DE1795737C3 - 3-(p-Aminophenyl)-3-(3-indolyl)phthalide und ihre Anwendung in druckempfindlichem Aufzeichnungsmaterial - Google Patents
3-(p-Aminophenyl)-3-(3-indolyl)phthalide und ihre Anwendung in druckempfindlichem AufzeichnungsmaterialInfo
- Publication number
- DE1795737C3 DE1795737C3 DE1795737A DE1795737A DE1795737C3 DE 1795737 C3 DE1795737 C3 DE 1795737C3 DE 1795737 A DE1795737 A DE 1795737A DE 1795737 A DE1795737 A DE 1795737A DE 1795737 C3 DE1795737 C3 DE 1795737C3
- Authority
- DE
- Germany
- Prior art keywords
- ecm
- product
- benzene
- minutes
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B11/00—Diaryl- or thriarylmethane dyes
- C09B11/04—Diaryl- or thriarylmethane dyes derived from triarylmethanes, i.e. central C-atom is substituted by amino, cyano, alkyl
- C09B11/26—Triarylmethane dyes in which at least one of the aromatic nuclei is heterocyclic
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/124—Duplicating or marking methods; Sheet materials for use therein using pressure to make a masked colour visible, e.g. to make a coloured support visible, to create an opaque or transparent pattern, or to form colour by uniting colour-forming components
- B41M5/132—Chemical colour-forming components; Additives or binders therefor
- B41M5/136—Organic colour formers, e.g. leuco dyes
- B41M5/145—Organic colour formers, e.g. leuco dyes with a lactone or lactam ring
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B11/00—Diaryl- or thriarylmethane dyes
- C09B11/04—Diaryl- or thriarylmethane dyes derived from triarylmethanes, i.e. central C-atom is substituted by amino, cyano, alkyl
- C09B11/06—Hydroxy derivatives of triarylmethanes in which at least one OH group is bound to an aryl nucleus and their ethers or esters
- C09B11/08—Phthaleins; Phenolphthaleins; Fluorescein
Description
2,7 g der durch das in Beispiel 6 beschriebene Verfahren hergestellten 4'-Dimethylaminobenzophenon-2-carboxylsäure wurde mit 2,1 g 2-Phenylindol und 40 ecm Essigsäureanhydrid gemischt 4,4 g eines Rohprodukts wurden nach dem im Beispiel 6 beschriebenen Verfahren gewonnen und aus der Benzollösung umkristallisiert. Das gereinigte Produkt hatte seinen Schmelzpunkt bei 252 bis 253° C. Die Benzollösung des Produkts ergab auf der Phenolpolymerbeschichtung eines Papiers eine grüne Färbung.
Claims (2)
der allgemeinen Formel
Applications Claiming Priority (10)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US61252467A | 1967-01-30 | 1967-01-30 | |
US61249667A | 1967-01-30 | 1967-01-30 | |
US61255867A | 1967-01-30 | 1967-01-30 | |
US61236967A | 1967-01-30 | 1967-01-30 | |
US61245967A | 1967-01-30 | 1967-01-30 | |
US82153969A | 1969-01-24 | 1969-01-24 | |
US81089469A | 1969-01-24 | 1969-01-24 | |
US82153869A | 1969-01-24 | 1969-01-24 | |
US82153769A | 1969-01-24 | 1969-01-24 | |
US81759669A | 1969-01-24 | 1969-01-24 |
Publications (3)
Publication Number | Publication Date |
---|---|
DE1795737A1 DE1795737A1 (de) | 1976-09-09 |
DE1795737B2 DE1795737B2 (de) | 1977-10-27 |
