CN223366962U - Multifunctional reaction device for covalent organic framework materials - Google Patents

Multifunctional reaction device for covalent organic framework materials

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Publication number
CN223366962U
CN223366962U CN202422820722.3U CN202422820722U CN223366962U CN 223366962 U CN223366962 U CN 223366962U CN 202422820722 U CN202422820722 U CN 202422820722U CN 223366962 U CN223366962 U CN 223366962U
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fixedly connected
stirring
scraping
servo motor
organic framework
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CN202422820722.3U
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苟杏杏
李亚亚
王以寿
乔成芳
高佳香
贺静慧
陈瑜瑶
高佳雯
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Shangluo University
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Shangluo University
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  • Mixers Of The Rotary Stirring Type (AREA)
  • Crushing And Pulverization Processes (AREA)

Abstract

本实用新型公开了共价有机框架材料多功能反应装置,涉及有机框架材料技术领域,包括支撑座,支撑座的下部固定连接有L型板,L型板的上部固定连接有伺服电机,伺服电机上设置有刮除组件,刮除组件包括有刮除杆和刮除板,伺服电机上设置有搅拌击碎组件,搅拌击碎组件包括有搅拌棒和螺旋桨,支撑座远离伺服电机的一侧活动连接有倾斜板,支撑座远离L型板的一侧固定连接有搅拌桶,搅拌桶的外侧固定连接有出料口,通过设置刮除组件,能够有效清除反应过程中在材料表面或孔道内积累的副产物或杂质,通过设置搅拌击碎组件,能有效促进反应物在材料内部的均匀混合与分散。

The utility model discloses a multifunctional reaction device for covalent organic framework materials, which relates to the technical field of organic framework materials. The device comprises a support base, wherein the lower part of the support base is fixedly connected to an L-shaped plate, the upper part of the L-shaped plate is fixedly connected to a servo motor, a scraping assembly is provided on the servo motor, the scraping assembly comprises a scraping rod and a scraping plate, the servo motor is provided with a stirring and crushing assembly, the stirring and crushing assembly comprises a stirring rod and a propeller, a tilting plate is movably connected to a side of the support base away from the servo motor, a stirring barrel is fixedly connected to a side of the support base away from the L-shaped plate, and a discharge port is fixedly connected to the outer side of the stirring barrel. By arranging the scraping assembly, byproducts or impurities accumulated on the surface of the material or in the pores during the reaction process can be effectively removed, and by arranging the stirring and crushing assembly, uniform mixing and dispersion of reactants inside the material can be effectively promoted.

