle wird diese mit einer reduzierten Mahlhilfskörper-Füllung betrieben, was wiederum zu einer ungünstig breiten Mahlgut-Partikelgrößen-Verteilung führt. Da durch diese Reduktion der Mahlhilfskörper die Menge der durch die Mahlhilfskörper-Rückführ-Kanäle rücktransportierten Mahlhilfskörper verringert wird, wird die Gefahr vergrößert, dass ein sogenannter Mahlgut-Durchschuss stattfindet, d. h. dem Mahlgut-Zuführraum zugeführtes zu mahlendes bzw. dispergierendes Mahlgut kann im Kurzschluss durch die Mahlhilfskörper-Rückführ-Kanäle in Richtung zur Trenneinrichtung strömen.In such an agitating mill known from EP 0 824 964 B1 (corresponding to US Pat. No. 5,950,943), both the inner grinding chamber and the outer grinding chamber are smooth-walled without perforations and are free of stirring tools. The gap width, ie the radial extent of the outer grinding chamber is significantly greater than that of the inner grinding chamber. This is intended to achieve that the grinding and dispersion of the flowable, slurried grind takes place predominantly by shear effects in such a way that the local stress intensity of the grind over the entire Mahlweg is substantially constant. Due to the smooth-walled configuration of the cylindrical boundary walls of the outer grinding chamber and the inner grinding chamber, a flow is generated in which the auxiliary grinding bodies are moved in layers relative to one another. The shear gradient and thus the local stress intensity is constant in the outer grinding chamber on the one hand and in the inner grinding chamber on the other hand above the respective Mahlraumhöhe. Since the gap width of the inner grinding chamber is smaller than the gap width of the outer grinding chamber, the shear gradient in the outer grinding chamber and in the inner grinding chamber can be made the same size; it is then constant over virtually the entire grinding space. It has turned out to be problematical that, with a high grinding auxiliary body filling level, it is difficult to start up the agitator mill. Because of the problems with starting up the agitator mill, it is operated with a reduced grinding aid filling, which in turn leads to an unfavorably wide grinding stock particle size distribution. Because of this reduction of Mahlhilfskörper the amount of through the Mahlhilfskörper-return channels is reduced back, the risk increases that a so-called Mahlgut-shot takes place, ie the Mahlgut feed chamber supplied to be ground or dispersing regrind can flow in the short circuit through the Mahlhilfskörper-return channels in the direction of the separator.

Der Erfindung liegt die Aufgabe zugrunde, eine Rührwerksmühle der gattungsgemäßen Art so auszugestalten, dass das Anfahren der Rührwerksmühle erleichtert und während des Betriebes eine enge Mahlgut-Partikelgrößen-Verteilung erreicht wird.The invention has for its object to design a stirred mill of the generic type so that the startup of the stirred mill easier and during operation a narrow grinding material particle size distribution is achieved.

Diese Aufgabe wird erfindungsgemäß durch die Merkmale im Kennzeichnungsteil des Anspruches 1 gelöst. Durch die erfindungsgemäßen Maßnahmen wird erreicht, dass beim Abschalten der Rührwerksmühle insbesondere im Innen-Mahlraum kein Verkeilen der sich nach unten absetzenden Mahlhilfskörper mit den benachbarten Wänden stattfindet. Beim Anfahren der Rührwerksmühle können die Mahlhilfskörper also sehr leicht wieder in Bewegung versetzt werden. Durch die erfindungsgemäßen Maßnahmen wird weiterhin erreicht, dass ein Stau der Mahlhilfskörper im Außen-Mahlraum vor dem Innen-Mahlraum nicht auftritt, da die Spaltweite des Innen-Mahlraums größer ist als die des Außen-Mahlraums. Im Außen-Mahlraum findet eine Schermahlung statt. Da die Mahlhilfskörper das Bestreben haben, einer erhöhten Scherung zu entweichen, fließen sie durch den sich zum Innen-Mahlraum erweiternden Umlenkraum in den Innen-Mahlraum. Aufgrund der geschilderten Effekte kann die Rührwerksmühle mit einem hohen Mahlhilfskörper-Füllgrad betrieben werden, d. h. die Mahlhilfskörper-Füllung muss nicht reduziert werden. Dies führt wiederum zu einer besonders intensiven Mahlung unter gleichzeitiger Vermeidung eines Mahlgut-Durchschusses, da Mahlhilfskörper in ausreichender Menge durch die Mahlhilfskörper-Rückführ-Kanäle rücktransportiert werden.This object is achieved by the features in the characterizing part of claim 1. As a result of the measures according to the invention, when the agitator mill is switched off, in particular in the internal grinding space, there is no wedging of the downwardly settling grinding auxiliary bodies with the adjacent walls. When starting the agitator mill Mahlhilfskörper can therefore be very easily set in motion again. The inventive measures is further achieved that a jam Mahlhilfskörper does not occur in the outer grinding chamber in front of the inner grinding chamber, since the gap width of the inner grinding chamber is greater than that of the outer grinding chamber. In the outer grinding chamber, a shear grinding takes place. Since the Mahlhilfskörper strive to escape an increased shear, they flow through the expanding to the inner grinding chamber deflection into the inner grinding chamber. Due to the described effects, the agitator mill can be operated with a high Mahlhilfskörper filling level, ie the Mahlhilfskörper filling need not be reduced. This in turn leads to a particularly intensive grinding while avoiding a grinding stock pass, since Mahlhilfskörper be transported back in sufficient amount by the Mahlhilfskörper-return channels.

Die erfindungsgemäß angestrebten Effekte werden durch die Weiterbildung nach Anspruch 2 noch besonders günstig beeinflusst, wobei die Weiterbildung nach Anspruch 3 weiterhin unterstützend wirkt.The inventively desired effects are still particularly favorably influenced by the development according to claim 2, wherein the development according to claim 3 continues to be supportive.

Dieser Effekt der Auflockerung des Mahlguts im Innen-Mahlraum und damit eine Erleichterung des Durchflusses des Mahlgut-Mahlhilfskörper-Gemisches, wird durch die mindestens am Innen-Stator gemäß Anspruch 4 angebrachten Erhebungen unterstützt, die gemäß Anspruch 5 als Werkzeuge ausgebildet sein können. Durch die zumindest am Innen-Stator angebrachten Erhebungen bzw. Werkzeuge erfolgt eine intensive Verwirbelung der Mahlhilfskörper und damit wiederum eine intensive Beanspruchung des Mahlgutes. Durch diese intensive Durchwirbelung wird auch der Bildung einer ruhenden Grenzschicht an den Mahlraum-Begrenzungswänden entgegengewirkt, sodass eine verbesserte Kühlung des Mahlgutes erfolgt.This effect of loosening the ground material in the internal grinding chamber and thus facilitating the flow of Mahlgut Mahlhilfskörper mixture is supported by the mounted at least on the inner stator according to claim 4 surveys, which may be formed according to claim 5 as tools. By at least the inner stator mounted elevations or tools takes place an intensive turbulence of Mahlhilfskörper and thus again an intensive use of the ground material. This intensive turbulence also counteracts the formation of a stationary boundary layer on the grinding chamber boundary walls, so that improved cooling of the ground material takes place.

