CN218686536U

CN218686536U - Reaction device for adsorption experiment

Info

Publication number: CN218686536U
Application number: CN202222993904.1U
Authority: CN
Inventors: 邵俊; 刘建朋
Original assignee: Tangshan University
Current assignee: Tangshan University
Priority date: 2022-11-10
Filing date: 2022-11-10
Publication date: 2023-03-24
Anticipated expiration: 2032-11-10

Abstract

The utility model discloses an adsorption experiment reaction device, which comprises a reaction bottle, wherein a reaction separation structure is arranged in the reaction bottle; the reaction separation structure includes: the grinding head comprises a grinding plug, a threaded sleeve, a first threaded column, a middle rotating block, a second threaded column and a storage assembly; the utility model relates to a test utensil technical field, the reaction separation structure that this case adopted, the mill stopper with load the whole body of adopting of pipe and adopt the mode of components of a whole that can function independently connection, when clearing up loading pipe, through setting up in mill stopper upper end operation piece, be convenient for take out the clearance to loading pipe, simultaneously, when the reaction bottle in the face of different specifications, only need according to the bottleneck size of reaction bottle, change the mill stopper can, increase the application scope of loading pipe, avoid receiving the diameter restriction of loading pipe.

Description

Reaction device for adsorption experiment

Technical Field

The utility model relates to a test utensil technical field specifically is an adsorb experiment reaction unit.

Background

The prior patent discloses CN202123383946.5 a reaction unit for solid-liquid contact catalysis or adsorption experiment, the utility model discloses a reaction bottle and solid loading pipe, solid loading pipe lower part evenly distributed has the diameter to be 0.1-1 mm's aperture, solid loading pipe inserts and utilizes the outer mill mouth of pipe mouth and is connected with mill mouth in the reaction bottle bottleneck after the reaction bottle, solid catalyst or adsorbent in the solid loading pipe in the reaction process can realize the effectual contact of solid-liquid in the reaction process, can guarantee the quick separation of solid catalyst or adsorbent and reaction solution after the reaction, be applicable to detection and the sign in conventional solid catalytic reaction and absorption class reaction process, the loading pipe that this patent document adopted is the mounting means of direct embedding, after using to accomplish, because of the frictional force between loading pipe and the reaction bottle, lead to loading pipe to be difficult to take out in the reaction bottle, be not convenient for dismantling the clearance loading pipe, and receive the diameter restriction of loading pipe, lead to the applicable household utensils of loading pipe receive the restriction, the deep research to the problem, there is the present case to produce.

SUMMERY OF THE UTILITY MODEL

In order to achieve the above purpose, the utility model discloses a following technical scheme realizes: an adsorption experiment reaction device comprises a reaction bottle, wherein a reaction separation structure is arranged in the reaction bottle;

the reaction separation structure includes: the grinding head comprises a grinding plug, a threaded sleeve, a first threaded column, a transfer block, a second threaded column and a storage assembly;

the grinding plug is movably embedded at the upper end of the reaction bottle, the threaded sleeve is embedded at the lower end of the grinding plug, the first threaded column is embedded in the threaded sleeve, the transfer block is installed at the lower end of the first threaded column, the second threaded column is installed at the lower end of the transfer block, and the upper end of the storage component is movably sleeved at the upper end of the second threaded column.

Preferably, the storage assembly comprises: the connecting sleeve, the connecting shell and the loading pipe are arranged on the connecting shell;

the connecting sleeve is movably sleeved on the second threaded column, the upper end of the connecting shell is connected with the lower end of the connecting sleeve, and the loading pipe is installed at the lower end of the connecting shell.

Preferably, the upper end of the grinding plug is provided with an operating block.

Preferably, the lower wall surface of the reaction bottle is provided with anti-skid lines.

Preferably, the shape of the burr plug is conical.

Preferably, the operating block is spherical in shape.

Advantageous effects

The utility model provides an adsorb experiment reaction unit possesses following beneficial effect: the reaction separation structure that the present case adopted, the mill mouthful stopper with load the whole mode that adopts the components of a whole body coupling of pipe, when clearing up loading pipe, through setting up in mill mouthful stopper upper end operation piece, be convenient for take out the clearance loading pipe, simultaneously, when the reaction bottle in the face of different specifications, only need according to the bottleneck size of reaction bottle, to the mill mouthful stopper change can, increase the application scope who loads the pipe, avoid receiving the diameter restriction that loads the pipe.

