CN2610223Y - Small chemical vapour tester - Google Patents

Small chemical vapour tester Download PDF

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Publication number
CN2610223Y
CN2610223Y CN 03246329 CN03246329U CN2610223Y CN 2610223 Y CN2610223 Y CN 2610223Y CN 03246329 CN03246329 CN 03246329 CN 03246329 U CN03246329 U CN 03246329U CN 2610223 Y CN2610223 Y CN 2610223Y
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CN
China
Prior art keywords
steam
outer
cover
sleeve
utility model
Prior art date
Application number
CN 03246329
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Chinese (zh)
Inventor
贺雁广
Original Assignee
贺雁广
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Priority to CN 03246329 priority Critical patent/CN2610223Y/en
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Publication of CN2610223Y publication Critical patent/CN2610223Y/en

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Abstract

The utility model discloses a minitype chemical industry steam experimental device, which is a popular common chemical industry steam experimental device. The utility model is technically comprises a reactor, an outer seat and a steam producer. The reactor body is an inner cover produced by the corrosion resistant material, and the top of the inner cover is installed with a top cover board which is left with an observing hole, a feeding hole, a mixing hole, a temperature meter faucet and a liquid pouring slot. The lower taper portion of the inner cover has a plug hole which is connected with a closing valve. The upper portion of the outer seat is provided with a steam inlet, and the lower portion is provided with a steam outlet. The most inner layer of the outer seat is provided with an outer steam clamping cover, and a heat preservation layer is arranged between the outer steam clamping cover and the shell. The steam producer employs a common double insured pressure cooker, and is connected with the outer seat steam inlet through a safety valve on the pressure cooker cover. When the steam is accessed, the reacting temperature is controlled by employing the method of controlling the steam amount. The utility model is characterized in that the technical proposal is scientific and reasonable, and the structure is simple and practical. The utility model is also characterized in that the applying range is wide, the operation is convenient, and the heating reacting condition is very close to the industrial production, which is helpful for the product to change toward the industrial production. The utility model is superior to the chemical industry experimental methods in the prior art such as glassware heating, water bath or electric heating cover heating and so on.

Description

小型化工蒸汽实验装置 Small chemical vapor experimental device

一、技术领域 First, the technical field

:本实用新型涉及一种化工实验设备。 : The present invention relates to a chemical laboratory equipment. 具体地说:是一种大众化的通用小型化工蒸汽实验反应装置。 Specifically: a general experimental small chemical vapor reaction apparatus popular.

二、背景技术 Second, the technical background

:在化工产品实验阶段,研制人员往往迫于化工实验设备的制约,不得不利用反应釜之类的反应设备进行实验,这就存在着投料量大、设备使用不方便、实验周期长等种种弊病。 : Chemical products in the experimental stage, the development staff often forced to restrict chemical laboratory equipment, the reaction had to use equipment like the reactor experiments, which there are large feeding amount, equipment inconvenient to use, long experimental period and other ills . 而利用水浴或电热套等加热的反应装置又存在着离工业化加热生产条件太远的问题。 The reaction apparatus and the like using a water bath or electric heating jacket and heating there is a problem from the industrial production conditions too far.

三、发明内容 III. SUMMARY OF THE INVENTION

:本实用新型的目的是提供一种大众化的通用小型化工蒸汽实验装置。 : The object of the present invention is to provide a general small chemical vapor popular experimental device.