Description

Multifunctional reaction device for covalent organic framework material
Technical Field
The utility model relates to the technical field of organic framework materials, in particular to a multifunctional reaction device for covalent organic framework materials.
Background
The reaction kettle is widely applied to the fields of petroleum, chemical industry, rubber, pesticides, dyes, medicines, foods and the like, and is a pressure vessel for completing the technological processes of vulcanization, nitration, hydrogenation, hydrocarbylation, polymerization, condensation and the like, such as a reactor, a reaction kettle, a decomposing kettle, a polymerization kettle and the like, and is generally made of carbon-manganese steel, stainless steel, zirconium, nickel-based (Harbour, monel, murphy Kang Nie) alloy and other composite materials.
Through searching, the utility model patent with the Chinese patent number of CN219324207U discloses a multifunctional reaction device for covalent organic framework materials;
Compared with the prior art, the utility model patent with the Chinese patent number of CN219324207U has the advantages that through the structure of rapidly scraping the raw materials on the inner wall of the tank body, the raw materials adhered to the inner wall can be scraped through the first scraping frame and the second scraping frame, the raw materials adhered to the inner wall can be well stirred by matching with the stirring rod, the raw materials are heated and stirred in the early stage through the heat preservation cavity provided with the water storage source, the purpose of protection can be achieved, and the inner wall raw materials can be washed by matching with the cleaning pump in the later stage when the inner raw materials are cleaned, so that the novel scraper is convenient to use.
However, in the practical use process of the device, the first scraping frame and the second scraping frame are not easy to flexibly scrape the inner wall of the tank body, when the raw materials are tightly adhered to the inner wall of the tank body, the raw materials are required to be scraped for many times, the device is not easy to crush the raw materials, and the contact area of the raw materials during stirring is not easy to increase, so that the reaction rate is reduced, and therefore, the multifunctional reaction device for the covalent organic framework material is required to be provided.
Disclosure of utility model
The utility model aims to solve the defects that the inner wall of a tank body is difficult to scrape flexibly, raw materials are required to be scraped for a plurality of times, the raw materials are difficult to smash, the contact area of the raw materials during stirring is difficult to increase, and the reaction rate is reduced in the prior art.
In order to achieve the above purpose, the present utility model adopts the following technical scheme:
The utility model provides a multi-functional reaction unit of covalent organic frame material, includes the supporting seat, the lower part fixedly connected with L template of supporting seat, the upper portion fixedly connected with servo motor of L template, be provided with on the servo motor and strike off the subassembly, strike off the subassembly including striking off the pole and strike off the board, be provided with the stirring on the servo motor and hit garrulous subassembly, the stirring is hit garrulous subassembly including stirring rod and screw, one side swing joint that servo motor was kept away from to the supporting seat has the hang plate, one side fixedly connected with agitator of L template was kept away from to the supporting seat, the outside fixedly connected with discharge gate of agitator, through setting up and strike off the subassembly, can effectively clear away the accessory substance or the impurity of reaction in-process accumulation in material surface or pore.
The technical scheme further comprises the following steps:
the output shaft end part of the servo motor is fixedly connected with a rotating shaft, the outer side of the rotating shaft is fixedly connected with a plurality of stirring rods, and the stirring rods are linearly and uniformly arranged along the rotating shaft.
The outer side of the rotating shaft is fixedly connected with the scraping rods, and the number of the scraping rods is multiple and is uniformly arranged along the circumference of the rotating shaft.
The utility model discloses a scraper blade, including stirring barrel, scraping rod, spring, limiting plate, the scraping rod is close to one side symmetry of stirring barrel and has seted up the sliding tray, the inboard fixedly connected with spring of sliding tray, the one end fixedly connected with limiting plate that the sliding tray was kept away from to the spring.
One side of limiting plate far away from the spring is fixedly connected with connecting pipe, one end of connecting pipe far away from the limiting plate and scraping plate are fixedly connected.
The one end fixedly connected with filter screen of supporting seat is kept away from to the agitator, one side fixedly connected with annular pipe of stirring rod is kept away from to the filter screen, servo motor's one end is kept away from to the pivot runs through whole filter screen.
The one end that servo motor was kept away from to the pivot and fixed connection between the screw, the quantity of screw is the multiunit and is linear evenly arranged along the pivot, the size of screw and the big or small looks adaptation of ring pipe can effectively promote the reactant at the inside even mixing and the dispersion of material, and this has not only accelerated reaction rate.
The one end fixedly connected with feeding case that the agitator was kept away from to the annular pipe, fixed connection between the inboard of feeding case and the inclined plate, the quantity of inclined plate is multiunit and evenly alternately distributes along the feeding case.
The utility model has the following beneficial effects:
1. According to the utility model, by arranging the scraping component, byproducts or impurities accumulated on the surface of the material or in the pore canal in the reaction process can be effectively removed, the blockage phenomenon can be avoided by scraping, and the continuous operation of the device can be realized.
2. According to the utility model, by arranging the stirring and crushing assembly, the uniform mixing and dispersion of reactants in the material can be effectively promoted, the reaction efficiency is improved, and the generation of target products is more rapid and thorough.
Drawings
FIG. 1 is a schematic diagram of the overall structure of a multifunctional reaction device for covalent organic framework materials according to the present utility model;
FIG. 2 is a schematic diagram of a first perspective structure of a multifunctional reaction apparatus for covalent organic framework materials according to the present utility model;
FIG. 3 is a schematic diagram of a second perspective structure of the multifunctional reaction apparatus for covalent organic framework materials according to the present utility model;
FIG. 4 is an enlarged schematic view of the structure shown in FIG. 2A;
fig. 5 is an enlarged schematic view of the structure at B in fig. 1.
The device comprises a supporting seat, a 2, an L-shaped plate, a 3, a servo motor, a 4, a rotating shaft, a 5, a stirring rod, a 6, a stirring barrel, a 7, a scraping rod, a 8, a sliding groove, a 9, a spring, a 10, a discharge hole, a 11, a limiting plate, a 12, a connecting pipe, a 13, a scraping plate, a 14, an annular pipe, a 15, a filter screen, a 16, a screw, a 17, a feeding box, a 18 and an inclined plate.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Example 1
The utility model provides a multifunctional reaction device for covalent organic framework materials, which is shown in figures 1-5 and comprises a supporting seat 1, and is characterized in that the lower part of the supporting seat 1 is fixedly connected with an L-shaped plate 2, the upper part of the L-shaped plate 2 is fixedly connected with a servo motor 3, a scraping component is arranged on the servo motor 3 and comprises a scraping rod 7 and a scraping plate 13, a stirring and crushing component is arranged on the servo motor 3 and comprises a stirring rod 5 and a screw 16, one side of the supporting seat 1, which is far away from the servo motor 3, is movably connected with an inclined plate 18, one side of the supporting seat 1, which is far away from the L-shaped plate 2, is fixedly connected with a stirring barrel 6, and the outer side of the stirring barrel 6 is fixedly connected with a discharge hole 10;
The end part of the output shaft of the servo motor 3 is fixedly connected with a rotating shaft 4, the outer side of the rotating shaft 4 is fixedly connected with a plurality of stirring rods 5, and the stirring rods 5 are linearly and uniformly arranged along the rotating shaft 4;
The outer side of the rotating shaft 4 is fixedly connected with the scraping rods 7, and the number of the scraping rods 7 is a plurality of the scraping rods and the scraping rods are uniformly arranged along the circumference of the rotating shaft 4;
A sliding groove 8 is symmetrically formed in one side of the scraping rod 7, which is close to the stirring barrel 6, a spring 9 is fixedly connected to the inner side of the sliding groove 8, and a limiting plate 11 is fixedly connected to one end, which is far away from the sliding groove 8, of the spring 9;
One side of the limiting plate 11, which is far away from the spring 9, is fixedly connected with a connecting pipe 12, and one end of the connecting pipe 12, which is far away from the limiting plate 11, is fixedly connected with a scraping plate 13;
In this embodiment, drive pivot 4 through start servo motor 3 and rotate, can strike off the raw materials on the agitator 6 many times, hang the in-process of removing, can not destroy the structure of agitator 6, and in particular embodiment, the effect of supporting seat 1 is for supporting whole device, guarantee the stability of whole device, L template 2's effect is for connecting supporting seat 1 and servo motor 3, when servo motor 3 starts, servo motor 3's output shaft tip can drive pivot 4 and rotate, can drive stirring rod 5 and rotate when pivot 4 rotates, thereby stir the inside raw materials of agitator 6, the outside of pivot 4 is fixed connection scraping rod 7 still, scraping rod 7 is close to one side of agitator 6 and has been offered sliding tray 8, the effect of spring 9 is for connecting scraping board 13 through limiting plate 11 and connecting pipe 12, when scraping board 13 and hanging the inner wall of agitator 6, can carry out the one deck to scrape down through spring 9, thereby prevent the destruction to agitator 6 inner wall, scraping rod 7 still contacts with the bottom of agitator 6, when scraping rod 7 rotates, can play and stir the bottom to stir while stirring 6.
Example two
As shown in fig. 1-5, based on the first embodiment, a filter screen 15 is fixedly connected to one end of the stirring barrel 6 away from the supporting seat 1, an annular pipe 14 is fixedly connected to one side of the filter screen 15 away from the stirring rod 5, and one end of the rotating shaft 4 away from the servo motor 3 penetrates through the whole filter screen 15;
one end of the rotating shaft 4 far away from the servo motor 3 is fixedly connected with the propellers 16, the number of the propellers 16 is multiple groups, the propellers 16 are linearly and uniformly arranged along the rotating shaft 4, and the size of the propellers 16 is matched with the size of the annular tube 14;
One end of the annular pipe 14 far away from the stirring barrel 6 is fixedly connected with a feeding box 17, the inner side of the feeding box 17 is fixedly connected with inclined plates 18, and the number of the inclined plates 18 is multiple groups and evenly and crosswise distributed along the feeding box 17.
In this embodiment, when the raw materials pour into the feeding case 17, can increase the area of contact of raw materials step by step, and concrete implementation is, the raw materials brings into the feeding case 17, because of the slope nature of hang plate 18, and the raw materials can one deck drop downwards, when dropping to the annular pipe 14 inside, because of servo motor 3 drives screw 16 and rotates, can smash the raw materials when screw 16 rotates, and the raw materials of smashing can flow into the inside of below agitator 6 through filter screen 15 to further realize that the raw materials can increase the area of contact of raw materials before the stirring.
Although embodiments of the present utility model have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.

Claims (8)

1.共价有机框架材料多功能反应装置,包括支撑座(1),其特征在于,所述支撑座(1)的下部固定连接有L型板(2),所述L型板(2)的上部固定连接有伺服电机(3),所述伺服电机(3)上设置有刮除组件,所述刮除组件包括有刮除杆(7)和刮除板(13),所述伺服电机(3)上设置有搅拌击碎组件,所述搅拌击碎组件包括有搅拌棒(5)和螺旋桨(16),所述支撑座(1)远离伺服电机(3)的一侧活动连接有倾斜板(18),所述支撑座(1)远离L型板(2)的一侧固定连接有搅拌桶(6),所述搅拌桶(6)的外侧固定连接有出料口(10)。1. A multifunctional reaction device for covalent organic framework materials, comprising a support base (1), characterized in that the lower portion of the support base (1) is fixedly connected to an L-shaped plate (2), the upper portion of the L-shaped plate (2) is fixedly connected to a servo motor (3), a scraping assembly is provided on the servo motor (3), the scraping assembly includes a scraping rod (7) and a scraping plate (13), a stirring and crushing assembly is provided on the servo motor (3), the stirring and crushing assembly includes a stirring rod (5) and a propeller (16), the support base (1) is movably connected to an inclined plate (18) on a side away from the servo motor (3), the support base (1) is fixedly connected to a stirring barrel (6) on a side away from the L-shaped plate (2), and the outer side of the stirring barrel (6) is fixedly connected to a discharge port (10). 2.根据权利要求1所述的共价有机框架材料多功能反应装置,其特征在于,所述伺服电机(3)的输出轴端部固定连接有转轴(4),所述转轴(4)的外侧固定连接有多个搅拌棒(5),多个所述搅拌棒(5)沿转轴(4)呈线性均匀排列。2. The multifunctional reaction device for covalent organic framework materials according to claim 1 is characterized in that the output shaft end of the servo motor (3) is fixedly connected to a rotating shaft (4), and a plurality of stirring rods (5) are fixedly connected to the outer side of the rotating shaft (4), and the plurality of stirring rods (5) are linearly and evenly arranged along the rotating shaft (4). 3.根据权利要求2所述的共价有机框架材料多功能反应装置,其特征在于,所述转轴(4)的外侧和刮除杆(7)之间固定连接,所述刮除杆(7)的数量为多个并沿转轴(4)呈圆周均匀排列。3. The multifunctional reaction device of covalent organic framework materials according to claim 2 is characterized in that the outer side of the rotating shaft (4) and the scraping rod (7) are fixedly connected, and the scraping rods (7) are multiple and evenly arranged in a circle along the rotating shaft (4). 4.根据权利要求3所述的共价有机框架材料多功能反应装置,其特征在于,所述刮除杆(7)靠近搅拌桶(6)的一侧对称开设有滑动槽(8),所述滑动槽(8)的内侧固定连接有弹簧(9),所述弹簧(9)远离滑动槽(8)的一端固定连接有限位板(11)。4. The multifunctional reaction device for covalent organic framework materials according to claim 3 is characterized in that a sliding groove (8) is symmetrically provided on one side of the scraping rod (7) close to the stirring barrel (6), a spring (9) is fixedly connected to the inner side of the sliding groove (8), and the end of the spring (9) away from the sliding groove (8) is fixedly connected to a limiting plate (11). 5.根据权利要求4所述的共价有机框架材料多功能反应装置,其特征在于,所述限位板(11)远离弹簧(9)的一侧固定连接有连接管(12),所述连接管(12)远离限位板(11)的一端和刮除板(13)之间固定连接。5. The multifunctional reaction device of covalent organic framework materials according to claim 4 is characterized in that a connecting tube (12) is fixedly connected to the side of the limiting plate (11) away from the spring (9), and the end of the connecting tube (12) away from the limiting plate (11) is fixedly connected to the scraping plate (13). 6.根据权利要求2所述的共价有机框架材料多功能反应装置,其特征在于,所述搅拌桶(6)远离支撑座(1)的一端固定连接有过滤网(15),所述过滤网(15)远离搅拌棒(5)的一侧固定连接有环形管(14),所述转轴(4)远离伺服电机(3)的一端贯穿整个过滤网(15)。6. The multifunctional reaction device for covalent organic framework materials according to claim 2 is characterized in that the end of the stirring barrel (6) away from the support seat (1) is fixedly connected to a filter screen (15), the side of the filter screen (15) away from the stirring rod (5) is fixedly connected to an annular tube (14), and the end of the rotating shaft (4) away from the servo motor (3) passes through the entire filter screen (15). 7.根据权利要求2所述的共价有机框架材料多功能反应装置,其特征在于,所述转轴(4)远离伺服电机(3)的一端和螺旋桨(16)之间固定连接,所述螺旋桨(16)的数量为多组并沿转轴(4)呈线性均匀排列,所述螺旋桨(16)的大小和环形管(14)的大小相适配。7. The multifunctional reaction device of covalent organic framework materials according to claim 2 is characterized in that the end of the rotating shaft (4) away from the servo motor (3) is fixedly connected to the propeller (16), the number of the propellers (16) is multiple groups and they are linearly and evenly arranged along the rotating shaft (4), and the size of the propellers (16) is adapted to the size of the annular tube (14). 8.根据权利要求7所述的共价有机框架材料多功能反应装置,其特征在于,所述环形管(14)远离搅拌桶(6)的一端固定连接有进料箱(17),所述进料箱(17)的内侧和倾斜板(18)之间固定连接,所述倾斜板(18)的数量为多组并沿进料箱(17)均匀交叉分布。8. The multifunctional reaction device for covalent organic framework materials according to claim 7 is characterized in that the end of the annular tube (14) away from the stirring barrel (6) is fixedly connected to a feed box (17), the inner side of the feed box (17) and the inclined plate (18) are fixedly connected, and the number of the inclined plates (18) is multiple groups and is evenly cross-distributed along the feed box (17).
CN202422820722.3U 2024-11-19 2024-11-19 Multifunctional reaction device for covalent organic framework materials Active CN223366962U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202422820722.3U CN223366962U (en) 2024-11-19 2024-11-19 Multifunctional reaction device for covalent organic framework materials

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Application Number Priority Date Filing Date Title
CN202422820722.3U CN223366962U (en) 2024-11-19 2024-11-19 Multifunctional reaction device for covalent organic framework materials

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CN223366962U true CN223366962U (en) 2025-09-23

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