CN218924700U - Ionic liquid synthesis reaction device - Google Patents
Ionic liquid synthesis reaction device Download PDFInfo
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- CN218924700U CN218924700U CN202223605288.4U CN202223605288U CN218924700U CN 218924700 U CN218924700 U CN 218924700U CN 202223605288 U CN202223605288 U CN 202223605288U CN 218924700 U CN218924700 U CN 218924700U
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- reaction
- ionic liquid
- tank body
- fixed mounting
- reaction tank
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- 239000002608 ionic liquid Substances 0.000 title claims abstract description 31
- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 19
- 238000006243 chemical reaction Methods 0.000 claims abstract description 52
- 238000003756 stirring Methods 0.000 claims abstract description 30
- 239000007788 liquid Substances 0.000 claims abstract description 25
- 230000001681 protective effect Effects 0.000 claims description 13
- 244000309464 bull Species 0.000 claims description 6
- 239000002994 raw material Substances 0.000 abstract description 15
- 239000000463 material Substances 0.000 abstract description 13
- 230000005484 gravity Effects 0.000 abstract description 4
- 230000036632 reaction speed Effects 0.000 abstract 1
- 238000002156 mixing Methods 0.000 description 15
- 150000001450 anions Chemical class 0.000 description 5
- 150000001768 cations Chemical class 0.000 description 5
- 230000000694 effects Effects 0.000 description 3
- 230000007547 defect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
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Abstract
The utility model relates to the technical field of reaction devices, in particular to an ionic liquid synthesis reaction device which comprises a reaction tank body, wherein a feeding pipe is fixedly arranged at the upper end of the reaction tank body, a liquid discharge pipe is fixedly arranged at the bottom end of the reaction tank body, and a feeding hole is formed in the upper surface of the reaction tank body. According to the utility model, the rotary table is driven to rotate through the rotation of the gear II, when the position of the liquid adding pipe is coincident with the position of the notch, raw materials in the liquid storage tank leak out of the notch due to gravity, enter the reaction tank body from the connecting pipe and the charging port and react with materials in the reaction tank body, the stirring shaft rotates and drives the stirring blade to rotate, the synthetic reaction raw materials in the reaction tank body are stirred and mixed through the rotation of the stirring blade, the reaction speed between the reaction raw materials is accelerated, and the reaction device is used for stirring while charging, so that the materials are mixed more fully, the reaction is more thorough, and the synthetic efficiency of the ionic liquid is improved.
Description
Technical Field
The utility model relates to the technical field of reaction devices, in particular to an ionic liquid synthesis reaction device.
Background
Ionic liquids are liquids that are entirely composed of ions and are liquid at or near room temperature, and are also referred to as room temperature ionic liquids, room temperature molten salts, and the like, and currently there is no uniform name but there is a tendency for ionic liquids to be abbreviated. In ionic liquids, the acting force between anions and cations is coulombic force, the size of the acting force is related to the charge quantity and radius of the anions and cations, the larger the ionic radius is, the smaller the acting force between the anions and cations is, the lower the melting point of the ionic liquid is, the larger the volume of the anions and cations of certain ionic liquids is, the loose structure is, and the acting force between the anions and cations is lower, so that the melting point is close to room temperature.
At present, in the actual use process of the ionic liquid synthesis reaction device on the market, two or more synthesis raw materials are generally added into a reaction tank at the same time and then are mixed by being matched with a stirring structure, the reaction mode has the defect of insufficient mixing, the mixing degree among the materials is reduced, the final synthesis reaction efficiency is influenced, and therefore, the ionic liquid synthesis reaction device is provided for solving the problems.
Disclosure of Invention
In order to overcome the defects in the prior art, the utility model provides an ionic liquid synthesis reaction device.
