CN222804701U

CN222804701U - A chemical reagent separation device

Info

Publication number: CN222804701U
Application number: CN202421653014.9U
Authority: CN
Inventors: 蔡冠军; 胡伟明
Original assignee: Dongguan Shangwei Electronic Materials Co ltd
Current assignee: Dongguan Shangwei Electronic Materials Co ltd
Priority date: 2024-07-12
Filing date: 2024-07-12
Publication date: 2025-04-29
Anticipated expiration: 2034-07-12

Abstract

The utility model discloses a chemical reagent separation device, which relates to the technical field of chemical reagent separation, and comprises a liquefaction separation tank, wherein a collecting tank is arranged at the lower end of the liquefaction separation tank, an air delivery pipe is passed through the liquefaction separation tank, the lower end of the air delivery pipe extends into the collecting tank, the upper end of the air delivery pipe is connected with a distillation mechanism, and the distillation mechanism comprises: a distillation tank and a water bath tank, wherein a stirring mechanism is arranged inside the water bath tank, a heating pipe is fixed inside the water bath tank, and the distillation tank is placed at the center of the heating pipe; the chemical reagent separation device, by arranging the distillation mechanism, drives a motor to drive a stirring rod to rotate so that the boiling efficiency inside the water bath tank is higher, which can not only save the use of electricity, but also improve the efficiency of distillation by improving the boiling efficiency.

Description

Chemical reagent splitter

Technical Field

The utility model relates to the technical field of chemical reagent separation, in particular to chemical reagent separation equipment.

Background

The purification and separation of chemical reagents are particularly important in experiments, and various modes exist for separating the chemical reagents, wherein distillation is a common method in the separation of the chemical reagents.

CN213589740U, discloses a separation device for chemical reagents, where the chemical reagents are filled in an evaporation tank after distillation, and a collecting bucket is located inside the evaporation tank, so that gas is not completely transported, and the liquefaction efficiency of the chemical reagents is reduced, and meanwhile, the conventional heating efficiency is low during distillation in a water bath tank, so that the distillation efficiency is reduced.

Disclosure of utility model

Aiming at the defects of the prior art, the utility model provides chemical reagent separation equipment, which solves the problems of the prior art.

The chemical reagent separation equipment comprises a liquefaction separation tank, wherein a collection tank is arranged at the lower end of the liquefaction separation tank, a gas pipe penetrates through the liquefaction separation tank, the lower end of the gas pipe extends into the collection tank, the upper end of the gas pipe is connected with a distillation mechanism, the distillation mechanism comprises a distillation tank and a water bath tank, a stirring mechanism is arranged in the water bath tank, a heating pipe is fixed in the water bath tank, and the distillation tank is arranged in the center of the heating pipe.

Further, the stirring mechanism comprises a placing plate, a limiting block is fixedly connected to the upper end of the placing plate, inserting pipes are fixedly connected to the lower end of the distillation tank, the inserting pipes are in matched insertion connection with the limiting block, a rotating plate is rotatably connected to the upper end of the rotating plate, a driving motor is fixedly connected to the lower end of the water bath tank, the output end of the driving motor is fixedly connected to the lower end of the rotating plate, stirring rods are fixed to the edge of the upper end of the rotating plate, the stirring rods are arranged in a plurality, and the distance between the stirring rods is equal.

Further, the lower extreme of gas-supply pipe is arranged in the collection jar, and the tip extends to the outside setting of collection jar, the delivery port has been seted up to the lower extreme of gas-supply pipe, fixedly connected with baffle in the gas-supply pipe, the scavenge port has been seted up to the lower extreme of gas-supply pipe, delivery port, baffle and scavenge port set gradually from a left side to the right side.

Further, the upper end threaded connection of retort has the lid, the conical surface has been seted up to the lower extreme inner wall of lid, the gas-supply pipe is connected with the upper end intercommunication of lid.

Further, a heat preservation sleeve is sleeved on the outer side of the gas pipe.

Further, a penetrating strip-shaped hole is formed in the stirring rod.

Compared with the background technology, the chemical reagent separation equipment provided by the application comprises separation equipment which is very mature in technology at present and a distillation mechanism which is used as a core component, and the principle relies on the fact that the boiling efficiency is improved by stirring water in a water bath tank, so that the distillation efficiency of chemical reagents is improved.

