EP1060795B1 - Control for an electrostatic spray coating apparatus - Google Patents
Control for an electrostatic spray coating apparatus Download PDFInfo
- Publication number
- EP1060795B1 EP1060795B1 EP00110032A EP00110032A EP1060795B1 EP 1060795 B1 EP1060795 B1 EP 1060795B1 EP 00110032 A EP00110032 A EP 00110032A EP 00110032 A EP00110032 A EP 00110032A EP 1060795 B1 EP1060795 B1 EP 1060795B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- voltage
- spray
- current
- value
- coating apparatus
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B5/00—Electrostatic spraying apparatus; Spraying apparatus with means for charging the spray electrically; Apparatus for spraying liquids or other fluent materials by other electric means
- B05B5/08—Plant for applying liquids or other fluent materials to objects
- B05B5/10—Arrangements for supplying power, e.g. charging power
Definitions
- the invention relates to a spray coating device according to the preamble of claim 1.
- a spray coating device of this kind is known from EP 0 734 778 A2 known.
- a spray coating device in which an operator can enter via a keyboard a desired voltage value and a desired current value, which should be kept constant by a control device.
- a threshold value is provided for the distance between the spray device and the object to be coated. If the distance is greater than the threshold value, then the high voltage at the high voltage electrode of the spraying device is kept constant independently of the object distance, whereby the spraying current of the high voltage electrode increases with increasing object distance becomes smaller or with decreasing object distance. If the distance is less than the threshold, then the spray current is kept constant independent of changes in distance by counteracting a current increase by a corresponding voltage reduction. Immediately before the object touches the spray device, the high voltage breaks down completely (contact protection).
- Spray current from the electrode to the object to be coated is indirectly measured by measuring the electric current flowing through a primary winding of a transformer to the secondary winding of which a high voltage cascade circuit with rectifiers and capacitors is connected, which generates the high voltage DC voltage for the electrode.
- a spray coating device in which an increase in the spray flow when an object to be coated approaches the spray device is counteracted by a corresponding reduction of the high voltage in order to keep the spray flow constant.
- the spray current is measured indirectly by measuring the current flowing in the secondary winding between the transformer and a high voltage cascade circuit.
- a spray coating device is known, in which also the input voltage of a high voltage generator is changed inversely to the spraying current, wherein the spraying current is measured indirectly at an electrical resistance upstream of the high voltage electrode by measuring a voltage drop.
- the invention enables the problem to be solved to avoid the dangers of excessive electrical voltage to the high voltage electrode at a large distance of an electrically conductive object or too high a current or short-circuit current in close proximity of an object to the high voltage electrode, wherein the object be coated object or an operator or other object, and at the same time form the spray coating device such that optimum coating results are achieved with minimal electrical energy expenditure.
- the invention is particularly advantageous in connection with a counter electrode which is connected to a potential which has a high electrical voltage difference to the high voltage potential of the high voltage electrode, e.g. B. is connected to ground potential to dissipate free electric particles, in particular ions and electrons, which emanate from the Hochspannunselektrode, but freely herumavagundieren, instead of with the spray coating material from the sprayer to the flying object.
- Counter electrodes are z. B. from the EP 0 756 899 A2 known.
- the spray coating device shown schematically in Fig. 1 comprises a spraying device 2 for spraying coating material 4 in the form of liquid or preferably powder on an object to be coated 6. It is assumed that the objects to be coated consist of electrically conductive material and connected to ground potential 8 are.
- the objects 6 are transported in the case of automatic systems through a conveying device, not shown, past the spraying device 2 and thereby reach the spray jet of the coating material 4 schematically represented by an arrow.
- the spray device 2 is provided with at least one high voltage electrode 10 for electrostatically charging the coating material 4, which is supplied by a high voltage DC voltage source 12 in the range between 1 kV and 150 kV, preferably one therebetween lying value, is supplied.
- the high voltage generator may include, in a known manner, a transformer for stepping up a low AC voltage to a higher AC voltage and a cascade circuit which in a known manner contains a plurality of rectifiers and capacitors and converts the AC voltage to the DC high voltage.
- the low alternating voltage is generated by an oscillator 14 in response to a control voltage U-ST, which is a manipulated variable for the high voltage of the high voltage electrode 10.
