DE1222351B - Verfahren zum Phosphatieren von Metallen mit im wesentlichen nichtwaessrigen Loesungen - Google Patents
Verfahren zum Phosphatieren von Metallen mit im wesentlichen nichtwaessrigen LoesungenInfo
- Publication number
- DE1222351B DE1222351B DEM45941A DEM0045941A DE1222351B DE 1222351 B DE1222351 B DE 1222351B DE M45941 A DEM45941 A DE M45941A DE M0045941 A DEM0045941 A DE M0045941A DE 1222351 B DE1222351 B DE 1222351B
- Authority
- DE
- Germany
- Prior art keywords
- solution
- phosphoric acid
- aqueous solutions
- solubilizer
- boiling point
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229910052751 metal Inorganic materials 0.000 title claims description 14
- 239000002184 metal Substances 0.000 title claims description 14
- 238000000034 method Methods 0.000 title claims description 12
- 150000002739 metals Chemical class 0.000 title claims description 4
- 239000012457 nonaqueous media Substances 0.000 title claims description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 21
- 239000000243 solution Substances 0.000 claims description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 11
- 239000002904 solvent Substances 0.000 claims description 11
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 6
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 6
- 150000008282 halocarbons Chemical class 0.000 claims description 6
- -1 aliphatic alcohols Chemical class 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 3
- 229910052793 cadmium Inorganic materials 0.000 claims description 3
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 150000002894 organic compounds Chemical group 0.000 claims description 3
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 3
- 244000019137 Indigofera linnaei Species 0.000 claims description 2
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 claims description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
- 229950011008 tetrachloroethylene Drugs 0.000 claims description 2
- 229910052725 zinc Inorganic materials 0.000 claims description 2
- 239000011701 zinc Substances 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims 1
- JGUQDUKBUKFFRO-CIIODKQPSA-N dimethylglyoxime Chemical compound O/N=C(/C)\C(\C)=N\O JGUQDUKBUKFFRO-CIIODKQPSA-N 0.000 claims 1
- 239000010410 layer Substances 0.000 description 15
- 235000011007 phosphoric acid Nutrition 0.000 description 9
- 238000000576 coating method Methods 0.000 description 7
- 229910019142 PO4 Inorganic materials 0.000 description 6
- 235000021317 phosphate Nutrition 0.000 description 6
- 239000010452 phosphate Substances 0.000 description 5
- 229910000831 Steel Inorganic materials 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- 238000011282 treatment Methods 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 238000007598 dipping method Methods 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 229910000398 iron phosphate Inorganic materials 0.000 description 2
- WBJZTOZJJYAKHQ-UHFFFAOYSA-K iron(3+) phosphate Chemical compound [Fe+3].[O-]P([O-])([O-])=O WBJZTOZJJYAKHQ-UHFFFAOYSA-K 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 description 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 1
- 241000531891 Alburnus alburnus Species 0.000 description 1
- 241001062009 Indigofera Species 0.000 description 1
- 235000000177 Indigofera tinctoria Nutrition 0.000 description 1
- ILRRQNADMUWWFW-UHFFFAOYSA-K aluminium phosphate Chemical compound O1[Al]2OP1(=O)O2 ILRRQNADMUWWFW-UHFFFAOYSA-K 0.000 description 1
- NRGIRRZWCDKDMV-UHFFFAOYSA-H cadmium(2+);diphosphate Chemical compound [Cd+2].[Cd+2].[Cd+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O NRGIRRZWCDKDMV-UHFFFAOYSA-H 0.000 description 1
- KYKAJFCTULSVSH-UHFFFAOYSA-N chloro(fluoro)methane Chemical compound F[C]Cl KYKAJFCTULSVSH-UHFFFAOYSA-N 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- QNDQILQPPKQROV-UHFFFAOYSA-N dizinc Chemical compound [Zn]=[Zn] QNDQILQPPKQROV-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical class FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910000039 hydrogen halide Inorganic materials 0.000 description 1
- 239000012433 hydrogen halide Substances 0.000 description 1
- 229940097275 indigo Drugs 0.000 description 1
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 230000007257 malfunction Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- TVDSBUOJIPERQY-UHFFFAOYSA-N prop-2-yn-1-ol Chemical compound OCC#C TVDSBUOJIPERQY-UHFFFAOYSA-N 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/02—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using non-aqueous solutions
- C23C22/03—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using non-aqueous solutions containing phosphorus compounds
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
- Chemical Treatment Of Metals (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEM45941A DE1222351B (de) | 1960-07-15 | 1960-07-15 | Verfahren zum Phosphatieren von Metallen mit im wesentlichen nichtwaessrigen Loesungen |
| FR867071A FR1294077A (fr) | 1960-07-15 | 1961-07-05 | Procédé de phosphatation des métaux dans des solvants non aqueux |
| BE605858A BE605858A (fr) | 1960-07-15 | 1961-07-07 | Procédé de phosphatation des métaux dans des solvants non aqueux |
| CH821461A CH409576A (de) | 1960-07-15 | 1961-07-12 | Verfahren zum Phosphatieren von Metallen |