为解决上述任务,本实用新型所采用的解决方案是:小型化工蒸汽实验装置主要由反应器、外座、蒸汽发生器等组成,反应器主体是一由耐腐蚀材料制成的内套,在内套的顶部装有一顶盖板,顶盖板上面留有观察孔、加料口、搅拌孔、温度计插口和倒液槽,顶盖板与内套之间加有密封圈,在内套的下部锥形部位有一放料口,放料口联接一截止阀,在内套的锥形部位底部有阳螺纹;在外座的上部设有进汽口、下部设有排气口,在外座的最里层装有外夹汽套,在外夹汽套与外壳之间是保温层,在外座的底部开有和内套下部锥形部位相配合的通孔,内套的锥形部位底部的阳螺纹穿出外座底部的通孔,通过密封圈和一内有阴螺纹的旋紧螺母相联接;蒸汽发生器利用通用双保险高压锅,通过高压锅盖上的安全阀与外座的进汽口相联,接入蒸汽,利用控制蒸汽 To solve the above task, the solution of the present invention is used: small chemical vapor experimental device consists of the reactor, an outer race, vapor generator, the reactor body is made of a corrosion resistant material within the sleeve, in a lower portion of the top of the inner sleeve is provided with a top cover plate, the cover plate remains above the observation hole, a sealing ring is applied between the charging port, hole stirring, thermometer socket and down tank, the cover plate and the inner sleeve, the inner sleeve a tapered portion having a discharge opening, a discharge opening coupled shut-off valve, a male threaded tapered bottom portion of the inner sheath; outer race is provided with an upper steam inlet, with a lower portion of the exhaust port, the outer race of the innermost steam jacket layer with an outer clamp, the outer insulating layer is interposed between the steam jacket and the housing, and the inner sleeve has a tapered lower portion of the through-hole cooperating opening at the bottom of the outer housing, the conical bottom portion of the male thread within the wear sleeve via bottom seat go through the inner ring and a tightening nut having a female thread coupled; steam generator using a universal double insurance autoclave, the autoclave cover through steam inlet valve and the associated outer race, access steam by controlling the steam 的方法,控制反应温度。 The method of controlling the reaction temperature.

由于采用了上述的技术解决方案,本实用新型具有技术方案科学,合理、构造简单实用、适用范围广、操作方便、加热反应条件十分接近工业生产等特点,有利于产品向工业生产转化。 As a result of the above technical solutions, the present invention has the technical solutions scientific, rational, simple and practical structure, wide application, easy to operate, heating the reaction conditions very close to the industrial production and so on, is conducive to industrial products into production. 优于现有技术中玻璃器皿加热、水浴或电热套加热等种种化工实验手段。 Various experimental methods than chemical glassware heating, water bath heating or heating units prior art.

四、附图说明 IV BRIEF DESCRIPTION

:下面结合附图和一个实施例对本实用新型作进一步详细说明;附图为本实用新型的实施例的结构示意图;附图中标明的内套1、外座2、顶盖板3、观察孔4、加料口5、搅拌孔6、温度计插口7、倒液槽8、密封圈9、放料口10、截止阀11、密封圈12、旋紧螺母13、进汽口14、排汽口15、外夹汽套16、外壳17、保温层18。 : The following further detailed description of the present invention and as an embodiment in conjunction with the accompanying drawings; structural diagram of an embodiment of the invention the present drawings; in the drawings indicate the inner sleeve 1, an outer housing 2, a top cover plate 3, viewing aperture 4, the feeding port 5, stirred holes 6, 7 thermometer socket, down tank 8, ring 9, the discharge opening 10, shut-off valve 11, the seal ring 12, tighten the nut 13, steam inlet port 14, exhaust port 15 an outer steam jacket clip 16, housing 17, insulating layer 18.

五、具体实施方式 V. DETAILED DESCRIPTION

:本实施例中,反应体的主体是由一塘瓷容器制成的内套1、在内套1的顶部装有一顶盖板3,在顶盖板3上面留有观察孔4、加料口5、搅拌孔6、温度计插口7和倒液槽8,顶盖板3与内套1之间加有密封圈9,在内套1的下部锥形部位有一放料口10,放料口10联接一截止阀11,在内套1的锥形部底部有阳螺纹;在外座2的上部设有进汽口14、下部设有排汽口15,在外座2的最里层装有由塘瓷材料制成的外夹汽套16,在外夹汽套16与外壳17之间是保温层18,在外座2的底部开有和内套1下部锥形部位相配合的通孔,内套1的锥形部位底部的阳螺纹穿出外座2底部的通孔,通过密封圈和一内有阴螺纹的旋紧螺母13相联接;蒸汽发生器利用通用双保险高压锅,通过高压锅盖上的安全阀与外座的进汽口相联,接入蒸汽,利用控制蒸汽量的方法,控制反应温度。 : Inner sleeve embodiment, the main reaction body is made of a porcelain pond container 1 of the present embodiment, the inner sleeve 1 is provided with a top cover plate 3 provided on the top plate 3 is left observation hole 4, feed port 5, 6 holes stirring, thermometer socket 7 and 8 down tank, the top cover plate 3 and the inner sleeve 9 between the seal ring 1 added, the lower conical portion of the inner sleeve 1 is provided with a discharge opening 10, the discharge opening 10 coupling a shut-off valve 11, the inner sleeve has a tapered male threaded portion 1 of the bottom; the outer race 2 is provided with an upper steam inlet 14, provided with a lower exhaust port 15, the most inner layer of the outer race 2 with a pond made of ceramic material is sandwiched outer steam jacket 16, the outer steam jacket is interposed between the housing 16 and insulation 17 18, the bottom of the outer race 2 and the inner sleeve opening and has a tapered lower through holes mating portion, the inner sleeve 1 a tapered male screw portion of the bottom of the through hole piercing the bottom of the outer housing 2, is coupled with a tightening nut 13 with a female thread and an inner ring through; steam generator using a universal double insurance pressure cooker, pressure cooker lid security and the outer valve seat associated steam inlet, a steam access, using the method of controlling the amount of steam, controlling the reaction temperature.