Drawings

Fig. 1 is a schematic view of a structure of an adsorption experiment reaction device according to the present invention.

Fig. 2 is the utility model discloses an adsorption experiment reaction unit's mill mouthful stopper spatial structure sketch map.

Fig. 3 is a schematic diagram of a reaction separation structure of an adsorption experiment reaction device according to the present invention.

Fig. 4 is a schematic view of a three-dimensional structure of a storage assembly of an adsorption experiment reaction device.

In the figure: 1. reaction bottle, 2, ground stopper, 3, screw sleeve, 4, first screw post, 5, transfer piece, 6, second screw post, 7, connecting sleeve, 8, connecting shell, 9, loading tube, 10, operation piece, 11, anti-skidding line.

Detailed Description

Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-4, embodiments: an adsorption experiment reaction device comprises a reaction bottle 1, wherein a reaction separation structure is arranged in the reaction bottle 1;

the reaction separation structure includes: the grinding plug 2, the threaded sleeve 3, the first threaded column 4, the transfer block 5, the second threaded column 6 and the storage assembly;

the grinding plug 2 is movably embedded at the upper end of the reaction bottle 1, the threaded sleeve 3 is embedded at the lower end of the grinding plug 2, the first threaded column 4 is embedded in the threaded sleeve 3, the transit block 5 is installed at the lower end of the first threaded column 4, the second threaded column 6 is installed at the lower end of the transit block 5, and the upper end of the storage component is movably sleeved at the upper end of the second threaded column 6.

It should be noted that, when carrying out the adsorption experiment, the staff firstly introduces the reaction solution into the reaction bottle 1 through the glass rod, and then the staff changes the ground plug 2 according to the bore of the reaction bottle 1, put the adsorbent into the storage component, connect the storage component with the second threaded column 6, store the adsorbent in the storage component, and then embed the first threaded column 4 at the upper end of the transfer block 5 into the threaded sleeve 3, so as to realize the connection between the storage component and the ground plug 2, and most of all, the storage component is integrally embedded into the reaction bottle 1, and the storage component is in contact with the bore of the reaction bottle 1 through the ground plug 2, so that the storage component is located in the reaction bottle 1, and the reaction solution is adsorbed through the adsorbent in the storage component, after the reaction is completed, the ground plug 2 is taken down at the upper end of the reaction bottle 1, and the storage component is directly taken out, and the storage component can be cleaned or temporarily stored.

In a specific implementation, the storage assembly comprises: a connecting sleeve 7, a connecting housing 8 and a loading tube 9;

the connecting sleeve 7 is movably sleeved on the second threaded column 6, the upper end of the connecting shell 8 is connected with the lower end of the connecting sleeve 7, and the loading pipe 9 is installed at the lower end of the connecting shell 8.

It should be noted that, when installing the loading tube 9, the worker firstly puts the adsorbent into the loading tube 9, and then fits with the second threaded post 6 through the connecting sleeve 7 at the upper end of the connecting shell 8, connects the loading tube 9 with the transfer block 5, and finally fits with the threaded sleeve 3 through the first threaded post 4, connects the loading tube 9 with the grinding plug 2, and through the openings formed at the upper end of the loading tube 9, the adsorbent in the loading tube 9 can react with the reaction solution.

In the concrete implementation process, the upper end of the grinding plug 2 is provided with an operation block 10.

In the specific implementation process, the lower wall surface of the reaction bottle 1 is provided with anti-skid lines 11.

In a specific implementation, the shape of the burr plug 2 is conical.

In the specific implementation, the operation block 10 is spherical in shape.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. An adsorption experiment reaction device comprises a reaction bottle, and is characterized in that a reaction separation structure is arranged in the reaction bottle;

the reaction separation structure includes: the grinding head comprises a grinding plug, a threaded sleeve, a first threaded column, a middle rotating block, a second threaded column and a storage assembly;

2. The apparatus of claim 1, wherein the storage assembly comprises: the connecting sleeve, the connecting shell and the loading pipe are arranged on the connecting shell;

3. The reaction device for adsorption experiments according to claim 1, wherein the upper end of the grinding plug is provided with an operating block.

4. The reaction device for adsorption experiments according to claim 1, wherein the lower wall surface of the reaction flask is provided with anti-skid lines.

5. An adsorption experimental reaction device according to claim 1, wherein the shape of the grinding plug is conical.

6. An adsorption experiment reaction device according to claim 3, wherein the operation block is spherical.