CN221491527U - Zirconium adsorbent removes fluorine reaction equipment - Google Patents
Zirconium adsorbent removes fluorine reaction equipment Download PDFInfo
- Publication number
- CN221491527U CN221491527U CN202323501019.8U CN202323501019U CN221491527U CN 221491527 U CN221491527 U CN 221491527U CN 202323501019 U CN202323501019 U CN 202323501019U CN 221491527 U CN221491527 U CN 221491527U
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- China
- Prior art keywords
- fixedly arranged
- adsorbent
- reaction tank
- defluorination
- guide rail
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- 239000003463 adsorbent Substances 0.000 title claims abstract description 40
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 34
- 229910052726 zirconium Inorganic materials 0.000 title claims abstract description 21
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 title claims abstract description 20
- 239000011737 fluorine Substances 0.000 title claims abstract description 15
- 229910052731 fluorine Inorganic materials 0.000 title claims abstract description 15
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 title claims description 9
- 238000003756 stirring Methods 0.000 claims abstract description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 35
- 238000006115 defluorination reaction Methods 0.000 claims abstract description 24
- 229910052751 metal Inorganic materials 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- 230000000149 penetrating effect Effects 0.000 claims description 3
- 239000007788 liquid Substances 0.000 abstract description 30
- -1 fluorine ions Chemical class 0.000 abstract description 8
- 230000002457 bidirectional effect Effects 0.000 description 6
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 5
- 238000004140 cleaning Methods 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 244000309464 bull Species 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 150000003754 zirconium Chemical class 0.000 description 1
Landscapes
- Water Treatment By Sorption (AREA)
Abstract
The utility model provides zirconium adsorbent defluorination reaction equipment, which relates to the technical field of defluorination and comprises a reaction tank, wherein an electric guide rail is fixedly arranged on one side of the reaction tank through a support frame, and a right-angle frame is fixedly arranged at the moving end of the electric guide rail. According to the utility model, a worker drives the stirring rod to ascend by starting the electric guide rail, then the worker controls the two right angle plates to move relatively, so that the connecting ring moves to the lower part of the corresponding stirring rod, then the worker controls the moving end of the electric guide rail to move reciprocally, so that the stirring rod moves reciprocally in the connecting ring, the bristles in the connecting ring clean the stirring rod, the adsorbent on the surface of the stirring rod falls off and is discharged out of the reaction tank along with water flow, and the situation that fluorine ions of battery liquid are increased and normal operation of defluorination is influenced due to the fact that the adsorbent is mixed with the next batch of battery liquid is avoided.
Description
Technical Field
The utility model relates to the technical field of defluorination, in particular to zirconium adsorbent defluorination reaction equipment.
Background
In the process of removing fluorine from battery liquid, after the black powder solution is subjected to iron and aluminum removal and the pH value is regulated to a required range, a certain amount of zirconium-based adsorbent is added, and fluorine is adsorbed from the solution by utilizing the high-efficiency selectivity of the adsorbent to fluorine, so that the purpose of removing fluorine is achieved. After the battery liquid is poured into the reaction tank in the defluorination reaction device by a worker, the zirconium-based adsorbent is added, and then the battery liquid is mixed with the zirconium-based adsorbent by the worker by using the stirring mechanism in the device, so that the adsorbent is in uniform and sufficient contact with the battery liquid to adsorb fluorine ions in the battery liquid, but after the defluorination work is finished, the battery liquid in the reaction tank is discharged, as the stirring mechanism continuously stirs the battery liquid, after the battery liquid is discharged, the surface of the stirring mechanism can adhere to part of the adsorbent, and after the adsorbents are mixed with the next batch of battery liquid, fluorine ions can be released again, so that the fluorine ions of the battery liquid are increased, and the normal performance of the defluorination work is influenced.
Disclosure of utility model
The utility model mainly aims to provide the zirconium adsorbent defluorination reaction equipment, which can effectively solve the problems that after the defluorination reaction equipment in the background technology is completed in defluorination work, after the battery liquid in a reaction tank is discharged, the stirring mechanism is used for continuously stirring the battery liquid, so that after the battery liquid is discharged, the surface of the stirring mechanism is adhered with partial adsorbents, fluorine ions can be released again after the adsorbents are mixed with the next batch of battery liquid, so that the fluorine ions of the battery liquid are increased, and the normal operation of defluorination work is influenced.
