EP0887318A1 - Method and apparatus for fusing an optical fiber preform - Google Patents

Method and apparatus for fusing an optical fiber preform Download PDF

Info

Publication number
EP0887318A1
EP0887318A1 EP98305070A EP98305070A EP0887318A1 EP 0887318 A1 EP0887318 A1 EP 0887318A1 EP 98305070 A EP98305070 A EP 98305070A EP 98305070 A EP98305070 A EP 98305070A EP 0887318 A1 EP0887318 A1 EP 0887318A1
Authority
EP
European Patent Office
Prior art keywords
preform
fusing
oxidative gas
optical fiber
burner
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP98305070A
Other languages
German (de)
French (fr)
Other versions
EP0887318B1 (en
Inventor
Shinji c/o Shin-Etsu Chemicals Co. Ltd. Suzuki
Hideo c/o Shin-Etsu Chemicals Co. Ltd. Hirasawa
Tadakatsu Shin-Etsu Chemicals Co. Ltd. Shimada
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shin Etsu Chemical Co Ltd
Original Assignee
Shin Etsu Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shin Etsu Chemical Co Ltd filed Critical Shin Etsu Chemical Co Ltd
Publication of EP0887318A1 publication Critical patent/EP0887318A1/en
Application granted granted Critical
Publication of EP0887318B1 publication Critical patent/EP0887318B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B29/00Reheating glass products for softening or fusing their surfaces; Fire-polishing; Fusing of margins
    • C03B29/04Reheating glass products for softening or fusing their surfaces; Fire-polishing; Fusing of margins in a continuous way
    • C03B29/14Reheating glass products for softening or fusing their surfaces; Fire-polishing; Fusing of margins in a continuous way with vertical displacement of the products
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B29/00Reheating glass products for softening or fusing their surfaces; Fire-polishing; Fusing of margins
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments
    • C03B37/01205Manufacture of preforms for drawing fibres or filaments starting from tubes, rods, fibres or filaments

