EP0674764A1 - Determination des caracteristiques de moteurs a combustion interne par mesure optique de plusieurs grandeurs dans la chambre de combustion - Google Patents
Determination des caracteristiques de moteurs a combustion interne par mesure optique de plusieurs grandeurs dans la chambre de combustionInfo
- Publication number
- EP0674764A1 EP0674764A1 EP94918283A EP94918283A EP0674764A1 EP 0674764 A1 EP0674764 A1 EP 0674764A1 EP 94918283 A EP94918283 A EP 94918283A EP 94918283 A EP94918283 A EP 94918283A EP 0674764 A1 EP0674764 A1 EP 0674764A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- raman
- quantities
- measured
- laser
- combustion chamber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000002485 combustion reaction Methods 0.000 title claims abstract description 35
- 238000005259 measurement Methods 0.000 title claims abstract description 32
- 230000003287 optical effect Effects 0.000 title claims description 11
- 238000012512 characterization method Methods 0.000 title claims description 3
- 239000007789 gas Substances 0.000 claims abstract description 54
- 238000001069 Raman spectroscopy Methods 0.000 claims abstract description 37
- 238000000034 method Methods 0.000 claims abstract description 24
- 239000000446 fuel Substances 0.000 claims abstract description 21
- 239000000203 mixture Substances 0.000 claims abstract description 20
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 4
- 230000002452 interceptive effect Effects 0.000 claims abstract description 4
- 239000001301 oxygen Substances 0.000 claims abstract description 4
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 4
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract 2
- 239000002245 particle Substances 0.000 claims description 17
- 230000010287 polarization Effects 0.000 claims description 12
- 238000002347 injection Methods 0.000 claims description 5
- 239000007924 injection Substances 0.000 claims description 5
- 238000005457 optimization Methods 0.000 claims description 5
- 230000001364 causal effect Effects 0.000 claims description 3
- 238000005033 Fourier transform infrared spectroscopy Methods 0.000 claims description 2
- 238000004847 absorption spectroscopy Methods 0.000 claims description 2
- 239000003344 environmental pollutant Substances 0.000 claims description 2
- 231100000719 pollutant Toxicity 0.000 claims description 2
- 229910001868 water Inorganic materials 0.000 abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 6
- 230000008569 process Effects 0.000 abstract description 5
- 238000004458 analytical method Methods 0.000 abstract description 3
- 230000005284 excitation Effects 0.000 abstract description 3
- 238000000926 separation method Methods 0.000 abstract description 3
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 125000004122 cyclic group Chemical group 0.000 abstract 1
- 238000009532 heart rate measurement Methods 0.000 abstract 1
- 238000011144 upstream manufacturing Methods 0.000 abstract 1
- 238000010521 absorption reaction Methods 0.000 description 9
- 230000000694 effects Effects 0.000 description 5
- 239000000700 radioactive tracer Substances 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- 238000001514 detection method Methods 0.000 description 2
- 238000000691 measurement method Methods 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 230000003595 spectral effect Effects 0.000 description 2
- 230000002745 absorbent Effects 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 239000003570 air Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000000295 emission spectrum Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J5/00—Radiation pyrometry, e.g. infrared or optical thermometry
- G01J5/60—Radiation pyrometry, e.g. infrared or optical thermometry using determination of colour temperature
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02B—INTERNAL-COMBUSTION PISTON ENGINES; COMBUSTION ENGINES IN GENERAL
- F02B77/00—Component parts, details or accessories, not otherwise provided for
- F02B77/08—Safety, indicating, or supervising devices
- F02B77/085—Safety, indicating, or supervising devices with sensors measuring combustion processes, e.g. knocking, pressure, ionization, combustion flame
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
- G01M15/00—Testing of engines
- G01M15/04—Testing internal-combustion engines
- G01M15/10—Testing internal-combustion engines by monitoring exhaust gases or combustion flame
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02F—CYLINDERS, PISTONS OR CASINGS, FOR COMBUSTION ENGINES; ARRANGEMENTS OF SEALINGS IN COMBUSTION ENGINES
- F02F7/00—Casings, e.g. crankcases or frames
- F02F7/0085—Materials for constructing engines or their parts
- F02F2007/0092—Transparent materials
Definitions
- the measurements can also be averaged over different cycles. In this case - without knowing the individual fluctuations - it can be determined at which average values of stoichiometry and exhaust gas content the engine works.