In order to achieve the above purpose, the technical scheme adopted by the utility model is as follows:
The zirconium adsorbent defluorination reaction equipment comprises a reaction tank, wherein an electric guide rail is fixedly arranged on one side of the reaction tank through a supporting frame, a right-angle frame is fixedly arranged at the moving end of the electric guide rail, a rotating rod is rotatably arranged on the lower surface of the right-angle frame, a transverse plate is fixedly arranged at the lower end of the rotating rod, and stirring rods are fixedly arranged on two sides of the lower surface of the transverse plate;
The reaction tank opposite side fixed mounting has the movable plate, the activity of movable plate upper surface both sides is provided with the right-angle plate, two the right-angle plate is relative one side all has the go-between through horizontal pole fixed mounting, two go-between inner wall is all fixed mounting has a plurality of brush hair.
Preferably, the rotary rod body is sleeved with a first gear;
The lower surface of the right-angle frame is fixedly provided with a first motor at one side close to the first gear, a second gear is sleeved on one side of the shaft body of the output shaft of the first motor, and the second gear is meshed with the first gear.
Preferably, a moving groove is formed in the upper surface of the moving plate, two moving blocks are slidably arranged in the moving groove, and the upper surfaces of the two moving blocks are fixedly connected with corresponding right angle plates respectively;
And a bidirectional screw rod is rotatably arranged between two sides of the inner wall of the movable groove, a second motor is fixedly arranged on one side of the movable plate, and one end of the bidirectional screw rod penetrates through the movable plate and is fixedly connected with the output shaft end of the second motor.
Preferably, cavities are formed in the connecting rings, and drain holes are formed in the inner wall surfaces of the two cavities in a penetrating manner;
And a water inlet pipe is fixedly arranged on the upper surface of each connecting ring.
Preferably, a water tank is fixedly arranged on one side, close to the electric guide rail, of the reaction tank, a booster pump is fixedly arranged on the upper surface of the water tank, and the input end of the booster pump is fixedly connected with the water tank through a connecting pipe;
two output ends of the booster pump are fixedly connected with corresponding water inlet pipes through water delivery pipes respectively.
Preferably, the water pipe is a metal corrugated pipe.
Compared with the prior art, the utility model has the following beneficial effects:
(1) The staff makes it drive the stirring rod through starting electric guide rail and rises, then the staff control two right angle boards relative movement for the go-between removes to the stirring rod below that corresponds, and then the staff control electric guide rail removes end reciprocating motion, make the stirring rod at the inside reciprocating motion of go-between, make the inside brush hair of go-between clean the stirring rod, make the adsorbent on stirring rod surface drop and follow rivers discharge reaction tank outside, avoid these adsorbents and the mixed back of next batch battery liquid, fluoride ion can be released again, the fluoride ion that leads to the battery liquid increases, influence the condition emergence that removes fluorine work normal clear.
Drawings
FIG. 1 is a schematic diagram of the overall structure of a zirconium adsorbent defluorination reaction apparatus according to the present utility model;
FIG. 2 is a schematic top view of a zirconium adsorbent defluorination reactor apparatus according to the present utility model;
FIG. 3 is a schematic view of the cross-sectional structure of the zirconium adsorbent defluorination reaction apparatus of FIG. 2 at A-A;
FIG. 4 is an enlarged schematic view of the structure A in FIG. 3 of a zirconium adsorbent defluorination reaction apparatus according to the present utility model.
In the figure: 1. a reaction tank; 2. a support frame; 201. an electric guide rail; 202. a right angle frame; 203. a rotating rod; 204. a cross plate; 205. a stirring rod; 3. a moving plate; 301. a right angle plate; 302. a cross bar; 303. a connecting ring; 304. brushing; 4. a first gear; 5. a first motor; 501. a second gear; 6. a moving groove; 601. a moving block; 602. a two-way screw rod; 7. a second motor; 8. a cavity; 801. a drain hole; 9. a water inlet pipe; 10. a water tank; 1001. a booster pump; 1002. a connecting pipe; 1003. a water pipe.
Detailed Description
The technical solutions of the embodiments of the present utility model will be clearly and completely described below in conjunction with the embodiments of the present utility model, and it is apparent that the described embodiments are only some embodiments of the present utility model, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
As shown in fig. 1-4, an embodiment of the utility model provides a zirconium adsorbent defluorination reaction device, which comprises a reaction tank 1, wherein an electric guide rail 201 is fixedly arranged on one side of the reaction tank 1 through a supporting frame 2, a right-angle frame 202 is fixedly arranged at the moving end of the electric guide rail 201, a rotating rod 203 is rotatably arranged on the lower surface of the right-angle frame 202, and a transverse plate 204 is fixedly arranged at the lower end of the rotating rod 203. Stirring rods 205 are fixedly arranged on two sides of the lower surface of the transverse plate 204;
The other side of the reaction tank 1 is fixedly provided with a movable plate 3, both sides of the upper surface of the movable plate 3 are movably provided with rectangular plates 301, one opposite side of the two rectangular plates 301 is fixedly provided with a connecting ring 303 through a transverse rod 302, and the inner walls of the two connecting rings 303 are fixedly provided with a plurality of bristles 304.
