Distillation device
Technical Field
The utility model belongs to the field of m-tert-butylphenol production and processing, and particularly relates to a distillation device.
Background
M-tert-butylphenol is an important organic chemical raw material and is widely applied to the fields of medicines, pesticides, dyes and the like. Distillation is an essential link in the production of m-tert-butylphenol. However, the conventional distillation apparatus has various disadvantages in stirring effect and distillation efficiency, such as uneven stirring, easy deposition of materials, etc., which seriously affect the distillation effect and production efficiency of m-tert-butylphenol. Therefore, the development of a novel m-tert-butylphenol distillation device has important significance for improving the distillation effect and the production efficiency.
The prior art discloses a m-tert-butylphenol distillation device (CN 219879114U), which comprises a shell, wherein a feed inlet is formed in one side of the shell, and a feed pipe is fixedly connected to the inside of the feed inlet. The m-tert-butylphenol distillation device has the advantages that m-tert-butylphenol is added into a feeding pipeline, a first motor is started, so that a transmission auger transmits the m-tert-butylphenol and falls into the shell, a second motor is started, an output shaft of the second motor rotates to drive one belt pulley to rotate, the two belt pulleys rotate one by one under the action of a belt, the first stirring rod and the second stirring rod rotate one by one, the second stirring rod further stirs the m-tert-butylphenol positioned at the bottom of the shell, and the problems that materials are not stirred in place, are easy to deposit on the bottom surface and the distillation effect is affected are solved.
The bottom surface is deposited to the m-tert-butylphenol easily in the stirring process, and although the second stirring rod stirs m-tert-butylphenol that is located the shell bottom in prior art, because the second stirring rod is the horizontally state with the shell bottom, the shell is the cylinder, and the second stirring rod size is limited, and the m-tert-butylphenol that is located the position of shell wall and the piled up m-tert-butylphenol in corner position still is difficult to stir, leads to stirring inefficiency and insufficient stirring problem.
The present utility model has been made in view of this.
Disclosure of utility model
In order to solve the technical problem of insufficient stirring, the utility model adopts the basic conception of the technical scheme that:
a distillation apparatus comprising, a distillation apparatus characterized by comprising
The supporting plate is arranged on the ground to keep stable in structure, a mixing barrel is arranged above the supporting plate, and a barrel cover is arranged at the top of the mixing barrel;
The feeding structure is arranged at one side of the mixing barrel and used for adding m-tertiary butyl phenol;
The distillation pipe structure is arranged above the mixing bucket and is used for discharging distilled water;
the heat conducting plate structure is arranged at the bottom of the mixing barrel and is used for heating the mixture of m-tertiary butyl phenol and water;
Stirring structure, stirring structure sets up inside being used for accelerating m-tert-butylphenol and water mixing at the bung, stirring structure includes servo motor, a gear, first dwang, the rotary rod, the connecting rod, the rack, go-between and ring, the one end of rotary rod passes the bottom surface of bung and go-between and one end top surface fixed connection of connecting rod, the rotary rod passes through the bearing and rotates with the bung to be connected, the top of rotary rod and servo motor's axis of rotation fixed connection, servo motor passes through support fixed mounting at the top surface of bung, the rotary rod is connected with the ring, the top of first dwang passes the top surface of connecting rod one end and the bottom fixed connection of gear, the below of first dwang is provided with first agitator, first dwang passes through the bearing and rotates with the connecting rod to be connected, the rack has been seted up to the wall of ring, gear and rack mesh.
As a preferred embodiment of the utility model, the connecting ring is arranged in the middle of the circular ring, the wall surface of the connecting ring is provided with a plurality of connecting rods, the wall surface of the connecting ring is fixedly connected with one end of each connecting rod, the other end of each connecting rod is fixedly connected with the inner wall surface of the circular ring, and the rotating rod is rotatably connected with the connecting ring through a bearing.
As a preferred embodiment of the utility model, the end of the connecting rod which is rotatably connected to the first rotary rod is inclined in the direction of the support plate.
As a preferred embodiment of the present utility model, the whole of the gear, the first rotating rod and the first agitator is inclined toward the center of the bottom surface of the mixing bowl.
As a preferable implementation mode of the utility model, the bottom surface of one end of the connecting rod connected with the rotary rod is also fixedly connected with a second rotary rod, and a second stirrer is arranged below the second rotary rod.
As a preferred embodiment of the utility model, the first stirrer and the second stirrer are composed of a plurality of arc-shaped metal rods and a connecting plate, one ends of the arc-shaped metal rods are fixedly connected with the wall surface of the same connecting plate, and the top surfaces of the connecting plates of the first stirrer and the second stirrer are fixedly connected with the bottom ends of the first rotating rod and the second rotating rod respectively.