Definitions

  • This invention relates to method and apparatus for making an optical fiber preform, and more particularly, to improved method and apparatus for making an optical fiber preform wherein when a large-sized mother ingot for optical fiber is thermally drawn along a vertical direction and is fused to continuously obtain rods with a tapered portion at opposite sides thereof, deposition of a so-called silica cloud generated in the course of the fusing can be well prevented.
  • An optical fiber preform is obtained by drawing an ingot to have a given diameter depending on a fiber drawing machine used. If the ingot has a bend, such a bend is corrected during the course of the drawing. Thereafter, a dammy glass is welded to the preform at opposite sides thereof, followed by drawing by use of a fiber drawing machine.
  • the optical fiber made of silica glass and flawed in the surfaces thereof becomes very embrittled. Accordingly, if an optical fiber is flawed at the time of the fiber drawing of an optical fiber preform, strength lowers.
  • fire polishing has been usually effected wherein after finishing with a given diameter, an optical fiber preform is exposed to a weak flame to remove foreign matters from the outer surfaces thereof.
  • silica glass when a preform is heated until its surface temperature arrives at about 2000°C, part of the silica glass sublimates into SiO. This SiO combines with moisture present in a surrounding atmosphere and converts again to glass fine particles, followed by re-deposition on the surfaces of the preform. It is also known that when silica glass is fused by means of a flame, a so-called silica cloud appears just outside the strongly heated portion. This cloud has the possibility of flawing the fiber surfaces at the time of the fiber drawing. Thus, it is necessary that the cloud be removed prior to the fiber drawing. The cloud may be removed by slowly heating the rod with a relatively weak flame.
  • the heating of the preform may become inadequate depending on the amounts of gases used and the moving speed of a burner. This leads to a great strain being left in the preform, with the great possibility that only a slight degree of impact applied to the preform results in cracking.
  • a residual strain becomes small, but with the re ⁇ appearance of a band ⁇ shaped cloud.
  • a method for fusing an optical fiber preform which is obtained by drawing a large-sized mother ingot along a vertical direction under heating conditions and subsequently fusing the resultant preform by use of a fusingburner in the form of a preform piece having a tapered portion at opposite sides thereof wherein the preform is fused while blowing an oxygen gas from upper and lower sides relative to the fusing burner whereby a silica cloud is prevented from deposition on the tapered portion of the preform piece.
  • an apparatus for fusing an optical fiber preform which comprises a drawing unit having a rotary chuck, a feeding means, an electric furnace, and a drawing chuck, and a fusing unit associated in connection with the drawing unit and having a fusing burner and a fusion chuck, wherein the fusing unit includes a plurality of nozzles located above and below the fusing burner unit and capable of blowing an oxidative gas against a preform being fused at an angle, ⁇ , of the blowing relative to the length of the preform, which is in the range of 20° ⁇ 60°.
  • FIG. 1 there is shown an apparatus A of manufacturing a preform.
  • the apparatus A includes a drawing unit D and a fusing unit F.
  • the drawing unit D has a rotary chuck 1, a feed mechanism 2, an electric furnace 3, and a drawing chuck 4 as shown.
  • the fusing mechanism F includes fusing burners 5, a chuck 6, and nozzles 7 for preventing deposition of a silica cloud.
  • an ingot 8 made of silica glass is fixedly attached to the rotary chuck 1 and fed to the electric furnace 3 by means of the feed mechanism 2 at a feed rate V 1 .
  • the ingot is heated and softened, under which it is drawn by movement of the drawing chuck 4 at a take-up rate V 2 .
  • the resultant preform 9 being moved at the rate of V 2 is fused to a given length by means of a fusing chuck 6 at a fusing rate V 3 to obtain a product rod.