- the oscillator 14 may be a part of the high voltage generator 12 and be integrated as such in the spray device 2, or according to FIG. 1 integrated into a control unit, which forms a total of a control device 16.
- the control device 16 includes an operating parameter memory 18, which via a data transfer path 19 from a data input station, such as a higher-level computer or manually, z. B. via a keyboard, variably adjustable at least one high-voltage limiting value HV-BG and at least one Sprühstrombegrenzungswert I-BG each for the maximum achievable value at the high voltage electrode can be entered and stored therein.
- a data input station such as a higher-level computer or manually, z. B. via a keyboard
- variably adjustable at least one high-voltage limiting value HV-BG and at least one Sprühstrombegrenzungswert I-BG each for the maximum achievable value at the high voltage electrode can be entered and stored therein.
- a plurality of such values can be stored for different operating situations, in particular for different objects to be coated and different spray coating materials.
- the stored values may be non-settable fixed values in another embodiment.
- the high voltage limit value HV-BG is input from the operating parameter memory 18 into a high voltage limiting circuit 20.
- the spray current limit value I-BG is input from the operating parameter memory 18 to a spray current controller 22.
- the spraying current of the high-voltage electrode 10 flowing from an object 6 to be coated to earth is measured by a spray current circuit 24 on the side of the objects 6 connected to ground 8 and also input into the spray current regulator as the actual spray current value I-S.
- the spray current controller 22 compares the actual spray current value 1-S- with the spray current limit value I-BG and, in response thereto, generates a high-voltage regulator quantity U-RG which is given by the spray current regulator 22 to the high voltage limit circuit 20.
- the spray current controller 22 is preferably a P-I controller (proportional-integral controller).
- the high voltage limiting circuit 20 generates depending on the Hochgêtsbegrenzungswert HV-BG and the high-voltage regulator size U-RG the control voltage U-ST, which is supplied to the oscillator 14 in the form of a DC input voltage and the manipulated variable for the high voltage of the high voltage electrode 10.
- FIG. 2 shows the spray current in ⁇ A on the horizontal axis and the corresponding high voltage in kV on the vertical axis.
- the top characteristic 26 with filled squares is a standard characteristic. It shows how in known devices with decreasing distance between the high voltage electrode 10 and an object to be coated 6, the spray current of the high voltage electrode 10 increases and at the same time the high voltage drops.
- the high voltage has its maximum value at the greatest possible distance or infinitely large distance of the object 6 to be coated or another electrically conductive object from the high-voltage electrode 10.
- the middle curve 27 with the non-filled squares relates to an embodiment in which the maximum DC high voltage of the high voltage electrode 10 is limited to a maximum value HV-BG of 80 kV, but no current limiting I-BG was made.
- the spraying device 2 is shown in somewhat more detail. It shows that one or more high voltage electrodes 10 may be disposed outside or within a coating material channel 30. He is coating material, for. As coating powder, via a line 31, z. B. a hose supplied.
- the spray device 2 with a reference potential, z. Ground potential, connected counterelectrodes 32 (arrester electrodes) may be provided, which absorb free electric charges (ions, electrons), which are discharged from the electrodes 10, and divert them to earth potential. It has been found that substantially less free electrical particles are formed by the invention, in particular free ions, and thus also a lower power loss.
- the oscillator 14 is connected via an electrical cable 36 to the high voltage generator 12, which is integrated into the spray device 2, but also separated from it, z. B. in the control device 16 could be arranged.
Abstract
Description
Die Erfindung betrifft eine Sprühbeschichtungseinrichtung gemäß dem Oberbegriff von Anspruch 1.The invention relates to a spray coating device according to the preamble of
Eine Sprühbeschichtungseinrichtung dieser Art ist aus der
Ferner ist aus der
Aus der
Aus der
Durch die Erfindung soll die Aufgabe gelöst werden, die Gefahren einer zu hohen elektrischen Spannung an der Hochspannungselektrode bei einem großen Abstand eines elektrisch leitenden Objektes oder einen zu hohen Strom oder Kurzschlußstrom bei zu naher Annäherung eines Objektes an die Hochspannungselektrode zu vermeiden, wobei das Objekt ein zu beschichtender Gegenstand oder eine Bedienungsperson oder ein anderer Gegenstand sein kann, und gleichzeitig die Sprühbeschichtungseinrichtung derart auszubilden, daß mit geringstem elektrischem Energieaufwand optimale Beschichtungsergebnisse erzielt werden.The invention enables the problem to be solved to avoid the dangers of excessive electrical voltage to the high voltage electrode at a large distance of an electrically conductive object or too high a current or short-circuit current in close proximity of an object to the high voltage electrode, wherein the object be coated object or an operator or other object, and at the same time form the spray coating device such that optimum coating results are achieved with minimal electrical energy expenditure.