The utility model provides chemical reagent separation equipment. Compared with the prior art, the method has the following beneficial effects:

this chemical reagent splitter, through setting up distillation mechanism, driving motor drives the puddler and rotates and make the inside boiling efficiency of water bath higher, not only can save the electricity used like this, can improve the efficiency of distillation through the efficiency that improves boiling moreover.

Drawings

FIG. 1 is a schematic view of the overall structure of the present utility model;

FIG. 2 is a schematic view of the cross-section of the water bath tank of the present utility model;

FIG. 3 is a schematic cross-sectional view of a collection tank according to the present utility model;

FIG. 4 is an enlarged schematic view of FIG. 2A;

FIG. 5 is an enlarged schematic view of the structure of FIG. 2B;

Fig. 6 is an enlarged schematic view of the structure at C in fig. 3.

The device comprises a water bath tank 1, a liquefaction separation tank 2, a collection tank 3, a heating pipe 4, a distillation tank 5, a cover 6, a conical surface 7, a gas pipe 8, a heat insulation sleeve 9, a water outlet 10, a partition plate 11, a partition plate 12, a ventilation port 13, a cannula 14, a placing plate 15, a limiting block 16, a rotating plate 17, a stirring rod 18, a strip-shaped hole 19 and a driving motor.

Detailed Description

The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.

Referring to fig. 1-6, the utility model provides a technical scheme that the chemical reagent separation device comprises a liquefaction separation tank 2, wherein a collecting tank 3 is arranged at the lower end of the liquefaction separation tank 2, a gas pipe 8 is arranged in the liquefaction separation tank 2 in a penetrating way, the lower end of the gas pipe 8 extends into the collecting tank 3, a distillation mechanism is connected to the upper end of the gas pipe 8, the distillation mechanism comprises a distillation tank 5 and a water bath tank 1, a stirring mechanism is arranged in the water bath tank 1, a heating pipe 4 is fixed in the water bath tank 1, the distillation tank 5 is arranged in the center of the interior of the heating pipe 4, when chemical reagents are distilled and separated, the chemical reagents are poured into the distillation tank 5, then the distillation tank 5 is placed in the water bath tank 1, water in the water bath tank 1 is heated through the heating pipe 4, the water is conducted into the distillation tank 5 after the water is heated, the chemical reagents needed to be separated are vaporized, the chemical reagents in the water bath separation tank 2 enter the liquefaction tank 2 through the gas pipe 8, then the liquefied chemicals are led into the collecting tank 3 through the gas pipe 8, and the efficiency of boiling of the water can be increased through the stirring mechanism in the water bath tank 1.

As shown in fig. 2 and 4, the stirring mechanism comprises a placing plate 14, a limiting block 15 is fixedly connected to the upper end of the placing plate 14, a cannula 13 is fixedly connected to the lower end of the distillation tank 5, the cannula 13 and the limiting block 15 are in matched and inserted connection, a rotating plate 16 is rotatably connected with the upper end of the placing plate 14, a driving motor 19 is fixedly connected to the lower end of the water bath tank 1, the output end of the driving motor 19 is fixedly connected with the lower end of the rotating plate 16, stirring rods 17 are fixed to the upper edge of the rotating plate 16, the stirring rods 17 are arranged in a plurality of mode and are equal in space, the cannula 13 at the lower end of the distillation tank 5 is placed corresponding to the limiting block 15 at the upper end of the placing plate 14, the distillation tank 5 can be stably placed, meanwhile, the rotating plate 16 is driven to rotate through the driving motor 19 at the lower end, the placing plate 14 is rotatably connected with the rotating plate 16, the placing plate 14 cannot rotate with the distillation tank 5, the stirring rods 17 with the fixed edges are driven to rotate, and water inside the water bath tank 1 is driven to flow through the stirring rods 17, and therefore the efficiency of boiling of water inside the water is improved.

As shown in FIG. 6, the lower end of the gas pipe 8 is positioned in the collecting tank 3, the end part of the gas pipe extends to the outer side of the collecting tank 3, a water outlet 10 is formed in the lower end of the gas pipe 8, a partition 11 is fixedly connected in the gas pipe 8, a ventilation opening 12 is formed in the lower end of the gas pipe 8, the water outlet 10, the partition 11 and the ventilation opening 12 are sequentially arranged from left to right, vaporized chemical reagent enters the liquefying separation tank 2 from the gas pipe 8 and flows into the collecting tank 3 along the gas pipe 8 to be collected, the liquefied chemical reagent enters the collecting tank 3 from the water outlet 10, and air in the collecting tank 3 exchanges with the air outside through the ventilation opening 12, so that the internal air pressure balance is achieved, and more liquefied chemical reagent can be collected without leakage.

