DEL0017318MA - - Google Patents

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Publication number

DEL0017318MA

DEL0017318MA DEL0017318MA DE L0017318M A DEL0017318M A DE L0017318MA DE L0017318M A DEL0017318M A DE L0017318MA

Authority

DE

Germany

Prior art keywords

hydrofluoric acid

diazonium

boiling

fluoronitrobenzenes

nitroaniline

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 22
• 239000012954 diazonium Substances 0.000 claims description 5
• 238000006243 chemical reaction Methods 0.000 claims description 4
• IJGRMHOSHXDMSA-UHFFFAOYSA-O diazynium Chemical compound [NH+]#N IJGRMHOSHXDMSA-UHFFFAOYSA-O 0.000 claims description 4
• 238000000034 method Methods 0.000 claims description 3
• 150000004812 organic fluorine compounds Chemical class 0.000 claims description 2
• 239000000126 substance Substances 0.000 claims 1
• 238000009835 boiling Methods 0.000 description 9
• IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
• TYMLOMAKGOJONV-UHFFFAOYSA-N 4-nitroaniline Chemical compound NC1=CC=C([N+]([O-])=O)C=C1 TYMLOMAKGOJONV-UHFFFAOYSA-N 0.000 description 3
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
• WFQDTOYDVUWQMS-UHFFFAOYSA-N 1-fluoro-4-nitrobenzene Chemical compound [O-][N+](=O)C1=CC=C(F)C=C1 WFQDTOYDVUWQMS-UHFFFAOYSA-N 0.000 description 2
• ICMFHHGKLRTCBM-UHFFFAOYSA-N 4-nitrobenzenediazonium Chemical compound [O-][N+](=O)C1=CC=C([N+]#N)C=C1 ICMFHHGKLRTCBM-UHFFFAOYSA-N 0.000 description 2
• KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 2
• 239000004327 boric acid Substances 0.000 description 2
• 238000004519 manufacturing process Methods 0.000 description 2
• VBEGHXKAFSLLGE-UHFFFAOYSA-N n-phenylnitramide Chemical class [O-][N+](=O)NC1=CC=CC=C1 VBEGHXKAFSLLGE-UHFFFAOYSA-N 0.000 description 2
• 229910052757 nitrogen Inorganic materials 0.000 description 2
• KMRSVJOEUGWWBX-UHFFFAOYSA-M 2-nitrobenzenediazonium;chloride Chemical compound [Cl-].[O-][N+](=O)C1=CC=CC=C1[N+]#N KMRSVJOEUGWWBX-UHFFFAOYSA-M 0.000 description 1
• 239000010425 asbestos Substances 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 238000000354 decomposition reaction Methods 0.000 description 1
• 150000001989 diazonium salts Chemical class 0.000 description 1
• 238000006193 diazotization reaction Methods 0.000 description 1
• 238000006266 etherification reaction Methods 0.000 description 1
• 239000000203 mixture Substances 0.000 description 1
• QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
• 238000010992 reflux Methods 0.000 description 1
• 229910052895 riebeckite Inorganic materials 0.000 description 1
• 238000001256 steam distillation Methods 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1