  • the fusing burners 5 and the nozzles 7 are both moved at the rate of V 2 , which is equal to the take-up rate, while blowing an oxidative gas against the preform being drawn.
  • the rates V 1 , V 2 and V 3 should be so set that V 2 >V 1 and V 3 >V 2 .
  • Fig. 2 is a view showing the detail of the fusing unit F of the apparatus A, with which the preform 9 is fused into product rods having a given length.
  • two fusing burners are located in face-to-face relation via the preform 9, and four nozzles 7 are each arranged at a preset angle, ⁇ , between the flow of an oxidative gas and the preform being drawn.
  • This angle should be in the range of 20° ⁇ 60°. If this blowing angle is less than 20°, the nozzles may contact the preform being rotated in view of the structural arrangement of the apparatus.
  • the angle exceeds 60°, a greater amount of a gas used to the blowing may be necessary for attaining a deposition-preventing effect similar to that attained at the defined angle.
  • the sublimation of silica glass proceeds rapidly in a reductive atmosphere.
  • the sublimation of SiO can be suppressed when a heating atmosphere consists of an oxidative gas.
  • the oxidative gas used in the practice of the invention includes oxygen, air, or an oxygen-rich oxyhydrogen flame.
  • the amount of a gas being blown against the preform is in the range of 1/5 to 1/2 of the amount of a gas supplied to the fusing burner. If the amount is smaller, a satisfactory deposition preventing effect may not be expected. On the other hand, if the amount is in excess, the burner flame may be undesirably disturbed, causing the preform to be heated unsatisfactorily.
  • the invention is more particularly described by way of examples.
  • an ingot having an outer diameter of 150 mm was attached to a rotary chuck, and drawn into a preform having an outer diameter of 60 mm at a feed rate of V 1 , of 20 mm/minute, a take-up rate, V 2 , of 125 mm/minute, and a fusing chuck take-up rate, V 3 , of 150 mm.
  • Two fusing burners of a fusing unit were arranged and opposed at an angle of 180°, and two small-size gas burner nozzles were, respectively, set at upper and lower positions relative to the fusing burners so that two burner nozzles at each position were opposed at an angle of 180°, with an angle of blowing against the preform being at 50°.
  • H 2 and O 2 gases were fed to the fusing burners at rates of 400 liters/minute of H 2 and 230 liters/minute of O 2 .
  • 150 liters/minute of O 2 was fed to each burner nozzle.
  • the resultant preform pieces had a length of about 1000 mm and an outer diameter of 60 mm, on which no silica cloud was deposited. Thus, any finishing fire polishing was not necessary, resulting in the significant reduction of time. Moreover, a residual strain was slightly observed, but at a level of no problem.
  • Example 1 The general procedure of Example 1 was repeated using the same drawing conditions as in Example 1, except that H 2 and O 2 were passed to the fusing burners at rates of 400 liters/minute and 230 liters/minute, respectively, and air was passed t the respective small-size gas burner nozzles at a rate of 150 liters/minute and blown against the preform at a blowing angle of 30°. As a result, no silica deposition was found on the resultant preform products having an outer diameter of 60 mm, with similar results as in Example 1.
  • Example 1 The general procedure of Example 1 was repeated using the same drawing conditions as in Example 1, except that H 2 and O 2 were passed to the fusing burners at rates of 400 liters/minute and 230 liters/minute, respectively, and an oxyhydrogen flame in an oxygen-rich condition was blown against the preform at a blowing angle of 30° while passing 100 liters/minute of H 2 and 60 liters/minute of O 2 to each small-size gas burner nozzle. As a result, no deposition of silica cloud was found on preform products having an outer diameter of 60 mm, with similar results as in Example 1. Moreover, no residual strain was found in the products.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacturing & Machinery (AREA)
  • Manufacture, Treatment Of Glass Fibers (AREA)
  • Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)
  • Glass Melting And Manufacturing (AREA)
  • Gas Burners (AREA)

