Multifunctional reaction device for covalent organic framework material
Technical Field
The utility model relates to the technical field of organic framework materials, in particular to a multifunctional reaction device for covalent organic framework materials.
Background
The reaction kettle is widely applied to the fields of petroleum, chemical industry, rubber, pesticides, dyes, medicines, foods and the like, and is a pressure vessel for completing the technological processes of vulcanization, nitration, hydrogenation, hydrocarbylation, polymerization, condensation and the like, such as a reactor, a reaction kettle, a decomposing kettle, a polymerization kettle and the like, and is generally made of carbon-manganese steel, stainless steel, zirconium, nickel-based (Harbour, monel, murphy Kang Nie) alloy and other composite materials.
Through searching, the utility model patent with the Chinese patent number of CN219324207U discloses a multifunctional reaction device for covalent organic framework materials;
Compared with the prior art, the utility model patent with the Chinese patent number of CN219324207U has the advantages that through the structure of rapidly scraping the raw materials on the inner wall of the tank body, the raw materials adhered to the inner wall can be scraped through the first scraping frame and the second scraping frame, the raw materials adhered to the inner wall can be well stirred by matching with the stirring rod, the raw materials are heated and stirred in the early stage through the heat preservation cavity provided with the water storage source, the purpose of protection can be achieved, and the inner wall raw materials can be washed by matching with the cleaning pump in the later stage when the inner raw materials are cleaned, so that the novel scraper is convenient to use.
However, in the practical use process of the device, the first scraping frame and the second scraping frame are not easy to flexibly scrape the inner wall of the tank body, when the raw materials are tightly adhered to the inner wall of the tank body, the raw materials are required to be scraped for many times, the device is not easy to crush the raw materials, and the contact area of the raw materials during stirring is not easy to increase, so that the reaction rate is reduced, and therefore, the multifunctional reaction device for the covalent organic framework material is required to be provided.
Disclosure of utility model
The utility model aims to solve the defects that the inner wall of a tank body is difficult to scrape flexibly, raw materials are required to be scraped for a plurality of times, the raw materials are difficult to smash, the contact area of the raw materials during stirring is difficult to increase, and the reaction rate is reduced in the prior art.
In order to achieve the above purpose, the present utility model adopts the following technical scheme:
The utility model provides a multi-functional reaction unit of covalent organic frame material, includes the supporting seat, the lower part fixedly connected with L template of supporting seat, the upper portion fixedly connected with servo motor of L template, be provided with on the servo motor and strike off the subassembly, strike off the subassembly including striking off the pole and strike off the board, be provided with the stirring on the servo motor and hit garrulous subassembly, the stirring is hit garrulous subassembly including stirring rod and screw, one side swing joint that servo motor was kept away from to the supporting seat has the hang plate, one side fixedly connected with agitator of L template was kept away from to the supporting seat, the outside fixedly connected with discharge gate of agitator, through setting up and strike off the subassembly, can effectively clear away the accessory substance or the impurity of reaction in-process accumulation in material surface or pore.
The technical scheme further comprises the following steps:
the output shaft end part of the servo motor is fixedly connected with a rotating shaft, the outer side of the rotating shaft is fixedly connected with a plurality of stirring rods, and the stirring rods are linearly and uniformly arranged along the rotating shaft.
The outer side of the rotating shaft is fixedly connected with the scraping rods, and the number of the scraping rods is multiple and is uniformly arranged along the circumference of the rotating shaft.
The utility model discloses a scraper blade, including stirring barrel, scraping rod, spring, limiting plate, the scraping rod is close to one side symmetry of stirring barrel and has seted up the sliding tray, the inboard fixedly connected with spring of sliding tray, the one end fixedly connected with limiting plate that the sliding tray was kept away from to the spring.
One side of limiting plate far away from the spring is fixedly connected with connecting pipe, one end of connecting pipe far away from the limiting plate and scraping plate are fixedly connected.
The one end fixedly connected with filter screen of supporting seat is kept away from to the agitator, one side fixedly connected with annular pipe of stirring rod is kept away from to the filter screen, servo motor's one end is kept away from to the pivot runs through whole filter screen.
The one end that servo motor was kept away from to the pivot and fixed connection between the screw, the quantity of screw is the multiunit and is linear evenly arranged along the pivot, the size of screw and the big or small looks adaptation of ring pipe can effectively promote the reactant at the inside even mixing and the dispersion of material, and this has not only accelerated reaction rate.
The one end fixedly connected with feeding case that the agitator was kept away from to the annular pipe, fixed connection between the inboard of feeding case and the inclined plate, the quantity of inclined plate is multiunit and evenly alternately distributes along the feeding case.
The utility model has the following beneficial effects:
1. According to the utility model, by arranging the scraping component, byproducts or impurities accumulated on the surface of the material or in the pore canal in the reaction process can be effectively removed, the blockage phenomenon can be avoided by scraping, and the continuous operation of the device can be realized.
2. According to the utility model, by arranging the stirring and crushing assembly, the uniform mixing and dispersion of reactants in the material can be effectively promoted, the reaction efficiency is improved, and the generation of target products is more rapid and thorough.