- the influence for example, of the influence of different injection variants, the load or the ignition timing on the gas mixture before ignition and the power output can be determined.
- the measurement of the amounts of air, fuel and the amount of the remaining exhaust gas fraction is carried out according to the patented method using optical measurement technology.
- Raman scattering One of the methods is Raman scattering. It is well known that Raman scattering can be used to measure the density of majority species (Eckbreth: Laser Diagnostics for Combustion: Temperature and Species. AEGupta, DG Liley eds. Vol. 7 of Energy and Engineering Sciences, Abacus Press Cambridge, MA 1988). However, due to the relatively weak intensity of the Raman scattering and the simultaneous occurrence of other light phenomena caused by the laser, it is difficult (I) to obtain enough signal to distinguish the small cyclical fluctuations and (II) to distinguish the Raman emission from the other emissions. It is well known that the use of Raman scattering - e.g. in the combustion of hydrocarbons - is significantly restricted in accuracy by these other emissions (see Eckbreth).
- the background can be determined in an analogous manner - without rotating the electrical vector of the laser light - by analyzing the emission in the direction of observation for polarization components (for example using polarization filters). Again the one delivers
- the analysis of polarized emissions is important and patent-relevant, since it allows the differentiation of the emissions and thus a selective measurement of the individual gas components in gas mixtures with a complex composition.
- the high intensity of the Raman scattering is important and relevant to the patent because it makes the measuring precision so high that the cyclical fluctuations in the gas composition that actually occur can be measured.
- the density of the particles - integrated over locations along the absorption light path - in the combustion chamber is determined by the decrease in the incident light.
- the "direct" absorption by the naturally present molecules or the absorption by tracer can be used.
- the water density (for determining the residual gas content) and the fuel density e.g. can be determined via IR absorption.
- the oxygen content can e.g. can be determined via the absorption in the deep UV (e.g. Schumann Runge bands).
- Another absorption technique results from the selective addition of substances ("tracers").
- a tracer e.g. acetone
- the density of the tracer e.g. the acetone density
- the fuel density can be determined.
- other absorbent molecules can be added to the air to measure the air density.
- the residual gas content in the fresh charge can also be determined by injecting a tracer into the combustion chamber at the time of gas discharge (e.g. in the area of top dead center). The stoichiometry and the residual gas content can in turn be determined from the data on fuel, air and residual gas by forming the ratio.
- the particle densities can also be determined by adding tracers that can be excited to glow with lasers (laser-induced emissions). So you can add different tracers to the fuel, air and residual gas and select the excitation wavelength of the laser and the emission wavelengths so that one
- REPLACEMENT LEAF spectral separation of the emissions is possible and thus the components are detected simultaneously.
- the density of fuel, air and residual gas can then be determined from the intensity of the laser-induced emissions, and the stoichiometry and the residual gas content can be determined by forming the ratio.
- Pollutants can be determined under which conditions the engine works and whether
- Power output on the Z-axis shows the dependence of the power output on stoichiometry and the proportion of exhaust gas. This comparison of cause and effect gives a direct one
- the amount of exhaust gas in the engine combustion chamber from the previous cycle can be determined from the ratio of H2O / N2 (since the amount of water in the air supplied is negligible) or from the ratio O2 N2.
- the simultaneous, precise acquisition of various measured variables makes it possible to determine causal relationships in individual combustion cycles and thereby characterize the operating conditions of the engine and use the knowledge as a basis for optimization.
- the simultaneous measurement of the stoichiometry and the proportion of exhaust gas in a certain measurement volume before the ignition simultaneously with the recording of the pressure curve for the current combustion cycle may be mentioned as an example.
- REPLACEMENT LEAF Measurement makes it possible to link the cause (mixture composition before ignition) with the effect (power output). By simultaneously measuring other variables (e.g. NO density via LIF, temperatures, ...) in the same cycle, further statements about cause and effect can be made. It is also essential for the present invention that the small fluctuations in the mixture composition can be detected precisely enough before ignition.