Abstract

A method for fusing an optical fiber perform comprises fusing the preform while blowing an oxidative gas against the preform to be fused from upper and lower directions of a fusing burner unit. An apparatus for carrying out the method includes a plurality of nozzles for preventing deposition of silica cloud, which are each set at an angle, , of blowing the oxidative gas relative to the preform being drawn such 20°≤≤60°.

Description

This invention relates to method and apparatus for making an optical fiber preform, and more particularly, to improved method and apparatus for making an optical fiber preform wherein when a large-sized mother ingot for optical fiber is thermally drawn along a vertical direction and is fused to continuously obtain rods with a tapered portion at opposite sides thereof, deposition of a so-called silica cloud generated in the course of the fusing can be well prevented.
An optical fiber preform is obtained by drawing an ingot to have a given diameter depending on a fiber drawing machine used. If the ingot has a bend, such a bend is corrected during the course of the drawing. Thereafter, a dammy glass is welded to the preform at opposite sides thereof, followed by drawing by use of a fiber drawing machine. The optical fiber made of silica glass and flawed in the surfaces thereof becomes very embrittled. Accordingly, if an optical fiber is flawed at the time of the fiber drawing of an optical fiber preform, strength lowers. For the purpose of suppressing the occurrence of flaws, fire polishing has been usually effected wherein after finishing with a given diameter, an optical fiber preform is exposed to a weak flame to remove foreign matters from the outer surfaces thereof.
As is known in the art, when a preform is heated until its surface temperature arrives at about 2000°C, part of the silica glass sublimates into SiO. This SiO combines with moisture present in a surrounding atmosphere and converts again to glass fine particles, followed by re-deposition on the surfaces of the preform. It is also known that when silica glass is fused by means of a flame, a so-called silica cloud appears just outside the strongly heated portion. This cloud has the possibility of flawing the fiber surfaces at the time of the fiber drawing. Thus, it is necessary that the cloud be removed prior to the fiber drawing. The cloud may be removed by slowly heating the rod with a relatively weak flame. In this connection, however, the heating of the preform may become inadequate depending on the amounts of gases used and the moving speed of a burner. This leads to a great strain being left in the preform, with the great possibility that only a slight degree of impact applied to the preform results in cracking. On the other hand, when the preform is heated to an extent greater than required, a residual strain becomes small, but with the re·appearance of a band·shaped cloud.
To avoid this, it is usual to measure a residual strain by use of a strain gauge and determine fire polishing conditions in such a way that gas conditions and burner moving speed conditions, under which a residual strain is at a level involving no problem therein, and also gas conditions and burner moving speed conditions, which are determined by appearance inspection, are determined by trial and error. As a matter of course, these conditions differ depending on the diameter of a preform and the nature of individual burner. Accordingly, the work for determining these conditions has, in fact, required much labor and time. In addition, in view of the results of the determination of these conditions, it is required that in order not to cause any cloud to develop, a relatively weak flame be used so that the surface temperature of a preform is not raised and that in order to make a small residual strain, the moving speed of a burner be low sufficient to permit heat to be satisfactorily transmitted to the inside of a preform. These requirements need much time. More particularly, to fuse a preform by a conventional manner allows a silica cloud to be deposited and once again requires fire polishing at a final stage. The work of determining the final-stage fire polishing further requires much time and labor.
It is therefore an aim of the invention to provide a method for fusing an optical fiber preform while reducing or preventing deposition of a silica cloud generated at the time of heating the preform in a fusing step of a continuous process of manufacturing preform rods with a tapered portion at opposite sides thereof by drawing a large-sized mother ingot in an electric furnace in a vertical direction and subsequently fusing the drawn preform.
It in another aim of the invention to provide an apparatus for fusing an optical fiber preform whereby a silica cloud deposited on a tapered portion at opposite sides of preforms can be reduced or prevented.
According to one embodiment of the invention, there is provided a method for fusing an optical fiber preform which is obtained by drawing a large-sized mother ingot along a vertical direction under heating conditions and subsequently fusing the resultant preform by use of a fusingburner in the form of a preform piece having a tapered portion at opposite sides thereof wherein the preform is fused while blowing an oxygen gas from upper and lower sides relative to the fusing burner whereby a silica cloud is prevented from deposition on the tapered portion of the preform piece.
According to another embodiment of the invention, there is also provided an apparatus for fusing an optical fiber preform, which comprises a drawing unit having a rotary chuck, a feeding means, an electric furnace, and a drawing chuck, and a fusing unit associated in connection with the drawing unit and having a fusing burner and a fusion chuck, wherein the fusing unit includes a plurality of nozzles located above and below the fusing burner unit and capable of blowing an oxidative gas against a preform being fused at an angle, , of the blowing relative to the length of the preform, which is in the range of 20°≤≤60°.
The invention will be described below with reference to an exemplary embodiment and the accompanying drawings, in which:-