Diese Aufgabe wird gemäß der Erfindung durch die Kombination der Merkmale von Anspruch 1 gelöst.This object is achieved according to the invention by the combination of the features of
Durch das kennzeichnende Merkmal von Anspruch 1, einer direkten Messung des Sprühstromes, erhält man unverfälschte Messergebnisse und eine schnelle Reaktion der Regeleinrichtung auf Abweichungen von Istwerten von Sollwerten.By the characterizing feature of
Weitere Merkmale der Erfindung sind in den Unteransprüchen enthalten.Further features of the invention are contained in the subclaims.
Die Erfindung ist besonders vorteilhaft in Verbindung mit einer Gegenelektrode, welche an ein Potential angeschlossen ist, das zum Hochspannungspotential der Hochspannungselektrode eine große elektrische Spannungsdifferenz hat, z. B. an Erdpotential angeschlossen ist, um freie elektrische Teilchen, insbesondere Ionen und Elektronen, abzuleiten, welche von der Hochspannunselektrode ausströmen, jedoch frei herumvagabundieren, anstatt mit dem Sprühbeschichtungsmaterial von der Sprühvorrichtung auf das zu beschichtende Objekt zu fliegen. Gegenelektroden sind z. B. aus der
Die Erfindung wird im folgenden mit Bezug auf die Zeichnungen anhand von einer bevorzugten Ausführungsform als Beispiel beschrieben. In den Zeichnungen zeigen:
- Fig. 1
- schematisch eine Sprühbeschichtungseinrichtung nach der Erfindung,
- Fig. 2
- ein Hochspannungs-Sprühstrom-Diagramm der Sprühbeschichtungseinrichtung von Fig. 1,
- Fig. 3
- schematisch eine Sprühvorrichtung der Sprühbeschichtungseinrichtung von Fig. 1.
- Fig. 1
- schematically a spray coating device according to the invention,
- Fig. 2
- a high-voltage spray current diagram of the spray coating device of Fig. 1,
- Fig. 3
- 1 schematically shows a spray device of the spray coating device of FIG. 1.
Die in Fig. 1 schematisch gezeigte Sprühbeschichtungseinrichtung enthält eine Sprühvorrichtung 2 zum Besprühen von Beschichtungsmaterial 4 in Form von Flüssigkeit oder vorzugweise Pulver auf ein zu beschichtendes Objekt 6. Dabei wird angenommen, daß die zu beschichtenden Objekte aus elektrisch leitendem Material bestehen und an Erdpotential 8 angeschlossen sind. Die Objekte 6 werden bei automatischen Anlagen durch eine, nicht gezeigte, Fördervorrichtung an der Sprühvorrichtung 2 vorbei transportiert und gelangen dadurch in deren durch einen Pfeil schematisch dargestellten Sprühstrahl des Beschichtungsmaterials 4.The spray coating device shown schematically in Fig. 1 comprises a
Die Sprühvorrichtung 2 ist mit mindestens einer Hochspannungselektrode 10 zur elektrostatischen Aufladung des Beschichtungsmaterials 4 versehen, welche von einem Hochspannungserzeuger 12 mit Gleichstrom-Hochspannung im Bereich zwischen 1 kV und 150 kV, vorzugsweise einem dazwischen liegenden Wert, versorgt wird. Der Hochspannungserzeuger kann in bekannter Weise einen Transformator zur Hochtransformierung einer niedrigen Wechselspannung in eine höhere Wechselspannung und eine Kaskadenschaltung enthalten, welche in bekannter Weise eine Vielzahl von Gleichrichtern und Kondensatoren enthält und die Wechselspannung in die Gleichstrom-Hochspannung umwandelt.The
Die niedrige Wechselspannung wird von einem Oszillator 14 in Abhängigkeit von einer Steuerspannung U-ST erzeugt, welche eine Stellgröße für die Hochspannung der Hochspannungselektrode 10 ist.The low alternating voltage is generated by an
Der Oszillator 14 kann ein Teil des Hochspannungserzeugers 12 sein und als solcher in die Sprühvorrichtung 2 integriert sein, oder entsprechend Fig. 1 in ein Steuergerät integriert sein, welches insgesamt eine Regeleinrichtung 16 bildet.The