Durch die Weiterbildung nach den Ansprüchen 6 und 7 wird verhindert, dass sich an der Innenwand des Rotors Mahlhilfskörper ablagern; durch die schraubenlinienförmige Anordnung der Werkzeuge an dem Außenmantel des Innen-Stators wird die Innenwand des Rotors vollständig überstrichen und damit von solchen Ablagerungen freigehalten.Through the development according to claims 6 and 7 it is prevented that deposit on the inner wall of the rotor Mahlhilfskörper; due to the helical arrangement of the tools on the outer jacket of the inner stator, the inner wall of the rotor is completely swept over and thus kept free of such deposits.

Durch die Weiterbildung nach Anspruch 8 kann erreicht werden, dass eine gewisse Rückstauwirkung auf den Innen-Mahlraum ausgeübt wird, sodass die Dispergier- und die Mahl-Intensität erhöht wird. Dieser Effekt kann insbesondere durch eine Weiterbildung nach Anspruch 9 erreicht werden. Durch eine solche Stau-Einrichtung kann eine örtliche Erhöhung der Mahlhilfskörper-Konzentration im oberen Endbereich des Innen-Mahlraums erreicht werden, was wiederum zu einer besonders intensiven Mahlung bzw. Dispergierung und dadurch zu einer sehr engen Mahlgut-Partikelgrößen-Verteilung führt. Eine solche gesondert eingebaute Stau-Einrichtung kann nach Anspruch 10 als gesondertes Bauteil jedem konkreten Anwendungsfall angepasst werden. Hierbei kann die Spaltweite des Abström-Kanals in Richtung zur Trenneinrichtung konstant sein, oder aber gemäß Anspruch 11 zunehmen.By the development according to claim 8 can be achieved that a certain backpressure effect is exerted on the internal grinding chamber, so that the dispersing and the grinding intensity is increased. This effect can be achieved in particular by a development according to claim 9. By such a congestion device, a local increase in Mahlhilfskörper concentration be achieved in the upper end of the inner grinding chamber, which in turn leads to a particularly intensive grinding or dispersion and thereby to a very narrow Mahlgut particle size distribution. Such a separately installed storage device can be adapted according to claim 10 as a separate component of each specific application. In this case, the gap width of the outflow channel can be constant in the direction of the separating device, or else increase in accordance with claim 11.

Grundsätzlich ist es besonders vorteilhaft, wenn der Innen-Stator im Bereich des Abström-Kanals nach Anspruch 12 mit einem Verschleiß-Schutz versehen ist, der insbesondere von Vorteil ist, wenn die Spaltweite des Abström-Kanals sich zur Trenneinrichtung, also radial nach innen, nicht vergrößert, wenn also der Durchströmquerschnitt verringert wird mit einer entsprechenden Beschleunigung der Mahlgut-Mahlhilfskörper-Strömung.In principle, it is particularly advantageous if the inner stator is provided in the region of the outflow channel according to claim 12 with a wear protection, which is particularly advantageous if the gap width of the outflow channel to the separating device, ie radially inwardly, not enlarged, so if the flow area is reduced with a corresponding acceleration of the Mahlgut Mahlhilfskörper flow.

Durch die Weiterbildung nach Anspruch 13 und insbesondere Anspruch 14 wird es ermöglicht, die Größe der Mahlhilfskörper-Rückführ-Kanäle auch in einfacher Weise den Mahl- bzw. Dispergier-Zielen anzupassen. Durch die Ausbildung dieser Rückführ-Kanäle in einem Mahlhilfskörper-Rückführ-Modul können sie von einer Seite in das Modul eingearbeitet werden, was fertigungstechnisch besonders einfach ist. Diese Ausgestaltung ermöglicht es auch, den Mahlhilfskörper-Rückführ-Kanälen mit einfachen Fertigungsmaßnahmen beliebige gewünschte Konturen zu geben. Diese einfache Fertigung ermöglicht auch eine Optimierung der Durchströmquerschnitte der Mahlhilfskörper-Rückführ-Kanäle in ihrem Verlauf von innen nach außen, wobei Anspruch 15 optimale Bereiche für das Verhältnis der Weiten der Eintrittsöffnungen und Austrittsöffnungen zueinander angibt.The development according to claim 13 and in particular claim 14, it is possible to adjust the size of Mahlhilfskörper-return channels also in a simple way the grinding or dispersing goals. By forming these return channels in a Mahlhilfskörper-return module they can be incorporated from one side into the module, which is particularly easy to manufacture. This configuration also makes it possible to give the Mahlhilfskörper-return channels with simple manufacturing measures any desired contours. This simple production also makes it possible to optimize the flow cross sections of the grinding aid body return channels in their course from the inside to the outside, whereby claim 15 specifies optimal ranges for the ratio of the widths of the inlet openings and outlet openings to one another.

Dadurch, dass die Höhe der Mahlhilfskörper-Rückführ-Kanäle in Richtung der Mittel-Längs-Achse verhältnismäßig klein gemacht werden kann, kann weiterhin die Gefahr eines Durchschusses der Mahlhilfskörper reduziert werden, ohne dass eine gute Abtrennung der Mahlhilfskörper vom Mahlgut beeinträchtigt wird. Anspruch 16 gibt hierzu optimale Randbedingungen an. Derartige optimale Bedingungen werden weiterhin durch die Ausgestaltung nach den Ansprüchen 17 und 18 verbessert.The fact that the height of the Mahlhilfskörper-return channels in the direction of the central longitudinal axis can be made relatively small, the risk of a passage through the Mahlhilfskörper can continue to be reduced without a good separation of Mahlhilfskörper is affected by the ground material. Claim 16 specifies optimum boundary conditions for this purpose. Such optimal conditions are further improved by the embodiment according to claims 17 and 18.

Weitere Merkmale und Vorteile der Erfindung ergeben sich aus der nachfolgenden Beschreibung von Ausführungsbeispielen anhand der Zeichnung. Es zeigt

Fig. 1
eine schematische Darstellung einer Rührwerksmühle in einer Seitenansicht,
Fig. 2
einen Längsschnitt durch ein erstes Ausführungsbeispiel eines Mahlbehälters der Rührwerksmühle,
Fig. 3
einen Querschnitt durch den Mahlbehälter gemäß der Schnittlinie III-III in Fig. 2,
Fig. 4
eine Seiten-Längs-Ansicht eines Innen-Stators der Rührwerksmühle,
Fig. 5
eine perspektivische Ansicht eines Mahlhilfskörper-Rückführ-Moduls der Rührwerksmühle nach den Fig. 2 bis 4,
Fig. 6
einen Längsschnitt durch ein zweites Ausführungsbeispiel eines Mahlbehälters der Rührwerksmühle,
Fig. 7
eine perspektivische Ansicht des Mahlhilfskörper-Rückführ-Moduls der Rührwerksmühle nach Fig. 6,
Fig. 8
einen Längsschnitt durch ein drittes Ausführungsbeispiel eines Mahlbehälters der Rührwerksmühle,
Fig. 9
einen Längsschnitt durch ein viertes Ausführungsbeispiel eines Mahlbehälters der Rührwerksmühle,
Fig. 10
einen Längsschnitt durch ein fünftes Ausführungsbeispiel eines Mahlbehälters der Rührwerksmühle,
Fig. 11
einen Längsschnitt durch ein sechstes Ausführungsbeispiel eines Mahlbehälters der Rührwerksmühle,
Fig. 12
eine Seitenansicht eines Mahlhilfskörper-Rückführ-Moduls der Rührwerksmühle nach Fig. 11, und
Fig. 13
eine Ansicht des Mahlhilfskörper-Rückführ-Moduls nach Fig. 12 von unten.
Further features and advantages of the invention will become apparent from the following description of exemplary embodiments with reference to the drawing. It shows
Fig. 1
a schematic representation of a stirred mill in a side view,
Fig. 2
a longitudinal section through a first embodiment of a grinding container of the agitator mill,
Fig. 3
a cross section through the grinding container according to the section line III-III in Fig. 2,
Fig. 4
a side longitudinal view of an internal stator of the agitator mill,
Fig. 5
3 is a perspective view of a grinding aid return module of the agitator mill according to FIGS. 2 to 4,
Fig. 6
a longitudinal section through a second embodiment of a grinding container of the agitator mill,
Fig. 7
6 is a perspective view of the grinding aid return module of the agitator mill of FIG. 6, FIG.
Fig. 8
a longitudinal section through a third embodiment of a grinding container of the agitator mill,
Fig. 9
a longitudinal section through a fourth embodiment of a grinding container of the agitator mill,
Fig. 10
a longitudinal section through a fifth embodiment of a grinding container of the agitator mill,
Fig. 11
a longitudinal section through a sixth embodiment of a grinding container of the agitator mill,
Fig. 12
a side view of Mahlhilfskörper-return module of the agitator mill of FIG. 11, and
Fig. 13
a view of the Mahlhilfskörper feedback module of FIG. 12 from below.