The staff pours battery liquid into the reaction tank 1 and adds the adsorbent, then the staff controls the rotating rod 203 to rotate, so that the staff drives the two stirring rods 205 to rotate, the stirring rods 205 are used for mixing the battery liquid in the reaction tank 1 with the adsorbent, after the adsorption operation is finished, the staff opens a valve at a discharge port of the reaction tank 1, the liquid flows out of the reaction tank 1, then the staff starts the electric guide rail 201, so that the staff drives the stirring rods 205 to rise, then the staff controls the two right angle plates 301 to relatively move, the connecting rings 303 are enabled to move to the positions below the corresponding stirring rods 205, then the staff controls the moving ends of the electric guide rail 201 to reciprocate, so that the stirring rods 205 reciprocate in the connecting rings 303, the bristles 304 in the connecting rings 303 are used for cleaning the stirring rods 205, so that the adsorbent on the surface of the stirring rods 205 falls and is discharged out of the reaction tank 1 along with water flow, and the situation that fluoride ions of the battery liquid are increased and fluoride ions of the battery liquid are prevented from being released again after the adsorbent is mixed with the next battery liquid, and normal fluoride removal operation is affected.
In another embodiment of the present utility model, the rotary rod 203 is sleeved with the first gear 4;
The lower surface of the right-angle frame 202 is fixedly provided with a first motor 5 at one side close to the first gear 4, a second gear 501 is sleeved at one side of the shaft body of the output shaft of the first motor 5, and the second gear 501 is meshed with the first gear 4.
The staff drives the second gear 501 to rotate by starting the first motor 5, and the rotating rod 203 drives the stirring rod 205 to rotate under the meshing action of the second gear 501 and the first gear 4.
In another embodiment of the present utility model, a moving slot 6 is formed on the upper surface of the moving plate 3, two moving blocks 601 are slidably disposed in the moving slot 6, and the upper surfaces of the two moving blocks 601 are fixedly connected with the corresponding right angle plates 301 respectively;
A bidirectional screw rod 602 is rotatably arranged between two sides of the inner wall of the movable groove 6, a second motor 7 is fixedly arranged on one side of the movable plate 3, and one end of the bidirectional screw rod 602 penetrates through the movable plate 3 and is fixedly connected with the output shaft end of the second motor 7.
The worker starts the second motor 7 to drive the output shaft of the second motor to rotate the bidirectional screw rod 602, and the rotating bidirectional screw rod 602 drives the two moving plates 3 to move relatively in a threaded screwing mode, so that the connecting ring 303 moves to the position below the corresponding stirring rod 205.
In another embodiment of the present utility model, cavities 8 are formed inside the two connection rings 303, and drain holes 801 are formed on the inner wall surfaces of the two cavities 8 in a penetrating manner;
the upper surface of each connecting ring 303 is fixedly provided with a water inlet pipe 9.
A water tank 10 is fixedly arranged on one side of the reaction tank 1, which is close to the electric guide rail 201, a booster pump 1001 is fixedly arranged on the upper surface of the water tank 10, and the input end of the booster pump 1001 is fixedly connected with the water tank 10 through a connecting pipe 1002;
two output ends of the booster pump 1001 are fixedly connected with corresponding water inlet pipes 9 through water delivery pipes 1003 respectively.
The water pipe 1003 is a metal corrugated pipe.
When the brush hair 304 in the connecting ring 303 cleans the stirring rod 205, staff can start the booster pump 1001, so that water in the water tank 10 is finally discharged from the water discharge hole 801 through the water pipe 1003 and the cavity 8, the water in the water tank 10 can flush the stirring rod 205, and the adsorbed firm adsorbent can fall off from the stirring rod 205 under the cooperation of water flow flushing and brush hair 304 cleaning, so that the cleaning effect is enhanced.
By providing the water pipe 1003 as a metal bellows, breakage of the water pipe 1003 when bending or moving is avoided.