In order to solve the technical problems, the utility model provides the following technical scheme: the utility model provides an ionic liquid synthesis reaction unit, includes the retort body, the upper end fixed mounting of the retort body has the inlet pipe, the bottom fixed mounting of the retort body has the fluid-discharge tube, the charge door has been seted up to the upper surface of the retort body, the upper end fixed mounting of the retort body has the motor, the output shaft fixedly connected with (mixing) shaft of motor, the (mixing) shaft rotates and installs in the retort body, equal distance fixed mounting has the stirring leaf on the (mixing) shaft, (mixing) shaft upper end fixed mounting has gear one, the upper end fixed mounting of the retort body has the liquid storage pot, the bottom fixed mounting of liquid storage pot has the liquid feeding pipe, be provided with reinforced structure on the retort body, reinforced structure includes bull stick, carousel and protecting crust, the bull stick rotates the upper end of installing at the retort body, carousel fixed mounting is on the bull stick, carousel movable mounting is in the shell, the protecting crust rotates with the bull stick to be connected, the bottom circumference fixed mounting of the supporting leg, the outside fixed mounting of the reacting pot body has the shell, the inside temperature control pipe that sets up of shell.
As a preferable technical scheme of the utility model, notches are formed in the circumference of the upper surface of the rotary table at equal intervals, the number of the notches is four, and the bottom surface of the liquid adding pipe is attached to the upper surface of the rotary table.
As a preferable technical scheme of the utility model, a second gear is fixedly arranged on the rotating rod, and the second gear is meshed with the first gear.
As a preferable technical scheme of the utility model, both sides of the bottom end of the protective shell are fixedly provided with the fixed blocks, and both the fixed blocks are fixedly arranged at the upper end of the reaction tank body.
As a preferable technical scheme of the utility model, a connecting pipe is fixedly arranged at the bottom end of the protective shell, and the connecting pipe is movably inserted into the charging hole.
Compared with the prior art, the utility model has the following beneficial effects:
the rotation through the (mixing) shaft can drive gear one and rotate, can drive gear two through gear one's rotation and rotate, can drive the carousel through gear two's rotation and rotate, when the position of filling pipe and the position of breach coincide, the raw materials in the liquid storage pot can leak from the breach because gravity, and it is internal to get into the retort from connecting pipe and charge door, and react with the internal material of retort, can drive the stirring leaf in the (mixing) shaft pivoted and rotate, can stir the synthetic reaction raw materials in the retort through the rotation of stirring leaf, accelerate the reaction rate between each reaction raw materials, this reaction unit is through the stirring of reinforced limit, make mixing more abundant between each material, the reaction is more thorough, ionic liquid's synthetic efficiency has been improved.
The upper end of the reaction tank body is fixedly provided with the protective shell, the turntable is movably arranged in the protective shell, the ionic liquid can be prevented from being scattered and leaked out, the outer side of the reaction tank body is fixedly provided with the shell, the temperature of the reaction tank body can be controlled, the reaction between materials is accelerated, the liquid storage tank is fixedly arranged at the upper end of the reaction tank body, and the space occupied by the upper part of the device to the device is reduced.
Drawings
FIG. 1 is a schematic structural diagram of an ionic liquid synthesis reaction device according to the present utility model;
FIG. 2 is a schematic diagram of a turntable according to the present utility model;
FIG. 3 is a schematic view of the reaction tank in the sectional structure;
FIG. 4 is a schematic structural view of the protective shell of the present utility model.
Wherein: 1. a reaction tank body; 11. a feed pipe; 12. a liquid discharge pipe; 13. a feed inlet; 14. support legs; 15. a housing; 2. a stirring shaft; 21. stirring the leaves; 22. a first gear; 3. a motor; 4. a liquid storage tank; 41. a liquid adding tube; 5. a rotating rod; 51. a second gear; 6. a turntable; 61. a notch; 7. a protective shell; 71. a fixed block; 72. and (5) connecting pipes.
Detailed Description
In order that the manner in which the above recited features, objects and advantages of the present utility model are obtained will become readily apparent, a more particular description of the utility model will be rendered by reference to specific embodiments thereof which are illustrated in the appended drawings. Based on the examples in the embodiments, those skilled in the art can obtain other examples without making any inventive effort, which fall within the scope of the utility model. The experimental methods in the following examples are conventional methods unless otherwise specified, and materials, reagents, etc. used in the following examples are commercially available unless otherwise specified.