Die in Fig. 1 dargestellte Rührwerksmühle weist in üblicher Weise einen Ständer 1 auf, an dem ein zylindrischer Mahlbehälter 2 anbringbar ist. In dem Ständer 1 ist ein elektrischer Antriebsmotor 3 untergebracht, der mit einer Keilriemenscheibe 4 versehen ist, von der über Keilriemen 5 eine mit einer Antriebs-Welle 6 drehfest verbundene Keilriemenscheibe 7 drehend antreibbar ist.The agitator mill shown in Fig. 1 has in the usual way a stand 1, to which a cylindrical grinding container 2 can be attached. In the stator 1, an electric drive motor 3 is housed, which is provided with a V-belt pulley 4, of which via V-belt 5 with a drive shaft 6 rotatably connected V-belt pulley 7 is rotationally driven.

Wie insbesondere aus Fig. 2 und 3 hervorgeht, besteht der Mahlbehälter 2 aus einer zylindrischen, einen Mahlraum 8 umgebenden Innenwand 9, die von einem im Wesentlichen zylindrischen Außenmantel 10 umgeben ist. Die Innenwand 9 und der Außenmantel 10 begrenzen zwischen sich einen Kühlraum 11. Der untere Abschluss des Mahlraumes 8 ist durch eine kreisringförmige Bodenplatte 12 gebildet, die am Mahlbehälter 2 mittels Schrauben 13 befestigt ist.As is apparent in particular from FIGS. 2 and 3, the grinding container 2 consists of a cylindrical inner wall 9 surrounding a grinding chamber 8, which is surrounded by a substantially cylindrical outer jacket 10. The lower wall of the grinding chamber 8 is formed by an annular bottom plate 12, which is fastened to the grinding container 2 by means of screws 13.

Der Mahlbehälter 2 weist einen oberen Ringflansch 14 auf, mittels dessen er an der Unterseite eines Traggehäuses 15 mittels Schrauben 16 befestigt ist, das am Ständer 1 der Rührwerksmühle angebracht ist. Der Mahlraum 8 ist mittels eines Deckels 17 verschlossen. Das Traggehäuse 15 weist ein mittleres Lager- und Dichtungsgehäuse 18 auf, das koaxial zur Mittel-Längs-Achse 19 des Mahlbehälters 2 angeordnet ist. Dieses Lager- und Dichtungsgehäuse 18 wird von der ebenfalls koaxial zur Achse 19 verlaufenden Antriebs-Welle 6 durchsetzt, an der ein Rührwerk 20 angebracht ist. In den dem Mahlraum 8 benachbarten Bereich des Lager- und Dichtungsgehäuses 18 mündet eine Mahlgut-Zuführleitung 21 ein.The grinding container 2 has an upper annular flange 14, by means of which it is attached to the underside of a support housing 15 by means of screws 16 which is mounted on the stator 1 of the agitator mill. The grinding chamber 8 is closed by means of a lid 17. The support housing 15 has a central bearing and seal housing 18 which is arranged coaxially to the central longitudinal axis 19 of the grinding container 2. This bearing and seal housing 18 is penetrated by the likewise coaxial to the axis 19 extending drive shaft 6, to which a stirrer 20 is mounted. In the grinding chamber 8 adjacent region of the bearing and seal housing 18 opens a regrind supply line 21 a.

An der kreisringförmigen Bodenplatte 12 ist ein in den Mahlraum 8 hineinragender, etwa topfförmig ausgebildeter, zylindrischer Innen-Stator 22 befestigt, der aus einem den Mahlraum 8 begrenzenden, zur Achse 19 koaxialen, zylindrischen Außenmantel 23 und einem ebenfalls zur Achse 19 koaxialen, zylindrischen Innenmantel 24 besteht. Sie begrenzen zwischen sich einen Kühlraum 25. Der Kühlraum 25 ist mit einem Kühlraum 26 in der Bodenplatte 12 verbunden, dem Kühlwasser über einen Kühlwasser-Zuführanschluss 27 zugeführt wird, das über einen Kühlwasser-Abführanschluss 28 abgeführt wird. Dem Kühlraum 11 des Mahlbehälters 2 wird Kühlwasser über einen Kühlwasser-Zuführstutzen 29 zugeführt, das über einen Kühlwasser-Abführstutzen 30 abgeführt wird.On the annular bottom plate 12 a projecting into the grinding chamber 8, approximately cup-shaped, cylindrical inner stator 22 is attached, consisting of a grinding chamber 8 bounding, coaxial to the axis 19, cylindrical outer shell 23 and a likewise coaxial to the axis 19, cylindrical inner shell 24 exists. They limit between a cooling space 25. The cooling space 25 is connected to a cooling space 26 in the bottom plate 12, the cooling water via a cooling water supply port 27 is supplied, which is discharged via a cooling water discharge port 28. The cooling space 11 of the grinding container 2 is supplied with cooling water via a cooling water supply pipe 29, which is discharged via a cooling water discharge pipe 30.