As a preferred embodiment of the utility model, the top surface of the supporting plate is provided with a plurality of supporting columns, the top surface of the supporting plate is fixedly connected with the bottom surface of each supporting column, the top surface of each supporting column is fixedly connected with the bottom surface of the same supporting ring, and the inner wall surface of the supporting ring is fixedly connected with the outer wall surface of the mixing barrel.
As a preferable implementation mode of the utility model, the bottom surface of the barrel cover is provided with a piston, and the barrel cover is movably connected with the mixing barrel through the piston at the bottom surface.
Compared with the prior art, the utility model has the following beneficial effects:
1. The support of backup pad, support column and holding ring makes the blow off pipe use more convenient, does not connect sewage below the fixed plate, and the swing joint of bung and compounding bucket is convenient for later stage compounding bucket inner structure's maintenance and maintenance.
2. Through first dwang and first agitator slope around making circular motion, compounding barrel bottom edge portion and corner can all be stirred by first agitator, in addition the rotation of self and rotation stirring of second agitator and second dwang, the liquid in the whole compounding barrel obtains fully stirring.
Drawings
In the drawings:
FIG. 1 is a schematic diagram of the overall structure of the present utility model;
FIG. 2 is a schematic diagram of the stirring structure of the present utility model;
FIG. 3 is a schematic view of the stirring structure of the present utility model;
FIG. 4 is a schematic view of the stirring structure of the present utility model;
fig. 5 is a schematic structural view of a support frame according to the present utility model.
The device comprises a mixing drum 1, a supporting ring 2, a supporting column 3, a drum cover 4, a servo motor 5, a gear 6, a first rotating rod 7, a first stirrer 8, a first rotating rod 9, a rotating rod 10, a connecting rod 11, a rack 12, a connecting ring 13, a connecting rod 14, a circular ring 15 and a supporting plate.
Detailed Description
For the purpose of making the objects, technical solutions and advantages of the embodiments of the present utility model more apparent, the technical solutions in the embodiments will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model, and the following embodiments are used to illustrate the present utility model.
A distilling apparatus is shown in fig. 1 and 2, a supporting plate 15 is arranged on the ground, the structure is stable, a mixing drum 1 is arranged above the supporting plate 15, a drum cover 4 is arranged at the top of the mixing drum 1, a feeding structure is arranged on one side of the mixing drum 1 and used for adding m-tertiary butyl phenol, the feeding structure comprises a feeding pipe, a feeding pipeline and a transmission auger, a distilling pipe structure is arranged above the mixing drum 1 and used for discharging distilled water, the distilling pipe structure comprises a distilling pipe, a heat conducting plate structure is arranged at the bottom of the mixing drum 1 and used for heating a mixture of m-tertiary butyl phenol and water, the heat conducting plate structure comprises a heat conducting plate and a drain pipe, the top surface of the supporting plate 15 is provided with a dry mixing drum 1, the top surface of the supporting plate 15 is fixedly connected with the bottom surface of each supporting column 3, the top surface of each supporting column 3 is fixedly connected with the bottom surface of one supporting ring 2, the inner wall surface of the supporting ring 2 is fixedly connected with the outer wall surface of the mixing drum 1, the bottom surface of the drum cover 4 is provided with a piston, the drum cover 4 is movably connected with the mixing drum 1 through the piston on the bottom surface, the feeding pipe, the heat conducting plate is arranged on the bottom of the drum and the mixing drum 1 is used for heating mixture, and the mixture of m-tertiary butyl phenol is not in the prior art, and the distillation apparatus is disclosed in 219879114.
The support of backup pad 15, support column 3 and holding ring 2 makes the blow off pipe use more convenient, does not connect sewage below the fixed plate, and the swing joint of bung 4 and compounding bucket 1 is convenient for later stage compounding bucket 1 inner structure's maintenance and maintenance.