当高压锅作为蒸汽发生器使用时,在灶具上可利用可调火焰支架调节,充分利用火焰内、外焰温度的不同来调节蒸发生量。 When used as a steam generator pressure cooker, the cooker can be used in the adjustable bracket flame adjustment to adjust the amount of steam occurs within the full use of the flame, Waiyan different temperatures. 在有蒸汽源的场合可加装气量调节器使用。 In the case of steam source can be installed using the gas regulator.

当然,本实施例仅仅表达了本实用新型的一种设计思路,凡仅仅变换本实用新型附属结构而达到本实用新型发明目的的各种变换,均应落在本实用新型的保护范围之内。 Of course, the present embodiment of the present invention express only a design idea, the present invention where only transform subsidiary structure of the present invention to achieve the object of various modifications of the invention shall fall within the scope of protection of the present invention.

Claims (1)

1.一种小型化工蒸汽实验装置,主要由反应器、外座、蒸汽发生器等组成,其特征在于:反应器主体是一由耐腐蚀材料制成的内套,在内套的顶部装有一顶盖板,顶盖板上面留有观察孔、加料口、搅拌孔、温度计插口和倒液槽,顶盖板与内套之间加有密封圈,在内套的下部锥形部位有一放料口,放料口联接一截止阀,在内套的锥形部位底部有阳螺纹;在外座的上部设有进汽口、下部设有排气口,在外座的最里层装有外夹汽套,在外夹汽套与外壳之间是保温层,在外座的底部开有和内套下部锥形部位相配合的通孔,内套的锥形部位底部的阳螺纹穿出外座底部的通孔,通过密封圈和一内有阴螺纹的旋紧螺母相联接;蒸汽发生器利用通用双保险高压锅,通过高压锅盖上的安全阀与外座的进汽口相联。 A small chemical vapor experimental device, mainly from the reactor, outside the seat, vapor generator, comprising: a reactor main body is made of a corrosion resistant material within the sleeve, the inner sleeve is provided with a top top cover plate, the cover plate remains above the observation hole, a sealing ring is applied between the charging port, hole stirring, thermometer socket and down tank, the cover plate and the inner sleeve, the inner sleeve has a lower conical portion of discharge port, a discharge port coupled shut-off valve, a male threaded tapered bottom portion of the inner sleeve; upper portion of the outer race is provided with steam inlet, a lower portion of an exhaust port, the most inner layer with the outer race of the outer clip vapor sleeve, the outer sleeve interposed between the housing and the vapor layer of insulation, and the through-hole opened lower conical portion of the inner sleeve cooperating outer seat bottom, a tapered male screw portion of the bottom of the sleeve within the outer housing through the bottom piercing holes, coupled through the inner ring and a tightening nut having a female thread; steam generator using a universal double insurance autoclave, the autoclave cover through steam inlet valve and the associated outer race.
CN 03246329 2003-04-11 2003-04-11 Small chemical vapour tester CN2610223Y (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103240045A (en) * 2012-02-10 2013-08-14 中国科学院海洋研究所 Anticorrosion high pressure reactor
CN104353512A (en) * 2014-09-30 2015-02-18 深圳市理邦精密仪器股份有限公司 All-surrounding type water bath circulating constant-temperature heating device

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103240045A (en) * 2012-02-10 2013-08-14 中国科学院海洋研究所 Anticorrosion high pressure reactor
CN103240045B (en) * 2012-02-10 2015-05-13 中国科学院海洋研究所 Anticorrosion high pressure reactor
CN104353512A (en) * 2014-09-30 2015-02-18 深圳市理邦精密仪器股份有限公司 All-surrounding type water bath circulating constant-temperature heating device
CN104353512B (en) * 2014-09-30 2016-06-01 深圳市理邦精密仪器股份有限公司 A kind of full encirclement formula water-bath circulation constant temperature heating unit

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