An dem oberen, oberhalb des Mahlraums 8 befindlichen ringförmigen Stimteil 31 des Innen-Stators 22 ist eine Mahlgut-Mahlhilfskörper-Trenneinrichtung 32 angeordnet, die mit einer Mahlgut-Ablaufleitung 33 verbunden ist. Zwischen der Trenneinrichtung 32 und der Ablaufleitung 33 ist ein Mahlgut-Sammeltrichter 34 vorgesehen. Die Ablaufleitung 33 ist im Bereich der Bodenplatte 12 mit einem Haltebügel 35 versehen, der mittels Schrauben 36 mit der Bodenplatte 12 bzw. dem fest mit dieser verbundenen Innen-Stator 22 lösbar verbunden ist. Die Trenneinrichtung 32 ist gegenüber dem ringförmigen Stimteil 31 des Innen-Stators 22 mittels einer Dichtung 37 abgedichtet und kann nach Lösen der Schrauben 36 zusammen mit der Ablaufleitung 33 und dem Sammeltrichter 34 aus dem Innen-Stator 22 nach unten herausgezogen werden. Die Trenneinrichtung 32 kann also aus dem Mahlraum 8 herausgezogen werden, ohne dass die in diesem befindlichen Mahlhilfskörper 38 aus dem Mahlraum 8 entfernt werden müssen, da die Füllung des Mahlraums 8 mit diesen Mahlhilfskörpern 38 bei nicht angetriebenem Rührwerk 20 nicht bis zum Stirnteil 31 reicht.At the upper, located above the grinding chamber 8 annular end portion 31 of the inner stator 22, a Mahlgut Mahlhilfskörper-separating device 32 is arranged, which is connected to a regrind discharge line 33. Between the separator 32 and the drain line 33, a grinding stock hopper 34 is provided. The drain line 33 is provided in the region of the bottom plate 12 with a mounting bracket 35, which is releasably connected by means of screws 36 with the bottom plate 12 and the fixedly connected to this inner stator 22. The separating device 32 is sealed relative to the annular end portion 31 of the inner stator 22 by means of a seal 37 and can be pulled out after loosening the screws 36 together with the drain line 33 and the collecting hopper 34 from the inner stator 22 down. The separating device 32 can thus be pulled out of the grinding chamber 8, without the Mahlhilfskörper located in this 38 must be removed from the grinding chamber 8, since the filling of the grinding chamber 8 with these Mahlhilfskörpern 38 with non-driven agitator 20 does not reach to the front part 31.

Das Rührwerk 20 ist in seinem Grundaufbau topfförmig, d. h. es weist einen im Wesentlichen ringzylindrischen Rotor 39 auf. Der Rotor 39 weist eine eine zylindrische Außenwand 40 und eine koaxial hierzu und koaxial zur Achse 19 angeordnete zylindrische Innenwand 41 auf. Die Außenwand 40 und die Innenwand 41 sind glattwandig und als geschlossene Flächen ausgebildet, weisen also keine Durchbrechungen auf. Zwischen der Außenwand 40 und der Innenwand 41 des Rotors 39 ist ein Kühlraum 42 ausgebildet.The agitator 20 is cup-shaped in its basic structure, ie it has a substantially annular cylindrical rotor 39. The rotor 39 has a cylindrical inner wall 41, which has a cylindrical outer wall 40 and a coaxial with it and coaxial with the axis 19. The outer wall 40 and the inner wall 41 are smooth-walled and as closed surfaces trained, so have no openings. Between the outer wall 40 and the inner wall 41 of the rotor 39, a cooling space 42 is formed.

An seinem oberen Ende ist das Rührwerk 20 mit einem deckelartigen Abschlussteil 43 versehen, an dessen dem Rotor 39 zugewandten Unterseite eine Abschlussplatte 44 befestigt ist. Das Abschlussteil 43 und die Abschlussplatte 44 sind an der Antriebs-Welle 6 angebracht.At its upper end, the agitator 20 is provided with a cover-like termination part 43, to whose bottom side facing the rotor 39, a closure plate 44 is attached. The termination part 43 and the end plate 44 are attached to the drive shaft 6.

Zwischen dem Rotor 39 und der Abschlussplatte 44 des Rührwerks 20 ist ein Mahlhilfskörper-Rückführ-Modul 45 angeordnet. Der Rotor 39, das Rückführ-Modul 45 und die Abschlussplatte 44 sind mittels Zugankern 46 lösbar miteinander verbunden. Die Zu- und Abfuhr von Kühlwasser zum Kühlraum 42 erfolgt über in der Welle 6 und im Rückführ-Modul 45 ausgebildete Kühlwasserkanäle 47, 48.Between the rotor 39 and the end plate 44 of the agitator 20, a Mahlhilfskörper-return module 45 is arranged. The rotor 39, the return module 45 and the end plate 44 are detachably connected together by tie rods 46. The supply and removal of cooling water to the cooling chamber 42 via formed in the shaft 6 and in the return module 45 cooling water channels 47, 48th

Durch die glattwandige Ausgestaltung der Innenwand 9 des Mahlbehälters 2, die also keine Werkzeuge aufweist, und die ebenfalls glattwandige Ausgestaltung der Außenwand 40 des Rotors 39 wird ein Außen-Mahlraum 8a gebildet. Durch die ebenfalls werkzeugfreie glattwandige Ausgestaltung der Innenwand 41 des Rotors 39 und den Außenmantel 23 des Innen-Stators 22 wird ein Innen-Mahlraum 8b begrenzt. In diesen Innen-Mahlraum 8b ragen am Außenmantel 23 des Innen-Stators 22 angebrachte, als stiftförmige Werkzeuge 49 ausgebildete Erhebungen hinein, die - wie insbesondere aus Fig. 4 hervorgeht - schraubenlinienförmig über den Umfang und die Länge des Außenmantels 23 angeordnet sind. Wie sich insbesondere aus Fig. 4 ergibt, sind in Umfangsrichtung des Innen-Stators 22 benachbarte Werkzeuge 49 einander in Richtung der Mittel-Längs-Achse 19 überlappend angeordnet, sodass bei einer Umdrehung des Rotors 39 dessen Innenwand 41 vollständig von den Werkzeugen 49 überstrichen wird.Due to the smooth-walled configuration of the inner wall 9 of the grinding container 2, which thus has no tools, and the likewise smooth-walled configuration of the outer wall 40 of the rotor 39, an outer grinding chamber 8a is formed. By the likewise tool-free smooth-walled configuration of the inner wall 41 of the rotor 39 and the outer jacket 23 of the inner stator 22, an inner grinding chamber 8b is limited. In this inner grinding chamber 8b protrude on the outer surface 23 of the inner stator 22 mounted, designed as a pin-shaped tools 49 surveys in which - as is apparent in particular from Fig. 4 - are arranged helically over the circumference and the length of the outer shell 23. As can be seen in particular from FIG. 4, adjacent tools 49 in the circumferential direction of the inner stator 22 overlap one another in the direction of the central longitudinal axis 19 arranged so that in one revolution of the rotor 39 whose inner wall 41 is completely swept by the tools 49.

Wie sich aus dem Vorstehenden ergibt, wird der Mahlraum 8 also in einen zylinderringförmigen Außen-Mahlraum 8a einerseits und einen zylinderringförmigen Innen-Mahlraum 8b andererseits unterteilt, die durch einen sich von außen nach innen stetig erweiternden Umlenkraum 50 in der Nähe der Bodenplatte 12 miteinander verbunden sind.As can be seen from the above, the grinding chamber 8 is thus divided into a cylindrical outer grinding chamber 8a on the one hand and a cylindrical annular grinding chamber 8b on the other hand, connected by a constantly widening from outside to inside deflection space 50 in the vicinity of the bottom plate 12 are.

Wie aus den Fig. 2 und 4 hervorgeht, besteht die zylindrische Trenneinrichtung 32 aus einem Stapel von Ringscheiben 51, zwischen denen jeweils ein Trennspalt 52 freigelassen ist, dessen Weite in der Regel kleiner als der Durchmesser der kleinsten verwendeten Mahlhilfskörper 38 ist; die Weite kann aber auch größer sein, da die Abtrennung der Mahlhilfskörper 38 vor Erreichen der Trenneinrichtung 32 erfolgt. Der Stapel von Ringscheiben 51 ist stirnseitig, also an der der Abschlussplatte 44 zugewandten Seite, durch eine Verschlussplatte 53 abgeschlossen. Die Trenneinrichtung 32 ist innerhalb des Rückführ-Moduls 45 angeordnet.As is apparent from Figs. 2 and 4, the cylindrical separator 32 consists of a stack of annular disks 51, between each of which a separating gap 52 is left free, the width of which is generally smaller than the diameter of the smallest grinding auxiliary body 38 used; However, the width can also be greater, since the separation of the Mahlhilfskörper 38 takes place before reaching the separator 32. The stack of annular discs 51 is the end side, ie at the end plate 44 facing side, completed by a closure plate 53. The separator 32 is disposed within the return module 45.

