DE69803067D1 - VERFAHREN ZUR HERSTELLUNG VON GaN KRISTALLEN MIT HOHEM WIDERSTAND - Google Patents

VERFAHREN ZUR HERSTELLUNG VON GaN KRISTALLEN MIT HOHEM WIDERSTAND

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Publication number
DE69803067D1
DE69803067D1 DE69803067T DE69803067T DE69803067D1 DE 69803067 D1 DE69803067 D1 DE 69803067D1 DE 69803067 T DE69803067 T DE 69803067T DE 69803067 T DE69803067 T DE 69803067T DE 69803067 D1 DE69803067 D1 DE 69803067D1
Authority
DE
Germany
Prior art keywords
high resistance
gan crystals
producing gan
metals
concentration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69803067T
Other languages
English (en)
Other versions
DE69803067T2 (de
Inventor
Boleslaw Lucznik
Tadeusz Suski
Miroslaw Wroblewski
Sylwester Porowski
Michal Bockowski
Izabella Grzegory
Stanislaw Krukowski
Michal Leszczynski
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CT BADAN WYSOKOCISNIENIOWYCH P
Original Assignee
CT BADAN WYSOKOCISNIENIOWYCH P
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CT BADAN WYSOKOCISNIENIOWYCH P filed Critical CT BADAN WYSOKOCISNIENIOWYCH P
Application granted granted Critical
Publication of DE69803067D1 publication Critical patent/DE69803067D1/de
Publication of DE69803067T2 publication Critical patent/DE69803067T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B9/00—Single-crystal growth from melt solutions using molten solvents
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B11/00—Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10—Inorganic compounds or compositions
    • C30B29/40—AIIIBV compounds wherein A is B, Al, Ga, In or Tl and B is N, P, As, Sb or Bi
    • C30B29/403—AIII-nitrides
    • C30B29/406—Gallium nitride
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S117/00—Single-crystal, oriented-crystal, and epitaxy growth processes; non-coating apparatus therefor
    • Y10S117/906—Special atmosphere other than vacuum or inert
    • Y10S117/907—Refluxing atmosphere
DE69803067T 1997-06-05 1998-06-03 VERFAHREN ZUR HERSTELLUNG VON GaN KRISTALLEN MIT HOHEM WIDERSTAND Expired - Lifetime DE69803067T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
PL97320392A PL186905B1 (pl) 1997-06-05 1997-06-05 Sposób wytwarzania wysokooporowych kryształów objętościowych GaN
PCT/PL1998/000023 WO1998055671A1 (en) 1997-06-05 1998-06-03 THE METHOD OF FABRICATION OF HIGHLY RESISTIVE GaN BULK CRYSTALS

Publications (2)

Publication Number Publication Date
DE69803067D1 true DE69803067D1 (de) 2002-01-31
DE69803067T2 DE69803067T2 (de) 2002-07-18

Family

ID=20070025

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69803067T Expired - Lifetime DE69803067T2 (de) 1997-06-05 1998-06-03 VERFAHREN ZUR HERSTELLUNG VON GaN KRISTALLEN MIT HOHEM WIDERSTAND

Country Status (7)

Country Link
US (1) US6273948B1 (de)
EP (1) EP0986655B1 (de)
JP (1) JP4198762B2 (de)
AT (1) ATE211189T1 (de)
DE (1) DE69803067T2 (de)
PL (1) PL186905B1 (de)
WO (1) WO1998055671A1 (de)

Families Citing this family (76)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5679152A (en) * 1994-01-27 1997-10-21 Advanced Technology Materials, Inc. Method of making a single crystals Ga*N article
FR2796657B1 (fr) * 1999-07-20 2001-10-26 Thomson Csf Procede de synthese de materiaux massifs monocristallins en nitrures d'elements de la colonne iii du tableau de la classification periodique
US6447604B1 (en) 2000-03-13 2002-09-10 Advanced Technology Materials, Inc. Method for achieving improved epitaxy quality (surface texture and defect density) on free-standing (aluminum, indium, gallium) nitride ((al,in,ga)n) substrates for opto-electronic and electronic devices
AU2002219966A1 (en) 2000-11-30 2002-06-11 North Carolina State University Methods and apparatus for producing m'n based materials
AU2002235146A1 (en) 2000-11-30 2002-06-11 North Carolina State University Non-thermionic sputter material transport device, methods of use, and materials produced thereby
AU2002328130B2 (en) * 2001-06-06 2008-05-29 Ammono Sp. Z O.O. Process and apparatus for obtaining bulk monocrystalline gallium-containing nitride
PL207400B1 (pl) 2001-06-06 2010-12-31 Ammono Społka Z Ograniczoną Odpowiedzialnością Sposób i urządzenie do otrzymywania objętościowego monokryształu azotku zawierającego gal
CA2464083C (en) 2001-10-26 2011-08-02 Ammono Sp. Z O.O. Substrate for epitaxy
KR100679387B1 (ko) 2001-10-26 2007-02-05 암모노 에스피. 제트오. 오. 질화물 반도체 레이저 소자 및 이의 제조방법
JP3910047B2 (ja) * 2001-11-20 2007-04-25 松下電器産業株式会社 半導体記憶装置
US7125453B2 (en) 2002-01-31 2006-10-24 General Electric Company High temperature high pressure capsule for processing materials in supercritical fluids
US7063741B2 (en) 2002-03-27 2006-06-20 General Electric Company High pressure high temperature growth of crystalline group III metal nitrides
EP1514958B1 (de) 2002-05-17 2014-05-14 Ammono S.A. Vorrichtung zur herstellung von volumeneinkristallen unter einsatz von überkritischem ammoniak
WO2004003261A1 (en) * 2002-06-26 2004-01-08 Ammono Sp. Z O.O. Process for obtaining of bulk monocrystallline gallium-containing nitride
TWI334890B (en) * 2002-12-11 2010-12-21 Ammono Sp Zoo Process for obtaining bulk mono-crystalline gallium-containing nitride, eliminating impurities from the obtained crystal and manufacturing substrates made of bulk mono-crystalline gallium-containing nitride
US7101433B2 (en) * 2002-12-18 2006-09-05 General Electric Company High pressure/high temperature apparatus with improved temperature control for crystal growth
US20060169996A1 (en) * 2002-12-27 2006-08-03 General Electric Company Crystalline composition, wafer, and semi-conductor structure
US7786503B2 (en) * 2002-12-27 2010-08-31 Momentive Performance Materials Inc. Gallium nitride crystals and wafers and method of making
US8089097B2 (en) * 2002-12-27 2012-01-03 Momentive Performance Materials Inc. Homoepitaxial gallium-nitride-based electronic devices and method for producing same
US7098487B2 (en) 2002-12-27 2006-08-29 General Electric Company Gallium nitride crystal and method of making same
US9279193B2 (en) 2002-12-27 2016-03-08 Momentive Performance Materials Inc. Method of making a gallium nitride crystalline composition having a low dislocation density
US8357945B2 (en) * 2002-12-27 2013-01-22 Momentive Performance Materials Inc. Gallium nitride crystal and method of making same
US7638815B2 (en) * 2002-12-27 2009-12-29 Momentive Performance Materials Inc. Crystalline composition, wafer, and semi-conductor structure
US7859008B2 (en) * 2002-12-27 2010-12-28 Momentive Performance Materials Inc. Crystalline composition, wafer, device, and associated method
US20070040181A1 (en) * 2002-12-27 2007-02-22 General Electric Company Crystalline composition, wafer, and semi-conductor structure
