CN224009805U

CN224009805U - An easy-to-clean reaction vessel for the production of metal-organic frameworks

Info

Publication number: CN224009805U
Application number: CN202520588600.8U
Authority: CN
Inventors: 栾奕; 吴卓恒
Original assignee: Wuxi Boston Environmental Protection Technology Co ltd
Current assignee: Wuxi Boston Environmental Protection Technology Co ltd
Priority date: 2025-03-31
Filing date: 2025-03-31
Publication date: 2026-03-20
Anticipated expiration: 2035-03-31

Abstract

The utility model discloses an easy-to-clean reaction kettle for metal organic framework production, which comprises a kettle body, wherein a feed pipe is fixedly arranged on the left side of the kettle body, a stirring assembly is arranged at the bottom of the kettle body, a scraping plate is arranged in the kettle body through the stirring assembly, a conveying assembly is arranged at the top of the kettle body, a U-shaped pipe is arranged at the top of the kettle body through the conveying assembly and is in sliding connection with the kettle body, a ring-shaped pipe is fixedly arranged at the bottom of the U-shaped pipe, a spray head is fixedly arranged at the bottom of the ring-shaped pipe, a fixing frame is fixedly arranged at the top of the kettle body, a driving assembly is arranged on the opposite surface of the fixing frame, and a moving block is arranged in the fixing frame through the driving assembly. The dual function can effectively remove residues with various properties and different adhesion degrees, ensures that the inner wall of the kettle body can be cleaned, greatly improves the cleaning quality, and is matched with the height adjustment function of the spray head to cover the pollution areas with different heights in a whole way, so that the whole cleaning process is efficient and orderly.

Description

Easy-to-clean reaction kettle for metal organic framework production

Technical Field

The utility model relates to the technical field of metal-organic framework production, in particular to an easy-to-clean reaction kettle for metal-organic framework production.

Background

The metal organic framework is a one-dimensional, two-dimensional or three-dimensional framework formed by metal atoms and organic bridging ligands through coordination bonds, and in the process of processing and producing the metal organic framework, the metal organic framework raw materials are required to be placed into a reaction kettle for treatment, the reaction kettle is widely understood to be a container with physical or chemical reaction, and the heating, evaporating, cooling and low-speed mixing functions required by the process are realized through the structural design and parameter configuration of the container.

In the use process of the existing reaction kettle, as the metal organic framework raw materials have certain adhesiveness, the metal organic framework raw materials can be adhered to the inner wall of the reaction kettle, and the traditional reaction kettle cleaning mode mainly depends on manual cleaning, however, the manual cleaning is extremely low in efficiency, a large amount of manpower and time cost are required to be consumed for each cleaning, a part of the reaction kettle adopts a pure high-pressure water flushing mode, a spray head is usually fixedly arranged at a certain position, and flexible adjustment cannot be carried out according to the pollution degree of different areas in the reaction kettle, so that the cleaning effect is greatly reduced.

Disclosure of utility model

Aiming at the defects of the prior art, the utility model provides an easy-to-clean reaction kettle for metal-organic framework production, which is used for solving the problems in the prior art.

In order to achieve the above purpose, the present utility model adopts the following technical scheme:

The utility model provides an easy clear reation kettle is used in metal organic framework production, includes the cauldron body, cauldron body left side fixed mounting has the inlet pipe, cauldron body bottom is provided with stirring subassembly, the internal portion of cauldron is provided with the scraper blade through stirring subassembly, cauldron body top is provided with conveying subassembly, cauldron body top is provided with U type pipe through conveying subassembly, U type pipe and cauldron body sliding connection, U type pipe bottom fixed mounting has ring type pipe, ring type pipe bottom fixed mounting has the shower nozzle, cauldron body top fixed mounting has the mount, the mount is provided with drive assembly in opposite directions, the inside movable block that is provided with through drive assembly of mount, movable block and U type pipe fixed connection.

Preferably, the stirring assembly comprises a rotating motor arranged at the bottom of the kettle body, a rotating shaft is fixedly arranged at the output end of the rotating motor, the rotating shaft is fixedly connected with the scraping plate, and a stirring rod is fixedly arranged on the surface of the rotating shaft.