Die Regeleinrichtung 16 enthält einen Betriebsparameter-Speicher 18, welchem über einen Datentransferweg 19 von einer Dateneingabestation, beispielsweise einem übergeordneten Rechner oder manuell, z. B. über eine Tastatur, variabel einstellbar mindestens ein Hochspannungsbegrenzungswert HV-BG und mindestens ein Sprühstrombegrenzungswert I-BG je für den maximal erreichbaren Wert an der Hochspannungselektrode eingebbar und darin speicherbar sind. Vorzugsweise sind mehrere solcher Werte für verschiedene Betriebssituationen, insbesondere für verschiedene zu beschichtende Objekte und verschiedene Sprühbeschichtungsmaterialien speicherbar. Die gespeicherten Werte können bei einer anderen Ausführungsform nicht versellbare Festwerte sein.The
Der Hochspannungsbegrenzungswert HV-BG wird von dem Betriebsparameter-Speicher 18 in eine Hochspannungsbegrenzungsschaltung 20 eingegeben. Der Sprühstrombegrenzungswert I-BG wird von dem Betriebsparameter-Speicher 18 in einen Sprühstromregler 22 eingegeben.The high voltage limit value HV-BG is input from the
Der von einem zu beschichtenden Objekt 6 auf Erde fließende Sprühstrom der Hochspannungselektrode 10 wird von einer Sprühstrommesschaltung 24 auf der mit Erde 8 verbundenen Seite der Objekte 6 gemessen und als Sprühstrom-Istwert I-S ebenfalls in den Sprühstromregler eingegeben.The spraying current of the high-
Der Sprühstromregler 22 vergleicht den Sprühstrom-Istwert 1-S- mit dem Sprühstrombegrenzungswert I-BG und erzeugt in Abhängigkeit hiervon eine Hochspannungs-Reglergrößen U-RG, welcher von dem Sprühstromregler 22 an die Hochspannungsbegrenzungsschaltung 20 gegeben wird. Der Sprühstromregler 22 ist vorzugsweise ein P-I-Regler (proportional-integral-Regler).The spray
Die Hochspannungsbegrenzungsschaltung 20 erzeugt in Abhängigkeit von dem Hochgspannungsbegrenzungswert HV-BG und der Hochspannungs-Reglergröße U-RG die Steuerspannung U-ST, welche in Form einer Gleichstrom-Eingangsspannung dem Oszillator 14 zugeführt wird und die Stellgröße für die Hochspannung der Hochspannungselektrode 10 ist.The high
Die Hochspannungsbegrenzungsschaltung 20 bewirkt, daß für den Fall, daß die Hochspannungs-Reglergröße U-RG größer oder gleich dem Hochspannungsbegrenzungswert HV-BG ist, der Gleichspannungswert der Steuerspannung U-ST gleich dem Hochspannungsbegrenzungswert HV-BG ist. Ferner bewirkt die Hochspannungsbegrenzungsschaltung 20, daß in allen den Fällen, wo die Hochspannungs-Reglergröße U-RG kleiner als der Hochspannungsbegrenzungswert HV-BG ist, daß die Steuerspannung U-ST gleich der Hochspannungs-Reglergröße U-RG ist. Dies läßt sich wie folgt darstellen:
Fig. 2 zeigt auf der horizontalen Achse den Sprühstrom in µA und auf der vertikalen Achse die korrespondierende Hochspannung in kV. Die oberste Kennlinie 26 mit ausgefüllten Quadraten ist eine Standard-Kennlinie. Sie zeigt, wie bei bekannten Einrichtungen mit kleiner werdendem Abstand zwischen der Hochspannungselektrode 10 und einem zu beschichtenden Objekt 6 der Sprühstrom der Hochspannungselektrode 10 ansteigt und gleichzeitig die Hochspannung abfällt. Die Hochspannung hat ihren Maximalwert bei größtmöglichem Abstand bzw. unendlich großem Abstand des zu beschichtenden Objektes 6 oder einens anderen elektrisch leitenden Gegenstandes von der Hochspannungselektrode 10.FIG. 2 shows the spray current in μA on the horizontal axis and the corresponding high voltage in kV on the vertical axis. The
Die mittlere Kurve 27 mit den nicht-ausgefüllten Quadraten betrifft eine Ausführungsform, bei welcher die maxiamale Gleichstrom-Hochspannung der Hochspannungselektrode 10 auf einen Maximalwert HV-BG von 80 kV begrenzt ist, jedoch keine Strombegrenzung I-BG vorgenommen wurde.The