DE1795737C3 true DE1795737C3 (de) | 1978-06-15 |
Family
ID=27581296
Family Applications (4)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE19681795749 Pending DE1795749A1 (de) | 1967-01-30 | 1968-01-29 | Chromogene verbindungen und ihre anwendung in druckempfindlichem aufzeichnungsmaterial |
DE68N32029A Expired DE1695581C3 (de) | 1967-01-30 | 1968-01-29 | 33-Bis-(3-indolyl)-phthalide |
DE19681795748 Pending DE1795748A1 (de) | 1967-01-30 | 1968-01-29 | Chromogene verbindungen und ihre anwendung in druckempfindlichem aufzeichnungsmaterial |
DE1795737A Expired DE1795737C3 (de) | 1967-01-30 | 1968-01-29 | 3-(p-Aminophenyl)-3-(3-indolyl)phthalide und ihre Anwendung in druckempfindlichem Aufzeichnungsmaterial |
Family Applications Before (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE19681795749 Pending DE1795749A1 (de) | 1967-01-30 | 1968-01-29 | Chromogene verbindungen und ihre anwendung in druckempfindlichem aufzeichnungsmaterial |
DE68N32029A Expired DE1695581C3 (de) | 1967-01-30 | 1968-01-29 | 33-Bis-(3-indolyl)-phthalide |
DE19681795748 Pending DE1795748A1 (de) | 1967-01-30 | 1968-01-29 | Chromogene verbindungen und ihre anwendung in druckempfindlichem aufzeichnungsmaterial |
Country Status (7)
Country | Link |
---|---|
US (7) | US3491116A (de) |
BE (3) | BE709999A (de) |
CH (4) | CH484250A (de) |
DE (4) | DE1795749A1 (de) |
FR (4) | FR1554986A (de) |
GB (4) | GB1162771A (de) |
NL (4) | NL6801358A (de) |
Families Citing this family (91)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3491116A (en) * | 1967-01-30 | 1970-01-20 | Ncr Co | 3-(phenyl)-3-(indol-3-yl)-phthalides |
GB1274667A (en) * | 1968-06-07 | 1972-05-17 | Wiggins Teape Res Dev | Coated fibrous sheet material |
GB1257205A (de) * | 1968-07-15 | 1971-12-15 | ||
IE33222B1 (en) * | 1968-07-15 | 1974-04-17 | Fuji Photo Film Co Ltd | Pressure-sensitive copying paper |
US3702245A (en) * | 1970-06-05 | 1972-11-07 | Polaroid Corp | Photographic diffusion-transfer processes and elements utilizing ph-sensitive optical filter agents to prevent fogging by extraneous actinic radiation during development |
US3849164A (en) * | 1970-11-16 | 1974-11-19 | Ncr | Pressure-sensitive record unit comprising a mixture of two chromogenic compounds |
US3857675A (en) * | 1970-11-16 | 1974-12-31 | H Schwab | Mixtures of two chromogenic compounds |
CA948639A (en) * | 1971-01-21 | 1974-06-04 | Polaroid Corporation | Indole phthalein indicator dyes |
US3931228A (en) * | 1971-01-21 | 1976-01-06 | Polaroid Corporation | Process for preparing phthalide and naphthalide indicator dyes |
US3736337A (en) * | 1971-04-27 | 1973-05-29 | Ncr Co | Tetrahalogenated chromogenic compounds and their use |
US3894168A (en) * | 1971-04-30 | 1975-07-08 | Ncr Co | Paper coating pigment material |
US3880656A (en) * | 1971-10-02 | 1975-04-29 | Canon Kk | Electrophotographic method for colored images |
GB1414995A (en) * | 1971-11-15 | 1975-11-26 | Canon Kk | Electrophotographic method |
US4001277A (en) * | 1971-11-26 | 1977-01-04 | Polaroid Corporation | 3,3-disubstituted phthalides and naphthalides |
