CN223128049U - A kind of bis(triphenylphosphine)palladium dichloride production and processing equipment - Google Patents
A kind of bis(triphenylphosphine)palladium dichloride production and processing equipmentInfo
- Publication number
- CN223128049U CN223128049U CN202422410921.7U CN202422410921U CN223128049U CN 223128049 U CN223128049 U CN 223128049U CN 202422410921 U CN202422410921 U CN 202422410921U CN 223128049 U CN223128049 U CN 223128049U
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- mixing tank
- water
- production
- tank
- palladium dichloride
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Abstract
The utility model discloses a production and processing device of bis (triphenylphosphine) palladium dichloride, which relates to the technical field of bis (triphenylphosphine) palladium dichloride production and solves the problem that the production and processing device is inconvenient to clean after the use is finished, and comprises a bottom plate, wherein the top of the bottom plate is fixedly connected with a mixing tank through a support plate, the inner cavity of the mixing tank is provided with a stirring mechanism, the left side of the mixing tank is provided with a cleaning mechanism, the utility model is characterized in that the mixing tank, the stirring mechanism and a heating plate are arranged, can be convenient for carry out the mixed reaction to palladium chloride and triphenylphosphine, carry out preliminary production to bis-triphenylphosphine palladium dichloride, through setting up storage water tank, water pump, drinking-water pipe, drain pipe and water spray board, can wash to the inside water spray of blending tank, through setting up the brush board, can be convenient for scrub the inside of blending tank, can wash down the impurity that blending tank surface bonds, this mode is good to the cleaning performance of blending tank, facilitates the next time and uses.
Description
Technical Field
The utility model relates to the technical field of production of bis (triphenylphosphine) palladium dichloride, in particular to production and processing equipment of bis (triphenylphosphine) palladium dichloride.
Background
The method for producing the ditriphenylphosphine palladium dichloride comprises an aqueous solution method and a direct synthesis method, wherein the direct synthesis method has high production efficiency, low cost and wide application, the direct synthesis method needs stirring and mixing the palladium chloride and triphenylphosphine during production, and in order to improve the production quantity, the processing equipment is generally required to be used for mixing, the currently used ditriphenylphosphine palladium dichloride production and processing equipment has single function, the equipment is inconvenient to clean after the use is finished, raw materials are easy to remain in the equipment, and the next use is unfavorable, so the improvement is needed.
Disclosure of utility model
In order to solve the problem that the production and processing equipment is inconvenient to clean after the use is finished, the utility model provides the production and processing equipment for bis triphenylphosphine palladium dichloride.
The utility model provides a production and processing device of bis triphenylphosphine palladium dichloride, which adopts the following technical scheme:
the production and processing equipment for the bis triphenylphosphine palladium dichloride comprises a bottom plate, wherein the top of the bottom plate is fixedly connected with a mixing tank through a support plate, the inner cavity of the mixing tank is provided with a stirring mechanism, the left side of the mixing tank is provided with a cleaning mechanism, and the bottom of the inner surface of the mixing tank is fixedly connected with a heating plate;
The cleaning mechanism comprises a water storage tank, the water storage tank is fixedly arranged at the top of the left side of the mixing tank, the top of the water storage tank is fixedly connected with a water pump, the bottom of the water pump is communicated with a water suction pipe, the bottom of the water suction pipe extends to the bottom of an inner cavity of the water storage tank, the top of the water pump is communicated with a water discharge pipe, the top of the inner cavity of the mixing tank is fixedly connected with a water spray plate, and one end of the water discharge pipe away from the water pump is communicated with the top of the water spray plate.
Through adopting above-mentioned technical scheme, can wash to the inside water spray of blending tank, can also be convenient for scrub the inside of blending tank, can wash down the impurity that blending tank surface bonds, this mode is good to the cleaning performance of blending tank, facilitates the use next time.