  • Fig. 1 is a schematic longitudinal sectional view illustrating an apparatus of fusing an optical fiber preform according to the invention; and
  • Fig. 2 is a schematic, enlarged, longitudinal sectional view showing a fusing unit of the apparatus of Fig. 1.
  • Reference is now made to the accompanying drawings and particularly, to Fig. 1. In Fig. 1, there is shown an apparatus A of manufacturing a preform. The apparatus A includes a drawing unit D and a fusing unit F. The drawing unit D has a rotary chuck 1, a feed mechanism 2, an electric furnace 3, and a drawing chuck 4 as shown. The fusing mechanism F includes fusing burners 5, a chuck 6, and nozzles 7 for preventing deposition of a silica cloud.
    In operation, an ingot 8 made of silica glass is fixedly attached to the rotary chuck 1 and fed to the electric furnace 3 by means of the feed mechanism 2 at a feed rate V1. In the furnace 3, the ingot is heated and softened, under which it is drawn by movement of the drawing chuck 4 at a take-up rate V2. The resultant preform 9 being moved at the rate of V2 is fused to a given length by means of a fusing chuck 6 at a fusing rate V3 to obtain a product rod. At this time, the fusing burners 5 and the nozzles 7 are both moved at the rate of V2, which is equal to the take-up rate, while blowing an oxidative gas against the preform being drawn. The rates V1, V2 and V3 should be so set that V2>V1 and V3>V2.
    Fig. 2 is a view showing the detail of the fusing unit F of the apparatus A, with which the preform 9 is fused into product rods having a given length. As will be seen from the figure, two fusing burners are located in face-to-face relation via the preform 9, and four nozzles 7 are each arranged at a preset angle, , between the flow of an oxidative gas and the preform being drawn. This angle should be in the range of 20°≤≤60°. If this blowing angle is less than 20°, the nozzles may contact the preform being rotated in view of the structural arrangement of the apparatus. On the other hand, when the angle exceeds 60°, a greater amount of a gas used to the blowing may be necessary for attaining a deposition-preventing effect similar to that attained at the defined angle.
    It is known that the sublimation of silica glass proceeds rapidly in a reductive atmosphere. In contrast, the sublimation of SiO can be suppressed when a heating atmosphere consists of an oxidative gas. Examples of the oxidative gas used in the practice of the invention includes oxygen, air, or an oxygen-rich oxyhydrogen flame. The amount of a gas being blown against the preform is in the range of 1/5 to 1/2 of the amount of a gas supplied to the fusing burner. If the amount is smaller, a satisfactory deposition preventing effect may not be expected. On the other hand, if the amount is in excess, the burner flame may be undesirably disturbed, causing the preform to be heated unsatisfactorily.
    It will be noted that smaller-size burners may be used as the nozzles.
    In the method of the invention wherein product rods having a tapered portion at opposite sides thereof can be continuously manufactured by thermally drawing, into a preform, a large-sized silica glass ingot 8 having an outer diameter, for example, of 100 to 300 mm in a electric furnace 3 in a vertical direction, and subsequently fused, an oxidative gas is blown against the preform from upper and lower directions of fusing burners 5. As described before, when the surface temperature of the preform arrives at about 2000°C, part of the silica glass is sublimated into SiO. This SiO combines with moisture in a surrounding atmosphere and redeposited on the preform surface in the form of fine particles of silica. To avoid this, an oxidative gas is blown against the preform from upper and lower directions of the burner flame to blow the SiO off. Thus, the re-deposition of glass fine particles is prevented.
    The invention is more particularly described by way of examples.
    Example 1
    Using an apparatus of the type shown in Fig. 1, an ingot having an outer diameter of 150 mm was attached to a rotary chuck, and drawn into a preform having an outer diameter of 60 mm at a feed rate of V1, of 20 mm/minute, a take-up rate, V2, of 125 mm/minute, and a fusing chuck take-up rate, V3, of 150 mm. Two fusing burners of a fusing unit were arranged and opposed at an angle of 180°, and two small-size gas burner nozzles were, respectively, set at upper and lower positions relative to the fusing burners so that two burner nozzles at each position were opposed at an angle of 180°, with an angle of blowing against the preform being at 50°.
    H2 and O2 gases were fed to the fusing burners at rates of 400 liters/minute of H2 and 230 liters/minute of O2. For the prevention of silica deposition, 150 liters/minute of O2 was fed to each burner nozzle.
    The resultant preform pieces had a length of about 1000 mm and an outer diameter of 60 mm, on which no silica cloud was deposited. Thus, any finishing fire polishing was not necessary, resulting in the significant reduction of time. Moreover, a residual strain was slightly observed, but at a level of no problem.
    Example 2
    The general procedure of Example 1 was repeated using the same drawing conditions as in Example 1, except that H2 and O2 were passed to the fusing burners at rates of 400 liters/minute and 230 liters/minute, respectively, and air was passed t the respective small-size gas burner nozzles at a rate of 150 liters/minute and blown against the preform at a blowing angle of 30°. As a result, no silica deposition was found on the resultant preform products having an outer diameter of 60 mm, with similar results as in Example 1.
    Example 3
    The general procedure of Example 1 was repeated using the same drawing conditions as in Example 1, except that H2 and O2 were passed to the fusing burners at rates of 400 liters/minute and 230 liters/minute, respectively, and an oxyhydrogen flame in an oxygen-rich condition was blown against the preform at a blowing angle of 30° while passing 100 liters/minute of H2 and 60 liters/minute of O2 to each small-size gas burner nozzle. As a result, no deposition of silica cloud was found on preform products having an outer diameter of 60 mm, with similar results as in Example 1. Moreover, no residual strain was found in the products.

