CN217614728U - Neutralization treatment system is used in trifluoromethanesulfonic acid production - Google Patents
Neutralization treatment system is used in trifluoromethanesulfonic acid production Download PDFInfo
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- CN217614728U CN217614728U CN202221121109.7U CN202221121109U CN217614728U CN 217614728 U CN217614728 U CN 217614728U CN 202221121109 U CN202221121109 U CN 202221121109U CN 217614728 U CN217614728 U CN 217614728U
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- box
- plate
- fixedly connected
- trifluoromethanesulfonic acid
- acid production
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- 238000006386 neutralization reaction Methods 0.000 title claims abstract description 31
- ITMCEJHCFYSIIV-UHFFFAOYSA-N triflic acid Chemical compound OS(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 14
- 239000000463 material Substances 0.000 claims abstract description 4
- 238000003825 pressing Methods 0.000 claims description 18
- 238000004140 cleaning Methods 0.000 claims description 15
- 239000002699 waste material Substances 0.000 claims description 12
- 238000007790 scraping Methods 0.000 claims description 4
- 230000006978 adaptation Effects 0.000 claims description 3
- 230000000149 penetrating effect Effects 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 29
- 238000003756 stirring Methods 0.000 abstract description 18
- 239000000243 solution Substances 0.000 abstract description 12
- 239000012670 alkaline solution Substances 0.000 abstract description 11
- 238000006243 chemical reaction Methods 0.000 abstract description 11
- 239000003929 acidic solution Substances 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 10
- 238000009826 distribution Methods 0.000 abstract description 2
- 239000011550 stock solution Substances 0.000 description 15
- 238000007789 sealing Methods 0.000 description 13
- 239000010865 sewage Substances 0.000 description 7
- 239000007788 liquid Substances 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- WJKHJLXJJJATHN-UHFFFAOYSA-N triflic anhydride Chemical compound FC(F)(F)S(=O)(=O)OS(=O)(=O)C(F)(F)F WJKHJLXJJJATHN-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000006384 oligomerization reaction Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
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Abstract
The utility model belongs to the technical field of the trifluoromethanesulfonic acid production, a trifluoromethanesulfonic acid production is with neutralization processing system is disclosed, the power distribution box comprises a box body, the back intercommunication of box has the inlet pipe and arranges the material pipe, the interior roof of box rotates and is connected with the rotor plate, two electric putter of bottom fixedly connected with of rotor plate, the inner wall sliding connection of box has the clamp plate, the top of clamp plate respectively with two electric putter fixed connection. The utility model discloses a, after rotatory through the puddler, can be to the inside acidic solution of box and alkaline solution and stirring, and then let whole neutralization process go on more steadily, avoid the not stable enough condition of neutralization process to take place, after neutralization process ends, can also play the purpose to the solution clearance of reaction completion in addition, and then improve the practicality of device to it has the purpose that a small amount of stoste influences the next time reaction effect to reduce the box inner wall and adhere to.
Description
Technical Field
The utility model relates to a trifluoromethanesulfonic acid production technical field specifically is a trifluoromethanesulfonic acid production is with neutralization treatment system.
Background
The trifluoromethanesulfonic acid is a strong organic acid which is commonly used in laboratories, has strong corrosivity and hygroscopicity, can be used for preparing trifluoromethanesulfonic anhydride and various trifluoromethanesulfonic acid derivatives, can also be used as an effective catalyst for oligomerization and polymerization of alkene and ether, has small dosage, strong acidity and stable property, can replace traditional inorganic acids such as sulfuric acid and hydrochloric acid in many occasions, and plays a role in optimizing and improving the process.
In the prior art, most of trifluoromethanesulfonic acid neutralization treatment equipment enables an acidic solution and an alkaline solution to react freely, so that the whole neutralization process is not stable enough, and after the neutralization process is finished, the technical problem that the solution after the reaction is finished is not completely cleaned.
SUMMERY OF THE UTILITY MODEL
In view of the problems mentioned in the background art, the utility model aims to provide a neutralization treatment system for trifluoromethanesulfonic acid production.