Die unterste Kurve 28 mit den schwarz ausgefüllten Dreiecken ergibt sich mit der vorstehend beschriebenen Schaltung nach der Erfindung, bei welcher. sowohl der Sprühstrom als auch die Hochspannung je auf einen Maxiamalwert begrenzt sind. In Fig. 2 wurde angenommen, daß der Hochspannungsbegrenzungswert HV-BG 50 kV und der Sprühstrombegrenzungswert I-BG 20 µA (20 x 10-6 A) ist.The
In Fig. 3 ist die Sprühvorrichtung 2 etwas detailierter dargestellt. Sie zeigt, daß eine oder mehrere Hochspannungselektroden 10 außerhalb oder innerhalb eines Beschichtungsmaterialkanals 30 angeordnet sein können. Ihm wird Beschichtungsmaterial, z. B. Beschichtungspulver, über eine Leitung 31, z. B. ein Schlauch, zugeführt.In Fig. 3, the
Gemäß Fig. 3 kann die Sprühvorrichtung 2 mit an ein Bezugspotential, z. B. Erdpotential, angschlossenen Gegenelektroden 32 (Ableiterelektroden) versehen sein, welche freie elektrische Ladungen (Ionen, Elektronen), welche von den Elektroden 10 abgegeben werden, auffangen und auf Erdpotential ableiten. Es hat sich gezeigt, daß durch die Erfindung wesentlich weniger freie elektrische Teilchen entstehen, insbesondere freie Ionen, und damit auch ein geringerer Stromverlust.According to Fig. 3, the
In Fig. 3 ist der Oszillator 14 über ein elektrisches Kabel 36 an den Hochspannungserzeuger 12 angeschlossen, welcher in die Sprühvorrichtung 2 integriert ist, jedoch auch getrennt von ihr, z. B. in der Regeleinrichtung 16 angeordnet werden könnte.In Fig. 3, the
Claims (6)
- Spray-coating apparatus for spraying coating material onto articles to be coated by means of a spray device (2), which device has at least one high-voltage electrode (10) for the electrical charging of the coating material by means of the high-voltage of a high-voltage generator (12); wherein the spray coating apparatus has the following: a regulating means (16) for regulating an electrical spray current which flows, together with the coating material, from the high-voltage electrode (10) to an object (6) to be coated, a spray-current measuring circuit (24) in the electrical return current path from the object (6) to be coated back into the regulating means (16), in order to measure the spray current automatically in the return current path and in order in dependence thereon to counteract a current rise by a voltage reduction by means of the regulating device, means (18, 20, 22) for current limitation and for high-voltage limitation to a predetermined value in each case, characterized in that the means (18, 20, 22) have a spray-current regulator (22) and a high-voltage limitation circuit (20), of which the spray-current regulator (22) compares the spray-current actual value I-S with a spray-current limiting value I-BG prescribed to it and, in dependence on the result of the comparison, issues a high-voltage regulator variable U-RG to the high-voltage limitation circuit (20), and of which the high-voltage limitation circuit (20) generates a control voltage U-ST in dependence on the high-voltage regulator variable U-RG and in dependence on a high-voltage limitation value HV-BG prescribed to it, which control voltage is a manipulated variable for the high voltage of the high-voltage electrode (10), wherein the high-voltage limitation circuit (20) is formed in such a way that it has the effect that, in the event that the high-voltage regulator variable U-RG is greater than or equal to the high-voltage limitation value HV-BG, the voltage value of the control voltage U-ST is equal to the high-voltage limitation value HV-BG, and also has the effect that, in all the cases in which the high-voltage regulator variable U-RG is less than the high-voltage limitation value HV-BG, the control voltage U-ST is equal to the high-voltage regulator variable U-RG.