US3933849A (en) * | 1971-11-26 | 1976-01-20 | Polaroid Corporation | 3,3-Disubstituted phthalides and naphthalides |
BE791898A (fr) * | 1971-11-26 | 1973-05-24 | Ciba Geigy Ag | Procede de preparation de substances chromogenes a partir d'indoles et d'anhydrides d'acides dicarboxyliques vicinaux, aromatiques ou heteroaromatiques, nouveaux chromogenes de cette categorie et leur emploi |
US3932455A (en) * | 1971-11-26 | 1976-01-13 | Polaroid Corporation | Carbazole phthaleins |
DE2259409C2 (de) * | 1971-12-06 | 1985-10-10 | Appleton Papers Inc., Appleton, Wis. | Chromogene Furo[3,4-b]pyridin-7-one und -pyrazin-5-one |
BE795746A (fr) * | 1972-02-21 | 1973-08-21 | Wiggins Teape Ltd | Nouveaux formateurs de couleur |
JPS5122413B2 (de) * | 1972-06-24 | 1976-07-09 | ||
US4096176A (en) * | 1972-12-12 | 1978-06-20 | Sterling Drug Inc. | Benzoylbenzoic acids |
US3996405A (en) * | 1973-01-24 | 1976-12-07 | Ncr Corporation | Pressure-sensitive record material |
CH578432A5 (de) * | 1973-03-05 | 1976-08-13 | Ciba Geigy Ag | |
GB1460151A (en) * | 1973-05-21 | 1976-12-31 | Ciba Geigy | Nitrophthalides their mahufacture and their use in recording systems- |
GB1464251A (en) * | 1973-05-21 | 1977-02-09 | Ciba Geigy Ag | Thermo-reactive colour recording material |
US4186134A (en) * | 1973-05-21 | 1980-01-29 | Ciba-Geigy Corporation | 3-Indolyl-3-phenyl-phthalides |
GB1460751A (en) * | 1973-05-21 | 1977-01-06 | Ciba Geigy Ag | 3-indolyl-3-phenyl-phthalide compounds their manufacture and their use |
US3944523A (en) * | 1973-10-23 | 1976-03-16 | Minnesota Mining And Manufacturing Company | Poly(phenol/diene) resin and rubber adhesive compositions tackified therewith |
GB1467898A (en) * | 1974-04-09 | 1977-03-23 | Ciba Geigy Ag | Heterocyclic substituted lactone compounds their manufacture and use |
USRE30116E (en) * | 1975-03-24 | 1979-10-16 | Moore Business Forms, Inc. | Carbonless manifold business forms |
US3981523A (en) * | 1975-03-24 | 1976-09-21 | Moore Business Forms, Inc. | Carbonless manifold business forms |
US4020056A (en) * | 1975-04-10 | 1977-04-26 | Ncr Corporation | Di-vinyl phthalides color formers |
US4022771A (en) * | 1975-04-10 | 1977-05-10 | Ncr Corporation | Aminophenyl lactone compounds containing an ethyleno group |
JPS525746A (en) * | 1975-07-03 | 1977-01-17 | Kanzaki Paper Mfg Co Ltd | Novel process for preparation of triarymethane derivatives |
US3978270A (en) * | 1975-11-12 | 1976-08-31 | Ncr Corporation | Thermal sensitive materials |
CH594511A5 (de) * | 1976-01-16 | 1978-01-13 | Ciba Geigy Ag | |
US4182714A (en) * | 1976-12-29 | 1980-01-08 | Sterling Drug Inc. | Carbazole containing phthalides |
US4251446A (en) * | 1977-03-01 | 1981-02-17 | Sterling Drug Inc. | Phthalide compounds, processes and marking systems |
US4189171A (en) * | 1977-03-01 | 1980-02-19 | Sterling Drug Inc. | Marking systems containing 3-aryl-3-heterylphthalides and 3,3-bis(heteryl)phthalides |
US4595768A (en) * | 1977-05-04 | 1986-06-17 | The Hilton-Davis Chemical Co. | 3-(substituted phenyl)phthalides |