WO2004061923A1 (en) 2002-12-27 2004-07-22 General Electric Company Gallium nitride crystal, homoepitaxial gallium-nitride-based devices and method for producing same
US7170095B2 (en) * 2003-07-11 2007-01-30 Cree Inc. Semi-insulating GaN and method of making the same
US7009215B2 (en) * 2003-10-24 2006-03-07 General Electric Company Group III-nitride based resonant cavity light emitting devices fabricated on single crystal gallium nitride substrates
JP4489446B2 (ja) * 2004-01-21 2010-06-23 独立行政法人科学技術振興機構 ガリウム含有窒化物単結晶の製造方法
EP1740674A4 (de) * 2004-04-27 2009-09-09 Univ Arizona State Verfahren zur herstellung von hoch lumineszierend dotierten metallnitridpulvern
DE102004048453A1 (de) * 2004-10-05 2006-04-20 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Verfahren zur Erhöhung des Umsatzes von Gruppe-III-Metall zu Gruppe-III-Nitrid in einer Gruppe-III-haltigen Metallschmelze
DE102004050806A1 (de) * 2004-10-16 2006-11-16 Azzurro Semiconductors Ag Verfahren zur Herstellung von (AI,Ga)N Einkristallen
US7704324B2 (en) 2005-01-25 2010-04-27 General Electric Company Apparatus for processing materials in supercritical fluids and methods thereof
US7897490B2 (en) * 2005-12-12 2011-03-01 Kyma Technologies, Inc. Single crystal group III nitride articles and method of producing same by HVPE method incorporating a polycrystalline layer for yield enhancement
US7942970B2 (en) 2005-12-20 2011-05-17 Momentive Performance Materials Inc. Apparatus for making crystalline composition
WO2007083768A1 (ja) * 2006-01-20 2007-07-26 Matsushita Electric Industrial Co., Ltd. 半導体発光素子、ｉｉｉ族窒化物半導体基板、及びその製造方法
JP5187846B2 (ja) * 2006-03-23 2013-04-24 日本碍子株式会社 窒化物単結晶の製造方法および装置
US9909230B2 (en) 2006-04-07 2018-03-06 Sixpoint Materials, Inc. Seed selection and growth methods for reduced-crack group III nitride bulk crystals
US10161059B2 (en) 2006-04-07 2018-12-25 Sixpoint Materials, Inc. Group III nitride bulk crystals and their fabrication method
JP2007284267A (ja) * 2006-04-13 2007-11-01 Sumitomo Electric Ind Ltd ＧａＮ結晶の製造方法
US9157167B1 (en) 2008-06-05 2015-10-13 Soraa, Inc. High pressure apparatus and method for nitride crystal growth
US8097081B2 (en) 2008-06-05 2012-01-17 Soraa, Inc. High pressure apparatus and method for nitride crystal growth
US8871024B2 (en) * 2008-06-05 2014-10-28 Soraa, Inc. High pressure apparatus and method for nitride crystal growth
US9404197B2 (en) 2008-07-07 2016-08-02 Soraa, Inc. Large area, low-defect gallium-containing nitride crystals, method of making, and method of use
US10036099B2 (en) 2008-08-07 2018-07-31 Slt Technologies, Inc. Process for large-scale ammonothermal manufacturing of gallium nitride boules
US8979999B2 (en) 2008-08-07 2015-03-17 Soraa, Inc. Process for large-scale ammonothermal manufacturing of gallium nitride boules
US8878230B2 (en) 2010-03-11 2014-11-04 Soraa, Inc. Semi-insulating group III metal nitride and method of manufacture
US9543392B1 (en) 2008-12-12 2017-01-10 Soraa, Inc. Transparent group III metal nitride and method of manufacture
US20100147210A1 (en) * 2008-12-12 2010-06-17 Soraa, Inc. high pressure apparatus and method for nitride crystal growth
USRE47114E1 (en) 2008-12-12 2018-11-06 Slt Technologies, Inc. Polycrystalline group III metal nitride with getter and method of making
US9589792B2 (en) 2012-11-26 2017-03-07 Soraa, Inc. High quality group-III metal nitride crystals, methods of making, and methods of use
US8987156B2 (en) 2008-12-12 2015-03-24 Soraa, Inc. Polycrystalline group III metal nitride with getter and method of making
US9800017B1 (en) 2009-05-29 2017-10-24 Soraa Laser Diode, Inc. Laser device and method for a vehicle
US9250044B1 (en) 2009-05-29 2016-02-02 Soraa Laser Diode, Inc. Gallium and nitrogen containing laser diode dazzling devices and methods of use