In order to achieve the above purpose, the utility model adopts the following technical scheme.
The utility model provides a trifluoromethanesulfonic acid production is with neutralization treatment system, includes the box, the back intercommunication of box has the inlet pipe and arranges the material pipe, the interior roof of box rotates and is connected with the rotor plate, two electric putter of bottom fixedly connected with of rotor plate, the inner wall sliding connection of box has the clamp plate, the top of clamp plate respectively with two electric putter fixed connection, the top fixedly connected with motor of box, the output shaft fixedly connected with actuating lever of motor, the bottom of actuating lever runs through box, rotor plate and clamp plate in proper order and extends to the below of clamp plate, the front and the equal fixedly connected with puddler in the back of actuating lever, set up the logical groove with puddler looks adaptation on the clamp plate, the drain has all been seted up to the left and right sides of box, the inner wall sliding connection of box has the closing plate, the outside of closing plate respectively with the inner wall contact in two logical grooves, two springs of bottom fixedly connected with of closing plate.
As a further description of the above technical solution:
the inner wall of the box body is embedded with a support ring which is connected with the box body in a rotating mode, the inner side of the support ring is fixedly connected with two scraping plates, and the tops of the two scraping plates are inserted into the pressure plate and are in sliding connection with the pressure plate.
As a further description of the above technical solution:
the bottom fixedly connected with of clamp plate has two cleaning plates, two the relative one side of cleaning plate all contacts with the actuating lever.
As a further description of the above technical solution:
the equal fixedly connected with mounting box in the left and right sides of box, two the opening has all been seted up to one side of mounting box, two the top of mounting box all alternates there is rather than sliding connection's waste material box.
As a further description of the above technical solution:
the top fixed mounting of box has the controller, the output of controller is connected with electric putter and motor signal respectively.
Compared with the prior art, the utility model has the advantages of:
after the stirring rod is rotated, the stirring rod can stir the acidic solution and the alkaline solution inside the box body, so that the whole neutralization process is carried out more stably, the condition that the neutralization process is not stable enough is avoided, and after the neutralization process is finished, the purpose of cleaning the solution after the reaction is finished can be played, so that the practicability of the device is improved, and the purpose that a small amount of stock solution is attached to the inner wall of the box body to influence the next reaction effect is reduced.
Drawings
Fig. 1 is a schematic structural view of the present invention;
fig. 2 is a front sectional view of the present invention;
FIG. 3 is a diagram showing the positional relationship between the stirring rod and the through groove of the present invention;
fig. 4 is a position relationship diagram of the cleaning plate and the pressing plate of the present invention.
The reference numbers in the figures illustrate:
1. a box body; 2. a feed pipe; 3. a discharge pipe; 4. a rotating plate; 5. an electric push rod; 6. pressing a plate; 7. a motor; 8. a drive rod; 9. a stirring rod; 10. a through groove; 11. a sewage draining outlet; 12. a sealing plate; 13. a controller; 14. a spring; 15. a support ring; 16. a squeegee; 17. cleaning the plate; 18. mounting a box; 19. a port; 20. a waste material box.
Detailed Description
The technical solution in the embodiment of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiment of the present invention;
referring to fig. 1 to 4, in the present invention: the utility model provides a trifluoromethanesulfonic acid production is with neutralization treatment system, the power distribution box comprises a box body 1, the back intercommunication of box 1 has inlet pipe 2 and row's material pipe 3, the interior roof of box 1 rotates and is connected with rotor plate 4, two electric putter 5 of bottom fixedly connected with of rotor plate 4, the inner wall sliding connection of box 1 has clamp plate 6, the top of clamp plate 6 respectively with two electric putter 5 fixed connection, the top fixedly connected with motor 7 of box 1, the output shaft fixedly connected with actuating lever 8 of motor 7, box 1 is run through in proper order to the bottom of actuating lever 8, rotor plate 4 and clamp plate 6 and extend to the below of clamp plate 6, the front and the equal fixedly connected with puddler 9 in back of actuating lever 8, set up the logical groove 10 with puddler 9 looks adaptation on the clamp plate 6, drain 11 has all been seted up to the left and right sides of box 1, the inner wall sliding connection of box 1 has closing plate 12, the outside of closing plate 12 is respectively with the inner wall contact that leads to two logical grooves 10, two springs 14 of the bottom fixedly connected with of closing plate 12.