US4732991A (en) * | 1977-05-04 | 1988-03-22 | Hilton Davis Chemical Co. | Substituted phthalides |
US4188456A (en) * | 1977-12-23 | 1980-02-12 | Ncr Corporation | Pressure-sensitive recording sheet |
US4349679A (en) * | 1978-05-18 | 1982-09-14 | Giba-Geigy Corporation | Pyrrolidino and piperidino benz ring substituted phthalides |
GB2022575B (en) * | 1978-05-18 | 1982-10-27 | Ciba Geigy Ag | Mixed aromatic anhydrides their manufacture and use |
US4211872A (en) * | 1978-12-11 | 1980-07-08 | Hung William M | Substituted furopyridinones and furopyrazinones |
US4242513A (en) * | 1979-03-05 | 1980-12-30 | Appleton Papers Inc. | Lactone compounds containing a heterocyclic radical |
US4275206A (en) * | 1979-03-05 | 1981-06-23 | Appleton Papers Inc. | Lactone compounds containing an indolizine radical |
US4307018A (en) * | 1979-04-04 | 1981-12-22 | Sterling Drug Inc. | Heteroarylphthalides |
US4322352A (en) * | 1979-04-04 | 1982-03-30 | Sterling Drug Inc. | Indolyl phthalide compounds |
US4334072A (en) * | 1980-01-16 | 1982-06-08 | Appleton Papers Inc. | Lactone compounds containing an indolizine radical |
FI70036C (fi) * | 1980-01-31 | 1986-09-12 | Ciba Geigy Ag | Kromogena kinazolinfoereningar |
JPS57133093A (en) * | 1981-02-12 | 1982-08-17 | Jujo Paper Co Ltd | Developing sheet for pressure sensitive copying paper |
US4478842A (en) * | 1981-11-19 | 1984-10-23 | Ciba-Geigy Corporation | N-Substituted-2-pyridylindoles |
CH652733A5 (de) * | 1983-04-07 | 1985-11-29 | Ciba Geigy Ag | Verfahren zur herstellung von 4-azaphthalidverbindungen. |
US4431840A (en) * | 1982-10-22 | 1984-02-14 | Sterling Drug Inc. | Process for preparing 2-benzoylbenzoic acids |
US4736027A (en) * | 1985-06-17 | 1988-04-05 | Hilton Davis Chemical Co. | Indole-phthalide derivatives |
US4660060A (en) * | 1985-06-17 | 1987-04-21 | The Hilton-Davis Chemical Co. | Imaging systems containing 3-(indol-3-yl)-3-(4-substituted aminophenyl)phthalides |
US4788285A (en) * | 1985-06-17 | 1988-11-29 | Hung William M | Indole-phthalide derivatives |
US5220036A (en) * | 1985-12-16 | 1993-06-15 | Polaroid Corporation | Thiolactone dye precursors |
DE3609344A1 (de) * | 1986-03-20 | 1987-09-24 | Bayer Ag | Chromogene phthalide, ihre herstellung und verwendung |
GB2194070B (en) * | 1986-07-09 | 1990-01-10 | Fuji Photo Film Co Ltd | Sheet recording material containing dye-forming components |
EP0266310B1 (de) * | 1986-10-28 | 2001-12-05 | Ciba SC Holding AG | Chromogene Phthalide |
US4977131A (en) * | 1988-05-24 | 1990-12-11 | Moore Business Forms, Inc. | OCR scannable carbonless copying system and a method of producing OCR scannable images therewith |
EP0475908A1 (de) * | 1990-09-14 | 1992-03-18 | Ciba-Geigy Ag | Chromogene Lactamverbindungen und ihre Herstellung und Verwendung |
US5693374A (en) | 1994-06-23 | 1997-12-02 | Fuji Photo Film Co., Ltd. | Alpha-resorcyclic acid ester derivatives and recording materials using the same |
JPH10129021A (ja) * | 1996-10-25 | 1998-05-19 | Fuji Photo Film Co Ltd | 感熱記録システム |