Wie aus Fig. 2 und 5 hervorgeht, sind im Mahlhilfskörper-Rückführ-Modul 45 Mahlhilfskörper-Rückführ-Kanäle 54 ausgebildet. Deren jeweilige Eintrittsöffnung 55 befindet sich unmittelbar benachbart zur Trenneinrichtung 32. Ihre jeweilige Austrittsöffnung 56 mündet in einen ringzylindrischen Mahlgut-Zuführ-Bereich 57, der zwischen dem Rückführ-Modul 45 und der Innenwand 9 des Mahlbehälters 2 ausgebildet ist. Die Rückführ-Kanäle 54 haben ihre geringste Breite c an der Eintrittsöffnung 55 und ihre größte Breite d an der Austrittsöffnung 56, wobei die Breiten c bzw. d jeweils in Umfangsrichtung gemessen werden. Die Rückführ-Kanäle 54 sind von der Eintrittsöffnung 55 zur Austrittsöffnung 56 entgegen der Drehrichtung 58 des Rührwerks 20 gekrümmt, und zwar von innen nach außen gesehen, konvex gekrümmt. Für die Breite c gilt im Verhältnis zur Breite d:

  • d > c und bevorzugt
  • d ≥ 1,5 c.
As is apparent from FIGS. 2 and 5, grinding aid body return channels 54 are formed in the grinding aid body return module 45. Their respective inlet opening 55 is located immediately adjacent to the separating device 32. Their respective outlet opening 56 opens into a ring-cylindrical grinding material feed area 57, which is formed between the return module 45 and the inner wall 9 of the grinding container 2. The return channels 54 have their smallest width c at the inlet opening 55 and their largest width d at the outlet opening 56, wherein the widths c and d are respectively measured in the circumferential direction. The return channels 54 are opposite to the direction of rotation 58 from the inlet 55 to the outlet 56 of the agitator 20, seen from the inside out, convexly curved. For the width c applies in relation to the width d:
  • d> c and preferred
  • d ≥ 1.5 c.

In dem Ausführungsbeispiel nach den Fig. 2 bis 5 erstrecken sich die Rückführ-Kanäle 54 in Richtung der Achse 19 fast über die volle Höhe des Rückführ-Moduls 45, wobei ihre axiale Höhe e größer ist als die axiale Höhe f der Trenneinrichtung 32. Die Rückführ-Kanäle 54 erstrecken sich bei dieser Ausführungsform außer über die Trenneinrichtung 32 in Richtung der Achse 19 noch über einen vom oberen Ende des Innen-Mahlraums 8b schräg nach oben und innen zur Trenneinrichtung 32 führenden, sich also in Richtung zur Abschlussplatte 44 hin kegelstumpfförmig verjüngenden Abström-Kanal 59. Bei diesem Ausführungsbeispiel sind die Rückführ-Kanäle 54 auch zu dem Abström-Kanal 59 hin offen, wie Fig. 2 erkennen lässt. Der Abström-Kanal 59 ist nach oben also nicht räumlich begrenzt. Er ist vielmehr in Richtung der Mittel-Längs-Achse 19 zum Innen-Mahlraum 8b hin offen und somit für den Austritt der Mahlhilfskörper 38 durchlässig, während das Mahlgut durch den Abström-Kanal 59 in Richtung zur Trenneinrichtung 32 strömt.In the embodiment of FIGS. 2 to 5, the return channels 54 extend in the direction of the axis 19 almost over the full height of the return module 45, wherein its axial height e is greater than the axial height f of the separator 32. Die Return channels 54 extend in this embodiment except via the separator 32 in the direction of the axis 19 still obliquely upward from the upper end of the inner grinding chamber 8b and inside to the separator 32 leading, so tapering in the direction of the end plate 44 towards frustoconical Outflow channel 59. In this embodiment, the return channels 54 are also open to the outflow channel 59, as Fig. 2 reveals. The outflow channel 59 is therefore not spatially limited upwards. Rather, it is open in the direction of the central longitudinal axis 19 towards the internal grinding chamber 8b and thus permeable to the exit of the grinding auxiliary bodies 38, while the millbase flows through the outflow channel 59 in the direction of the separating device 32.

Das Mahlgut durchströmt den Mahlraum 8 entsprechend den Strömungs-Richtungspfeilen 60 von der Mahlgut-Zuführleitung 21 kommend durch einen Mahlgut-Zuführraum 61 zwischen dem Abschlussteil 43 des Rührwerks 20 einerseits und dem Deckel 17 und dem benachbarten Bereich der Innenwand 9 andererseits, den Mahlgut-Zuführ-Bereich 57, den Außen-Mahlraum 8a nach unten, durch den sich stetig erweiternden Umlenkraum 50 radial nach innen und von dort durch den Innen-Mahlraum 8b nach oben bis zum Abström-Kanal 59 und von dort zur Trenneinrichtung 32. Auf dem Wege durch den Außen-Mahlraum 8a, den Umlenkraum 50 und den Innen-Mahlraum 8b wird das Mahlgut bei drehend angetriebenem Rührwerk 20 im Zusammenwirken mit den Mahlhilfskörpern 38 gemahlen. Das Mahlgut verlässt den Innen-Mahlraum 8b durch die Trenneinrichtung 32, von wo es durch die Mahlgut-Ablaufleitung 33 abfließt.The material to be ground flows through the grinding chamber 8 corresponding to the flow direction arrows 60 coming from the grinding material supply line 21 through a Mahlgut feed chamber 61 between the end portion 43 of the agitator 20 on the one hand and the lid 17 and the adjacent region of the inner wall 9 on the other hand, the grinding material feed Area 57, the outer grinding chamber 8a down, by the steadily widening deflection space 50 radially inwardly and from there through the inner grinding chamber 8b after on the way up to the outflow channel 59 and from there to the separator 32. On the way through the outer grinding chamber 8a, the deflection space 50 and the inner grinding chamber 8b, the material to be ground is milled in rotationally driven agitator 20 in cooperation with the auxiliary grinding bodies 38. The ground material leaves the interior grinding chamber 8 b through the separating device 32, from where it flows through the grinding stock discharge line 33.

