CN218799119U - A kind of preparation device of flake silver powder for HJT silver paste - Google Patents

A kind of preparation device of flake silver powder for HJT silver paste Download PDF

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CN218799119U
CN218799119U CN202320000878.XU CN202320000878U CN218799119U CN 218799119 U CN218799119 U CN 218799119U CN 202320000878 U CN202320000878 U CN 202320000878U CN 218799119 U CN218799119 U CN 218799119U
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stirring
hjt
silver powder
feeding
silver paste
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游立
张轶
桂苗
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Csic Huanggang Precious Metals Co ltd
Wuhan Research Institute Of Marine Electric Propulsion No 712 Research Institute Of China Shipbuilding Corp
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Csic Huanggang Precious Metals Co ltd
Wuhan Research Institute Of Marine Electric Propulsion No 712 Research Institute Of China Shipbuilding Corp
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Abstract

本实用新型公开了一种HJT银浆用片状银粉的制备装置,包括自动进料漏斗、开关阀、搅拌系统、测温仪、压力监测仪、搅拌罐桶体、气动隔膜泵、冰水机、开关阀以及出料阀门。本制备装置按照HJT银浆用片状银粉生产的工艺流程进行设计,确保操作方便,运行可靠,极大地减少了片状银粉球磨过程中过热出现压力过大、球磨不均匀、亮片等不良现象,大大改善了HJT银浆用片状银粉生产制备的工序、品质及收率。

Figure 202320000878

The utility model discloses a preparation device of flake silver powder for HJT silver paste, which comprises an automatic feeding funnel, a switch valve, a stirring system, a temperature measuring instrument, a pressure monitoring instrument, a stirring tank body, a pneumatic diaphragm pump, and an ice water machine , switch valve and discharge valve. The preparation device is designed according to the production process of flake silver powder for HJT silver paste, which ensures convenient operation and reliable operation, and greatly reduces the adverse phenomena such as excessive pressure, uneven ball milling, and sequins caused by overheating in the ball milling process of flake silver powder. The process, quality and yield of the production and preparation of flake silver powder for HJT silver paste have been greatly improved.

Figure 202320000878

Description

一种HJT银浆用片状银粉的制备装置A kind of preparation device of flake silver powder for HJT silver paste

技术领域technical field

本实用新型涉及纳微米级金属粉体材料制备技术领域,具体涉及一种HJT银浆用片状银粉的制备装置。The utility model relates to the technical field of nano-micron-level metal powder material preparation, in particular to a preparation device for flaky silver powder for HJT silver paste.

背景技术Background technique

目前在片状银粉制备过程中,主要是通过人工向卧式球磨机中加入物料、磨球、球磨溶剂及分散剂,出粉过程中也几乎由人工进行磨球与银粉浆料、浆液的固液分离,整个过程周期长、收率低、银损耗量大。At present, in the preparation process of flake silver powder, it is mainly by manually adding materials, grinding balls, ball milling solvents and dispersants to the horizontal ball mill, and the solid-liquid of the grinding balls and silver powder slurry and slurry is almost manually performed during the powder extraction process. Separation, the whole process cycle is long, the yield is low, and the amount of silver loss is large.

卧式球磨无法保证球磨过程中磨球和银粉颗粒之间产生均匀的碰撞和剪切运动,同时球磨过程中可能存在局部过热造成冷焊、亮片等不良现象出现。The horizontal ball mill cannot guarantee the uniform collision and shearing motion between the ball and the silver powder particles during the ball milling process. At the same time, there may be local overheating during the ball milling process, which may cause cold welding, sequins and other undesirable phenomena.

实用新型内容Utility model content

本实用新型的目的是根据现有技术的不足,提供一种HJT银浆用片状银粉的制备装置。The purpose of this utility model is to provide a preparation device for flake silver powder for HJT silver paste according to the deficiencies of the prior art.

本实用新型解决其技术问题所采用的技术方案是:一种HJT银浆用片状银粉的制备装置,包括搅拌罐和搅拌系统,所述的搅拌罐包括搅拌罐桶体和设置在搅拌罐桶体外的夹套,所述的搅拌系统包括倒置在搅拌罐桶体顶部开口处的搅拌电机,所述的搅拌罐桶体内设置有搅拌螺旋桨叶,搅拌螺旋桨叶通过减速机连接搅拌电机,搅拌罐桶体顶部通过加料开关阀连接加料管,所述的加料管上设置有自动进料漏斗,通过自动进料漏斗向搅拌罐内供给球磨的原始银粉,搅拌罐桶体上下侧壁分别通过进料管和出料管连接气动隔膜泵,研磨的物料浆液通过气动隔膜泵循环往复送入搅拌罐桶体,夹套的上下侧壁分别通过出水管和进水管连接风冷式冰水机,夹套层由风冷式冰水机进行供给循环冷却水,搅拌罐底部通过出料开关阀连接出料阀门。The technical solution adopted by the utility model to solve the technical problems is: a preparation device for flake silver powder for HJT silver paste, including a stirring tank and a stirring system, and the stirring tank includes a stirring tank body and a mixing tank barrel The external jacket, the stirring system includes a stirring motor inverted at the top opening of the stirring tank body, the stirring tank body is provided with stirring propeller blades, the stirring propeller blades are connected to the stirring motor through a reducer, and the stirring tank barrel The top of the body is connected to the feeding pipe through the feeding switch valve. The feeding pipe is provided with an automatic feeding funnel, and the original silver powder of the ball mill is supplied to the mixing tank through the automatic feeding funnel. The upper and lower side walls of the mixing tank body pass through the feeding pipe The discharge pipe is connected to the pneumatic diaphragm pump, and the ground material slurry is sent to the mixing tank barrel reciprocatingly through the pneumatic diaphragm pump. The circulating cooling water is supplied by the air-cooled chiller, and the bottom of the mixing tank is connected to the discharge valve through the discharge switch valve.

所述的一种HJT银浆用片状银粉的制备装置,其搅拌罐顶部设置加料盖,所述的减速机和加料开关阀设置在加料盖上,加料盖上还设置有加料孔、压力监测仪和测温仪。The preparation device for flake silver powder for HJT silver paste, the top of the stirring tank is provided with a feeding cover, the speed reducer and the feeding switch valve are arranged on the feeding cover, and the feeding cover is also provided with a feeding hole, a pressure monitoring instruments and thermometers.

所述的一种HJT银浆用片状银粉的制备装置,还包括PLC控制器,所述的PLC控制器分别连接自动进料漏斗、搅拌系统、压力监测仪、测温仪、出料开关阀、加料开关阀、气动隔膜泵以及风冷式冰水机。The preparation device for flake silver powder for a kind of HJT silver paste also includes a PLC controller, and the PLC controller is respectively connected to an automatic feeding funnel, a stirring system, a pressure monitor, a thermometer, and a discharge switch valve , feeding switch valve, pneumatic diaphragm pump and air-cooled chiller.

所述的一种HJT银浆用片状银粉的制备装置,其风冷式冰水机由水箱式蒸发器、压缩机、散热器和散热风机组成,所述的水箱式蒸发器通过循环水泵连接出水管。The preparation device of flake silver powder for a kind of HJT silver paste, its air-cooled ice water machine is made up of water tank type evaporator, compressor, radiator and cooling fan, and described water tank type evaporator is circulated through The water pump is connected to the outlet pipe.

所述的一种HJT银浆用片状银粉的制备装置,其搅拌罐桶体内壁设置有不锈钢滤网。In the preparation device of flake silver powder for HJT silver paste, the inner wall of the stirring tank is provided with a stainless steel filter screen.

本实用新型的有益效果是:本装置过程中无中间产品转运,在一个封闭自动化程度较高的系统内进行,最大程度减少了人工因素干扰带来的产品质量不稳定性、人工成本,极大地减少了片状银粉球磨过程中过热出现压力过大、球磨不均匀、亮片等不良现象,大大改善了HJT银浆用片状银粉生产制备的工序、品质及收率。The beneficial effects of the utility model are: there is no intermediate product transfer in the process of the device, and it is carried out in a closed system with a high degree of automation, which reduces the instability of product quality and labor costs caused by the interference of artificial factors to the greatest extent, and greatly reduces the cost. It reduces the adverse phenomena such as overheating, excessive pressure, uneven ball milling, and sequins during the ball milling of flake silver powder, and greatly improves the process, quality and yield of the production and preparation of flake silver powder for HJT silver paste.

附图说明Description of drawings

图1为本实用新型的结构示意图;Fig. 1 is the structural representation of the utility model;

图2为搅拌球磨时内部状态的示意图。Fig. 2 is a schematic diagram of the internal state during stirring ball milling.

各附图标记为:a—自动进料漏斗,b—搅拌系统,c—搅拌罐桶体,d—搅拌螺旋桨叶,e—压力监测仪,f—测温仪,g—出料开关阀,h—加料开关阀,i—气动隔膜泵,j—风冷式冰水机,k—出料阀门,l—减速机,m—加料孔,11—水箱式蒸发器,12—压缩机,13—散热器,14—散热风机,15—循环水泵。The reference signs are: a—automatic feeding funnel, b—stirring system, c—stirring tank barrel, d—stirring propeller blade, e—pressure monitor, f—thermometer, g—discharging switch valve, h—feeding switch valve, i—pneumatic diaphragm pump, j—air-cooled chiller, k—discharging valve, l—reducer, m—feeding hole, 11—water tank evaporator, 12—compressor, 13—radiator, 14—cooling fan, 15—circulating water pump.

具体实施方式Detailed ways

下面将结合本实用新型实施例中的附图,对本实用新型实施例中的技术方案进行清楚、完整地描述。The following will clearly and completely describe the technical solutions in the embodiments of the present invention with reference to the drawings in the embodiments of the present invention.

参照图1所示,本实用新型公开的一种HJT银浆用片状银粉的制备装置,包括搅拌罐c和搅拌系统b,所述的搅拌罐c包括搅拌罐桶体c和设置在搅拌罐桶体c外的夹套,所述的搅拌系统b包括倒置在搅拌罐桶体c顶部开口处的搅拌电机,所述的搅拌罐桶体c内设置有搅拌螺旋桨叶d,搅拌螺旋桨叶d通过减速机l连接搅拌电机,搅拌罐桶体c顶部通过加料开关阀h连接加料管,所述的加料管上设置有自动进料漏斗a,通过自动进料漏斗a向搅拌罐内供给球磨的原始银粉,搅拌罐桶体c上下侧壁分别通过进料管和出料管连接气动隔膜泵i,研磨的物料浆液通过气动隔膜泵i循环往复送入搅拌罐桶体c,夹套的上下侧壁分别通过出水管和进水管连接风冷式冰水机j,夹套层由风冷式冰水机j进行供给循环冷却水,搅拌罐c底部通过出料开关阀g连接出料阀门k。所述的搅拌罐c顶部设置加料盖,所述的减速机l和加料开关阀h设置在加料盖上,加料盖上还设置有加料孔m、压力监测仪e和测温仪f。Referring to Fig. 1, a preparation device for flake silver powder for HJT silver paste disclosed by the utility model includes a stirring tank c and a stirring system b. The jacket outside the barrel c, the stirring system b includes a stirring motor inverted at the top opening of the barrel c of the stirring tank, the stirring propeller blade d is arranged in the barrel c of the stirring tank, and the stirring propeller blade d passes through The reducer l is connected to the stirring motor, and the top of the barrel c of the stirring tank is connected to the feeding pipe through the feeding switch valve h. The feeding pipe is provided with an automatic feeding funnel a, through which the raw material of the ball mill is supplied to the stirring tank. Silver powder, the upper and lower side walls of the mixing tank body c are respectively connected to the pneumatic diaphragm pump i through the feed pipe and the discharge pipe, and the ground material slurry is sent to the mixing tank body c reciprocatingly through the pneumatic diaphragm pump i, and the upper and lower side walls of the jacket The air-cooled chiller j is connected to the water outlet pipe and the water inlet pipe respectively. The jacket layer is supplied with circulating cooling water by the air-cooled chiller j. The bottom of the stirring tank c is connected to the discharge valve k through the discharge switch valve g. The top of the stirring tank c is provided with a feeding cover, the speed reducer 1 and the feeding switch valve h are arranged on the feeding cover, and the feeding cover is also provided with a feeding hole m, a pressure monitor e and a thermometer f.

本实用新型具体的生产过程中制备HJT银浆用片状银粉时,在搅拌罐桶体c内以一定球料比加入一定量磨球,自动进料漏斗a加入一定量原始银粉,再通过加料孔m加入一定量球磨溶剂和分散剂溶液,再通过搅拌系统b以一定转速充分搅拌均匀,开启风冷式冰水机j对搅拌桶体夹套内供应一定温度的循环冷却水,再开启气动隔膜泵i将银粉浆液进行循环泵送,使得磨球和银粉颗粒之间产生较均匀碰撞和剪切运动,从而把银粉颗粒进行研磨。搅拌罐桶体c内的测温仪f、压力监测仪e等可以对制备过程的体系温度和压强变化情况实时监控,最大程度排除人工因素干扰带来的产品质量不稳定性,整个片状银粉的制备过程适应性强、效率高,适用于片状金属及金属混合粉的微米级研磨,使用简单,具有精确的大规模生产再现性,非常适用于批量的生产。When preparing flake silver powder for HJT silver paste in the specific production process of the utility model, add a certain amount of grinding balls with a certain ball-to-material ratio in the mixing tank barrel c, add a certain amount of original silver powder into the automatic feeding funnel a, and then pass the feeding Add a certain amount of ball milling solvent and dispersant solution to hole m, and then fully stir evenly at a certain speed through the stirring system b, turn on the air-cooled ice water machine j to supply circulating cooling water at a certain temperature in the jacket of the mixing barrel, and then turn on the pneumatic Diaphragm pump i circulates the silver powder slurry, so that there is a relatively uniform collision and shearing motion between the grinding ball and the silver powder particles, thereby grinding the silver powder particles. The thermometer f and pressure monitor e in the barrel c of the mixing tank can monitor the temperature and pressure changes of the system in real time during the preparation process, and eliminate the instability of product quality caused by the interference of artificial factors to the greatest extent. The entire flaky silver powder The preparation process has strong adaptability and high efficiency, and is suitable for micron-scale grinding of flake metal and metal mixed powder. It is easy to use, has accurate mass production reproducibility, and is very suitable for batch production.

本装置还包括PLC控制器,所述的PLC控制器分别连接自动进料漏斗a、搅拌系统b、压力监测仪e、测温仪f、出料开关阀g、加料开关阀h、气动隔膜泵i以及风冷式冰水机j;通过基于PLC控制器的自动化控制系统可控制原始银粉的加入快慢,减少因人工操作造成的银粉损失和粉尘,减少人工因素干扰带来的产品质量不稳定性。The device also includes a PLC controller, and the PLC controller is respectively connected to the automatic feeding funnel a, the stirring system b, the pressure monitor e, the temperature measuring instrument f, the discharge switch valve g, the feed switch valve h, and the pneumatic diaphragm pump i and air-cooled ice water machine j; through the automatic control system based on PLC controller, the speed of adding the original silver powder can be controlled, reducing the loss of silver powder and dust caused by manual operation, and reducing the instability of product quality caused by human interference .

相比传统工艺,通过PLC自动化控制系统控制物料循环泵送的速率快慢、冷却循环水的水温、搅拌系统的转速、系统的温度、压力监测以及开关阀门的开关,可以保证银粉在制备过程中的产品批次稳定性,减少人工因素干扰带来的产品质量不稳定性,减少了片状银粉球磨过程中过热出现压力过大、球磨不均匀、亮片等不良现象,大大改善了HJT银浆用片状银粉生产制备的工序、品质及收率。Compared with the traditional process, the PLC automatic control system controls the speed of material circulation pumping, the water temperature of cooling circulating water, the rotation speed of the stirring system, the temperature and pressure monitoring of the system, and the switch of the switch valve, which can ensure the silver powder in the preparation process. The stability of product batches reduces the instability of product quality caused by the interference of artificial factors, reduces the adverse phenomena such as excessive pressure, uneven ball milling, and sequins caused by overheating in the ball milling process of flake silver powder, and greatly improves the use of HJT silver paste. The process, quality and yield of silver powder production and preparation.

同时,与物料、磨球接触的搅拌罐桶体c内壁设置有不锈钢滤网。银粉浆液与磨球的固液分离过程中,球磨结束通过开关阀g开启,搅拌系统b一定转速条件下使得银粉浆料通过不锈钢滤网经出料阀门k进行出粉,同时可以通过加料孔m加入一定量的球磨溶剂对磨球进行动态淋洗,最大程度提高产品的收率,减少损耗。其中风冷式冰水机j由水箱式蒸发器11、压缩机12、散热器13和散热风机14组成,所述的水箱式蒸发器11通过循环水泵15连接出水管。At the same time, the inner wall of the c barrel of the mixing tank that is in contact with the material and the grinding ball is provided with a stainless steel filter screen. During the solid-liquid separation process of the silver powder slurry and the ball, the on-off valve g is opened at the end of the ball milling, and the stirring system b is set at a certain speed to make the silver powder slurry pass through the stainless steel filter screen and discharge the silver powder through the discharge valve k, and at the same time, it can pass through the feeding hole m Add a certain amount of ball milling solvent to dynamically wash the balls, so as to maximize the yield of the product and reduce the loss. Wherein the air-cooled chiller j consists of a water tank evaporator 11 , a compressor 12 , a radiator 13 and a cooling fan 14 , and the water tank evaporator 11 is connected to a water outlet pipe through a circulating water pump 15 .

本装置是一款高效自动化程度高的HJT银浆用片状银粉的制备装置,整个过程几乎无人工转运,极大地减少了人工因素干扰带来的产品质量不稳定性、人工成本,该机器适应性强、效率高,适用于片状金属及金属混合粉的微米级研磨。使用简单,根据每批量之间的生产结果,具有精确的大规模生产再现性。它非常适用于批量的生产。This device is a high-efficiency and highly automated preparation device for flake silver powder for HJT silver paste. There is almost no manual transfer in the whole process, which greatly reduces the instability of product quality and labor costs caused by the interference of artificial factors. The machine is suitable for Strong performance and high efficiency, suitable for micron-scale grinding of flake metal and metal mixed powder. Simple to use with precise mass production reproducibility based on production results between batches. It is very suitable for mass production.

以上所述仅为本实用新型的较佳实施例而已,并不用以限制本实用新型,凡在本实用新型的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本实用新型的保护范围之内。The above descriptions are only preferred embodiments of the present utility model, and are not intended to limit the present utility model. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present utility model shall be included in the Within the protection scope of the present utility model.

Claims (5)