| NL267043D NL267043A (nl) | 1960-07-15 | 1961-07-13 | Werkwijze voor het fosfateren van metalen in niet-waterige oplosmiddelen |
| NL267043A NL121230C (nl) | 1960-07-15 | 1961-07-13 | Werkwijze voor het fosfateren van metalen |
| GB25813/61A GB912970A (en) | 1960-07-15 | 1961-07-17 | Improvements relating to the production of phosphate coatings |
| NL6414071A NL6414071A (enrdf_load_stackoverflow) | 1960-07-15 | 1964-12-03 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEM45941A DE1222351B (de) | 1960-07-15 | 1960-07-15 | Verfahren zum Phosphatieren von Metallen mit im wesentlichen nichtwaessrigen Loesungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1222351B true DE1222351B (de) | 1966-08-04 |
Family
ID=61160933
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEM45941A Pending DE1222351B (de) | 1960-07-15 | 1960-07-15 | Verfahren zum Phosphatieren von Metallen mit im wesentlichen nichtwaessrigen Loesungen |
Country Status (6)
| Country | Link |
|---|---|
| BE (1) | BE605858A (enrdf_load_stackoverflow) |
| CH (1) | CH409576A (enrdf_load_stackoverflow) |
| DE (1) | DE1222351B (enrdf_load_stackoverflow) |
| FR (1) | FR1294077A (enrdf_load_stackoverflow) |
| GB (1) | GB912970A (enrdf_load_stackoverflow) |
| NL (3) | NL121230C (enrdf_load_stackoverflow) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2611789A1 (de) * | 1975-03-20 | 1976-09-30 | Diamond Shamrock Corp | Organisches phosphatierungsmittel, dessen verwendung zur herstellung von wasserunloeslichen phosphatueberzuegen und die dabei erhaltenen produkte |
| DE2611790A1 (de) * | 1975-03-20 | 1976-10-07 | Diamond Shamrock Corp | Phosphatierung mit methylenchlorid |
| US4143205A (en) | 1976-10-05 | 1979-03-06 | Diamond Shamrock Corporation | Phosphatized and painted metal articles |
| US5588989A (en) * | 1994-11-23 | 1996-12-31 | Ppg Industries, Inc. | Zinc phosphate coating compositions containing oxime accelerators |
| US5653790A (en) * | 1994-11-23 | 1997-08-05 | Ppg Industries, Inc. | Zinc phosphate tungsten-containing coating compositions using accelerators |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ATE5780T1 (de) * | 1980-02-14 | 1984-01-15 | Akzo N.V. | Fluessige zusammensetzung zum phosphatieren von metalloberflaechen. |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE887139C (de) * | 1943-07-10 | 1953-08-20 | Parker Rust Proof Company | Phosphatierungsverfahren |
| BE584827A (fr) * | 1958-11-21 | 1960-03-16 | Du Pont | Solutions et procédé de phosphatation |
-
1960
- 1960-07-15 DE DEM45941A patent/DE1222351B/de active Pending
-
1961
- 1961-07-05 FR FR867071A patent/FR1294077A/fr not_active Expired
- 1961-07-07 BE BE605858A patent/BE605858A/fr unknown
- 1961-07-12 CH CH821461A patent/CH409576A/de unknown
- 1961-07-13 NL NL267043A patent/NL121230C/nl active
- 1961-07-13 NL NL267043D patent/NL267043A/nl unknown
- 1961-07-17 GB GB25813/61A patent/GB912970A/en not_active Expired
-
1964
- 1964-12-03 NL NL6414071A patent/NL6414071A/xx unknown
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE887139C (de) * | 1943-07-10 | 1953-08-20 | Parker Rust Proof Company | Phosphatierungsverfahren |
| BE584827A (fr) * | 1958-11-21 | 1960-03-16 | Du Pont | Solutions et procédé de phosphatation |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2611789A1 (de) * | 1975-03-20 | 1976-09-30 | Diamond Shamrock Corp | Organisches phosphatierungsmittel, dessen verwendung zur herstellung von wasserunloeslichen phosphatueberzuegen und die dabei erhaltenen produkte |
| DE2611790A1 (de) * | 1975-03-20 | 1976-10-07 | Diamond Shamrock Corp | Phosphatierung mit methylenchlorid |
| US4008101A (en) * | 1975-03-20 | 1977-02-15 | Diamond Shamrock Corporation | Methylene chloride phosphatizing |
| US4029523A (en) * | 1975-03-20 | 1977-06-14 | Diamond Shamrock Corporation | Solvent phosphatizing compositions yielding non water soluble coatings |
| US4070521A (en) * | 1975-03-20 | 1978-01-24 | Diamond Shamrock Corporation | Methylene chloride phosphatized coating |
| DE2611790B2 (de) * | 1975-03-20 | 1980-11-13 | Diamond Shamrock Corp., Cleveland, Ohio (V.St.A.) | Phosphatierungslösung und Verfahren zur Anwendung |
| DE2611790C3 (de) * | 1975-03-20 | 1989-07-20 | Metal Coatings International Inc., Chardon, Ohio | Phosphatierung mit Methylenchlorid |
| DK149458C (da) * | 1975-03-20 | 1993-03-15 | Metal Coatings Int Inc | Fremgangsmåde ved fremstilling af et phosphat-overtræk på overfladen af metaller, der er i stand til at reagere med phosphorsyre, og væskeblanding til brug ved fremgangsmåden |
| US4143205A (en) | 1976-10-05 | 1979-03-06 | Diamond Shamrock Corporation | Phosphatized and painted metal articles |
| US5588989A (en) * | 1994-11-23 | 1996-12-31 | Ppg Industries, Inc. | Zinc phosphate coating compositions containing oxime accelerators |
| US5653790A (en) * | 1994-11-23 | 1997-08-05 | Ppg Industries, Inc. | Zinc phosphate tungsten-containing coating compositions using accelerators |
Also Published As
| Publication number | Publication date |
|---|---|
| NL6414071A (enrdf_load_stackoverflow) | 1965-01-25 |
| GB912970A (en) | 1962-12-12 |
| FR1294077A (fr) | 1962-05-18 |
| BE605858A (fr) | 1961-11-03 |
| CH409576A (de) | 1966-03-15 |
| NL121230C (nl) | 1966-09-15 |
| NL267043A (nl) | 1964-08-10 |
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