Wie insbesondere aus Fig. 2 hervorgeht, ist die radiale Spaltweite g des Außen-Mahlraums 8a deutlich kleiner als die radiale Spaltweite h des Innen-Mahlraums 8b. Die Spaltweiten g und h verhalten sich so zueinander, dass die Querschnittsfläche Fb des Innen-Mahlraums 8b gleich oder größer ist als die Querschnittsfläche Fa des Außen-Mahlraums 8a. Sowohl der Außen-Mahlraum 8a als auch der Innen-Mahlraum 8b sind als Mahlspalte ausgebildet. Es gilt für die Spaltweite g des Außen-Mahlraums 8a im Verhältnis zum Durchmesser i der größten, in der Rührwerksmühle befindlichen Mahlhilfskörper 38:

  • g ≥ 3i,
wobei für den Durchmesser i gilt:
  • i ≤ 3,0 mm und bevorzugt 1 ≤ 1,5 mm.
Absolut gilt für die Spaltweite g des Außen-Mahlraums 8a:
  • g ≤ 9,0 mm und bevorzugt g ≤ 5,0 mm.
As can be seen in particular from FIG. 2, the radial gap width g of the outer grinding chamber 8a is significantly smaller than the radial gap width h of the inner grinding chamber 8b. The gap widths g and h are related to each other so that the cross-sectional area Fb of the inner grinding space 8b is equal to or larger than the cross-sectional area Fa of the outer grinding space 8a. Both the outer grinding chamber 8a and the inner grinding chamber 8b are formed as grinding gaps. The following applies to the gap width g of the outer grinding chamber 8a in relation to the diameter i of the largest grinding aid body 38 located in the agitator mill:
  • g ≥ 3i,
where for the diameter i:
  • i ≤ 3.0 mm and preferably 1 ≤ 1.5 mm.
Absolutely true for the gap width g of the outer grinding chamber 8a:
  • g ≤ 9.0 mm and preferably g ≤ 5.0 mm.

Für die Querschnittsfläche Fa des Außen-Mahlraums 8a gilt im Verhältnis zur Querschnittsfläche Fb des Innen-Mahlraums 8b:

  • Fa ≤ Fb und bevorzugt 1,2 Fa ≤ Fb ≤ 7 Fa.
For the cross-sectional area Fa of the outer grinding chamber 8a, in relation to the cross-sectional area Fb of the inner grinding chamber 8b:
  • Fa ≤ Fb and preferably 1.2 Fa ≤ Fb ≤ 7 Fa.

Das Ausführungsbeispiel nach den Fig. 6 und 7 unterscheidet sich von dem nach den Fig. 2 bis 5 im Wesentlichen dadurch, dass zwischen der Abschlussplatte 44 und dem Rotor 39 außer einem Mahlhilfskörper-Rückführ-Modul 45' noch eine Stau-Einrichtung 62 als Teil des Rührwerks 20' vorgesehen ist. Zwischen dem Stirnteil 31 des Innen-Stators 22 und dieser Stau-Einrichtung 62 wird der Abström-Kanal 59' begrenzt, der also abweichend von dem Ausführungsbeispiel nach den Fig. 2 bis 5 nicht nur an seiner Unterseite durch das Stirnteil 31, sondern auch an seiner Oberseite begrenzt wird, und zwar durch die Stau-Einrichtung 62. Anders als beim Ausführungsbeispiel nach den Fig. 2 bis 5 mündet der Innen-Mahlraum 8b an seinem oberen Ende nicht direkt in die Rückführ-Kanäle 54' ein, sondern das Mahlgut-Mahlhilfskörper-Gemisch wird durch die Stau-Einrichtung 62 zwingend schräg nach oben und innen in Richtung zur Trenneinrichtung 32' umgelenkt. In diesem Ausführungsbeispiel ist die Spaltweite j des Abström-Kanals 59' konstant.The embodiment of FIGS. 6 and 7 differs from that of FIGS. 2 to 5 essentially in that between the end plate 44 and the rotor 39 except a Mahlhilfskörper feedback module 45 'still a jam device 62 is provided as part of the agitator 20'. Between the front part 31 of the inner stator 22 and this storage device 62 of the outflow channel 59 'is limited, so deviating from the embodiment of FIGS. 2 to 5 not only on its underside by the front part 31, but also at Unlike in the embodiment according to FIGS. 2 to 5, the inner grinding chamber 8b does not open at its upper end directly into the return channels 54 ', but instead feeds the grinding material. Mahlhilfskörper mixture is forced by the jam device 62 obliquely upwards and inwards in the direction of the separator 32 '. In this embodiment, the gap width j of the outflow channel 59 'is constant.

Soweit im Übrigen Teile identisch mit denen nach dem Ausführungsbeispiel nach den Fig. 2 bis 5 sind, werden dieselben Bezugszeichen verwendet. Ansonsten werden bei funktionell gleichen und konstruktiv ähnlichen Teilen dieselben Bezugszeichen verwendet, denen ein hochgesetzter Strich hinzugefügt ist. Entsprechendes gilt für weitere Ausführungsbeispiele mit entsprechend mehreren hochgesetzten Strichen. Die Höhe e' der Rückführ-Kanäle 54' ist deutlich geringer als die Höhe e im Ausführungsbeispiel nach den Fig. 2 bis 5. Des Weiteren gilt, dass die Höhe e' deutlich geringer ist als die axiale Höhe f der Trenneinrichtung 32'. Es ist so in einfacher Weise eine Anpassung der Höhe e' der Rückführ-Kanäle 54' an geringere Mahlgut-Durchsätze und zusätzlich eine Verringerung der Gefahr von Mahlgut-Partikel-Durchschüssen insbesondere bei geringem Mahlgut-Durchsatz oder einer niedrigen Drehzahl des Rührwerks 10 möglich. Es gilt:

  • e' ≤ f' und insbesondere
  • e' ≤ 0,8 f' und ganz besonders
  • e' < 0,5 f'.
As far as parts are otherwise identical to those of the embodiment of FIGS. 2 to 5, the same reference numerals are used. Otherwise, the same reference numerals are used for functionally identical and structurally similar parts, to which a superscript bar is added. The same applies to further embodiments with correspondingly several elevated strokes. The height e 'of the return channels 54' is significantly less than the height e in the embodiment of FIGS. 2 to 5. Furthermore, the height e 'is significantly less than the axial height f of the separator 32'. It is thus possible in a simple manner to adjust the height e 'of the return channels 54' to lower grinding stock throughputs and, in addition, to reduce the risk of grinding stock particle passages, in particular with low grinding material throughput or a low rotational speed of the agitator 10. The following applies:
  • e '≤ f' and in particular
  • e '≤ 0.8 f' and especially
  • e '<0.5 f'.

Weiterhin erstreckt sich die Trenneinrichtung 32' nicht über den vollen Bereich oberhalb des Stimteils 31. Vielmehr ist zwischen dem Stirnteil 31 und der Trenneinrichtung 32' ein geschlossener Ring-Abschnitt als Verschleiß-Schutz 63 vorgesehen, der einteilig mit der Trenneinrichtung 32' ausgebildet ist. Vor ihm bzw. an ihm endet der Abström-Kanal 59', sodass aus dem Abström-Kanal 59' austretende und in eine achsparallele Bewegung umgelenkte Mahlhilfskörper 38 die Trenneinrichtung 32' nicht treffen.Furthermore, the separating device 32 'does not extend over the full area above the end portion 31. Rather, a closed ring portion as wear protection 63 is provided between the end portion 31 and the separator 32', which is formed integrally with the separator 32 '. Before him or on him the outflow channel ends 59 ', so that from the outflow channel 59' exiting and deflected in an axis-parallel motion Mahlhilfskörper 38, the separator 32 'do not hit.