1.一种HJT银浆用片状银粉的制备装置,其特征在于:包括搅拌罐和搅拌系统(b),所述的搅拌罐包括搅拌罐桶体(c)和设置在搅拌罐桶体(c)外的夹套,所述的搅拌系统(b)包括倒置在搅拌罐桶体(c)顶部开口处的搅拌电机,所述的搅拌罐桶体(c)内设置有搅拌螺旋桨叶(d),搅拌螺旋桨叶(d)通过减速机(l)连接搅拌电机,搅拌罐桶体(c)顶部通过加料开关阀(h)连接加料管,所述的加料管上设置有自动进料漏斗(a),搅拌罐桶体(c)上下侧壁分别通过进料管和出料管连接气动隔膜泵(i),夹套的上下侧壁分别通过出水管和进水管连接风冷式冰水机(j),搅拌罐底部通过出料开关阀(g)连接出料阀门(k)。1. A preparation device for flake silver powder for HJT silver paste, characterized in that it includes a stirring tank and a stirring system (b), and the stirring tank includes a stirring tank barrel (c) and is arranged on the stirring tank barrel ( c) outer jacket, the stirring system (b) includes a stirring motor inverted at the top opening of the stirring tank body (c), and the stirring tank body (c) is provided with stirring propeller blades (d ), the stirring propeller blade (d) is connected to the stirring motor through the reducer (l), the top of the mixing tank barrel (c) is connected to the feeding pipe through the feeding switch valve (h), and the feeding pipe is provided with an automatic feeding funnel ( a), the upper and lower side walls of the mixing tank body (c) are respectively connected to the pneumatic diaphragm pump (i) through the feed pipe and the discharge pipe, and the upper and lower side walls of the jacket are respectively connected to the air-cooled chiller through the water outlet pipe and the water inlet pipe (j), the bottom of the mixing tank is connected to the discharge valve (k) through the discharge switch valve (g). 2.根据权利要求1所述的一种HJT银浆用片状银粉的制备装置,其特征在于,所述的搅拌罐顶部设置加料盖,所述的减速机(l)和加料开关阀(h)设置在加料盖上,加料盖上还设置有加料孔(m)、压力监测仪(e)和测温仪(f)。2. The preparation device of flake silver powder for HJT silver paste according to claim 1, characterized in that, the top of the stirring tank is provided with a feeding cover, and the reducer (l) and the feeding switch valve (h ) is set on the feeding cover, which is also provided with a feeding hole (m), a pressure monitor (e) and a thermometer (f). 3.根据权利要求2所述的一种HJT银浆用片状银粉的制备装置,其特征在于,还包括PLC控制器,所述的PLC控制器分别连接自动进料漏斗(a)、搅拌系统(b)、压力监测仪(e)、测温仪(f)、出料开关阀(g)、加料开关阀(h)、气动隔膜泵(i)以及风冷式冰水机(j)。3. The preparation device of flake silver powder for HJT silver paste according to claim 2, characterized in that, it also includes a PLC controller, and the PLC controller is respectively connected to the automatic feeding funnel (a), the stirring system (b), pressure monitor (e), thermometer (f), discharge switch valve (g), feed switch valve (h), pneumatic diaphragm pump (i) and air-cooled chiller (j). 4.根据权利要求1或2或3所述的一种HJT银浆用片状银粉的制备装置,其特征在于,所述的风冷式冰水机(j)由水箱式蒸发器(11)、压缩机(12)、散热器(13)和散热风机(14)组成,所述的水箱式蒸发器(11)通过循环水泵(15)连接出水管。4. A preparation device for flake silver powder for HJT silver paste according to claim 1, 2 or 3, characterized in that, the air-cooled chiller (j) consists of a water tank evaporator (11 ), a compressor (12), a radiator (13) and a cooling fan (14), and the water tank evaporator (11) is connected to the water outlet pipe through a circulating water pump (15). 5.根据权利要求4所述的一种HJT银浆用片状银粉的制备装置,其特征在于,所述的搅拌罐桶体(c)内壁设置有不锈钢滤网。5 . The device for preparing flake silver powder for HJT silver paste according to claim 4 , characterized in that, the inner wall of the mixing tank (c) is provided with a stainless steel filter. 6 .
CN202320000878.XU 2023-01-03 2023-01-03 A kind of preparation device of flake silver powder for HJT silver paste Active CN218799119U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN121373434A (en) * 2025-12-24 2026-01-23 长春黄金研究院有限公司 Micro-nano flaky silver powder preparation line

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN121373434A (en) * 2025-12-24 2026-01-23 长春黄金研究院有限公司 Micro-nano flaky silver powder preparation line

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