    Claims (11)

    1. A method of fusing an optical fiber preform which is obtained by drawing a large-sized mother ingot along a vertical direction under heating conditions and subsequently fusing the resultant preform into piece products having a tapered portion at opposite sides thereof wherein the preform is fused while blowing an oxidative gas from upper and lower directions of a fusing burner unit whereby a silica cloud is prevented from deposition on the tapered portions of the preform piece products.
    2. A method according to Claim 1, wherein said oxidative gas is blown against said preform at a blow angle, , of 20°≤≤60° relative to the preform being passed.
    3. A method according to Claim 2, wherein said oxidative gas consists essentially of oxygen.
    4. A method according to Claim 2, wherein said oxidative gas consists essentially of air.
    5. A method according to Claim 2, wherein said oxidative gas consists essentially of an oxyhydrogen flame in an oxygen-rich condition.
    6. A method according to any one of claims 1 to 5, wherein said oxidative gas is blown by use of a plurality of burner nozzles.
    7. A method according to any one of the preceding claims, wherein said oxidative gas is fed at a rate of 1/5 to 1/2 of a flow rate of a gas mixture fed to said gas burner unit.
    8. A method according to any one of the preceding claims, wherein when an ingot feed rate is taken as V1, a preform take-up rate as V2, and a fusing rate as V3, V2>V1 and V3>V2.
    9. An apparatus for fusing an optical fiber preform, which comprises a drawing unit having a rotary chuck, a feeding means for feeding a mother ingot, an electric furnace, and a drawing chuck, and a fusing unit associated with said drawing unit and having a fusing burner unit and a fusing chuck, wherein said fusing unit includes a plurality of nozzles located above and below said fusing burner unit and capable of blowing an oxidative gas against a preform being drawn at a blow angle, , relative to the length of the preform being passed, which is in the range of 20°≤≤60°.
    10. An apparatus according to Claim 9, wherein said plurality of nozzles are each comprised of a small-size burner.
    11. A method of manufacturing an optical fiber or a device including optical fibers, the method including fusing an optical fiber preform according to the method of any one of claims 1 to 8.
    EP19980305070 1997-06-27 1998-06-26 Method and apparatus for separating an optical fiber preform by fusion Expired - Lifetime EP0887318B1 (en)

    Applications Claiming Priority (2)

    Application Number Priority Date Filing Date Title
    JP17143997A JP3274821B2 (en) 1997-06-27 1997-06-27 Method and apparatus for cutting optical fiber preform
    JP171439/97 1997-06-27

    Publications (2)

    Publication Number Publication Date
    EP0887318A1 true EP0887318A1 (en) 1998-12-30
    EP0887318B1 EP0887318B1 (en) 2006-09-27

    Family

    ID=15923151

    Family Applications (1)

    Application Number Title Priority Date Filing Date
    EP19980305070 Expired - Lifetime EP0887318B1 (en) 1997-06-27 1998-06-26 Method and apparatus for separating an optical fiber preform by fusion

    Country Status (3)

    Country Link
    EP (1) EP0887318B1 (en)
    JP (1) JP3274821B2 (en)
    DE (1) DE69835982T2 (en)

    Cited By (2)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    EP1065174A1 (en) * 1999-07-01 2001-01-03 Alcatel Plasma burner, method for making an optical preform and apparatus used therefor
    WO2021123738A1 (en) * 2019-12-17 2021-06-24 Lumenisity Limited Method for processing glass filament