Das Ausführungsbeispiel nach Fig. 8 unterscheidet sich von dem nach den Fig. 6 und 7 nur dadurch, dass die Mahlhilfskörper-Rückführ-Kanäle 54" eine für einen störungsfreien Betrieb bei geringen Mahlgut-Durchsätzen minimal erforderliche Höhe e" haben. Ansonsten schließt auch hier das Mahlhilfskörper-Rückführ-Modul 45" an die Stau-Einrichtung 62 an, wobei bei diesem Ausführungsbeispiel gleichermaßen wie bei den beiden zuvor erwähnten Ausführungsbeispielen die Rückführ-Kanäle 54" an ihrer Oberseite durch die Abschlussplatte 44 begrenzt werden. Die axiale Höhe k ist bei den Rückführ-Modulen 45' und 45" aber gleich.The embodiment according to FIG. 8 differs from that according to FIGS. 6 and 7 only in that the grinding aid return channels 54 "have a minimum required height e" for trouble-free operation at low grinding stock throughputs. Otherwise, the Mahlhilfskörper feedback module 45 "includes here to the jam means 62, wherein in this embodiment, as in the two aforementioned embodiments, the return channels 54" are bounded on their upper side by the end plate 44. The axial height k is the same in the return modules 45 'and 45 ".

Für die minimale axiale Höhe e" der Rückführ-Kanäle 54" gilt:

  • e" ≥ 3 i mindestens aber e" ≥ 4 mm.
For the minimum axial height e "of the return channels 54", the following applies:
  • e "≥ 3 i but at least e" ≥ 4 mm.

Das Ausführungsbeispiel nach Fig. 9 entspricht dem nach Fig. 6 mit dem Unterschied, dass kein Verschleißschutz 63 vorgesehen ist und dass andererseits die Abström-Kanäle 59"' sich zur Mahlhilfskörper-Trenneinrichtung 32 hin erweitern, d. h. die Spaltweite j"' des Abström-Kanals 59"' nimmt nach innen hin zu, und zwar in einem solchen Maße, dass die Gesamtquerschnittsfläche dieses Kanals 59"' in Richtung zur Trenneinrichtung 32 jedenfalls nicht kleiner wird, sodass keine Beschleunigung der Mahlgut-Mahlhilfskörper-Strömung im Abström-Kanal 59"' zur Trenneinrichtung 32 hin stattfindet. Aus diesem Grunde kann sich die Trenneinrichtung 32 bis zum Stirnteil 31 erstrecken, da die Mahlhilfskörper 38 nicht auf die Trenneinrichtung 32 auftreffen.The embodiment of FIG. 9 corresponds to that of FIG. 6 with the difference that no wear protection 63 is provided and that on the other hand the outflow channels 59 '' extend towards the grinding aid separator 32, ie the gap width j '' of the outflow channel 59 '' increases inwards to such an extent that the total cross-sectional area of this channel 59 '' In any case, it does not become smaller in the direction of the separating device 32 so that there is no acceleration of the grinding stock auxiliary body flow in the outflow channel 59 '' to the separating device 32. For this reason, the separating device 32 can extend to the front part 31, since the auxiliary grinding bodies 38 do not hit the separator 32.

Die Ausführungsform nach Fig. 10 entspricht im Wesentlichen der nach Fig. 9, wobei das Mahlhilfskörper-Rückführ-Modul 45"" nicht bis an die Trenneinrichtung 32 herangeführt ist. Die Eintrittsöffnungen 55"" der Mahlhilfskörper-Rückführ-Kanäle 54"" weisen also einen deutlichen radialen Abstand von der Trenneinrichtung 32 auf. In diesem Ringraum 64 sind mehrere Abstreifer 65 vorgesehen, die an der Abschlussplatte 44 angebracht sind und mit dem Rührwerk 20"" umlaufen.The embodiment of FIG. 10 substantially corresponds to that of FIG. 9, wherein the Mahlhilfskörper feedback module 45 "" is not brought up to the separator 32. The inlet openings 55 "" of the grinding auxiliary body return channels 54 "" thus have a clear radial distance from the separating device 32. In this annular space 64 a plurality of scrapers 65 are provided, which are attached to the end plate 44 and rotate with the agitator 20 "".

Das Ausführungsbeispiel nach den Fig. 11 bis 13 weist ein Mahlhilfskörper-Rückführ-Modul 45""' auf, das zur Stau-Einrichtung 62 hin an einem Zwischenring 66 anliegt. Das Modul 45""' ist also nach unten zum Mahlraum 8 hin, also zu einer Stirnseite 67, offen. Die axiale Höhe e""' ist von der jeweiligen Eintrittsöffnung 55""' zur Austrittsöffnung 56""' hin konstant und deutlich kleiner als die Höhe f' der Trenneinrichtung 32'. Die Abstreifer 65""' schließen sich übergangslos an die Rückführ-Kanäle 54""' an, sodass ein stetiger Übergang von diesen Abstreifern 65""' in die Rückführ-Kanäle 54""' gegeben ist, wie insbesondere Fig. 13 entnehmbar ist. Dies führt zu optimalen Strömungsverhältnissen. Wie Fig. 11 entnehmbar ist, erstrecken sich die Abstreifer 65""' in Richtung der Achse 19 etwa über die Höhe f' der Trenneinrichtung 32'.The exemplary embodiment according to FIGS. 11 to 13 has a grinding aid body return module 45 ""'which bears against an intermediate ring 66 toward the accumulation device 62. The module 45 ""'is thus down to the grinding chamber 8, ie to an end face 67, open. The axial height e ""'is constant from the respective inlet opening 55 ""' to the outlet opening 56 ""'and is significantly smaller than the height f' of the separating device 32 '. The scrapers 65 '''merge seamlessly with the return channels 54 "'', so that a continuous transition from these scrapers 65""' is given in the return channels 54""', as Fig. 13 in particular is removable , This leads to optimal flow conditions. As can be seen in FIG. 11, the wipers 65 '''extend in the direction of the axis 19 about the height f 'of the separator 32'.

Claims (18)

