Waste acid recycling device for sulfenamide nitrification and denitrification
Technical Field
The utility model belongs to the technical field of waste acid recycling, and particularly relates to a waste acid recycling device for nitrification and denitrification of sulfenamide.
Background
The utility model discloses a sulfenamide nitration reaction device with a publication number of CN216630774U, which relates to the technical field of sulfenamide synthesis. One side of the homogenizer is communicated with a first inlet, a second inlet and a circulating inlet, an outlet at the other side of the homogenizer is communicated with a feed inlet of the static mixer through a connecting pipe, a water pump is arranged on the connecting pipe, a discharge outlet of the static mixer is communicated with a feed inlet of the nitration kettle through a pipeline, a circulating outlet is arranged on the side face of the nitration kettle, the circulating outlet is communicated with the circulating inlet through a circulating pipeline, a tubular reactor is arranged on the circulating pipeline, the circulating pipeline is connected with a feed pipe through a three-way joint, the nitration kettle is communicated with the curing kettle, and a discharge outlet of the curing kettle is communicated with a transfer pot in reaction liquid through a pipeline. The utility model has the advantages that 70% of pre-reaction can be realized before the nitration kettle, the nitration reaction is more sufficient, the waste acid after nitration in the nitration kettle can enter a homogenizer for recycling after extraction, and the waste acid is recycled as a circulating liquid, thereby reducing the production cost.
However, the patent also has the following problems that the device does not filter raw materials in the use process, impurities can influence the reaction effect in the raw material reaction process, the device has limitations in use, the impurities can block a material conveying hole, the normal use of the device is influenced, the reaction efficiency of the device is reduced, and the device is inconvenient to use.
The present utility model has been made in view of this.
Disclosure of utility model
In order to solve the technical problems, the utility model adopts the basic conception of the technical scheme that:
The utility model provides a sulfentrazone nitrifies waste acid cyclic utilization device for denitrification, includes waste acid cyclic utilization device body, filter component and stirring subassembly, waste acid cyclic utilization device body includes the circulation case, and the top of circulation case is provided with the blowing structure of transportable material, and filter component includes annotates the material mouth, and the entrance to a cave has been seted up at the top of circulation case, annotates material mouth fixed mounting in the entrance to a cave at circulation case top, and stirring subassembly includes the agitator tank, the bottom of agitator tank and the inboard bottom fixed connection of circulation case.
As a preferred implementation mode of the utility model, the filter assembly further comprises a first filter, the bottom of the material injection port is fixedly provided with the first filter, the bottom of the first filter is provided with holes, a group of output pipes are fixedly arranged in the holes, and one end of each output pipe is fixedly provided with a second filter.
As a preferred embodiment of the utility model, the bottom of the inner side of the circulation box is fixedly provided with the supporting base, the inside of the supporting base is fixedly provided with the reaction kettle, the outer wall of one side of the second filter is fixedly provided with the connecting pipe, one end of the connecting pipe is fixedly connected with the outer wall of the reaction kettle, the second filter is communicated with the inside of the reaction kettle through the connecting pipe, the bottom of the inner side of the circulation box is fixedly provided with the first motor, the output shaft of the first motor is fixedly connected with the rotating rod through the coupler, and one end of the rotating rod extends and is rotatably arranged in the reaction kettle.
As a preferred implementation mode of the utility model, the top of the reaction kettle is provided with a hole, an exhaust port is fixedly arranged in the hole, one end of the exhaust port extends and is fixedly arranged outside the circulation box, and one end of the exhaust port can be externally connected with an exhaust pipe.
As a preferred embodiment of the utility model, the stirring assembly comprises a second motor, wherein the second motor is fixedly arranged on the inner wall of one side of the circulation box, an output shaft of the second motor is fixedly connected with a rotary rod through a coupler, one end of the rotary rod extends and is rotatably arranged in the stirring tank, stirring blades are fixedly arranged on the outer wall of the rotary rod, and the number of the stirring blades is three.
As a preferred implementation mode of the utility model, the front side of the stirring tank is provided with a groove hole, a filter material plate is slidably arranged in the groove hole, a pull rod is fixedly arranged on the front side of the filter material plate, a group of holes are formed in the outer wall of one side of the stirring tank, and a discharge pipe is fixedly arranged in the holes.