The zirconium adsorbent defluorination reaction equipment has the working principle that:
During the use, the staff is through pouring the battery liquid into reaction tank 1 and add the adsorbent, then staff control bull stick 203 rotates, make it drive two stirring rods 205 rotate, thereby make stirring rod 205 mix the inside battery liquid of reaction tank 1 with the adsorbent, after adsorbing the work, the staff opens the valve of reaction tank 1 discharge port, make liquid outflow reaction tank 1, then staff starts electric guide 201, make it drive stirring rod 205 rise, then staff control two right angle plates 301 relative movement, make go-between 303 remove to the stirring rod 205 below that corresponds, then staff control electric guide 201 remove the end reciprocating motion, make stirring rod 205 in the inside reciprocating motion of go-between 303, make the brush hair 304 of go-between 303 clean stirring rod 205, make the adsorbent on stirring rod 205 surface drop and follow rivers discharge reaction tank 1 outside, avoid these adsorbents to mix with next batch of battery liquid after, the fluoride ion can be released again, the fluoride ion that leads to the battery liquid increases, influence the normal condition of going on of removing fluorine.
It should be understood that the foregoing examples of the present utility model are merely illustrative of the present utility model and not limiting of the embodiments of the present utility model, and that various other changes and modifications can be made by those skilled in the art based on the above description, and it is not intended to be exhaustive of all of the embodiments, and all obvious changes and modifications that come within the scope of the utility model are defined by the following claims.
Claims (6)
1. Zirconium adsorbent removes fluorine reaction unit, including reaction tank (1), its characterized in that: an electric guide rail (201) is fixedly arranged on one side of the reaction tank (1) through a supporting frame (2), a right-angle frame (202) is fixedly arranged at the moving end of the electric guide rail (201), a rotating rod (203) is rotatably arranged on the lower surface of the right-angle frame (202), a transverse plate (204) is fixedly arranged at the lower end of the rotating rod (203), and stirring rods (205) are fixedly arranged on two sides of the lower surface of the transverse plate (204);
The reaction tank is characterized in that a movable plate (3) is fixedly arranged on the other side of the reaction tank (1), right-angle plates (301) are movably arranged on two sides of the upper surface of the movable plate (3), connecting rings (303) are fixedly arranged on the opposite sides of the right-angle plates (301) through transverse rods (302), and a plurality of bristles (304) are fixedly arranged on the inner walls of the connecting rings (303).
2. The zirconium adsorbent defluorination reaction apparatus of claim 1, wherein: the rotary rod (203) is sleeved with a first gear (4);
the right angle frame (202) lower surface is close to first gear (4) one side fixed mounting has first motor (5), first motor (5) output shaft body one side cover is equipped with second gear (501), second gear (501) meshes with first gear (4).
3. The zirconium adsorbent defluorination reaction apparatus according to claim 2, wherein: a moving groove (6) is formed in the upper surface of the moving plate (3), two moving blocks (601) are arranged in the moving groove (6) in a sliding mode, and the upper surfaces of the two moving blocks (601) are fixedly connected with corresponding right angle plates (301) respectively;
the two-way screw rod (602) is rotatably arranged between two sides of the inner wall of the movable groove (6), a second motor (7) is fixedly arranged on one side of the movable plate (3), and one end of the two-way screw rod (602) penetrates through the movable plate (3) and is fixedly connected with the output shaft end of the second motor (7).
4. A zirconium adsorbent defluorination reaction apparatus according to claim 3, wherein: a cavity (8) is formed in the two connecting rings (303), and drainage holes (801) are formed in the inner wall surfaces of the two cavities (8) in a penetrating manner;
The upper surface of each connecting ring (303) is fixedly provided with a water inlet pipe (9).
5. The zirconium adsorbent defluorination reaction apparatus according to claim 4, wherein: a water tank (10) is fixedly arranged on one side, close to the electric guide rail (201), of the reaction tank (1), a booster pump (1001) is fixedly arranged on the upper surface of the water tank (10), and the input end of the booster pump (1001) is fixedly connected with the water tank (10) through a connecting pipe (1002);
Two output ends of the booster pump (1001) are fixedly connected with corresponding water inlet pipes (9) through water conveying pipes (1003) respectively.
6. The zirconium adsorbent defluorination reaction apparatus according to claim 5, wherein: the water delivery pipe (1003) is a metal corrugated pipe.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202323501019.8U CN221491527U (en) | 2023-12-21 | 2023-12-21 | Zirconium adsorbent removes fluorine reaction equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202323501019.8U CN221491527U (en) | 2023-12-21 | 2023-12-21 | Zirconium adsorbent removes fluorine reaction equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN221491527U true CN221491527U (en) | 2024-08-09 |
Family
ID=92125133
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202323501019.8U Active CN221491527U (en) | 2023-12-21 | 2023-12-21 | Zirconium adsorbent removes fluorine reaction equipment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN221491527U (en) |
-
2023
- 2023-12-21 CN CN202323501019.8U patent/CN221491527U/en active Active
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