CN221334095U - Novel low-temperature centrifugal separation purification reaction kettle - Google Patents
Novel low-temperature centrifugal separation purification reaction kettle Download PDFInfo
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- CN221334095U CN221334095U CN202322901851.0U CN202322901851U CN221334095U CN 221334095 U CN221334095 U CN 221334095U CN 202322901851 U CN202322901851 U CN 202322901851U CN 221334095 U CN221334095 U CN 221334095U
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- kettle
- water cooling
- centrifugal separation
- insulating housing
- kettle body
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 55
- 238000000926 separation method Methods 0.000 title claims abstract description 25
- 238000000746 purification Methods 0.000 title claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 46
- 238000001816 cooling Methods 0.000 claims abstract description 38
- 238000003756 stirring Methods 0.000 claims abstract description 33
- 239000000463 material Substances 0.000 claims abstract description 20
- 238000004321 preservation Methods 0.000 claims abstract description 10
- 238000004140 cleaning Methods 0.000 claims description 17
- 238000007599 discharging Methods 0.000 claims description 11
- 238000002347 injection Methods 0.000 claims description 8
- 239000007924 injection Substances 0.000 claims description 8
- 239000000243 solution Substances 0.000 claims description 7
- 238000005119 centrifugation Methods 0.000 claims 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 239000007788 liquid Substances 0.000 description 8
- 238000002156 mixing Methods 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- 238000010586 diagram Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 230000008859 change Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 229910000617 Mangalloy Inorganic materials 0.000 description 1
- QFGIVKNKFPCKAW-UHFFFAOYSA-N [Mn].[C] Chemical compound [Mn].[C] QFGIVKNKFPCKAW-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000013064 chemical raw material Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000036632 reaction speed Effects 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model provides a novel low-temperature centrifugal separation and purification reaction kettle, which belongs to the technical field of reaction kettles and comprises the following components: the kettle body, the top of kettle cover is provided with stirring subassembly, the surface mounting of the kettle body has heat insulating housing, heat insulating housing's inside is provided with the heat preservation, heat insulating housing's internally mounted has the circulating water cooling pipe, the constant temperature water cooling box is installed to one side of heat insulating housing, the bottom of ejection of compact funnel is provided with centrifugal separation purification subassembly, can improve the efficiency of the internal material reaction of kettle through stirring subassembly, and centrifugal separation purification subassembly carries out purification to the material after the reaction is accomplished, and heat insulating housing and heat preservation can reduce the external influence to the internal temperature of kettle, use through the cooperation of constant temperature water cooling box, first circulating pipe and circulating water cooling pipe, make the inside of the kettle body can keep at invariable low temperature state, are favorable to the internal portion of kettle to reacting.
Description
Technical Field
The utility model belongs to the technical field of reaction kettles, and particularly relates to a novel low-temperature centrifugal separation and purification reaction kettle.
Background
The reaction kettle is widely understood to be a container with physical or chemical reaction, and through structural design and parameter configuration of the container, the functions of heating, evaporating, cooling and low-high-speed mixing required by the process are realized, and the reaction kettle is widely applied to the fields of petroleum, chemical industry, rubber, pesticides, dyes, medicines, food and the like, and is made of carbon-manganese steel, stainless steel and other composite materials, and consists of a kettle body, a kettle cover, a jacket, a stirrer, a transmission device, a shaft seal device, a support and the like.
The utility model discloses a low-temperature reaction kettle disclosed in publication No. CN202123382510.4, which comprises a kettle body, wherein a hollow inner cavity is formed in the kettle body, an opening communicated with the inner cavity is formed in the upper end of the kettle body, a kettle cover is arranged on the opening, a stirrer and a plurality of adding ports are arranged on the kettle cover, the upper end of the stirrer is positioned outside the kettle cover, the lower end of the stirrer penetrates into the inner cavity, a positioning clamping groove which is recessed downwards is formed in the bottom of the inner cavity, and the lower end of the stirrer penetrates into the positioning clamping groove.
However, the low-temperature reaction kettle in the scheme cannot maintain the temperature at a constant value in the operation process, cannot meet the temperature required by the reaction, is unfavorable for the use of the reaction kettle, and can easily influence the reaction rate and the reaction result in the reaction kettle, so that the practicability of the reaction kettle is reduced.
Disclosure of utility model
The utility model aims to provide a novel low-temperature centrifugal separation purification reaction kettle, and aims to solve the problems that the low-temperature reaction kettle in the prior art cannot maintain the temperature at a constant value in the operation process, cannot meet the temperature required by the reaction, is unfavorable for the use of the reaction kettle, easily influences the reaction rate and the reaction result in the reaction kettle and reduces the practicability of the reaction kettle.