Optionally, the rabbling mechanism includes the rotating electrical machines, rotating electrical machines fixed mounting is in the center department on blending tank right side, the output fixedly connected with pivot of rotating electrical machines, the left side of pivot is rotated through the bearing with the junction on blending tank inner chamber left side and is connected, the top and the bottom of pivot are from a left side to a right side evenly fixedly connected with puddler, the one end fixedly connected with brush board of pivot is kept away from to the puddler.
By adopting the technical scheme, the palladium chloride and the triphenylphosphine can be stirred and mixed, and the reaction efficiency is improved.
Optionally, the center department at blending tank top is through pole setting fixedly connected with storage box, the bottom intercommunication of storage box has the discharging pipe, the bottom of discharging pipe runs through the blending tank.
Through adopting above-mentioned technical scheme, can conveniently discharge the raw materials of storing into the blending tank.
Optionally, the right side at the top of the mixing tank is communicated with a feeding pipe, and the left bottom of the mixing tank is communicated with a discharging pipe.
Through adopting above-mentioned technical scheme, can conveniently throw the material to the blending tank in.
Optionally, the left side intercommunication at storage water tank top has the water injection pipe, and the mouth of pipe department of water injection pipe is provided with the apron.
By adopting the technical scheme, water can be conveniently injected into the water storage tank.
Optionally, the top intercommunication of storage case has the notes material pipe, and the top of notes material pipe is provided with sealed lid.
By adopting the technical scheme, the material is conveniently injected into the storage box of the box.
Optionally, the top fixed mounting of bottom plate has the power supply box, the top of bottom plate just is located the place ahead fixed mounting of power supply box has control panel.
By adopting the technical scheme, the equipment can be conveniently controlled.
In summary, the utility model has the following beneficial effects:
According to the utility model, through the arrangement of the mixing tank, the stirring mechanism and the heating plate, the mixing reaction of palladium chloride and triphenylphosphine can be conveniently carried out, the preliminary production of bis-triphenylphosphine palladium dichloride is carried out, through the arrangement of the water storage tank, the water pump, the water suction pipe, the water discharge pipe and the water spray plate, the water spray flushing can be carried out inside the mixing tank, through the arrangement of the hairbrush plate, the inside of the mixing tank can be conveniently scrubbed, and the residual raw materials adhered on the surface of the mixing tank can be conveniently cleaned.
Drawings
FIG. 1 is a schematic diagram of the structure of the present utility model;
FIG. 2 is a cross-sectional view of the structure of the present utility model;
FIG. 3 is a cross-sectional view of the water storage tank structure of the present utility model;
Fig. 4 is a left side cross-sectional view of the mixing tank structure of the present utility model.
In the figure, 1, a bottom plate, 2, a mixing tank, 3, a cleaning mechanism, 301, a water storage tank, 302, a water pump, 303, a water suction pipe, 304, a water discharge pipe, 305, a water spraying plate, 4, a stirring mechanism, 401, a rotating motor, 402, a rotating shaft, 403, a stirring rod, 404, a hairbrush plate, 5, a heating plate, 6, a storage box, 7, a discharge pipe, 8, a feed pipe, 9 and a discharge pipe.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Examples:
Referring to fig. 1-4, a production and processing device for bis triphenylphosphine palladium dichloride comprises a bottom plate 1, wherein the top of the bottom plate 1 is fixedly connected with a mixing tank 2 through a support plate, the inner cavity of the mixing tank 2 is provided with a stirring mechanism 4, the left side of the mixing tank 2 is provided with a cleaning mechanism 3, and the bottom of the inner surface of the mixing tank 2 is fixedly connected with a heating plate 5;
The cleaning mechanism 3 comprises a water storage tank 301, the water storage tank 301 is fixedly arranged at the top of the left side of the mixing tank 2, a water pump 302 is fixedly connected to the top of the water storage tank 301, a water suction pipe 303 is communicated with the bottom of the water pump 302, the bottom of the water suction pipe 303 extends to the bottom of the inner cavity of the water storage tank 301, a water discharge pipe 304 is communicated with the top of the water pump 302, a water spraying plate 305 is fixedly connected to the top of the inner cavity of the mixing tank 2, and one end, away from the water pump 302, of the water discharge pipe 304 is communicated with the top of the water spraying plate 305.