As shown in fig. 1, 2, 3 and 4, an ionic liquid synthesis reaction device comprises a reaction tank body 1, a feeding pipe 11 is fixedly arranged at the upper end of the reaction tank body 1, a liquid discharge pipe 12 is fixedly arranged at the bottom end of the reaction tank body 1, a feeding port 13 is arranged on the upper surface of the reaction tank body 1, a motor 3 is fixedly arranged at the upper end of the reaction tank body 1, an output shaft of the motor 3 is fixedly connected with a stirring shaft 2, the stirring shaft 2 is rotatably arranged in the reaction tank body 1, stirring blades 21 are fixedly arranged on the stirring shaft 2 at equal intervals, a gear one 22 is fixedly arranged at the upper end of the stirring shaft 2, a liquid storage tank 4 is fixedly arranged at the upper end of the reaction tank body 1, a liquid adding pipe 41 is fixedly arranged at the bottom end of the liquid storage tank 4, a feeding structure is arranged on the reaction tank body 1 and comprises a rotating rod 5, a rotating disc 6 and a protecting shell 7, the rotating rod 5 is rotatably arranged at the upper end of the reaction tank body 1, the rotary table 6 is fixedly arranged on the rotary table 5, the rotary table 6 is movably arranged in the protective shell 7, the protective shell 7 is rotationally connected with the rotary table 5, the bottom circumference of the reaction tank body 1 is fixedly provided with supporting legs 14 at equal intervals, the outer side of the reaction tank body 1 is fixedly provided with a shell 15, a temperature control tube is arranged in the shell 15, the circumference of the upper surface of the rotary table 6 is provided with notches 61 at equal intervals, the number of the notches 61 is four, the bottom surface of the liquid adding tube 41 is attached to the upper surface of the rotary table 6, the rotary table 5 is fixedly provided with a gear II 51, the gear II 51 is meshed with the gear I22, a part of synthetic raw materials 1 is fed into the reaction tank body 1 from the feed tube 11, then the raw materials 2 for synthesis reaction are fed into the liquid storage tank 4, the motor 3 is started, the stirring shaft 2 is enabled to rotate, the first gear 22 is driven to rotate through the rotation of the stirring shaft 2, the second gear 51 is driven to rotate through the rotation of the gear I22, the rotation through gear two 51 can drive carousel 6 and rotate, when the position of filling tube 41 overlaps with the position of breach 61, raw materials 2 in the liquid storage pot 4 can leak from breach 61 because of gravity, and get into in the retort body 1 from connecting pipe 72 and charge door 13, and react with raw materials 1 in the retort body 1, stirring axle 2 can drive stirring leaf 21 and rotate when rotating, can stir the material in the retort body 1 through stirring leaf 21's rotation, accelerate the mixing between each material, thereby promote the synthetic reaction of ionic liquid, this reaction unit is through the reinforced while stirring of being simultaneously, make the mixing more abundant between each material, the reaction is more thorough, the synthetic efficiency of ionic liquid has been improved. The upper end through the retort body 1 fixed mounting has the protecting crust 7, carousel 6 activity sets up in the protecting crust 7, can prevent that ionic liquid from spilling out, outside fixed mounting through the retort body 1 has shell 15, can play the effect of accuse temperature to ionic liquid in the retort body 1, the reaction between each material has been accelerated, reservoir 4 fixed mounting is in the upper end of the retort body 1, the space size that the device upper part occupied to the device has been reduced, the equal fixed mounting in both sides of protecting crust 7 bottom has fixed block 71, two fixed blocks 71 equal fixed mounting are in the upper end of the retort body 1, the bottom fixed mounting of protecting crust 7 has connecting pipe 72, connecting pipe 72 activity grafting is in charge door 13.
During the use, throw into the retort body 1 with partly synthetic raw materials 1 in the inlet pipe 11, the raw materials 2 that will be used for synthetic reaction next drops into the liquid storage pot 4, starter motor 3, make (mixing) shaft 2 rotate, can drive the first 22 of movable gear through the rotation of (mixing) shaft 2 and rotate, can drive gear two 51 and rotate through the rotation of gear two 51, can drive carousel 6 and rotate, when the position of filling pipe 41 overlaps with the position of breach 61, raw materials 2 in the liquid storage pot 4 can spill from breach 61 owing to gravity, and get into the retort body 1 from connecting pipe 72 and charge door 13, and carry out the reaction with synthetic raw materials 1 in the retort body 1, can drive stirring leaf 21 and rotate in the time of (mixing) shaft 2, can stir the material in the retort body 1 through the rotation of stirring leaf 21, thereby promote the synthetic reaction of ionic liquid, this reaction device is through the while stirring, make mixing more abundant between each material, the reaction thoroughly improves the synthetic efficiency of ionic liquid, the synthetic liquid has been improved, the reactor is equipped with at the reactor body 1 through the fixed part of the side of the fixed part of the reactor shell of the reactor 1 in the side of can be fixed to the reactor 1, the reactor shell of the reactor 1 has been realized, the reactor shell of the reactor 1 has been prevented, the reactor shell of the reactor 1 has been greatly improved, the reactor 1 has been installed, the reactor has been equipped with the reactor 1 has been fixed in the reactor 1, the reactor has been well-protecting equipment has been installed.