- 0.2 lies, i.e. e.g. that with an externally set ⁇ number of 1.0, the measured ⁇ number fluctuates between 0.9 and 1.1.
- Fig. 2 shows the results of measurements which, in addition to stoichiometry, also show the additional influence of the exhaust gas content. The picture shows the maximum pressure reached as a function of the stoichiometry and the proportion of exhaust gas and is referred to here as a map. Obviously, larger proportions of exhaust gas lead to lower pressures and thus less power output.
- the map which is here for the way the Mc> works, depends on the way the engine works. It can be used to differentiate between different ways of working.
- the pressure curve of the previous cycle also provides important information e.g. about the history of gas exchange in the combustion chamber. If e.g. the pressure in the previous cycle was high, you can find it in the following cycle - for a certain operating condition -
- the measurements can also be averaged over different cycles if the signal in the single shot does not provide enough intensity.
- the small fluctuations in the stoichiometry and in the exhaust gas are eliminated, so that in a representation as in Fig. 3 the fluctuations become much smaller and reproducible characteristic data are obtained.
- S is the sensitivity of the measuring system for the detection of particles i. S is in principle to be determined separately for each particle type and each location,
- REPLACEMENT LEAF is assumed to be constant here for the sake of simplicity. The following applies to the relative measurement of the densities of the particles i, j:
- FIG. 4 A specific arrangement for measuring is shown in Fig. 4 as one example from many.
- the intense pulsed UV laser beam (1) is shot through the combustion chamber of an engine.
- UV-transmitting windows (2) are used in the upper part.
- part of the intake manifold with the injection valve (5) is also shown in cross section. From a section
- the scattered Raman light is directed via a window in the bulb (6) and a deflecting mirror (7) to the spatially resolving optical multi-channel analyzer (8).
- An imaging optical system (9) images the laser beam axis (16) on the slit (10) of a spectrograph. This usually consists of several mirrors (11) and a dispersion grating (12). In the spectrograph, the different emissions are separated by wavelength (along the axis (14)) and detected with an intensified, short-opening CCD camera (13).
- the structure also enables a local assignment of the Raman emission along the section from the combustion chamber along the axis (15).
- the Rochon prism can be used for separation to determine the polarization of the different emissions. Except for the polarization analysis, the arrangement described is usually referred to with the keyword "locally resolved optical multi-channel analyzer".
- Fig.6 shows another realization of the measuring technique, the backscattering.
- the optical access to the motor is only realized through small windows (17) on the side.
- One of the windows (17) through which the laser exits the combustion chamber in Fig. 6 can optionally be dispensed with.
- the laser (1) is coupled into the combustion chamber via a dichroic mirror (18).
- the Raman emission - and also other emissions - are coupled out via one of the windows on the side (17) and in turn detected using an optical multi-channel analyzer (see Fig. 5) - and a polarization analyzer (8). In this case, (somewhat) local resolution may also be obtained in the medium if the window is extended in one direction.
- the measurement can also be carried out with other spectral filters and other polarization analyzers.