As a preferred implementation mode of the utility model, a group of holes are formed in the top of the circulation box, an input pipe is fixedly arranged in the holes, two groups of medicament controllers are fixedly arranged at the top of the input pipe, holes are formed in the outer wall of one side of each medicament controller, a conveying pipe is fixedly arranged in each hole, a medicament tank is fixedly arranged at one end of each conveying pipe, holes are formed in the top of each medicament tank, a pull handle is fixedly arranged in each hole, the bottom of the input pipe is fixedly connected with the outer wall of the reaction kettle, the input pipe is communicated with the inside of the reaction kettle, another group of output pipes are fixedly arranged on the outer wall of one side of the reaction kettle, and one end of each other group of output pipes is fixedly connected with the outer wall of the other side of the stirring tank.
Compared with the prior art, the utility model has the following beneficial effects:
1. The purpose of filtering waste acid is achieved, impurities in the waste acid are filtered and cleaned, the problem that the impurities block holes of the device is solved, the stability and flexibility of the device in use are improved, the device is replaced by manual cleaning, the reaction efficiency of the device to the medicament is improved, and the working efficiency is improved.
2. The device is stirred and mixed, so that the waste acid can be recycled after reaction, the use stability and safety of the device are improved, and the use experience of the device is optimized.
3. The purpose that the device automatically adds the medicament is achieved, the use flexibility of the device is improved, the use convenience of the device is improved, and the working pressure of workers is reduced.
The following describes the embodiments of the present utility model in further detail with reference to the accompanying drawings.
Drawings
In the drawings:
FIG. 1 is a front view of the present utility model;
FIG. 2 is a top view of the present utility model;
FIG. 3 is a left side perspective view of the present utility model;
FIG. 4 is a right side perspective view of the present utility model;
Fig. 5 is a section a node diagram of the present utility model.
In the figure, 10 parts of waste acid recycling device bodies, 11 parts of recycling boxes, 12 parts of material injection openings, 13 parts of first filters, 14 parts of output pipes, 15 parts of second filters, 16 parts of reaction kettles, 17 parts of supporting bases, 18 parts of first motors, 19 parts of rotating rods, 20 parts of exhaust ports, 21 parts of stirring tanks, 22 parts of second motors, 23 parts of rotating rods, 24 parts of stirring blades, 25 parts of filter material plates, 26 parts of pull rods, 27 parts of discharge pipes, 28 parts of input pipes, 29 parts of medicament controllers, 30 parts of medicament tanks, 31 parts of pull handles.
Detailed Description
For the purpose of making the objects, technical solutions and advantages of the embodiments of the present utility model more apparent, the technical solutions in the embodiments will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model, and the following embodiments are used to illustrate the present utility model.
According to the waste acid recycling device for the sulfenamide nitrification reaction, as shown in fig. 1, 2, 3 and 4 and 5, the waste acid recycling device body 10 comprises a circulation box 11, a filtering component and a stirring component, the top of the circulation box 11 is provided with a discharging structure capable of conveying materials, the filtering component comprises a material injection hole 12, the top of the circulation box 11 is provided with a hole, the material injection hole 12 is fixedly arranged in the hole at the top of the circulation box 11, the stirring component comprises a stirring tank 21, the bottom of the stirring tank 21 is fixedly connected with the inner side bottom of the circulation box 11, the filtering component further comprises a first filter 13, the bottom of the material injection hole 12 is fixedly provided with a first filter 13, the bottom of the first filter 13 is provided with a hole, a group of output pipes 14 are fixedly arranged in the hole, one end of the output pipes 14 is fixedly provided with a second filter 15, the inner bottom of the circulation box 11 is fixedly provided with a supporting base 17, the inside of the supporting base 17 is fixedly provided with a reaction kettle 16, one side outer wall of the second filter 15 is fixedly provided with a connecting pipe, one end of the connecting pipe is fixedly connected with the inner side of the motor 16, the inner side of the connecting pipe is fixedly connected with the inner side of the first filter 16 through the motor 16, and the inner side of the connecting pipe 19 is fixedly connected with the first output shaft 19 of the first filter 16 through the first filter 16 and the inner side of the motor 16, and the inner end of the first filter is fixedly connected with the first output shaft 19 through the rotating shaft 19.