As shown in fig. 1, 3, 4 and 5, the stirring structure is arranged in the barrel cover 4 and used for accelerating the mixing of m-tert-butylphenol and water, the stirring structure comprises a servo motor 5, a gear 6, a first rotating rod 7, a rotating rod 9, a connecting rod 10, a rack 11, a connecting ring 12 and a circular ring 14, one end of the rotating rod 9 penetrates through the bottom surfaces of the barrel cover 4 and the connecting ring 12 and is fixedly connected with one end top surface of the connecting rod 10, the rotating rod 9 is rotationally connected with the barrel cover 4 through a bearing, the top end of the rotating rod 9 is fixedly connected with the rotating shaft of the servo motor 5, the servo motor 5 is fixedly arranged on the top surface of the barrel cover 4 through a bracket, the rotating rod 9 is connected with the circular ring 14, the top end of the first rotating rod 7 penetrates through the top surface of one end of the connecting rod 10 and is fixedly connected with the bottom end of the gear 6, a first stirrer 8 is arranged below the first rotating rod 7 and is rotationally connected with the connecting rod 10 through a bearing, the wall surface of the circular ring 14 is provided with a rack 11, the gear 6 is meshed with the rack 11, the connecting ring 12 is arranged in the middle of the circular ring 14, the wall surface of the connecting ring 12 is provided with a plurality of connecting rods 13, the wall surface of the connecting ring 12 is fixedly connected with one end of each connecting rod 13, the other end of each connecting rod 13 is fixedly connected with the inner wall surface of the circular ring 14, the rotating rod 9 is rotationally connected with the connecting ring 12 through a bearing, the end part of the connecting rod 10 rotationally connected with the first rotating rod 7 inclines towards the direction of the supporting plate 15, the whole body formed by the gear 6, the first rotating rod 7 and the first stirrer 8 inclines towards the center of the bottom surface of the mixing drum 1, the bottom surface of one end of the connecting rod 10 connected with the rotating rod 9 is fixedly connected with a second rotating rod, a second stirrer is arranged below the second rotating rod, both the first stirrer 8 and the second stirrer consist of a plurality of arc-shaped metal rods and a connecting plate, one end fixed connection of a plurality of arc metal poles is the wall of the same connecting plate, the connecting plate top surface of first agitator 8 and second agitator respectively with the bottom fixed connection of first dwang 7 and second dwang, the top surface of backup pad 15 is provided with a plurality of support columns 3, the top surface of backup pad 15 and the bottom surface fixed connection of every support column 3, the bottom surface of the same supporting ring 2 of the top surface fixedly connected with of every support column 3, the inner wall of supporting ring 2 and the outer wall fixed connection of mixing vat 1, first agitator 8 and second agitator structure are the same, but the size is different, first dwang 7 and second dwang structure are the same, but the size is different.
The power of the servo motor 5 is connected, the rotating shaft of the servo motor 5 drives the rotating rod 9 to rotate, the rotating rod 9 drives the connecting rod 10 to rotate, the connecting rod 10 drives the first rotating rod 7 and the first stirrer 8 to do circular motion around the circular ring 14, meanwhile, the gear 6 rotates around the rack 11, the gear 6 drives the first rotating rod 7 to rotate in the connecting rod 10, the second rotating rod drives the second stirrer to rotate when the connecting rod 10 rotates, the first rotating rod 7 and the first stirrer 8 tilt around the circular ring 14 to do circular motion, the edge part and the corner of the bottom of the mixing bucket 1 can be stirred by the first stirrer 8, and the rotation of the first stirrer and the rotation stirring of the second stirrer and the second rotating rod are added, so that liquid in the whole mixing bucket 1 is fully stirred.
The utility model has the working principle that the support of the support plate 15, the support column 3 and the support ring 2 enables the sewage discharge pipe to be used more conveniently, the movable connection of the barrel cover 4 and the mixing barrel 1 is not needed under the fixed plate, the maintenance and the maintenance of the inner structure of the later mixing barrel 1 are facilitated, the power supply of the servo motor 5 is connected, the rotating shaft of the servo motor 5 drives the rotating rod 9 to rotate, the rotating rod 9 drives the connecting rod 10 to rotate, the connecting rod 10 drives the first rotating rod 7 and the first stirrer 8 to do circular motion around the circular ring 14, meanwhile, the gear 6 drives the first rotating rod 7 to rotate in the connecting rod 10, the second rotating rod drives the second stirrer to rotate, the edge part and the corner of the bottom of the mixing barrel 1 can be stirred by the first stirrer 8 in an inclined mode around the circular ring 14, and the rotation of the second stirrer and the second rotating rod are added, so that liquid in the whole mixing barrel 1 is fully stirred.
It will be understood that the utility model has been described in terms of several embodiments, and that various changes and equivalents may be made to these features and embodiments by those skilled in the art without departing from the spirit and scope of the utility model. In addition, many modifications may be made to adapt a particular situation or material to the teachings of the utility model without departing from the essential scope thereof. Therefore, it is intended that the utility model not be limited to the particular embodiment disclosed, but that the utility model will include all embodiments falling within the scope of the appended claims.