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- General Physics & Mathematics (AREA)
- Combustion & Propulsion (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
Abstract
Le fonctionnement de moteurs à combustion interne dépend dans une large mesure de grandeurs que l'on ne peut régler suffisamment précisément depuis l'extérieur, ainsi, par exemple, la st÷chiométrie du mélange carburant-air avant l'allumage, la proportion de gaz d'échappement contenus dans ce mélange gazeux et sa température. A cet égard, la mesure la plus simultanée et la plus précise possible de plusieurs de ces grandeurs dans la chambre de combustion est très utile pour comprendre les problèmes relatifs au fonctionnement du moteur. Le nouveau procédé de diffusion de lumière laser avec effet Raman permet par exemple de résoudre ce problème. Le procédé est sans contact et offre une résolution élevée dans le temps (c'est-à-dire par rapport à l'angle de vilebrequin) et en fonction de la position. On utilise comme source lumineuse d'excitation pour la diffusion par effet Raman et Rayleigh, des lasers à U.V. pulsés intensifs. La lumière laser (1) parvient dans la partie supérieure de la chambre de combustion, notamment pour analyser le gaz de queue avant l'allumage, en passant par une fenêtre (17) pratiquée dans la paroi du cylindre où s'effectue la mesure. Les émissions induites par laser (notamment diffusion par effet Raman et Rayleigh) peuvent être conduites à l'extérieur de la chambre de combustion de différentes manières, par exemple par l'intermédiaire de la même fenêtre (17) et d'un miroir (18) dichroïque. La mesure quantitative simultanée des différentes émissions, notamment des émissions par effet Raman de carburant, d'oxygène, d'azote, d'eau, etc., s'effectue par le biais des caméras ultra-rapides (CCD) à fonctionnement intensifié, en combinaison avec un système de séparation de longueur d'ondes (spectromètre) (8) monté en amont, ce qui permet d'obtenir également une résolution locale le long d'un axe de la chambre de combustion. La longueur d'ondes d'excitation dans les U.V. permet de procéder à des mesures extrêmement précises par impulsions individuelles de manière à pouvoir résoudre les légères variations cycliques intervenant dans la formation du mélange (et la combustion) dans le moteur. De plus, dans de nombreux cas, il est nécessaire de séparer les émissions par effet Raman des émissions (fluorescentes) qui interfèrent. Les propriétés de polarisation permettent d'y parvenir. Les grandeurs significatives en matière de combustion, comme la st÷chiométrie et la proportion de gaz d'échappement sont obtenues par calcul du rapport des intensités Raman, ce qui permet d'obtenir une précision de mesure particulièrement élevée.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19934320943 DE4320943C2 (de) | 1993-06-24 | 1993-06-24 | Verfahren zur Charakterisierung der Arbeitsweise von Verbrennungsmotoren durch Messen der Gaszusammensetzung im Brennraum durch Raman-Spektroskopie |
DE4320943 | 1993-06-24 | ||
PCT/DE1994/000696 WO1995000833A1 (fr) | 1993-06-24 | 1994-06-22 | Determination des caracteristiques de moteurs a combustion interne par mesure optique de plusieurs grandeurs dans la chambre de combustion |
Publications (1)
Publication Number | Publication Date |
---|---|
EP0674764A1 true EP0674764A1 (fr) | 1995-10-04 |
Family
ID=6491083
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP94918283A Withdrawn EP0674764A1 (fr) | 1993-06-24 | 1994-06-22 | Determination des caracteristiques de moteurs a combustion interne par mesure optique de plusieurs grandeurs dans la chambre de combustion |
Country Status (3)
Country | Link |
---|---|
EP (1) | EP0674764A1 (fr) |
DE (1) | DE4320943C2 (fr) |
WO (1) | WO1995000833A1 (fr) |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19809792C2 (de) * | 1998-03-09 | 2000-03-30 | Fraunhofer Ges Forschung | Vorrichtung zur Messung der Emission und/oder Absorption eines heißen Gases oder Plasmas |
DE19924284B4 (de) * | 1998-05-30 | 2004-12-09 | Christoph Nailis | Verfahren zur Messung eines Luft-Brennstoff-Verhältnisses in einem Brennraum |