As a technical optimization scheme of the utility model, further, the stirring mechanism 4 comprises a rotating motor 401, the rotating motor 401 is fixedly arranged at the center of the right side of the mixing tank 2, the output end of the rotating motor 401 is fixedly connected with a rotating shaft 402, the connection part of the left side of the rotating shaft 402 and the left side of the inner cavity of the mixing tank 2 is rotationally connected through a bearing, stirring rods 403 are uniformly and fixedly connected from left to right at the top and the bottom of the rotating shaft 402, and one end, far away from the rotating shaft 402, of the stirring rods 403 is fixedly connected with a hairbrush plate 404.
As a technical optimization scheme of the utility model, further, the center of the top of the mixing tank 2 is fixedly connected with a storage tank 6 through a vertical rod, the bottom of the storage tank 6 is communicated with a discharge pipe 7, and the bottom of the discharge pipe 7 penetrates through the mixing tank 2.
As a technical optimization scheme of the utility model, further, the right side of the top of the mixing tank 2 is communicated with a feed pipe 8, and the bottom of the left side of the mixing tank 2 is communicated with a discharge pipe 9.
As a technical optimization scheme of the utility model, further, a water injection pipe is communicated with the left side of the top of the water storage tank 301, and a cover plate is arranged at the pipe orifice of the water injection pipe.
As a technical optimization scheme of the utility model, further, the top of the storage box 6 is communicated with a material injection pipe, and the top of the material injection pipe is provided with a sealing cover.
As a technical optimization scheme of the utility model, further, the top of the bottom plate 1 is fixedly provided with a power supply box, and the top of the bottom plate 1 and the front of the power supply box are fixedly provided with a control panel.
In the embodiment, the mixing tank 2, the stirring mechanism 4 and the heating plate 5 are arranged, so that the mixing reaction of palladium chloride and triphenylphosphine can be conveniently carried out, the primary production of the bis-triphenylphosphine palladium dichloride is carried out, the water spraying flushing can be carried out to the inside of the mixing tank 2 through the arrangement of the water storage tank 301, the water pump 302, the water pumping pipe 303, the water discharging pipe 304 and the water spraying plate 305, the scrubbing of the inside of the mixing tank 2 can be conveniently carried out through the arrangement of the rotating motor 401, the rotating shaft 402, the stirring rod 403 and the brush plate 404, the residual raw materials adhered to the surface of the mixing tank 2 can be conveniently washed down, the cleaning effect of the mixing tank 2 is good, the next use is conveniently carried out, the storage of raw materials can be conveniently carried out through the arrangement of the discharging pipe 7, the reaction of the stored raw materials into the mixing tank 2 can be conveniently carried out, the reaction production of the other raw materials into the mixing tank 2 can be conveniently carried out through the arrangement of the discharging pipe 9, the bis-triphenylphosphine palladium dichloride after the production is conveniently carried out through the arrangement of the discharging pipe 9, and the control panel is conveniently carried out.
The method comprises the following steps of putting palladium chloride into a storage tank 6, putting palladium chloride into a mixing tank 2 through a discharge pipe 7 during production, putting triphenylphosphine into the mixing tank 2 from a feed pipe 8, starting a control switch of a rotating motor 401, driving a rotating shaft 402 to rotate by the rotating motor 401, driving a stirring rod 403 to rotate by the rotating shaft 402, stirring and mixing the palladium chloride and the triphenylphosphine, improving reaction efficiency, simultaneously starting a control switch of a heating plate 5, heating the inside of the mixing tank 2 through the heating plate 5, further improving reaction efficiency, finally discharging a produced product from a discharge pipe 9, carrying out subsequent filtering and purifying processing on the bis-triphenylphosphine dichloropalladium, starting a control switch of a water pump 302 when the mixing tank 2 is required to be cleaned, pumping water in a water storage tank 301 through a water pumping pipe 303, conveying the water into a water draining pipe 304, finally spraying the water spraying plate 305 to the inside of the mixing tank 2, flushing the inside of the mixing tank 2, and brushing the inside of the mixing tank 2 through a hairbrush plate 404.