In the utility model, when in use, firstly, the acidic solution and the alkaline solution are poured into the box body 1 from the inlet pipe 2, the function of supporting the sealing plate 12 is played through the elasticity of the spring 14, the sealing plate 12 can play the function of sealing the sewage outlet 11, at the moment, the acidic solution and the alkaline solution can be filled in the box body 1, at the moment, the motor 7 is started, the motor 7 can drive the driving rod 8 to rotate, because the driving rod 8 is a square rod, the driving rod 8 can drive the rotating plate 4 and the pressing plate 6 to rotate when rotating, and the driving rod 8 can drive the stirring rod 9 to rotate in the rotating process, after the stirring rod 9 rotates, the acidic solution and the alkaline solution in the box body 1 can be stirred, and then the whole neutralization process can be carried out more stably, after the neutralization process is finished, the processed stock solution can be discharged by opening the discharge pipe 3, after the stock solution is discharged, the user starts the electric push rod 5, the electric push rod 5 can drive the pressing plate 6 to slide downwards along the inner wall of the box body 1, the pressing plate 6 can scrape off the stock solution attached to the inner part of the box body 1 in the sliding process, and further, the aim of cleaning the inner part of the box body 1 is achieved, the aim that the next reaction effect is influenced by a small amount of stock solution attached to the inner wall of the box body 1 is reduced, in the moving process of the pressing plate 6, the stirring rod 9 can pass through the through groove 10, in the process, a small amount of stock solution on the stirring rod 9 can be scraped together, the practicability of the device is further improved, then, the scraped stock solution can be positioned between the pressing plate 6 and the sealing plate 12, along with the continuous descending of the pressing plate 6, the pressing plate 6 can push the sealing plate 12 to descend until the top of the sealing plate 12 is lower than the sewage discharge outlet 11, at the scraped stock solution can be discharged through the sewage discharge outlet 11, and the aim of cleaning the inner part of the box body 1 is achieved, the device passes through the puddler 9 rotatory back, can be to the inside acidic solution of box 1 and alkaline solution and stirring, and then let whole neutralization process go on more steadily, avoids the not stable condition of neutralization process to take place inadequately, and after neutralization process ends, can also play the purpose to the solution clearance that the reaction was accomplished, and then improve the practicality of device to it has the purpose that a small amount of stoste influences the next reaction effect to reduce box 1 inner wall and adhere to.
Please refer to fig. 2-4, wherein: the inner wall of the box body 1 is embedded with a support ring 15 which is connected with the box body in a rotating way, the inner side of the support ring 15 is fixedly connected with two scrapers 16, and the tops of the two scrapers 16 are inserted on the pressure plate 6 and are in sliding connection with the pressure plate.
The utility model discloses in, can play the effect that supports scraper blade 16 through the setting of support ring 15 to when motor 7 starts, motor 7 can drive clamp plate 6 rotatory, and clamp plate 6 contacts with scraper blade 16 again, and then drives scraper blade 16 and slides along the inner wall of box 1, and scraper blade 16 can strike off the inside adnexed stoste of box 1 at gliding in-process, and it leads to the extravagant condition of stoste to take place to reduce the stoste to adhere to at 1 inner wall of box, and then improves the practicality of device.
Please refer to fig. 2-4, wherein: two cleaning plates 17 are fixedly connected to the bottom of the pressure plate 6, and opposite sides of the two cleaning plates 17 are both in contact with the driving rod 8.