The waste acid is injected into the first filter 13 through the material injection port 12 for preliminary filtration, large particle impurities in the waste acid are cleaned through the output pipe 14 and the second filter 15, the waste acid is poured into the reaction kettle 16 through the connecting pipe, the first motor 18 is started to drive the rotating rod 19 to rotate in the reaction kettle 16, the waste acid is stirred and filtered, and the waste acid is discharged into the stirring tank 21 through the other group of output pipes 14.
Through circulation case 11, annotate material mouth 12, first filter 13, output tube 14, second filter 15, reation kettle 16, support base 17, first motor 18, the structure of bull stick 19, reach the purpose of filtering waste acid, filter the clearance to impurity in the waste acid, solve impurity and block up the problem in device hole, improve stability and the flexibility that the device used, replace the manual work to clear up the device, improve the reaction efficiency of device to the medicament, improve work efficiency.
In the second embodiment, as shown in fig. 1, 2, 3, 4 and 5, a hole is formed in the top of the reaction kettle 16, an exhaust port 20 is fixedly installed in the hole, one end of the exhaust port 20 extends and is fixedly installed outside the circulation box 11, one end of the exhaust port 20 can be externally connected with an exhaust pipe, the stirring assembly comprises a second motor 22, the second motor 22 is fixedly installed on one side inner wall of the circulation box 11, an output shaft of the second motor 22 is fixedly connected with a rotary rod 23 through a coupling, one end of the rotary rod 23 extends and is rotatably installed inside the stirring tank 21, stirring blades 24 are fixedly installed on the outer wall of the rotary rod 23, and the number of the stirring blades 24 is three.
The second motor 22 is started to drive the rotary rod 23 to rotate in the stirring tank 21, the waste acid after filtration and mixing is stirred to react, the reacted waste acid is collected through the discharging pipe 27, residual impurities are filtered through the filter material plate 25, the pull rod 26 is pulled to take the filter material plate 25 out of the bottom of the stirring tank 21, the impurities are cleaned, and waste gas in the device is discharged through the exhaust port 20.
Through the structure of gas vent 20, agitator tank 21, second motor 22, dwang 23, stirring vane 24, filter material board 25, pull rod 26 and discharging pipe 27, reach and stir the mixing to the device and handle, but make the waste acid recycle's after the reaction purpose, improve stability and the security that the device used, optimize the use experience of device.
In the third embodiment, as shown in fig. 1, 2, 3, 4 and 5, a slot hole is formed in the front side of the stirring tank 21, a filter material plate 25 is slidably mounted in the slot hole, a pull rod 26 is fixedly mounted on the front side of the filter material plate 25, a group of holes are formed in the outer wall of one side of the stirring tank 21, a discharging pipe 27 is fixedly mounted in the hole, a group of holes are formed in the top of the circulation tank 11, an input pipe 28 is fixedly mounted in the holes, two groups of medicament controllers 29 are fixedly mounted on the top of the input pipe 28, a hole is formed in the outer wall of one side of the medicament controllers 29, a conveying pipe is fixedly mounted in the hole, a medicament tank 30 is fixedly mounted at one end of the conveying pipe, a hole is formed in the top of the medicament tank 30, a pull handle 31 is fixedly mounted in the hole, the bottom of the input pipe 28 is fixedly connected with the outer wall of the reaction tank 16, the input pipe 28 is communicated with the inside of the reaction tank 16, another group of output pipes 14 is fixedly mounted on the outer wall of one side of the reaction tank 16, and one end of the other group of output pipes 14 is fixedly connected with the outer wall of the stirring tank 21.
Pulling handle 31 is pulled to open the top of medicine tank 30 and fill the inside with medicine, adds reactant to the inside of reaction kettle 16 through two sets of medicine tanks 30, controls the quantity of medicine through medicine controller 29, adds the medicine to the inside of reaction kettle 16 through input tube 28.
Through the structure of input tube 28, medicament controller 29, medicament jar 30 and pull handle 31, reach the device and add the purpose to the medicament automatically, improve the device flexibility of use, improve the convenience of device use, alleviate workman's operating pressure.
It will be understood that the utility model has been described in terms of several embodiments, and that various changes and equivalents may be made to these features and embodiments by those skilled in the art without departing from the spirit and scope of the utility model. In addition, many modifications may be made to adapt a particular situation or material to the teachings of the utility model without departing from the essential scope thereof. Therefore, it is intended that the utility model not be limited to the particular embodiment disclosed, but that the utility model will include all embodiments falling within the scope of the appended claims.