Preferably, the conveying assembly comprises a storage box arranged at the top of the kettle body, a conveying pump is fixedly arranged at the top of the storage box, a liquid suction pipe is fixedly arranged at the bottom of the conveying pump, the bottom end of the liquid suction pipe extends into the storage box, a hose is fixedly arranged at the top of the conveying pump, and the hose is communicated with the U-shaped pipe.

Preferably, the drive assembly is including setting up in the backup pad of mount face in opposite directions, backup pad top fixed mounting has biax motor, biax motor output fixed mounting has first bevel gear, first bevel gear surface engagement is provided with the second bevel gear, the inside fixed mounting of second bevel gear has the screw rod, the screw rod rotates with the mount to be connected, screw rod and movable block threaded connection.

Preferably, a discharging pipe is fixedly arranged at the bottom of the kettle body, and a control valve is arranged on the discharging pipe.

Preferably, the bottom of the kettle body is fixedly provided with a plurality of supporting legs.

Preferably, the fixing frame is of a rectangular frame body structure, and the moving block is in sliding connection with the inner wall of the fixing frame.

Compared with the prior art, the reaction kettle for producing the metal organic framework has the beneficial effects that when the inner wall of the kettle body is required to be cleaned, flushing liquid is conveyed into the U-shaped pipe through the conveying component and then enters the annular pipe and finally is sprayed out of the spray nozzle, so that the residues adhered to the inner wall of the kettle body are flushed, meanwhile, the stirring component drives the scraping plate to rotate, the residues adhered to the inner wall of the kettle body are scraped off, the moving block can move up and down along the fixing frame through the driving component, the heights of the U-shaped pipe, the annular pipe and the spray nozzle can be adjusted, the cleaning mode under multiple pipes is adopted, the residues are flushed out through the spray nozzle, the residues with different properties and different adhesion degrees can be effectively removed through the double effects, the cleaning quality of the inner wall of the kettle body is greatly improved, the production environment of the metal organic framework is pure, the height adjusting function of the spray nozzle is matched, and the whole cleaning process is effectively ensured.

Drawings

FIG. 1 is a three-dimensional perspective view of the present utility model;

FIG. 2 is a front cross-sectional view of the present utility model;

FIG. 3 is a schematic view of a partial structure of the present utility model;

fig. 4 is a left cross-sectional view of another partial structure of the present utility model.

In the figure, 1, a kettle body, 2, a feeding pipe, 3, a rotating motor, 4, a rotating shaft, 5, a stirring rod, 6, a scraping plate, 7, a storage box, 8, a liquid suction pipe, 9, a conveying pump, 10, a hose, 11, a U-shaped pipe, 12, a ring-shaped pipe, 13, a spray head, 14, a fixing frame, 15, a supporting plate, 16, a double-shaft motor, 17, a first bevel gear, 18, a second bevel gear, 19, a screw, 20, a moving block, 21, a blanking pipe, 22 and a supporting leg.

Detailed Description

The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.