US6294502B1 (en) | 1998-05-22 | 2001-09-25 | Bayer Aktiengesellschaft | Thermally-responsive record material |
DE60127079T2 (de) | 2000-12-04 | 2007-07-05 | Fujifilm Corp. | Thermisches Aufzeichnungsmaterial |
US7094731B2 (en) | 2001-06-26 | 2006-08-22 | Fuji Photo Film Co., Ltd. | Recording material |
JP2003094827A (ja) | 2001-09-27 | 2003-04-03 | Fuji Photo Film Co Ltd | 感熱記録材料 |
JP2003094826A (ja) | 2001-09-27 | 2003-04-03 | Fuji Photo Film Co Ltd | 感熱記録材料およびその製造方法 |
JP3776810B2 (ja) | 2002-01-25 | 2006-05-17 | 富士写真フイルム株式会社 | 感熱記録材料及び感熱記録方法 |
JP3822513B2 (ja) | 2002-03-26 | 2006-09-20 | 富士写真フイルム株式会社 | 感熱記録材料 |
CA2485207C (en) | 2002-11-12 | 2011-07-12 | Appleton Papers Inc. | Secure point of sale imageable substrate |
US7108190B2 (en) * | 2003-02-28 | 2006-09-19 | Appleton Papers Inc. | Token array and method employing authentication tokens bearing scent formulation information |
US6932602B2 (en) * | 2003-04-22 | 2005-08-23 | Appleton Papers Inc. | Dental articulation kit and method |
US20060063125A1 (en) * | 2003-04-22 | 2006-03-23 | Hamilton Timothy F | Method and device for enhanced dental articulation |
US20040251309A1 (en) * | 2003-06-10 | 2004-12-16 | Appleton Papers Inc. | Token bearing magnetc image information in registration with visible image information |
JP4442676B2 (ja) * | 2007-10-01 | 2010-03-31 | 富士ゼロックス株式会社 | 光定着用カラートナー及びその製造方法、並びに、静電荷像現像剤、プロセスカートリッジ及び画像形成装置 |
JP5247505B2 (ja) | 2009-02-04 | 2013-07-24 | 富士フイルム株式会社 | 熱分布表示体及び熱分布確認方法 |
KR102032749B1 (ko) | 2010-04-16 | 2019-10-16 | 에스더블유아이엠씨 엘엘씨 | 패키징 용품을 위한 코팅 조성물 및 코팅 방법 |
EP3415572B1 (de) | 2011-02-07 | 2021-04-14 | Swimc Llc | Beschichtungszusammensetzungen für behälter und andere gegenstände sowie beschichtungsverfahren |
EP2882818B1 (de) | 2012-08-09 | 2020-05-06 | Swimc Llc | Stabilisator und beschichtungszusammensetzungen daraus |
US10526502B2 (en) | 2012-08-09 | 2020-01-07 | Swimc Llc | Container coating system |
AU2013299578A1 (en) | 2012-08-09 | 2015-02-19 | Valspar Sourcing, Inc. | Compositions for containers and other articles and methods of using same |
EP2882792A4 (de) | 2012-08-09 | 2016-04-13 | Valspar Sourcing Inc | Polycarbonate |
WO2014025406A1 (en) | 2012-08-09 | 2014-02-13 | Valspar Sourcing, Inc. | Dental materials and method of manufacture |
US9475328B2 (en) | 2012-08-09 | 2016-10-25 | Valspar Sourcing, Inc. | Developer for thermally responsive record materials |
EP2954373B1 (de) | 2013-02-06 | 2019-04-24 | Fujifilm Hunt Chemicals US, Inc. | Chemische beschichtung für lasermarkierbares material |
WO2015160788A1 (en) | 2014-04-14 | 2015-10-22 | Valspar Sourcing, Inc. | Methods of preparing compositions for containers and other articles and methods of using same |
TWI614275B (zh) | 2015-11-03 | 2018-02-11 | Valspar Sourcing Inc | 用於製備聚合物的液體環氧樹脂組合物 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2505486A (en) * | 1944-01-31 | 1950-04-25 | Ncr Co | Process of making pressure sensitive record material |
US3268537A (en) * | 1961-08-31 | 1966-08-23 | Burroughs Corp | Chromogenous aminophenyl derivatives of benzodifurandione |