    Families Citing this family (2)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    DE102013101328B3 (en) * 2013-02-11 2014-02-13 Heraeus Quarzglas Gmbh & Co. Kg Blank made of TiO2-SiO2 glass for a mirror substrate for use in EUV lithography and method for its production
    EP3683195A1 (en) * 2019-01-15 2020-07-22 Heraeus Quartz North America LLC Automated large outside diameter preform tipping process

    Citations (6)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    FR2589461A1 (en) * 1985-10-31 1987-05-07 Fibres Optiques Ind Process for the manufacture of drawn components based on silica and components obtained
    EP0432791A1 (en) * 1989-12-15 1991-06-19 Sumitomo Electric Industries, Ltd. Method for heating glass body
    EP0519479A2 (en) * 1991-06-20 1992-12-23 Sumitomo Electric Industries, Ltd Method for flame abrasion of glass preform
    EP0525681A1 (en) * 1991-07-26 1993-02-03 Sumitomo Electric Industries, Ltd Method of flame abrasion of glass preform
    EP0612700A1 (en) * 1993-02-22 1994-08-31 Sumitomo Electric Industries, Ltd Method for flame abrasion glass preform
    GB2307907A (en) * 1995-12-06 1997-06-11 Sumitomo Electric Industries A method for elongating a glass preform

    Patent Citations (6)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    FR2589461A1 (en) * 1985-10-31 1987-05-07 Fibres Optiques Ind Process for the manufacture of drawn components based on silica and components obtained
    EP0432791A1 (en) * 1989-12-15 1991-06-19 Sumitomo Electric Industries, Ltd. Method for heating glass body
    EP0519479A2 (en) * 1991-06-20 1992-12-23 Sumitomo Electric Industries, Ltd Method for flame abrasion of glass preform
    EP0525681A1 (en) * 1991-07-26 1993-02-03 Sumitomo Electric Industries, Ltd Method of flame abrasion of glass preform
    EP0612700A1 (en) * 1993-02-22 1994-08-31 Sumitomo Electric Industries, Ltd Method for flame abrasion glass preform
    GB2307907A (en) * 1995-12-06 1997-06-11 Sumitomo Electric Industries A method for elongating a glass preform

    Cited By (5)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    EP1065174A1 (en) * 1999-07-01 2001-01-03 Alcatel Plasma burner, method for making an optical preform and apparatus used therefor
    FR2795715A1 (en) * 1999-07-01 2001-01-05 Cit Alcatel PROCESS FOR GLAZING THE EXTERNAL SURFACE OF AN OPTICAL FIBER PREFORM AND INSTALLATION FOR PRODUCING PREFORMS USING THE SAME
    US7121120B2 (en) 1999-07-01 2006-10-17 Alcatel Method of glazing an optical fiber preform with a plasma of reduced power
    WO2021123738A1 (en) * 2019-12-17 2021-06-24 Lumenisity Limited Method for processing glass filament
    CN114829312A (en) * 2019-12-17 2022-07-29 鲁曼斯蒂有限公司 Method for processing glass filaments

    Also Published As

    Publication number Publication date
    EP0887318B1 (en) 2006-09-27
    JP3274821B2 (en) 2002-04-15
    JPH1111972A (en) 1999-01-19
    DE69835982D1 (en) 2006-11-09
    DE69835982T2 (en) 2007-05-10

