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Způsob přípravy hydrografitu
CS237710B1
Czechoslovakia
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English - Inventor
Karel Klouda Ivo Peka Antonin Posta Vaclav Dedek
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Description
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| Reakce fluorografitu s nukleofilními činidly, reakční podmínky a vzniklá produkty | ||||
| Fluorografit | Nukleofilní činidlo | Rozpouětědlo | Teplota/reakčni doba (°C) | Produkty reakce |
| uaih4 | Éter | 30 až 35/3 | ^6^.27^.06¼ | |
| <Cř0.9>n | líaih4 | Dioxan | 95/24 | (C6H1,37F0.15¼ |
| <cpl.,>n | líaih4 | THF | 50 až 60/6 | (C6H1 .27^0.09¼ |
| (Cřl.06)n | CH-jCHgMgBr | THF | 60 až 65/6 | <C6H3.66F0.18)b |
| <CFl.06>« | (CH3)2CHIIgBr | THF | 60 až 65/6 | (C6H3.2F0.23)b |
| <CF1.2>n | CHjCHgMgBr | THF | 50 až 60/3 | ^653.66^0.22¼ |
| ^1.2¼ | Bu-MgBr | THF | 50 až 60/2.5 | ^6^.50^0,18¼ |
| <CF0.83>n | C6H5MgBr | Éter | 30 až 35/5 | ^2.7¼ |
| ^0.83¼ | CH^Mgl | Éter | 30 až 35/7 | (C6H0.91F0.75)« |
Claims (1)
Hide Dependent
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- PŘEDMĚT VYNÁLEZUZpůsob přípravy hydrografitu, vyznačený tím, že se na fluorografit (0Ρχ)η působí hydridovými či alkylovými anionty, která- poskytuje lithiumaluminiumhydrid nebo alkylmagnesiumhahogenld.