US8509275B1 (en) 2009-05-29 2013-08-13 Soraa, Inc. Gallium nitride based laser dazzling device and method
US9175418B2 (en) 2009-10-09 2015-11-03 Soraa, Inc. Method for synthesis of high quality large area bulk gallium based crystals
US9564320B2 (en) 2010-06-18 2017-02-07 Soraa, Inc. Large area nitride crystal and method for making it
US8729559B2 (en) 2010-10-13 2014-05-20 Soraa, Inc. Method of making bulk InGaN substrates and devices thereon
US9694158B2 (en) 2011-10-21 2017-07-04 Ahmad Mohamad Slim Torque for incrementally advancing a catheter during right heart catheterization
US10029955B1 (en) 2011-10-24 2018-07-24 Slt Technologies, Inc. Capsule for high pressure, high temperature processing of materials and methods of use
US10145026B2 (en) 2012-06-04 2018-12-04 Slt Technologies, Inc. Process for large-scale ammonothermal manufacturing of semipolar gallium nitride boules
US9275912B1 (en) 2012-08-30 2016-03-01 Soraa, Inc. Method for quantification of extended defects in gallium-containing nitride crystals
US9299555B1 (en) 2012-09-28 2016-03-29 Soraa, Inc. Ultrapure mineralizers and methods for nitride crystal growth
US9650723B1 (en) 2013-04-11 2017-05-16 Soraa, Inc. Large area seed crystal for ammonothermal crystal growth and method of making
TWI638071B (zh) * 2013-08-08 2018-10-11 三菱化學股份有限公司 自立ＧａＮ基板、ＧａＮ結晶、ＧａＮ單結晶之製造方法及半導體裝置之製造方法
EP3146093A1 (de) 2014-05-23 2017-03-29 Sixpoint Materials, Inc. Gruppe-iii-nitrid-massenkristalle und deren herstellungsverfahren
US11437774B2 (en) 2015-08-19 2022-09-06 Kyocera Sld Laser, Inc. High-luminous flux laser-based white light source
US10174438B2 (en) 2017-03-30 2019-01-08 Slt Technologies, Inc. Apparatus for high pressure reaction
US11421843B2 (en) 2018-12-21 2022-08-23 Kyocera Sld Laser, Inc. Fiber-delivered laser-induced dynamic light system
US11239637B2 (en) 2018-12-21 2022-02-01 Kyocera Sld Laser, Inc. Fiber delivered laser induced white light system
US11466384B2 (en) 2019-01-08 2022-10-11 Slt Technologies, Inc. Method of forming a high quality group-III metal nitride boule or wafer using a patterned substrate
US11884202B2 (en) 2019-01-18 2024-01-30 Kyocera Sld Laser, Inc. Laser-based fiber-coupled white light system
CN110643934A (zh) * 2019-09-20 2020-01-03 深圳市晶相技术有限公司 一种半导体设备
US11721549B2 (en) 2020-02-11 2023-08-08 Slt Technologies, Inc. Large area group III nitride crystals and substrates, methods of making, and methods of use
WO2021162727A1 (en) 2020-02-11 2021-08-19 SLT Technologies, Inc Improved group iii nitride substrate, method of making, and method of use
CN116040966A (zh) * 2023-01-17 2023-05-02 东华大学 一种利用热高压强处理的玻璃化学强化方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2313976A1 (fr) 1975-06-13 1977-01-07 Labo Electronique Physique Procede de fabrication de monocristaux de nitrure de gallium et monocristaux obtenus par la mise en oeuvre de ce procede
PL173917B1 (pl) * 1993-08-10 1998-05-29 Ct Badan Wysokocisnieniowych P Sposób wytwarzania krystalicznej struktury wielowarstwowej
WO1997013891A1 (en) * 1995-10-13 1997-04-17 Centrum Badan Wysokocisnieniowych METHOD OF MANUFACTURING EPITAXIAL LAYERS OF GaN OR Ga(A1,In)N ON SINGLE CRYSTAL GaN AND MIXED Ga(A1,In)N SUBSTRATES
JP3876473B2 (ja) * 1996-06-04 2007-01-31 住友電気工業株式会社 窒化物単結晶及びその製造方法
JPH107496A (ja) * 1996-06-25 1998-01-13 Hitachi Cable Ltd 窒化物結晶の製造方法およびその装置

Also Published As

Publication number Publication date
JP4198762B2 (ja) 2008-12-17
WO1998055671A1 (en) 1998-12-10
JP2002513375A (ja) 2002-05-08
DE69803067T2 (de) 2002-07-18
EP0986655A1 (de) 2000-03-22
ATE211189T1 (de) 2002-01-15
US6273948B1 (en) 2001-08-14
PL320392A1 (en) 1998-12-07
PL186905B1 (pl) 2004-03-31
EP0986655B1 (de) 2001-12-19

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