The embodiments of the present utility model have been described in detail with reference to the drawings, but the present utility model is not limited thereto, and various changes can be made within the knowledge of those skilled in the art without departing from the spirit of the present utility model.
Claims (6)
1. The utility model provides an ionic liquid synthesis reaction device, includes the retort body (1), its characterized in that, the upper end fixed mounting of retort body (1) has inlet pipe (11), the bottom fixed mounting of retort body (1) has fluid-discharge tube (12), charge door (13) have been seted up to the upper surface of retort body (1), the upper end fixed mounting of retort body (1) has motor (3), the output shaft fixedly connected with (2) of motor (3), (2) rotation installs in retort body (1), equal interval fixed mounting has (21) stirring leaf on (2) stirring shaft, (2) upper end fixed mounting has gear one (22), the upper end fixed mounting of retort body (1) has fluid-storage tank (4), the bottom fixed mounting of fluid-storage tank (4) has fluid-feeding tube (41), be provided with reinforced structure on retort body (1), reinforced structure includes bull stick (5), carousel (6) and protective housing (7), bull stick (5) rotation is installed on (6) rotation end at (6) in the protective housing (7), the protective shell (7) is rotationally connected with the rotating rod (5).
2. The ionic liquid synthesis reaction device according to claim 1, wherein supporting legs (14) are fixedly arranged at equal intervals on the circumference of the bottom end of the reaction tank body (1), a shell (15) is fixedly arranged on the outer side of the reaction tank body (1), and a temperature control tube is arranged inside the shell (15).
3. The ionic liquid synthesis reaction device according to claim 1, wherein notches (61) are formed in the circumference of the upper surface of the rotary table (6) at equal intervals, the number of the notches (61) is four, and the bottom surface of the liquid adding pipe (41) is attached to the upper surface of the rotary table (6).
4. The ionic liquid synthesis reaction device according to claim 1, wherein a second gear (51) is fixedly arranged on the rotating rod (5), and the second gear (51) is meshed with the first gear (22).
5. The ionic liquid synthesis reaction device according to claim 1, wherein two sides of the bottom end of the protective shell (7) are fixedly provided with fixing blocks (71), and the two fixing blocks (71) are fixedly arranged at the upper end of the reaction tank body (1).
6. The ionic liquid synthesis reaction device according to claim 1, wherein a connecting pipe (72) is fixedly arranged at the bottom end of the protective shell (7), and the connecting pipe (72) is movably inserted into the feed inlet (13).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202223605288.4U CN218924700U (en) | 2022-12-30 | 2022-12-30 | Ionic liquid synthesis reaction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202223605288.4U CN218924700U (en) | 2022-12-30 | 2022-12-30 | Ionic liquid synthesis reaction device |
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| Publication Number | Publication Date |
|---|---|
| CN218924700U true CN218924700U (en) | 2023-04-28 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202223605288.4U Active CN218924700U (en) | 2022-12-30 | 2022-12-30 | Ionic liquid synthesis reaction device |
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| Country | Link |
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| CN (1) | CN218924700U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN119349749A (en) * | 2024-12-03 | 2025-01-24 | 濮阳惠成新材料产业技术研究院有限公司 | A pyrrole triazine photoelectric material waste liquid treatment device |
-
2022
- 2022-12-30 CN CN202223605288.4U patent/CN218924700U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN119349749A (en) * | 2024-12-03 | 2025-01-24 | 濮阳惠成新材料产业技术研究院有限公司 | A pyrrole triazine photoelectric material waste liquid treatment device |
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