- Spray-coating apparatus according to Claim 1, characterized in that the return current path is connected to earth potential (8).
- Spray-coating apparatus according to Claim 1 or 2, characterized in that the current limiting value and/or the high-voltage limiting value can be variably adjusted.
- Spray-coating apparatus according to one of the preceding claims, characterized in that a memory (18) is provided for storing in each case at least one current limiting value (I-BG) and one high-voltage limiting value (HV-BG), the value being variably adjustable.
- Spray-coating apparatus according to one of the preceding claims, characterized in that an oscillator (14) is provided and, in dependence on the control voltage U-ST, generates a low alternating voltage, from which the high-voltage generator (12) generates the high voltage.
- Spray-coating apparatus according to one of the preceding claims, characterized in that at least one counterelectrode (32), which is connected to a potential differing sharply from the electrical potential of the high-voltage electrode (10), is provided on the spray device (2) at a distance from the high-voltage electrode (10), outside the stream of coating material, for the diversion of free ions and free electrons which are generated by the high-voltage electrode (10), but do not fly, together with the coating material, onto the object to be coated.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19926926 | 1999-06-14 | ||
DE19926926A DE19926926A1 (en) | 1999-06-14 | 1999-06-14 | Spray coating device |
Publications (3)
Publication Number | Publication Date |
---|---|
EP1060795A2 EP1060795A2 (en) | 2000-12-20 |
EP1060795A3 EP1060795A3 (en) | 2003-05-21 |
EP1060795B1 true EP1060795B1 (en) | 2007-11-07 |
Family
ID=7911088
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP00110032A Expired - Lifetime EP1060795B1 (en) | 1999-06-14 | 2000-05-12 | Control for an electrostatic spray coating apparatus |
Country Status (8)
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US (2) | US6537378B1 (en) |
EP (1) | EP1060795B1 (en) |
JP (1) | JP4638976B2 (en) |
AT (1) | ATE377453T1 (en) |
CA (1) | CA2311210C (en) |
DE (2) | DE19926926A1 (en) |
DK (1) | DK1060795T3 (en) |
ES (1) | ES2294985T3 (en) |
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DE19738142C1 (en) * | 1997-09-01 | 1999-05-20 | Wagner Int | Electrostatic coating system and method for detecting and coating workpieces in an electrostatic coating system |
US5972417A (en) * | 1997-11-14 | 1999-10-26 | Nordson Corporation | Spray gun power supply monitor |
US6047431A (en) | 1997-11-21 | 2000-04-11 | Olympus America Inc. | Methods and apparatus for cleaning channels |
-
1999
- 1999-06-14 DE DE19926926A patent/DE19926926A1/en not_active Withdrawn
-
2000
- 2000-05-12 DK DK00110032T patent/DK1060795T3/en active
- 2000-05-12 ES ES00110032T patent/ES2294985T3/en not_active Expired - Lifetime
- 2000-05-12 DE DE50014755T patent/DE50014755D1/en not_active Expired - Lifetime
- 2000-05-12 EP EP00110032A patent/EP1060795B1/en not_active Expired - Lifetime
- 2000-05-12 AT AT00110032T patent/ATE377453T1/en active
- 2000-06-13 US US09/593,297 patent/US6537378B1/en not_active Expired - Lifetime
- 2000-06-13 CA CA002311210A patent/CA2311210C/en not_active Expired - Fee Related
- 2000-06-14 JP JP2000178380A patent/JP4638976B2/en not_active Expired - Fee Related
-
2002
- 2002-12-09 US US10/314,356 patent/US6656536B2/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
CA2311210A1 (en) | 2000-12-14 |
US6656536B2 (en) | 2003-12-02 |
ES2294985T3 (en) | 2008-04-16 |
DK1060795T3 (en) | 2008-02-11 |
ATE377453T1 (en) | 2007-11-15 |
JP4638976B2 (en) | 2011-02-23 |
US6537378B1 (en) | 2003-03-25 |
EP1060795A2 (en) | 2000-12-20 |
DE19926926A1 (en) | 2000-12-21 |
JP2001025688A (en) | 2001-01-30 |
EP1060795A3 (en) | 2003-05-21 |
DE50014755D1 (en) | 2007-12-20 |
CA2311210C (en) | 2005-08-09 |
US20030064167A1 (en) | 2003-04-03 |
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