The above embodiments are not intended to limit the scope of the utility model, so that the equivalent changes of the structure, shape and principle of the utility model are covered by the scope of the utility model.
Claims (7)
1. The production and processing equipment for the bis triphenylphosphine palladium dichloride comprises a bottom plate (1) and is characterized in that the top of the bottom plate (1) is fixedly connected with a mixing tank (2) through a support plate, the inner cavity of the mixing tank (2) is provided with a stirring mechanism (4), the left side of the mixing tank (2) is provided with a cleaning mechanism (3), and the bottom of the inner surface of the mixing tank (2) is fixedly connected with a heating plate (5);
the cleaning mechanism (3) comprises a water storage tank (301), the water storage tank (301) is fixedly arranged at the top of the left side of the mixing tank (2), a water pump (302) is fixedly connected to the top of the water storage tank (301), a water suction pipe (303) is communicated with the bottom of the water pump (302), the bottom of the water suction pipe (303) extends to the bottom of an inner cavity of the water storage tank (301), a water drainage pipe (304) is communicated with the top of the water pump (302), a water spraying plate (305) is fixedly connected to the top of the inner cavity of the mixing tank (2), and one end, far away from the water pump (302), of the water drainage pipe (304) is communicated with the top of the water spraying plate (305).
2. The production and processing equipment for the bis triphenylphosphine palladium dichloride according to claim 1, wherein the stirring mechanism (4) comprises a rotating motor (401), the rotating motor (401) is fixedly arranged at the center of the right side of the mixing tank (2), the output end of the rotating motor (401) is fixedly connected with a rotating shaft (402), the connection part of the left side of the rotating shaft (402) and the left side of the inner cavity of the mixing tank (2) is rotationally connected through a bearing, stirring rods (403) are uniformly and fixedly connected at the top and the bottom of the rotating shaft (402) from left to right, and a hairbrush plate (404) is fixedly connected at one end, far away from the rotating shaft (402), of the stirring rods (403).
3. The production and processing equipment for the bis triphenylphosphine palladium dichloride according to claim 1 is characterized in that a storage box (6) is fixedly connected to the center of the top of the mixing tank (2) through a vertical rod, a discharge pipe (7) is communicated with the bottom of the storage box (6), and the bottom of the discharge pipe (7) penetrates through the mixing tank (2).
4. The production and processing equipment of the bis triphenylphosphine palladium dichloride according to claim 1 is characterized in that a feed pipe (8) is communicated with the right side of the top of the mixing tank (2), and a discharge pipe (9) is communicated with the bottom of the left side of the mixing tank (2).
5. The production and processing equipment of the bis triphenylphosphine palladium dichloride according to claim 1, wherein a water injection pipe is communicated with the left side of the top of the water storage tank (301), and a cover plate is arranged at the pipe orifice of the water injection pipe.
6. The production and processing equipment of the bis (triphenylphosphine) palladium dichloride is characterized in that a material injection pipe is communicated with the top of the material storage box (6), and a sealing cover is arranged at the top of the material injection pipe.
7. The production and processing equipment of the bis triphenylphosphine palladium dichloride is characterized in that a power supply box is fixedly arranged at the top of the bottom plate (1), and a control panel is fixedly arranged at the top of the bottom plate (1) and positioned in front of the power supply box.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202422410921.7U CN223128049U (en) | 2024-10-08 | 2024-10-08 | A kind of bis(triphenylphosphine)palladium dichloride production and processing equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202422410921.7U CN223128049U (en) | 2024-10-08 | 2024-10-08 | A kind of bis(triphenylphosphine)palladium dichloride production and processing equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN223128049U true CN223128049U (en) | 2025-07-22 |
Family
ID=96428772
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202422410921.7U Active CN223128049U (en) | 2024-10-08 | 2024-10-08 | A kind of bis(triphenylphosphine)palladium dichloride production and processing equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN223128049U (en) |
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2024
- 2024-10-08 CN CN202422410921.7U patent/CN223128049U/en active Active
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