    Similar Documents

    Publication Publication Date Title
    US4682003A (en) Laser beam glass cutting
    US7797965B2 (en) Method for producing tubes of quartz glass
    US20020152772A1 (en) Optical fiber manufacture method, preform manufacture method, and preform manufacture apparatus
    EP0111545B1 (en) Methods of and apparatus for straightening and configuring a preform tube from which lightguide fiber is drawn
    EP1440946B1 (en) Method and apparatus for processing a preform for an optical fibre using a burner
    US6532776B1 (en) Method and apparatus for fusing an optical fiber preform
    WO2005092807A1 (en) Method and apparatus for processing glass matrix for optical fiber
    US5979189A (en) Method of separating and glazing an optical fiber preform
    EP0887318B1 (en) Method and apparatus for separating an optical fiber preform by fusion
    WO2005049514A1 (en) Method and device for connecting optical fiber matrix and optical fiber
    WO2007039426A1 (en) Welding method for joining components consisting of a high-silica material, and apparatus for performing the method
    US5211730A (en) Method for heating glass body
    EP0432791B1 (en) Method for heating glass body
    US5922098A (en) Cleaning a glass preform with a high temperature inert gas during the drawing of an optical fiber
    CN114804612A (en) Method and apparatus for elongating glass base material
    TWI399349B (en) Method of fiber base material and fiber base material
    JP2960716B2 (en) Drawing method and drawing apparatus for optical fiber preform
    JP4377483B2 (en) Optical fiber preform and method for processing optical fiber preform
    JP2000128562A (en) Drawing apparatus for optical fiber preform
    US8613208B2 (en) Method for forming an improved weld between a primary preform and a silica bar
    JP3418679B2 (en) Apparatus and method for processing optical fiber preform
    CN111770903A (en) Device for impact orientation of tubular preform of optical fiber body
    JPS61122130A (en) Processing of fused quartz article
    JP2000072467A (en) Elongating device for optical fiber preform and elongating method therefor

    Legal Events

    Date Code Title Description
    PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

    Free format text: ORIGINAL CODE: 0009012

    AK Designated contracting states

    Kind code of ref document: A1

    Designated state(s): DE FR GB

    AX Request for extension of the european patent

    Free format text: AL;LT;LV;MK;RO;SI

    17P Request for examination filed

    Effective date: 19990421

    AKX Designation fees paid

    Free format text: DE FR GB

    17Q First examination report despatched

    Effective date: 20010522

    RTI1 Title (correction)

    Free format text: METHOD AND APPARATUS FOR SEPARATING AN OPTICAL FIBER PREFORM BY FUSION

    GRAP Despatch of communication of intention to grant a patent

    Free format text: ORIGINAL CODE: EPIDOSNIGR1

    GRAS Grant fee paid

    Free format text: ORIGINAL CODE: EPIDOSNIGR3

    GRAA (expected) grant

    Free format text: ORIGINAL CODE: 0009210

    AK Designated contracting states

    Kind code of ref document: B1

    Designated state(s): DE FR GB

    REG Reference to a national code

    Ref country code: GB

    Ref legal event code: FG4D

    REF Corresponds to:

    Ref document number: 69835982

    Country of ref document: DE

    Date of ref document: 20061109

    Kind code of ref document: P

    ET Fr: translation filed
    PLBE No opposition filed within time limit

    Free format text: ORIGINAL CODE: 0009261

    STAA Information on the status of an ep patent application or granted ep patent

    Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

    26N No opposition filed

    Effective date: 20070628

    PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

    Ref country code: GB

    Payment date: 20080702

    Year of fee payment: 11

    GBPC Gb: european patent ceased through non-payment of renewal fee

    Effective date: 20090626

    PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

    Ref country code: GB

    Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

    Effective date: 20090626

    PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

    Ref country code: FR

    Payment date: 20100709

    Year of fee payment: 13

    PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

    Ref country code: DE

    Payment date: 20100625

    Year of fee payment: 13

    REG Reference to a national code

    Ref country code: FR

    Ref legal event code: ST

    Effective date: 20120229

    REG Reference to a national code

    Ref country code: DE

    Ref legal event code: R119

    Ref document number: 69835982

    Country of ref document: DE

    Effective date: 20120103

    PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

    Ref country code: FR

    Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

    Effective date: 20110630

    Ref country code: DE

    Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

    Effective date: 20120103