In order to achieve the above purpose, the present utility model provides the following technical solutions:
A novel low-temperature centrifugal separation and purification reaction kettle, which comprises: the kettle body, the bottom evenly distributed of the kettle body installs multiunit supporting leg, the top detachable of the kettle body installs the kettle cover, the top of kettle cover is provided with stirring subassembly, the surface mounting of the kettle body has insulating housing, insulating housing's inside is provided with the heat preservation, insulating housing's internally mounted has circulating water cooling pipe, circulating water cooling pipe's one end extends to insulating housing's top and is connected with first circulating pipe, circulating water cooling pipe's bottom extends to insulating housing's bottom and is connected with the second circulating pipe, constant temperature water cooling box is installed to insulating housing's one side, the other end and the constant temperature water cooling box of first circulating pipe and second circulating pipe are connected, the bottom of the kettle body is connected with the ejection of compact funnel, the bottom of the ejection of compact funnel is provided with centrifugal separation purification subassembly.
As a preferable scheme of the utility model, the stirring assembly comprises a driving motor, the driving motor is arranged at the top of the kettle cover, the output end of the driving motor extends to the inside of the kettle body and is connected with a stirring shaft, a plurality of groups of stirring rods are arranged on the surface of the stirring shaft, and a cleaning assembly is arranged at the top of the stirring shaft.
As a preferable scheme of the utility model, the cleaning assembly comprises a connecting block, the connecting block is arranged at the bottom of the driving motor, one side of the connecting block is connected with a water injection interface, the surface of the stirring shaft is connected with a plurality of groups of cleaning plates, and one ends of the plurality of groups of cleaning plates are connected with spraying nozzles.
As a preferable scheme of the utility model, the stirring shaft is rotatably connected inside the connecting block, and the water injection interface is connected with the stirring shaft.
As a preferable scheme of the utility model, the centrifugal separation and purification assembly comprises a centrifugal separator, wherein the centrifugal separator is connected to the bottom of the discharging hopper, one side of the centrifugal separator is connected with a solution tank, and the bottom of the centrifugal separator is connected with a fixed material box.
As a preferable scheme of the utility model, the bottom of the discharging funnel is connected with a discharging pipe, the discharging pipe is connected with the centrifugal separator, and a control valve is arranged in the discharging pipe.
As a preferable scheme of the utility model, one side of the constant temperature water cooling box is provided with a control panel, and the control panel is electrically connected with the constant temperature water cooling box, the centrifugal separator and the driving motor.
Compared with the prior art, the utility model has the beneficial effects that:
According to the scheme, the efficiency of reaction of materials in the kettle body can be improved through the stirring assembly, solid-liquid separation is carried out on the materials after the reaction is completed through the centrifugal separation purification assembly after the reaction is completed, so that the materials after the reaction is completed are purified, the influence of the outside on the internal temperature of the kettle body can be reduced through the heat insulation shell and the heat preservation layer, the size change of the internal temperature of the kettle body is reduced, the internal temperature of the kettle body is matched with the first circulating pipe, the first circulating pipe and the circulating water cooling pipe to be used, the internal part of the kettle body can be kept in a constant low-temperature state, the internal reaction of the kettle is facilitated, the reaction speed and the reaction effect are improved, and the practicability of equipment is improved.
Drawings
The accompanying drawings are included to provide a further understanding of the utility model and are incorporated in and constitute a part of this specification, illustrate the utility model and together with the embodiments of the utility model, serve to explain the utility model.
In the drawings:
FIG. 1 is a schematic diagram of the overall structure of the present utility model;
FIG. 2 is a schematic cross-sectional view of an insulated housing according to the present utility model;
FIG. 3 is a schematic diagram of a cross-sectional structure of a kettle body according to the present utility model;
FIG. 4 is a schematic diagram of the structure of the centrifugal separation and purification assembly of the present utility model.
In the figure: 1. a heat insulating housing; 101. a heat preservation layer; 102. a circulating water cooling pipe; 2. a kettle body; 3. a kettle cover; 4. a constant temperature water cooling box; 401. a control panel; 402. a first circulation pipe; 403. a second circulation pipe; 5. support legs; 6. a centrifugal separator; 601. a solution tank; 602. fixing the feed box; 7. a driving motor; 701. a stirring shaft; 702. a stirring rod; 8. a connecting block; 801. a water injection interface; 802. cleaning the plate; 803. a spray port; 9. a discharge hopper; 901. and controlling the valve.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
Examples
Referring to fig. 1-4, the technical scheme provided by the present embodiment is as follows:
A novel low-temperature centrifugal separation and purification reaction kettle, which comprises: the kettle body 2, multiunit supporting leg 5 is installed to the bottom evenly distributed of the kettle body 2, the top detachable of the kettle body 2 installs the kettle cover 3, the top of kettle cover 3 is provided with stirring subassembly, the surface mounting of the kettle body 2 has insulating housing 1, insulating housing 1's inside is provided with heat preservation 101, insulating housing 101's internally mounted has circulating water cooling pipe 102, circulating water cooling pipe 102's one end extends to insulating housing 1's top and is connected with first circulating pipe 402, circulating water cooling pipe 102's bottom extends to insulating housing 1's bottom and is connected with second circulating pipe 403, constant temperature water cooling box 4 is installed to one side of insulating housing 1, the other end and the constant temperature water cooling box 4 of first circulating pipe 402 and second circulating pipe 403 are connected, the bottom of the kettle body 2 is connected with ejection of compact funnel 9, the bottom of ejection of compact funnel 9 is provided with centrifugal separation subassembly.
In the specific embodiment of the utility model, the reaction rate of the raw materials in the kettle body 2 can be improved through the stirring assembly, after the reaction is finished, the materials are subjected to solid-liquid separation through the centrifugal separation and purification assembly, the materials after the reaction is finished are subjected to purification treatment, the heat insulation shell 1 and the heat preservation layer 101 can reduce the influence of the outside on the internal temperature of the kettle body 2, the change of the internal temperature of the kettle body 2 is reduced, and the high temperature generated during the reaction in the kettle body 2 can be subjected to cooling treatment through the cooperation of the constant-temperature water cooling tank 4, the first circulating pipe 402 and the circulating water cooling pipe 102, so that the internal part of the kettle body 2 can be kept in a constant low-temperature state, the reaction in the kettle body 2 is facilitated, the reaction rate and the effect are improved, and the practicability of the equipment is improved.
Specifically, the stirring assembly includes driving motor 7, and driving motor 7 installs at the top of kettle cover 3, and driving motor 7's output extends to the inside of kettle body 2 and is connected with (mixing) shaft 701, and (mixing) shaft 701's surface mounting has multiunit puddler 702, and the top of (mixing) shaft 701 is provided with cleaning assembly.
In the embodiment of the utility model, the stirring shaft 701 can be driven to rotate by the driving motor 7, and the stirring rod 702 on the surface is driven to rotate when the stirring shaft 701 rotates, so that the liquid in the kettle body 2 is stirred, the precipitation reaction is facilitated, and the inside of the kettle body 2 can be cleaned after the reaction is completed by the cleaning component.
Specifically, the cleaning assembly comprises a connecting block 8, the connecting block 8 is arranged at the bottom of the driving motor 7, one side of the connecting block 8 is connected with a water injection interface 801, the surface of the stirring shaft 701 is connected with a plurality of groups of cleaning plates 802, and one end of each group of cleaning plates 802 is connected with a spraying opening 803.
In the embodiment of the present utility model, cleaning water is supplied to the inside of the cleaning plate 802 through the water injection port 801, and the inside of the tank 2 is cleaned by spraying the cleaning water to the inside of the tank 2 through the spraying port 803.
Specifically, the stirring shaft 701 is rotatably connected to the inside of the connection block 8, and the water injection port 801 is connected to the stirring shaft 701.
Specifically, the centrifugal separation assembly comprises a centrifugal separator 6, wherein the centrifugal separator 6 is connected to the bottom of a discharge hopper 9, one side of the centrifugal separator 6 is connected with a solution tank 601, and the bottom of the centrifugal separator 6 is connected with a fixed material box 602.
In the embodiment of the present utility model, the precipitated liquid is fixedly separated by the centrifugal separator 6, the separated liquid is fixedly introduced into the inside of the fixed tank 602, and the liquid is introduced into the inside of the solution tank 601 to be stored, thereby purifying the precipitated chemical raw material.
Specifically, the bottom of discharge hopper 9 is connected and is arranged the material pipe, arranges the material pipe and is connected with centrifugal separator 6, arranges the inside of material pipe and is provided with control valve 901.
In an embodiment of the utility model, the flow rate of the discharge hopper 9 can be controlled by controlling the valve 901.
Specifically, a control panel 401 is installed on one side of the constant temperature water cooling tank 4, and the control panel 401 is electrically connected with the constant temperature water cooling tank 4, the centrifugal separator 6 and the driving motor 7.
In the specific embodiment of the utility model, the equipment is conveniently operated by the constant-temperature water cooling box 4, so that the equipment is convenient for workers to use.
Working principle: when the reactor is used, equipment is connected with an external power supply and a controller, a material flow needing to be reacted is added into the reactor body 2, the reactor cover 3 is closed, the constant temperature water cooling tank 4 is opened through the control panel 401, low-temperature liquid in the constant temperature water cooling tank 4 is conveyed into the circulating water cooling pipe 102 after passing through the first circulating pipe 402 and the second circulating pipe 403, the circulating water cooling pipe 102 cools the inside of the heat preservation 101, the low temperature in the reactor body 2 is kept constant, the material flow in the reactor body 2 is stirred through the stirring assembly in the reaction process, the reaction efficiency is improved, the material discharging pipe is opened through the control valve 901 after the reaction is completed, the material flow after the reaction enters the centrifugal separator 6, the centrifugal separator 6 is started to separate and purify the material flow after the reaction, the separated solid enters the inside of the fixed material box 602 to be stored, the liquid enters the inside of the solution box 601 to be stored, and the purity of the material after the reaction is improved.
Finally, it should be noted that: the foregoing description is only a preferred embodiment of the present utility model, and the present utility model is not limited thereto, but it is to be understood that modifications and equivalents of some of the technical features described in the foregoing embodiments may be made by those skilled in the art, although the present utility model has been described in detail with reference to the foregoing embodiments. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present utility model should be included in the protection scope of the present utility model.
Claims (7)
1. Novel low temperature centrifugation purification reation kettle, its characterized in that includes: kettle body (2), multiunit supporting leg (5) are installed to the bottom evenly distributed of kettle body (2), kettle cover (3) are installed to the top detachable of kettle body (2), the top of kettle cover (3) is provided with stirring subassembly, the surface mounting of kettle body (2) has insulating housing (1), the inside of insulating housing (1) is provided with heat preservation (101), the internally mounted of heat preservation (101) has circulation water cooling tube (102), the one end of circulation water cooling tube (102) extends to the top of insulating housing (1) and is connected with first circulating pipe (402), the bottom of circulation water cooling tube (102) extends to the bottom of insulating housing (1) and is connected with second circulating pipe (403), constant temperature water cooling tank (4) are installed to one side of insulating housing (1), the other end and the constant temperature water cooling tank (4) of first circulating pipe (402) and second circulating pipe (403), the bottom of kettle body (2) is connected with ejection of compact funnel (9), the bottom of circulation water cooling tube (102) is provided with centrifugal subassembly.
2. The novel low-temperature centrifugal separation and purification reaction kettle according to claim 1, wherein: the stirring assembly comprises a driving motor (7), the driving motor (7) is arranged at the top of the kettle cover (3), the output end of the driving motor (7) extends to the inside of the kettle body (2) and is connected with a stirring shaft (701), a plurality of groups of stirring rods (702) are arranged on the surface of the stirring shaft (701), and a cleaning assembly is arranged at the top of the stirring shaft (701).
3. The novel low-temperature centrifugal separation and purification reaction kettle according to claim 2, wherein: the cleaning assembly comprises a connecting block (8), the bottom at driving motor (7) is installed to connecting block (8), one side of connecting block (8) is connected with water injection interface (801), the surface of (701) stirring axle is connected with multiunit cleaning plate (802), multiunit cleaning plate (802) one end is connected with sprinkler head (803).
4. A novel low-temperature centrifugal separation and purification reaction kettle according to claim 3, which is characterized in that: the stirring shaft (701) is rotatably connected inside the connecting block (8), and the water injection interface (801) is connected with the stirring shaft (701).
5. The novel low-temperature centrifugal separation and purification reaction kettle according to claim 1, wherein: the centrifugal separation assembly comprises a centrifugal separator (6), the centrifugal separator (6) is connected to the bottom of the discharging funnel (9), one side of the centrifugal separator (6) is connected with a solution tank (601), and the bottom of the centrifugal separator (6) is connected with a fixed material box (602).
6. The novel low-temperature centrifugal separation and purification reaction kettle according to claim 5, wherein: the bottom of the discharging funnel (9) is connected with a discharging pipe, the discharging pipe is connected with the centrifugal separator (6), and a control valve (901) is arranged in the discharging pipe.
7. The novel low-temperature centrifugal separation and purification reaction kettle according to claim 1, wherein: one side of the constant temperature water cooling box (4) is provided with a control panel (401), and the control panel (401) is electrically connected with the constant temperature water cooling box (4), the centrifugal separator (6) and the driving motor (7).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322901851.0U CN221334095U (en) | 2023-10-27 | 2023-10-27 | Novel low-temperature centrifugal separation purification reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202322901851.0U CN221334095U (en) | 2023-10-27 | 2023-10-27 | Novel low-temperature centrifugal separation purification reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN221334095U true CN221334095U (en) | 2024-07-16 |
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ID=91826611
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202322901851.0U Active CN221334095U (en) | 2023-10-27 | 2023-10-27 | Novel low-temperature centrifugal separation purification reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN221334095U (en) |
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2023
- 2023-10-27 CN CN202322901851.0U patent/CN221334095U/en active Active
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