US3244549A (en) * | 1961-08-31 | 1966-04-05 | Burroughs Corp | Manifold sheets coated with lactone and related chromogenous compounds and reactive phenolics and method of marking |
US3336337A (en) * | 1961-08-31 | 1967-08-15 | Burroughs Corp | Chromogenous tetrakis(aminophenyl) derivatives of benzodifuran |
US3455721A (en) * | 1964-12-21 | 1969-07-15 | Ncr Co | Color sensitized record material comprising phenolic resin and acid type mineral |
US3491116A (en) * | 1967-01-30 | 1970-01-20 | Ncr Co | 3-(phenyl)-3-(indol-3-yl)-phthalides |
-
1967
- 1967-01-30 US US612459A patent/US3491116A/en not_active Expired - Lifetime
- 1967-01-30 US US612524A patent/US3491112A/en not_active Expired - Lifetime
- 1967-01-30 US US612369A patent/US3491111A/en not_active Expired - Lifetime
- 1967-01-30 US US612496A patent/US3509173A/en not_active Expired - Lifetime
-
1968
- 1968-01-10 GB GB0387/68A patent/GB1162771A/en not_active Expired
- 1968-01-10 GB GB1388/68A patent/GB1161387A/en not_active Expired
- 1968-01-10 GB GB1389/68A patent/GB1160940A/en not_active Expired
- 1968-01-10 GB GB1386/68A patent/GB1161386A/en not_active Expired
- 1968-01-29 DE DE19681795749 patent/DE1795749A1/de active Pending
- 1968-01-29 FR FR137726A patent/FR1554986A/fr not_active Expired
- 1968-01-29 FR FR137728A patent/FR1554988A/fr not_active Expired
- 1968-01-29 BE BE709999D patent/BE709999A/xx not_active IP Right Cessation
- 1968-01-29 DE DE68N32029A patent/DE1695581C3/de not_active Expired
- 1968-01-29 FR FR137727A patent/FR1554987A/fr not_active Expired
- 1968-01-29 BE BE709998D patent/BE709998A/xx not_active IP Right Cessation
- 1968-01-29 DE DE19681795748 patent/DE1795748A1/de active Pending
- 1968-01-29 DE DE1795737A patent/DE1795737C3/de not_active Expired
- 1968-01-29 BE BE710000D patent/BE710000A/xx unknown
- 1968-01-29 FR FR137729A patent/FR1572222A/fr not_active Expired
- 1968-01-30 CH CH150868A patent/CH484250A/fr not_active IP Right Cessation
- 1968-01-30 CH CH150668A patent/CH484248A/fr not_active IP Right Cessation
- 1968-01-30 CH CH150968A patent/CH484251A/fr not_active IP Right Cessation
- 1968-01-30 NL NL6801358A patent/NL6801358A/xx unknown
- 1968-01-30 CH CH150768A patent/CH484249A/fr not_active IP Right Cessation
- 1968-01-30 NL NL686801359A patent/NL144942B/xx not_active IP Right Cessation
- 1968-01-30 NL NL686801355A patent/NL145240B/xx not_active IP Right Cessation
- 1968-01-30 NL NL686801354A patent/NL145243B/xx not_active IP Right Cessation
-
1969
- 1969-01-24 US US817596*A patent/US3540910A/en not_active Expired - Lifetime
- 1969-01-24 US US821537*A patent/US3540911A/en not_active Expired - Lifetime
- 1969-01-24 US US821538*A patent/US3540912A/en not_active Expired - Lifetime
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Free format text: WEICKMANN, H., DIPL.-ING. FINCKE, K., DIPL.-PHYS. DR. WEICKMANN, F., DIPL.-ING. HUBER, B., DIPL.-CHEM. LISKA, H., DIPL.-ING. DR.-ING. PRECHTEL, J., DIPL.-PHYS. DR.RER.NAT., PAT.-ANW., 8000 MUENCHEN |