DE19827533C2 (de) * | 1998-06-20 | 2001-09-06 | Alfred Leipertz | Verfahren zur Bestimmung der Dampfphasenzusammensetzung und der Temperatur mittels linearer Raman-Streuung in Gegenwart von Phasengrenzflächen, insbesondere von Tröpfchen, insbesondere bei motorischen Einspritzprozessen |
DE19925583C2 (de) | 1999-06-04 | 2002-06-13 | Lavision Gmbh | Verfahren zur Bestimmung der räumlichen Konzentration der einzelnen Komponenten eines Gemisches, insbes. eines Gasgemisches in einem Brennraum, insbes. eines Motors sowie eine Anordnung zur Durchführung des Verfahrens |
FR2816056B1 (fr) * | 2000-11-02 | 2003-05-16 | Centre Nat Rech Scient | Dispositif de mesure de richesse d'une combustion et procede afferent de reglage |
DE10124235B4 (de) * | 2001-05-18 | 2004-08-12 | Esytec Energie- Und Systemtechnik Gmbh | Verfahren und Vorrichtung zur umfassenden Charakterisierung und Kontrolle des Abgases und der Regelung von Motoren, speziell von Verbrennungsmotoren, und von Komponenten der Abgasnachbehandlung |
US6803563B2 (en) | 2002-08-02 | 2004-10-12 | Flender Service Gmbh | Method and apparatus for monitoring the quality of lubricant |
DE10235612B4 (de) * | 2002-08-02 | 2012-06-21 | Siemens Aktiengesellschaft | Verfahren und Vorrichtung zur Überwachung der Qualität von Schmieröl |
DE102004057718B4 (de) * | 2004-11-26 | 2006-08-03 | Iav Gmbh Ingenieurgesellschaft Auto Und Verkehr | Vorrichtung zur Analyse von Strömungsvorgängen in der Kolbenmulde einer Brennkraftmaschine |
DE102004057609B4 (de) * | 2004-11-29 | 2006-10-19 | Lavision Gmbh | Vorrichtung zur Ermittlung von laserinduzierter Emission elektromagnetischer Strahlung von in einem Hohlkörper befindlichen Gasen, Fluiden und Gemischen hieraus |
DE102005012776B4 (de) * | 2005-03-19 | 2020-07-02 | Bayerische Motoren Werke Aktiengesellschaft | Verfahren und Vorrichtung zur Identfikation von gasdynamischen Effekten |
DE102006043700A1 (de) * | 2006-09-18 | 2008-03-27 | Siemens Ag | Abtastung von Brennraumsignalen |
DE102006057783B3 (de) * | 2006-12-06 | 2008-05-08 | Technische Universität München | Anordnung und Verfahren zur optischen Überwachung eines Druckraums bzw. einer Brennkammer |
DE102006058285B4 (de) * | 2006-12-08 | 2009-04-16 | Technische Universität München | Druckkammer und Verfahren zu deren optischer Überwachung |
DE102007060905B4 (de) * | 2007-12-14 | 2010-05-27 | Smetec Gmbh | Verfahren zur Ermittlung des lokalen Luftverhältnisses |
SE535798C2 (sv) | 2011-03-08 | 2012-12-27 | Vattenfall Ab | Förfarande och system för gasmätning i förbränningskammare |
WO2014071016A1 (fr) * | 2012-10-31 | 2014-05-08 | The Regents Of The University Of Michigan | Spectroscopie à métaux alcalins pour imagerie de paramètres dans une chambre de combustion d'un moteur à combustion interne |
CN104236917B (zh) * | 2014-09-05 | 2017-02-08 | 北京动力机械研究所 | 全环微小尺寸回流燃烧室试验器 |
DE102014221862A1 (de) | 2014-10-27 | 2016-04-28 | Robert Bosch Gmbh | Einrichtung zur optischen Überwachung eines Druckraumes oder einer Brennkammer, insbesondere eines Verbrennungsmotors |
DE102022208770A1 (de) | 2022-08-24 | 2024-02-29 | Hochschule Reutlingen, Körperschaft des öffentlichen Rechts | Vorrichtung zum Erfassen von mindestens einer gasförmigen Komponente in einem Gas |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5882039A (ja) * | 1981-11-11 | 1983-05-17 | Hitachi Ltd | 内燃機関用空気燃料比制御装置 |
DE4127712C2 (de) * | 1991-08-22 | 1993-10-07 | Kernforschungsz Karlsruhe | Laser-Raman-Meßzelle |
-
1993
- 1993-06-24 DE DE19934320943 patent/DE4320943C2/de not_active Expired - Fee Related
-
1994
- 1994-06-22 WO PCT/DE1994/000696 patent/WO1995000833A1/fr not_active Application Discontinuation
- 1994-06-22 EP EP94918283A patent/EP0674764A1/fr not_active Withdrawn
Non-Patent Citations (1)
Title |
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See references of WO9500833A1 * |
Also Published As
Publication number | Publication date |
---|---|
DE4320943C2 (de) | 2001-02-15 |
WO1995000833A1 (fr) | 1995-01-05 |
DE4320943A1 (de) | 1995-01-05 |
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