DE2615632C2 - Verfahren und Vorrichtung zum Behandeln von Cellulose-Material mit Siliciumhalogeniden - Google Patents
Verfahren und Vorrichtung zum Behandeln von Cellulose-Material mit SiliciumhalogenidenInfo
- Publication number
- DE2615632C2 DE2615632C2 DE2615632A DE2615632A DE2615632C2 DE 2615632 C2 DE2615632 C2 DE 2615632C2 DE 2615632 A DE2615632 A DE 2615632A DE 2615632 A DE2615632 A DE 2615632A DE 2615632 C2 DE2615632 C2 DE 2615632C2
- Authority
- DE
- Germany
- Prior art keywords
- vapors
- treatment
- chamber
- silicon halide
- paper
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000463 material Substances 0.000 title claims description 63
- 238000000034 method Methods 0.000 title claims description 25
- 229910052710 silicon Inorganic materials 0.000 title claims description 23
- 239000010703 silicon Substances 0.000 title claims description 23
- -1 silicon halides Chemical class 0.000 title claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 229910000039 hydrogen halide Inorganic materials 0.000 claims description 19
- 239000012433 hydrogen halide Substances 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 18
- 239000005871 repellent Substances 0.000 claims description 14
- 229920002678 cellulose Polymers 0.000 claims description 11
- 239000001913 cellulose Substances 0.000 claims description 11
- 239000003517 fume Substances 0.000 claims description 5
- YGZSVWMBUCGDCV-UHFFFAOYSA-N chloro(methyl)silane Chemical compound C[SiH2]Cl YGZSVWMBUCGDCV-UHFFFAOYSA-N 0.000 claims description 4
- 238000007599 discharging Methods 0.000 claims 1
- 239000000123 paper Substances 0.000 description 28
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 25
- 229910000077 silane Inorganic materials 0.000 description 25
- 239000007789 gas Substances 0.000 description 17
- 239000000047 product Substances 0.000 description 14
- 238000006243 chemical reaction Methods 0.000 description 13
- 238000010586 diagram Methods 0.000 description 10
- 230000000717 retained effect Effects 0.000 description 10
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- 239000006227 byproduct Substances 0.000 description 9
- 230000015556 catabolic process Effects 0.000 description 9
- 238000006731 degradation reaction Methods 0.000 description 9
- 239000002253 acid Substances 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 238000000354 decomposition reaction Methods 0.000 description 6
- LIKFHECYJZWXFJ-UHFFFAOYSA-N dimethyldichlorosilane Chemical compound C[Si](C)(Cl)Cl LIKFHECYJZWXFJ-UHFFFAOYSA-N 0.000 description 5
- 239000002655 kraft paper Substances 0.000 description 5
- 239000005055 methyl trichlorosilane Substances 0.000 description 5
- JLUFWMXJHAVVNN-UHFFFAOYSA-N methyltrichlorosilane Chemical compound C[Si](Cl)(Cl)Cl JLUFWMXJHAVVNN-UHFFFAOYSA-N 0.000 description 5
- 239000000376 reactant Substances 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- KTQYJQFGNYHXMB-UHFFFAOYSA-N dichloro(methyl)silicon Chemical compound C[Si](Cl)Cl KTQYJQFGNYHXMB-UHFFFAOYSA-N 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000012442 inert solvent Substances 0.000 description 4
- 239000005048 methyldichlorosilane Substances 0.000 description 4
- 238000006386 neutralization reaction Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 150000004820 halides Chemical class 0.000 description 3
- 229910052736 halogen Inorganic materials 0.000 description 3
- 150000002367 halogens Chemical class 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- 239000012159 carrier gas Substances 0.000 description 2
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 150000004756 silanes Chemical class 0.000 description 2
- 241000251730 Chondrichthyes Species 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 238000010000 carbonizing Methods 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 229920001973 fluoroelastomer Polymers 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 230000002940 repellent Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000009864 tensile test Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/46—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/59—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paper (AREA)
- Materials Applied To Surfaces To Minimize Adherence Of Mist Or Water (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Sampling And Sample Adjustment (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US56622075A | 1975-04-09 | 1975-04-09 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2615632A1 DE2615632A1 (de) | 1976-10-28 |
| DE2615632C2 true DE2615632C2 (de) | 1986-01-30 |
Family
ID=24262002
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2615632A Expired DE2615632C2 (de) | 1975-04-09 | 1976-04-09 | Verfahren und Vorrichtung zum Behandeln von Cellulose-Material mit Siliciumhalogeniden |
Country Status (12)
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59216980A (ja) * | 1983-05-20 | 1984-12-07 | 株式会社クラレ | 制電性繊維構造物の製造方法 |
| CA2823754C (en) * | 2011-01-18 | 2018-07-03 | Dow Corning Corporation | Method for treating substrates with halosilanes |
| CN111005223B (zh) * | 2019-12-31 | 2022-05-27 | 四川文理学院 | 一种玄武岩纤维基超疏水材料的制备方法、其产品及应用 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB575696A (en) * | 1944-05-15 | 1946-02-28 | British Thomson Houston Co Ltd | Improvements in and relating to the treatment of materials to render them water repellent |
| GB845118A (en) * | 1957-02-15 | 1960-08-17 | Robbart Edward | Shrinkproofing cellulosic textile fabrics |
| GB845119A (en) * | 1957-02-15 | 1960-08-17 | Robbart Edward | A process of treating cellulosic textile fabrics with organo silicon halides |
-
1976
- 1976-03-31 DK DK152476A patent/DK152476A/da not_active IP Right Cessation
- 1976-04-02 CA CA249,465A patent/CA1106110A/en not_active Expired
- 1976-04-05 NO NO761155A patent/NO147844C/no unknown
- 1976-04-06 FR FR7609915A patent/FR2307078A1/fr active Granted
- 1976-04-07 IT IT22050/76A patent/IT1059616B/it active
- 1976-04-07 SE SE7604069A patent/SE416319B/sv not_active IP Right Cessation
- 1976-04-08 NL NL7603725A patent/NL7603725A/xx not_active Application Discontinuation
- 1976-04-09 JP JP51039430A patent/JPS51135888A/ja active Granted
- 1976-04-09 BE BE166007A patent/BE840578A/xx unknown
- 1976-04-09 GB GB14566/76A patent/GB1547293A/en not_active Expired
- 1976-04-09 FI FI760981A patent/FI60266C/fi not_active IP Right Cessation
- 1976-04-09 DE DE2615632A patent/DE2615632C2/de not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| NL7603725A (nl) | 1976-10-12 |
| NO147844B (no) | 1983-03-14 |
| SE7604069L (sv) | 1976-10-10 |
| NO761155L (enrdf_load_stackoverflow) | 1976-10-12 |
| FR2307078A1 (fr) | 1976-11-05 |
| FI760981A7 (enrdf_load_stackoverflow) | 1976-10-10 |
| FR2307078B1 (enrdf_load_stackoverflow) | 1980-06-13 |
| NO147844C (no) | 1983-06-22 |
| IT1059616B (it) | 1982-06-21 |
| JPS51135888A (en) | 1976-11-25 |
| BE840578A (fr) | 1976-08-02 |
| JPH0253559B2 (enrdf_load_stackoverflow) | 1990-11-19 |
| DE2615632A1 (de) | 1976-10-28 |
| FI60266B (fi) | 1981-08-31 |
| DK152476A (da) | 1976-10-10 |
| SE416319B (sv) | 1980-12-15 |
| FI60266C (fi) | 1981-12-10 |
| CA1106110A (en) | 1981-08-04 |
| GB1547293A (en) | 1979-06-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |