Macroporous resin regeneration treatment device for pseudo-ginseng extraction
Technical Field
The utility model relates to the technical field of macroporous resin regeneration, in particular to a macroporous resin regeneration treatment device for pseudo-ginseng extraction.
Background
The Notoginseng radix has total saponins as main active ingredient, and can be used for preventing and treating cardiovascular and cerebrovascular diseases such as hyperlipidemia, hypertension, atherosclerosis, myocardial ischemia, and ischemic cerebral apoplexy. The extraction method mainly comprises the steps of crushing dry notoginseng, extracting with ethanol, recovering ethanol under reduced pressure, adsorbing, eluting with ethanol, recovering ethanol under reduced pressure, decoloring, concentrating, drying and the like. Macroporous resin is used in the process of extracting and adsorbing the pseudo-ginseng active ingredients, and the macroporous resin is a macromolecular adsorption resin which does not contain exchange groups and has a macroporous structure, has a good macroporous net structure and a larger specific surface area, and can selectively adsorb organic matters in the aqueous solution through physics. The adsorption capacity of the macroporous resin is reduced after the macroporous resin is used for a certain time, and the macroporous resin needs to be regenerated for continuous use after the macroporous resin is used for a certain time in order not to reduce the extraction effect of the effective components of the pseudo-ginseng.
The prior art has the problems that the macroporous resin is not completely cleaned and the regeneration effect is poor, so that the subsequent normal use of the macroporous resin is affected, the traditional method adopts a long-time soaking mode in the cleaning process, the time consumption is long, the cleaning efficiency is low, the contact between the macroporous resin and cleaning liquid is promoted in a stirring or vibrating mode and the like for improving the efficiency, the macroporous resin is fragile, the macroporous resin is cracked, the macroporous resin is lost and wasted, and the use cost of the macroporous resin is increased. Therefore, the macroporous resin regeneration treatment device for the notoginseng extraction, which is thoroughly cleaned, high in regeneration efficiency and not easy to crack, is objectively required.
Disclosure of utility model
The utility model aims to provide a macroporous resin regeneration treatment device for pseudo-ginseng extraction, which has thorough cleaning, high regeneration efficiency and difficult fragmentation.
The utility model aims at realizing the technical scheme that the novel automatic feeding device comprises a tank body and a feeding hole, wherein a liquid inlet is formed in the tank body, a vertical cylinder is concentrically arranged in the tank body, a plurality of rectangular vertical grooves are uniformly distributed on the circumference of the outer wall of the vertical cylinder, the rectangular vertical grooves are mutually communicated with the vertical cylinder, a plurality of through holes are respectively formed in two sides of the rectangular vertical grooves, a bottom plate is arranged at the bottoms of the vertical cylinder and the rectangular vertical grooves, a motor is arranged at the bottom of the tank body, an output shaft of the motor is fixedly connected with the center of the bottom plate after extending into the tank body, a circular plate is arranged at the upper part in the vertical cylinder, an air cylinder is arranged at the top of the tank body, a piston rod of the air cylinder is rotatably connected with the center of the circular plate, a plurality of rectangular plates are arranged around the circular plate, the edges of the rectangular plates are matched with the inner walls of the rectangular vertical grooves, the circular plates are connected with the rectangular plates through connecting rods, an annular blanking channel is arranged between the circular plate and the rectangular plates, the feeding hole is positioned at the top of the tank body above the blanking channel, and a discharging pipe is arranged at the bottom of the tank body.
Further, a solid-liquid separator, a dryer and a screening machine are sequentially arranged on the discharge pipe.
Further, the output shaft of the motor is connected with the bottom plate through a flange.
Further, a flow guide pipe is obliquely arranged on the through hole of the rectangular vertical groove, and the lower end of the flow guide pipe is communicated with the through hole.
Further, a discharging pipe is arranged on the side wall of the bottom of the rectangular vertical groove, and a gate valve is arranged on the discharging pipe.
Further, a scraping plate is arranged on an output shaft of the motor, and the lower end face of the scraping plate is in contact with the bottom of the tank body.
Further, a plurality of ventilation holes are formed in the bottom plate, an air distributor is arranged in the tank body below the bottom plate, and an air pipe communicated with the air distributor is arranged on the tank body.
Further, rubber layers are arranged on the inner walls of the vertical cylinder and the rectangular vertical groove.
Further, a turbulent vertical plate is arranged on the inner wall of the tank body.
When the utility model operates, a proper amount of cleaning liquid is firstly introduced into the tank body from the liquid inlet, the cleaning liquid can be selected from clear water, acid liquor, alkali liquor, ethanol and the like according to the requirements, then the motor is started, the cleaning liquid enters the rectangular vertical groove and the inside of the vertical cylinder from the through holes, the motor drives the bottom plate, the vertical cylinder, the rectangular vertical groove, the circular plate and the rectangular plate to synchronously rotate, macroporous resin needing regeneration is introduced into the tank body from the feed inlet, falls into the inside of the vertical cylinder from the blanking channel and rotates along with the tank, is scattered around under the action of centrifugal force and gradually enters each rectangular vertical groove, at the moment, the cleaning liquid enters the rectangular vertical groove from the through holes at one side of the rectangular vertical groove and then is discharged from the through holes at the other side of the rectangular vertical groove, in the process, the cleaning liquid contacts the macroporous resin in the flowing process, and the cleaning liquid can continuously permeate into the inside of the macroporous resin due to a certain impact force, and the cleaning regeneration of the macroporous resin is realized. In the utility model, macroporous resin is firstly led into the vertical cylinder and then enters the rectangular vertical groove under the action of centrifugal force, at the moment, the macroporous resin forms a vertical wall in the rectangular vertical groove, when the vertical wall rotates, the cleaning liquid in the tank body is pushed, the cleaning liquid close to the vertical wall enters the rectangular vertical groove from the through hole to clean the macroporous resin, the cleaning liquid is in a continuous flowing state and has a certain impact stirring effect on the macroporous resin, the macroporous resin can be continuously turned over, impurities adsorbed in the macroporous resin can be rapidly taken away, the macroporous resin is thoroughly cleaned and regenerated, the regeneration effect is better, and the subsequent normal use of the macroporous resin is ensured as much as possible; secondly, aiming at the characteristic that macroporous resin floats in cleaning liquid, the device can drive the circular plate and the rectangular plate to downwards press the macroporous resin into the cleaning liquid through the cylinder in the process of regenerating the macroporous resin, then lift the circular plate and the rectangular plate, the macroporous resin floats upwards along with the upward floating, the macroporous resin can float in the cleaning liquid and further play a role of turning the macroporous resin, the macroporous resin is in a motion state, the cleaning efficiency and the regeneration effect of the macroporous resin are improved, in addition, compared with the traditional method, the cleaning liquid and the macroporous resin in the device are in a relative motion state in a long-time soaking mode, the cleaning efficiency is improved, the stirring or vibration mode is canceled, the mode of driving the macroporous resin to rotate by adopting the vertical cylinder and the rectangular vertical groove, and the mode of pushing the macroporous resin downwards by adopting the circular plate and the rectangular plate are more gentle, on the premise of achieving efficient cleaning and regeneration, the mode of promoting the macroporous resin and the full contact is more gentle, the probability and possibility of cracking of macroporous resin can be reduced, the loss and waste of macroporous resin are reduced, the integrity of macroporous resin in the regeneration process is ensured, and the use cost of macroporous resin is further reduced. In conclusion, the utility model has the advantages of thorough cleaning, high regeneration efficiency and difficult fragmentation.
Drawings
FIG. 1 is a schematic diagram of the overall structure of the present utility model;
FIG. 2 is a schematic cross-sectional view of A-A of FIG. 1;
FIG. 3 is a schematic view of the rectangular vertical trough 3 and draft tube 16 according to the present utility model;
In the figure, the device comprises a 1-tank body, a 2-vertical cylinder, a 3-rectangular vertical groove, a 4-bottom plate, a 5-motor, a 6-circular plate, a 7-cylinder, an 8-rectangular plate, a 9-connecting rod, a 10-blanking channel, an 11-feeding port, a 12-solid-liquid separator, a 13-dryer, a 14-screening machine, a 15-flange, a 16-flow guiding pipe, a 17-discharging pipe, an 18-scraping plate, a 19-gas distributor, a 20-gas pipe, a 21-rubber layer and a 22-turbulent vertical plate.
Detailed Description
The utility model is further described below with reference to the accompanying drawings, without limiting the utility model in any way, and any alterations or modifications based on the utility model are within the scope of the utility model.
As shown in fig. 1-3, the utility model comprises a tank body 1 and a feed inlet 11, wherein the tank body 1 is provided with the feed inlet, a vertical cylinder 2 is concentrically arranged in the tank body 1, a plurality of rectangular vertical grooves 3 are uniformly distributed on the circumference of the outer wall of the vertical cylinder 2, the rectangular vertical grooves 3 are mutually communicated with the vertical cylinder 2, two sides of the rectangular vertical grooves 3 are respectively provided with a plurality of through holes, the size of the through holes is determined according to the particle size of macroporous resin, the size of the through holes is ensured to be smaller than that of the macroporous resin, the bottoms of the vertical cylinder 2 and the rectangular vertical grooves 3 are provided with a bottom plate 4, the bottom of the tank body 1 is provided with a motor 5, an output shaft of the motor 5 stretches into the tank body 1 and is fixedly connected with the center of the bottom plate 4, the upper part of the vertical cylinder 2 is provided with a rectangular circular plate 6, the top of the tank body 1 is provided with a cylinder 7, a piston rod of the cylinder 7 is rotationally connected with the center of the circular plate 6, a plurality of circular plates 8 are arranged around the circular plate 6, the edges of the rectangular plates 8 are matched with the inner walls of the corresponding rectangular vertical grooves 3, the circular plates 6 are connected with the rectangular plates 8 through connecting rods 9, blanking annular channels 10 are arranged between the circular plates 6 and the rectangular plates 8, and the blanking annular channels 10 can be smoothly fed into the rectangular channels 10, and can smoothly enter the annular channels 11, and can smoothly enter the annular channels, and enter the resin channels 11. When the macroporous resin regeneration device is in operation, the motor 5 can be adopted to rotate forward and backward, so that the vertical cylinder 2 and the rectangular vertical groove 3 rotate forward for a period of time and then turn over for a period of time, the stirring effect of macroporous resin is improved, and the regeneration efficiency of macroporous resin is improved.
The feed inlet 11 is located the jar body 1 top of blanking passageway 10 top, and the bottom of jar body 1 is provided with row material pipe. The motor 5 and the cylinder 7 are existing devices and can be purchased, installed and used in the market according to actual parameters.
When the utility model operates, a proper amount of cleaning liquid is firstly introduced into the tank body 1 from the liquid inlet, the cleaning liquid can be selected from clear water, acid liquor, alkali liquor, ethanol and the like according to the requirements, then the motor 5 is started, the cleaning liquid enters the rectangular vertical groove 3 and the inside of the vertical cylinder 2 from the through holes, the motor 5 drives the bottom plate 4, the vertical cylinder 2, the rectangular vertical groove 3, the circular plate 6 and the rectangular plate 8 to synchronously rotate, macroporous resin needing regeneration treatment is led into the tank body 1 from the feed inlet, falls into the vertical cylinder 2 from the blanking channel 10 and rotates along with the vertical groove, is dispersed around under the effect of centrifugal force and gradually enters each rectangular vertical groove 3, at the moment, the cleaning liquid enters the rectangular vertical groove 3 from the through holes at one side and is discharged from the through holes at the other side, and in the process, the cleaning liquid is contacted with the macroporous resin in the flowing process, and the cleaning liquid can continuously permeate into the macroporous resin due to a certain impact force, so that the cleaning regeneration of the macroporous resin is realized. In the utility model, macroporous resin is firstly led into the vertical cylinder 2 and then enters the rectangular vertical groove 3 under the action of centrifugal force, at this time, the macroporous resin forms a vertical wall in the rectangular vertical groove 3, when the vertical wall rotates, the cleaning liquid in the tank body 1 is pushed, the cleaning liquid close to the vertical wall enters the rectangular vertical groove 3 from the through hole to clean the macroporous resin, the cleaning liquid is in a continuous flowing state, and has a certain impact stirring effect on the macroporous resin, so that the macroporous resin can be continuously turned over, impurities adsorbed in the macroporous resin can be rapidly taken away, the cleaning and regeneration of the macroporous resin are realized, the cleaning is thorough, the regeneration effect is good, and the subsequent normal use of the macroporous resin is ensured as much as possible; secondly, aiming at the characteristic that macroporous resin floats in cleaning liquid, the device can drive the circular plate 6 and the rectangular plate 8 to downwards press through the cylinder 7 in the process of regenerating the macroporous resin, press the macroporous resin into the cleaning liquid, then lift the circular plate 6 and the rectangular plate 8 back, and the macroporous resin floats in the cleaning liquid continuously, thereby playing a role of turning the macroporous resin, leading the macroporous resin to be in a motion state, improving the cleaning efficiency and the regeneration effect of the macroporous resin, in addition, compared with the traditional method, the cleaning liquid and the macroporous resin in the device are in a relative motion state in a long-time soaking mode, thereby being beneficial to shortening the cleaning time, improving the cleaning efficiency, and simultaneously canceling the stirring or vibration mode, but adopting the mode of driving the macroporous resin to rotate by adopting the vertical cylinder 2 and the rectangular vertical groove 3, and adopting the mode of pressing the macroporous resin by the circular plate 6 and the rectangular plate 8, on the premise of achieving efficient cleaning and regeneration, the method for promoting the macroporous resin to be fully contacted with the cleaning liquid is milder, the probability and possibility of fragmentation of the macroporous resin can be reduced, the loss and waste of the macroporous resin are reduced, the integrity of the macroporous resin in the regeneration process is ensured, and the use cost of the macroporous resin is further reduced.
The solid-liquid separator 12, the dryer 13 and the screening machine 14 are sequentially arranged on the discharging pipe, the solid-liquid separator 12, the dryer 13 and the screening machine 14 are all existing equipment, the solid-liquid separator 12 is used for separating macroporous resin from cleaning liquid, the dryer 13 is used for drying the macroporous resin, and the screening machine 14 is used for screening the macroporous resin and separating scraps and fine impurities.
The output shaft of the motor 5 is connected with the bottom plate 4 through the flange 15, and in order to facilitate the disassembly and assembly between the output shaft of the motor 5 and the bottom plate 4, the connection is realized in the form of the flange 15, and in the actual use process, the connection structure in other structural forms can be adopted according to the actual situation.
The through hole of the rectangular vertical groove 3 is obliquely provided with the flow guide pipe 16, the lower end of the flow guide pipe 16 is communicated with the through hole, the flow guide pipe 16 rotates synchronously along with the rectangular vertical groove 3, cleaning liquid enters the rectangular vertical groove 3 from the upper end of the flow guide pipe 16, then enters the rectangular vertical groove 3 from the lower end of the flow guide pipe, and water flow is in an inclined downward flowing state, so that macroporous resin can sink to the lower part of the cleaning liquid while impacting the macroporous resin, then floats upwards under the action of a floating force, and the cleaning and regenerating effects of the macroporous resin can be promoted by continuously reciprocating the process.
The side wall of the bottom of the rectangular vertical groove 3 is provided with a discharge pipe 17, the discharge pipe 17 is provided with a gate valve, after the macroporous resin is washed and regenerated, the discharge pipe 17 is arranged for being conveniently discharged, the macroporous resin is firstly pressed down through the circular plate 6 and the rectangular plate 8, the gate valve is opened, the macroporous resin is discharged from the discharge pipe 17 under the action of centrifugal force, and finally the macroporous resin is discharged through the discharge pipe.
The scraper 18 is arranged on the output shaft of the motor 5, the lower end face of the scraper 18 is in contact with the bottom of the tank body 1, the scraper 18 can scrape impurities deposited at the bottom of the tank body 1 away so that the impurities can be discharged from the discharge pipe along with cleaning liquid, meanwhile, when macroporous resin is discharged from the bottom of the rectangular vertical groove 3, the macroporous resin falls at the bottom of the tank body 1, the scraper 18 can play a role in stirring the macroporous resin, the cleaning effect of the macroporous resin is further improved, and in order to prevent the scraper 18 from crushing the macroporous resin, the surface of the scraper 18 can be wrapped with a layer of rubber material.
A plurality of ventilation holes are processed on the bottom plate 4, an air distributor 19 is arranged in the tank body 1 below the bottom plate 4, and an air pipe 20 communicated with the air distributor 19 is arranged on the tank body 1. The gas distributor 19 is in the prior art and is used for uniformly distributing gas on the cross section of the tank body 1, the gas is sprayed into the cleaning liquid from the gas distributor 19 to form a plurality of tiny bubbles, the bubbles enter the rectangular vertical groove 2 and the vertical cylinder 2 through the vent holes, the macroporous resin can be stirred in the rising process of the bubbles, and the regeneration effect of the macroporous resin is improved. When the cleaning liquid adopts ethanol, cold air can be introduced into the air pipe 20, and the cold air can absorb heat in the ethanol and macroporous resin, so that the temperature of the ethanol and macroporous resin is reduced, and the aim of freezing is achieved.
Be provided with rubber layer 21 on the inner wall of the vertical tube 2 and the rectangle vertical tank 3, macroporous resin is comparatively fragile, if it directly strikes on the inner wall of the vertical tube 2 and the rectangle vertical tank 3, produces cracked problem easily, leads to macroporous resin's waste, and has set up behind the rubber layer 21, because rubber layer 21 has certain flexibility and elasticity, can play the effect of buffering, and then reduce macroporous resin cracked possibility.
Be provided with vortex riser 22 on jar body 1's the inner wall, this device is when the operation, it rotates to drive the vertical section of thick bamboo 2 and the perpendicular groove of rectangle 3 by motor 5, and drive the washing liquid and rotate, the velocity of flow of washing liquid can constantly improve, finally be close the rotational speed of perpendicular groove of rectangle 3, at this moment, the washing liquid that gets into in the perpendicular inslot of rectangle 3 will be less, macroporous resin's cleaning efficiency will reduce, the vortex riser 22 has been set up for improving this condition, when the washing liquid flows on the vortex riser 22, receive the baffle of vortex riser 22, the flow direction and the velocity of flow of partial washing liquid change, and then produce the influence to the washing liquid on every side, produce the vortex, prevent the problem that the whirl velocity of washing liquid and the rotational speed of perpendicular groove of rectangle 3 are close, ensure macroporous resin's cleaning efficiency.