As shown in fig. 5, the upper end of the distillation tank 5 is in threaded connection with a cover body 6, the inner wall of the lower end of the cover body 6 is provided with a conical surface 7, the gas pipe 8 is communicated and connected with the upper end of the cover body 6, the lower end of the cover body 6 is provided with a conical surface 7, a connecting port between the cover body 6 and the gas pipe 8 can be enlarged through the conical surface 7, and the gas inlet efficiency is improved.

As shown in fig. 5, the outer side of the air pipe 8 is sleeved with a heat insulation sleeve 9, the heat insulation sleeve 9 can insulate the air pipe 8 exposed outside, the vaporized chemical agent is prevented from being cooled and liquefied in the conveying process, and the use cost is low.

As shown in fig. 4, the stirring rod 17 is provided with a penetrating bar-shaped hole 18, the rotation resistance of the stirring rod 17 can be reduced by the bar-shaped hole 18, and the stirring efficiency can be improved by the bar-shaped hole 18 when the stirring rod 17 rotates.

The present utility model is not limited in any way by the above-described preferred embodiments, but is not limited to the above-described preferred embodiments, and any person skilled in the art will appreciate that the present utility model can be embodied in the form of a program for carrying out the method of the present utility model, while the above disclosure is directed to various equivalent embodiments, which are capable of being modified or altered in some ways, any simple modification, equivalent variations and alterations made to the above embodiments according to the technical principles of the present utility model will still fall within the scope of the technical aspects of the present utility model.

Claims

1. The chemical reagent separating device comprises a liquefaction separating tank (2), and is characterized in that a collecting tank (3) is arranged at the lower end of the liquefaction separating tank (2), a gas pipe (8) is arranged in the liquefaction separating tank (2) in a penetrating mode, the lower end of the gas pipe (8) extends into the collecting tank (3), a distillation mechanism is connected to the upper end of the gas pipe (8), the distillation mechanism comprises a distillation tank (5) and a water bath tank (1), a stirring mechanism is arranged in the water bath tank (1), a heating pipe (4) is fixed in the water bath tank (1), and the distillation tank (5) is arranged in the center inside the heating pipe (4).

2. A chemical reagent separating apparatus according to claim 1, wherein the stirring mechanism comprises:

The distillation device comprises a placement plate (14), wherein the upper end of the placement plate (14) is fixedly connected with a limiting block (15), the lower end of the distillation tank (5) is fixedly connected with a cannula (13), and the cannula (13) is in matched insertion connection with the limiting block (15);

The water bath device comprises a rotating plate (16), wherein the upper end of the rotating plate (16) is rotationally connected with a placing plate (14), the lower end of the water bath tank (1) is fixedly connected with a driving motor (19), and the output end of the driving motor (19) is fixedly connected with the lower end of the rotating plate (16);

stirring rod (17), stirring rod (17) are fixed in the upper end edge of revolving board (16), the number of stirring rod (17) is a plurality of settings, and the interval equals.

3. The chemical reagent separating device according to claim 2, wherein the lower end of the gas pipe (8) is located in the collecting tank (3), the end portion of the gas pipe extends to the outer side of the collecting tank (3), the lower end of the gas pipe (8) is provided with a water outlet (10), a partition plate (11) is fixedly connected in the gas pipe (8), the lower end of the gas pipe (8) is provided with a ventilation opening (12), and the water outlet (10), the partition plate (11) and the ventilation opening (12) are sequentially arranged from left to right.

4. A chemical reagent separating device according to claim 2, wherein the upper end of the distillation tank (5) is in threaded connection with a cover body (6), the inner wall of the lower end of the cover body (6) is provided with a conical surface (7), and the gas pipe (8) is connected with the upper end of the cover body (6) in a communicating manner.

5. A chemical reagent separating apparatus according to claim 3, wherein the outer side of the gas pipe (8) is provided with a heat retaining jacket (9).

6. A chemical reagent separating device according to claim 2, wherein the stirring rod (17) is provided with a through strip-shaped hole (18).