Referring to FIGS. 1-4, a reaction kettle for producing a metal organic framework is easy to clean, comprising a kettle body 1, wherein a feed pipe 2 is fixedly arranged at the left side of the kettle body 1, a stirring component is arranged at the bottom of the kettle body 1, a scraping plate 6 is arranged in the kettle body 1 through the stirring component, a conveying component is arranged at the top of the kettle body 1, a U-shaped pipe 11 is arranged at the top of the kettle body 1 through the conveying component, the conveying component comprises a storage tank 7 arranged at the top of the kettle body 1, a conveying pump 9 is fixedly arranged at the top of the storage tank 7, a liquid suction pipe 8 is fixedly arranged at the bottom of the conveying pump 9, the bottom end of the liquid suction pipe 8 extends into the storage tank 7, a hose 10 is fixedly arranged at the top of the conveying pump 9, the hose 10 is communicated with the U-shaped pipe 11, sufficient flushing liquid can be stored in the storage tank 7 in advance, the conveying pump 9 provides stable power, the flushing liquid is pumped from the storage tank 7 through the liquid suction pipe 8 and is rapidly conveyed to the U-shaped pipe 11 through the hose 10, the flushing liquid is ensured to be continuously supplied in the flushing process, the cleaning work is ensured to be continuously carried out, the cleaning efficiency is improved, the U-shaped pipe 11 is in sliding connection with the kettle body 1, the annular pipe 12 is fixedly arranged at the bottom of the U-shaped pipe 11, the spray head 13 is fixedly arranged at the bottom of the annular pipe 12, the fixed frame 14 is fixedly arranged at the top of the kettle body 1, the driving component is arranged on the opposite surface of the fixed frame 14, the movable block 20 is arranged in the fixed frame 14 through the driving component, the fixed frame 14 is in a rectangular frame structure, the movable block 20 is in sliding connection with the inner wall of the fixed frame 14, the movable block 20 is fixedly connected with the U-shaped pipe 11, the driving component comprises a supporting plate 15 arranged on the opposite surface of the fixed frame 14, the top of the supporting plate 15 is fixedly provided with a double-shaft motor 16, the output end of the double-shaft motor 16 is fixedly provided with a first bevel gear 17, the surface of the first bevel gear 17 is meshed with a second bevel gear 18, the screw 19 is fixedly arranged in the second bevel gear 18, the screw 19 is rotationally connected with the fixed frame 14, the screw 19 is in threaded connection with the movable block 20, the driving force is conveniently provided for the upper and lower parts of the movable block 20 through the arrangement of the driving component, so that the height of the spray head 13 is conveniently adjusted, an operator can precisely control the position of the spray head 13 according to actual pollution conditions, the serious pollution area is mainly washed, the cleaning pertinence and effect are improved, the support legs 22 are fixedly arranged at the bottom of the kettle body 1, the number of the support legs 22 is multiple, the metal organic framework is used for producing the reaction kettle easy to clean, when the inner wall of the kettle body 1 needs to be cleaned, flushing fluid is conveyed into the U-shaped pipe 11 through the conveying component, then enters the annular pipe 12 and is finally sprayed out from the spray head 13, so that residues adhered to the inner wall of the kettle body 1 are washed, meanwhile, the scraper blade 6 is driven to rotate through the stirring component, the residues adhered to the inner wall of the kettle body 1 are scraped, the movable block 20 can be made to move up and down along the fixed frame 14 through the driving component, and the U-shaped pipe 11 is made, The annular pipe 12 and the spray head 13 move up and down, the height of the spray head 13 can be adjusted, the cleaning mode under multiple pipes is adopted, flushing liquid sprayed out by the spray head 13 is used for flushing residues, the scraping plate 6 is utilized for rotating and scraping the residues, the dual effects can effectively remove the residues with various properties and different adhesion degrees, the inner wall of the kettle body 1 is ensured to be cleaned, the cleaning quality is greatly improved, the production environment of the metal organic framework is ensured to be pure, the height adjustment function of the spray head 13 is matched, the pollution areas with different heights are covered on the whole, and the whole cleaning process is efficient and orderly.

Specifically, the stirring subassembly is including setting up in the rotating electrical machines 3 of cauldron body 1 bottom, and rotating electrical machines 3 output fixed mounting has pivot 4, and pivot 4 and scraper blade 6 fixed connection, and pivot 4 surface fixed mounting has puddler 5, and at the material reaction stage, can fully stir the material in the cauldron body 1, makes the required various raw materials homogeneous mixing of metal organic framework production promote chemical reaction fully to go on.

Specifically, the bottom of the kettle body 1 is fixedly provided with the blanking pipe 21, the blanking pipe 21 is provided with a control valve, the control valve can completely close the blanking pipe 21 when blanking is not needed, the leakage of materials from the kettle body 1 under the condition of unplanned is effectively prevented, the safety and the neatness of the production environment are ensured, and the safety accidents, the environmental pollution and the material waste possibly caused by the leakage of the materials are reduced.

The electrical components in the connection device are all connected with an external main controller and 220V mains supply, and the main controller can be conventional known equipment for controlling a computer and the like.