  1. An agitator mill for treating free-flowing grinding stock, comprising
    a grinding receptacle (2) which defines a substantially closed grinding chamber (8) by means of an inner wall (9); and
    an agitator (20) which is rotarily drivably disposed therein and which is cup-shaped in relation to a common central longitudinal axis (19), having an annular cylindrical rotor (39) which has a closed wall (40, 41); and
    an interior stator (22) which is disposed within the rotor (39) and fixedly joined to the grinding receptacle (2);
    wherein an annular cylindrical exterior grinding chamber (8a) in the form of an annular gap is formed between the inner wall (9) of the grinding receptacle (2) and an outer wall (40) of the rotor (39), the exterior grinding chamber (8a) having a radial gap width g;
    wherein an annular cylindrical interior grinding chamber (8b) in the form of an annular gap is formed between an inner wall (41) of the rotor (39) and an outer casing (23) of the interior stator (22), the interior grinding chamber (8b) being arranged coaxially within the exterior grinding chamber (8a) and connected thereto via a deflection chamber (50) and having a radial gap width h;
    wherein the exterior grinding chamber (8a), the deflection chamber (50) and the interior grinding chamber (8b) constitute the grinding chamber (8) which is partially filled with auxiliary grinding bodies (38);
    wherein a grinding-stock supply area (57), which is disposed upstream of the exterior grinding chamber (8a) and opens into the exterior grinding chamber (8a) in the direction of flow (60) of the grinding stock, and a separator device (32), which is disposed downstream of the interior grinding chamber (8b) in the direction of flow (60), are disposed approximately on the same side of the grinding receptacle (2) for the grinding stock to pass through;
    wherein auxiliary-grinding-body return conduits (54) are provided in the agitator (20) for returning the auxiliary grinding bodies (38) from the vicinity of the separator device (32) into the grinding-stock supply area (57), the return conduits (54) connecting the end of the interior grinding chamber (8b) to the beginning of the exterior grinding chamber (8a);
    wherein the inner wall (9) of the grinding receptacle (2) and the outer wall (40) and the inner wall (41) of the rotor (39) are free of interruptions, and the inner wall (9) of the grinding receptacle (2) and the outer wall (40) of the rotor (39) are smooth and free of agitator implements;
    characterized
    in that g < h applies to the radial gap width g of the exterior grinding chamber (8a) in relation to the radial gap width h of the interior grinding chamber (8b).
  2. An agitator mill according to claim 1, characterized
    in that Fa ≤ Fb, and preferably 1.2 Fa ≤ Fb ≤ 7 Fa, applies to the cross-sectional area Fa of the exterior grinding chamber (8a) in relation to the cross-sectional area Fb of the interior grinding chamber (8b).
  3. An agitator mill according to claim 1 or 2, characterized
    in that g ≥ 3i applies to the gap width g of the exterior grinding chamber (8a) in relation to the diameter i of the biggest auxiliary grinding bodies (38) in the grinding chamber (8);
    wherein i ≤ 3.0 mm, and preferably i ≤ 1.5 mm, applies to the diameter i of the auxiliary grinding bodies (38);
    and wherein g ≤ 9.0 mm, and preferably g ≤ 5.0 mm, applies to the gap width g of the exterior grinding chamber (8a).
  4. An agitator mill according to any of claims 1 to 3, characterized
    in that the outer casing (23) of the interior stator (22) is equipped with elevations which project into the interior grinding chamber (8b).
  5. An agitator mill according to claim 4, characterized
    in that the elevations are implements (49), in particular implements in the form of pegs.
  6. An agitator mill according to claim 4, characterized
    in that the elevations are disposed helically on the interior stator (22).
  7. An agitator mill according to any of claims 1 to 6, characterized
    in that the inner wall (41) of the rotor (39) is smooth, free of agitator implements.
  8. An agitator mill according to any of claims 1 to 7, characterized
    in that the interior grinding chamber (8b) is followed by a discharge conduit (59) in the shape of a truncated cone which is directed towards the separator device (32).
  9. An agitator mill according to claim 8, characterized
    in that the discharge conduit (59) is defined by a face (31), neighbouring the separator device (32), of the interior stator (22) and a dam-up device (62).
  10. An agitator mill according to claim 9, characterized
    in that the dam-up device (62) is an independent component part of the agitator (20).
  11. An agitator mill according to claim 8, characterized
    in that the gap width j of the discharge conduit (59) grows in a direction towards the separator device (32).
  12. An agitator mill according to any of claims 8 to 11, characterized
    in that the interior stator (22) is provided with a wearing protection (63) in the vicinity of the discharge conduit (59).
  13. An agitator mill according to any of claims 8 to 12, characterized
    in that the auxiliary-grinding-body return conduits (54) are formed in an independent auxiliary-grinding-body return module (45).
  14. An agitator mill according to claim 13,
    wherein the auxiliary-grinding-body return conduits (54) are open towards a front (67) of the return module (45).
  15. An agitator mill according to any of claims 1 to 14, characterized
    in that the return conduits (54) have an inlet (5) of a width c and an outlet (56) of a width d; and
    in that d > c, and preferably d ≥ 1.5 c, applies to the width c of the inlet (55) in relation to the width d of the outlet (56).
  16. An agitator mill according to any of claim 1 to 15, characterized
    in that the auxiliary-grinding-body return conduits (54) have a height e and the separator device (32) has a height f - each in the direction of the central longitudinal axis (1); and
    wherein e ≤ f, and preferably e < 0.5 f, applies to the height e in relation to the height f.
  17. An agitator mill according to any of claims 13 to 16, characterized
    in that the return module (45), in vicinity to the separator device (32), is provided with wipers (65) which pass continuously without interruption into the return conduits (54).
  18. An agitator mill according to claim 17, characterized
    in that the wipers (65) extend along the height (f) of the auxiliary-grinding-body separator device (32).
EP05010815A 2005-05-19 2005-05-19 Stirring mill Not-in-force EP1724022B1 (en)

Priority Applications (8)

Application Number Priority Date Filing Date Title
AT05010815T ATE361146T1 (en) 2005-05-19 2005-05-19 AGITATOR MILL
DE502005000670T DE502005000670D1 (en) 2005-05-19 2005-05-19 agitating mill
ES05010815T ES2285603T3 (en) 2005-05-19 2005-05-19 MILL AGITATOR.
EP05010815A EP1724022B1 (en) 2005-05-19 2005-05-19 Stirring mill
US11/171,319 US7216822B2 (en) 2005-05-19 2005-07-01 Agitator mill
JP2006138920A JP5010853B2 (en) 2005-05-19 2006-05-18 Stirrer mill
KR1020060044818A KR101245478B1 (en) 2005-05-19 2006-05-18 Agitator mill
CNB2006100826375A CN100544892C (en) 2005-05-19 2006-05-19 Mixing plant

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP05010815A EP1724022B1 (en) 2005-05-19 2005-05-19 Stirring mill

Publications (2)

Publication Number Publication Date
EP1724022A1 EP1724022A1 (en) 2006-11-22
EP1724022B1 true EP1724022B1 (en) 2007-05-02

Family

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Family Applications (1)

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EP05010815A Not-in-force EP1724022B1 (en) 2005-05-19 2005-05-19 Stirring mill

Country Status (8)

Country Link
US (1) US7216822B2 (en)
EP (1) EP1724022B1 (en)
JP (1) JP5010853B2 (en)
KR (1) KR101245478B1 (en)
CN (1) CN100544892C (en)
AT (1) ATE361146T1 (en)
DE (1) DE502005000670D1 (en)
ES (1) ES2285603T3 (en)

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US20090212141A1 (en) * 2005-06-08 2009-08-27 Alan Taylor Milling apparatus
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CN109746088A (en) * 2017-11-08 2019-05-14 深圳市微纳达智能设备有限公司 The vertical closing of one kind is without mechanical seal pipe net discharging medium stirring mill
IT201800003874A1 (en) * 2018-03-22 2019-09-22 Certech Spa Con Socio Unico Mill for ceramic materials
EP3650123A1 (en) * 2018-11-09 2020-05-13 Bühler AG Ring gap grinder
CN110900822B (en) * 2019-11-08 2021-08-24 南京赛诺特斯材料科技有限公司 Composite additive for improving ceramic performance of zirconia powder
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EP4032615A1 (en) 2021-01-25 2022-07-27 Wilhelm Niemann GmbH & Co KG Agitator mill
DE102021101527A1 (en) 2021-01-25 2022-07-28 Wilhelm Niemann Gmbh & Co. agitator mill
DE102021101527B4 (en) 2021-01-25 2023-05-17 Wilhelm Niemann Gmbh & Co. agitator mill

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JP2006320898A (en) 2006-11-30
KR20060120465A (en) 2006-11-27
US20060261200A1 (en) 2006-11-23
EP1724022A1 (en) 2006-11-22
CN100544892C (en) 2009-09-30
KR101245478B1 (en) 2013-03-25
ATE361146T1 (en) 2007-05-15
US7216822B2 (en) 2007-05-15
CN1864928A (en) 2006-11-22
JP5010853B2 (en) 2012-08-29
ES2285603T3 (en) 2007-11-16
DE502005000670D1 (en) 2007-06-14

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