Drawings
FIG. 1 is a schematic diagram of the overall structure of a multifunctional reaction device for covalent organic framework materials according to the present utility model;
FIG. 2 is a schematic diagram of a first perspective structure of a multifunctional reaction apparatus for covalent organic framework materials according to the present utility model;
FIG. 3 is a schematic diagram of a second perspective structure of the multifunctional reaction apparatus for covalent organic framework materials according to the present utility model;
FIG. 4 is an enlarged schematic view of the structure shown in FIG. 2A;
fig. 5 is an enlarged schematic view of the structure at B in fig. 1.
The device comprises a supporting seat, a 2, an L-shaped plate, a 3, a servo motor, a 4, a rotating shaft, a 5, a stirring rod, a 6, a stirring barrel, a 7, a scraping rod, a 8, a sliding groove, a 9, a spring, a 10, a discharge hole, a 11, a limiting plate, a 12, a connecting pipe, a 13, a scraping plate, a 14, an annular pipe, a 15, a filter screen, a 16, a screw, a 17, a feeding box, a 18 and an inclined plate.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Example 1
The utility model provides a multifunctional reaction device for covalent organic framework materials, which is shown in figures 1-5 and comprises a supporting seat 1, and is characterized in that the lower part of the supporting seat 1 is fixedly connected with an L-shaped plate 2, the upper part of the L-shaped plate 2 is fixedly connected with a servo motor 3, a scraping component is arranged on the servo motor 3 and comprises a scraping rod 7 and a scraping plate 13, a stirring and crushing component is arranged on the servo motor 3 and comprises a stirring rod 5 and a screw 16, one side of the supporting seat 1, which is far away from the servo motor 3, is movably connected with an inclined plate 18, one side of the supporting seat 1, which is far away from the L-shaped plate 2, is fixedly connected with a stirring barrel 6, and the outer side of the stirring barrel 6 is fixedly connected with a discharge hole 10;
The end part of the output shaft of the servo motor 3 is fixedly connected with a rotating shaft 4, the outer side of the rotating shaft 4 is fixedly connected with a plurality of stirring rods 5, and the stirring rods 5 are linearly and uniformly arranged along the rotating shaft 4;
The outer side of the rotating shaft 4 is fixedly connected with the scraping rods 7, and the number of the scraping rods 7 is a plurality of the scraping rods and the scraping rods are uniformly arranged along the circumference of the rotating shaft 4;
A sliding groove 8 is symmetrically formed in one side of the scraping rod 7, which is close to the stirring barrel 6, a spring 9 is fixedly connected to the inner side of the sliding groove 8, and a limiting plate 11 is fixedly connected to one end, which is far away from the sliding groove 8, of the spring 9;
One side of the limiting plate 11, which is far away from the spring 9, is fixedly connected with a connecting pipe 12, and one end of the connecting pipe 12, which is far away from the limiting plate 11, is fixedly connected with a scraping plate 13;
In this embodiment, drive pivot 4 through start servo motor 3 and rotate, can strike off the raw materials on the agitator 6 many times, hang the in-process of removing, can not destroy the structure of agitator 6, and in particular embodiment, the effect of supporting seat 1 is for supporting whole device, guarantee the stability of whole device, L template 2's effect is for connecting supporting seat 1 and servo motor 3, when servo motor 3 starts, servo motor 3's output shaft tip can drive pivot 4 and rotate, can drive stirring rod 5 and rotate when pivot 4 rotates, thereby stir the inside raw materials of agitator 6, the outside of pivot 4 is fixed connection scraping rod 7 still, scraping rod 7 is close to one side of agitator 6 and has been offered sliding tray 8, the effect of spring 9 is for connecting scraping board 13 through limiting plate 11 and connecting pipe 12, when scraping board 13 and hanging the inner wall of agitator 6, can carry out the one deck to scrape down through spring 9, thereby prevent the destruction to agitator 6 inner wall, scraping rod 7 still contacts with the bottom of agitator 6, when scraping rod 7 rotates, can play and stir the bottom to stir while stirring 6.
Example two
As shown in fig. 1-5, based on the first embodiment, a filter screen 15 is fixedly connected to one end of the stirring barrel 6 away from the supporting seat 1, an annular pipe 14 is fixedly connected to one side of the filter screen 15 away from the stirring rod 5, and one end of the rotating shaft 4 away from the servo motor 3 penetrates through the whole filter screen 15;
one end of the rotating shaft 4 far away from the servo motor 3 is fixedly connected with the propellers 16, the number of the propellers 16 is multiple groups, the propellers 16 are linearly and uniformly arranged along the rotating shaft 4, and the size of the propellers 16 is matched with the size of the annular tube 14;
One end of the annular pipe 14 far away from the stirring barrel 6 is fixedly connected with a feeding box 17, the inner side of the feeding box 17 is fixedly connected with inclined plates 18, and the number of the inclined plates 18 is multiple groups and evenly and crosswise distributed along the feeding box 17.
In this embodiment, when the raw materials pour into the feeding case 17, can increase the area of contact of raw materials step by step, and concrete implementation is, the raw materials brings into the feeding case 17, because of the slope nature of hang plate 18, and the raw materials can one deck drop downwards, when dropping to the annular pipe 14 inside, because of servo motor 3 drives screw 16 and rotates, can smash the raw materials when screw 16 rotates, and the raw materials of smashing can flow into the inside of below agitator 6 through filter screen 15 to further realize that the raw materials can increase the area of contact of raw materials before the stirring.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.