When the automatic kettle is used, raw materials are added from the feed pipe 2 to the kettle body 1, the raw materials react in the kettle body 1, meanwhile, the rotating shaft 4 is rotated through the rotating motor 3, the stirring rod 5 is rotated, the raw materials are stirred by the stirring rod 5, after the reaction is completed, the control valve on the blanking pipe 21 is opened, the reacted raw materials are discharged from the blanking pipe 21, when the inner wall of the kettle body 1 needs to be cleaned, flushing liquid in the storage tank 7 is conveyed from the liquid suction pipe 8 to the hose 10 through the conveying pump 9, then enters the U-shaped pipe 11 and then enters the annular pipe 12, finally, the flushing liquid is sprayed out from the spray nozzle 13, so that residues adhered to the inner wall of the kettle body 1 are flushed, meanwhile, the rotating shaft 4 is rotated through the rotating motor 3, the scraping plate 6 is used for scraping the residues adhered to the inner wall of the kettle body 1, the first bevel gear 17 is rotated through the double-shaft motor 16, the second bevel gear 18 is rotated, the screw 19 is rotated, the moving block 20 is moved up and down along the fixing frame 14, and the U-shaped pipe 11 and the annular pipe 12 and the spray nozzle 13 can be adjusted in height.

It is noted that relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.

Claims

1. A cleanable reaction vessel for the production of metal-organic frameworks, comprising a vessel body (1), characterized in that a feed pipe (2) is fixedly installed on the left side of the vessel body (1), a stirring assembly is provided at the bottom of the vessel body (1), a scraper (6) is provided inside the vessel body (1) through the stirring assembly, a conveying assembly is provided at the top of the vessel body (1), a U-shaped tube (11) is provided at the top of the vessel body (1) through the conveying assembly, the U-shaped tube (11) is slidably connected to the vessel body (1), an annular tube (12) is fixedly installed at the bottom of the U-shaped tube (11), a nozzle (13) is fixedly installed at the bottom of the annular tube (12), a fixed frame (14) is fixedly installed at the top of the vessel body (1), a driving assembly is provided on the opposite side of the fixed frame (14), a moving block (20) is provided inside the fixed frame (14) through the driving assembly, and the moving block (20) is fixedly connected to the U-shaped tube (11).

2. The easy-to-clean reaction vessel for the production of metal-organic frameworks according to claim 1, characterized in that the stirring assembly includes a rotary motor (3) disposed at the bottom of the vessel body (1), a rotating shaft (4) is fixedly installed at the output end of the rotary motor (3), the rotating shaft (4) is fixedly connected to a scraper (6), and a stirring rod (5) is fixedly installed on the surface of the rotating shaft (4).

3. The easy-to-clean reaction vessel for the production of metal-organic frameworks according to claim 1, characterized in that the conveying assembly includes a storage tank (7) disposed on the top of the vessel body (1), a conveying pump (9) is fixedly installed on the top of the storage tank (7), a suction pipe (8) is fixedly installed on the bottom of the conveying pump (9), the bottom end of the suction pipe (8) extends into the interior of the storage tank (7), a hose (10) is fixedly installed on the top of the conveying pump (9), and the hose (10) is connected to a U-shaped pipe (11).

4. The easy-to-clean reaction vessel for the production of metal-organic frameworks according to claim 1, characterized in that the driving assembly includes a support plate (15) disposed on the opposing surface of the fixed frame (14), a dual-axis motor (16) is fixedly installed on the top of the support plate (15), a first bevel gear (17) is fixedly installed at the output end of the dual-axis motor (16), a second bevel gear (18) is meshed on the surface of the first bevel gear (17), a screw (19) is fixedly installed inside the second bevel gear (18), the screw (19) is rotatably connected to the fixed frame (14), and the screw (19) is threadedly connected to the moving block (20).

5. The easy-to-clean reaction vessel for the production of metal-organic frameworks according to claim 1, characterized in that a feed pipe (21) is fixedly installed at the bottom of the vessel body (1), and a control valve is provided on the feed pipe (21).

6. The easy-to-clean reaction vessel for the production of metal-organic frameworks according to claim 1, characterized in that a support leg (22) is fixedly installed at the bottom of the vessel body (1), and the number of the support legs (22) is multiple.

7. The easy-to-clean reaction vessel for the production of metal-organic frameworks according to claim 1, characterized in that the fixed frame (14) has a rectangular frame structure, and the movable block (20) is slidably connected to the inner wall of the fixed frame (14).