The utility model discloses in, extrude the back with the waste liquid through drain 11, starting motor 7 drives clamp plate 6 rotatory back, and clamp plate 6 can drive cleaning plate 17 rotatory along box 1's inner bottom wall, and cleaning plate 17 can clean box 1's inner bottom wall at rotatory in-process, and then guarantees the clean effect to box 1.
Please refer to fig. 1 and 2, wherein: the equal fixedly connected with mounting box 18 of the left and right sides of box 1, opening 19 has all been seted up to one side of two mounting boxes 18, and the top of two mounting boxes 18 all alternates there is rather than sliding connection's waste material box 20.
The utility model discloses in, the mounting box 18 through the equal fixed connection in 1 left and right sides of box can be used for collecting the waste liquid, and the waste liquid can flow into the mounting box 18 through opening 19 after passing through drain 11 and discharging, and the waste liquid can fall into waste material box 20 after that, and the user can clear up the waste material through taking waste material box 20 out, and then the use of improving device avoids the waste liquid to cause the pollution to operational environment.
Please refer to fig. 1, in which: the top of the box body 1 is fixedly provided with a controller 13, and the output end of the controller 13 is respectively in signal connection with the electric push rod 5 and the motor 7.
The utility model discloses in, controller 13 through 1 top fixed mounting of box can the person of facilitating the use control electric putter 5 and motor 7, and then improve device's practicality.
The working principle is as follows: when the device is used, firstly, acidic solution and alkaline solution are poured into the box body 1 from the feeding pipe 2, the effect of supporting the sealing plate 12 is achieved through the elastic force of the spring 14, the sealing plate 12 can achieve the effect of sealing the sewage discharge outlet 11, at the moment, the acidic solution and the alkaline solution can be filled in the box body 1, the motor 7 is started, the motor 7 can drive the driving rod 8 to rotate, the driving rod 8 can drive the rotating plate 4 and the pressing plate 6 to rotate due to the fact that the driving rod 8 is a square rod, the driving rod 8 can drive the stirring rod 9 to rotate in the rotating process, the stirring rod 9 can stir the acidic solution and the alkaline solution in the box body 1 after rotating, the whole neutralization process is conducted more stably, the processed stock solution can be discharged by opening the discharge pipe 3 until the neutralization process is finished, after the stock solution is discharged, a user starts the electric push rod 5, the electric push rod 5 can drive the pressing plate 6 to slide downwards along the inner wall of the box body 1, the pressing plate 6 can scrape off the stock solution attached to the inner part of the box body 1 in the sliding process, so that the aim of cleaning the inner part of the box body 1 is fulfilled, the aim of influencing the next reaction effect by a small amount of stock solution attached to the inner wall of the box body 1 is reduced, in the moving process of the pressing plate 6, the stirring rod 9 can penetrate through the through groove 10, in the process, a small amount of stock solution on the stirring rod 9 can be scraped off together, so that the practicability of the device is improved, then the scraped stock solution can be positioned between the pressing plate 6 and the sealing plate 12, along with the continuous descending of the pressing plate 6, the pressing plate 6 can push the sealing plate 12 to descend until the top of the sealing plate 12 is lower than the sewage discharge outlet 11, at the moment, the scraped stock solution can be discharged through the sewage outlet 11, the aim of cleaning the inner part of the box body 1 is fulfilled, and after the device rotates through the stirring rod 9, can be to the inside acid solution and alkaline solution and the stirring of box 1, and then let whole neutralization process go on more steadily, avoid the not stable condition of neutralization process to take place inadequately, after neutralization process ends, can also play the purpose to the solution clearance that the reaction was accomplished, and then improve the practicality of device to it has the purpose that a small amount of stoste influences the reaction effect next time to reduce box 1 inner wall and adhere to.
The above is only a preferred embodiment of the present invention; the scope of the present invention is not limited thereto. Any person skilled in the art should also be able to cover the technical scope of the present invention by replacing or changing the technical solution and the improvement concept of the present invention with equivalents and modifications within the technical scope of the present invention.
Claims (5)
1. A neutralization treatment system for trifluoromethanesulfonic acid production, includes box (1), its characterized in that: the back intercommunication of box (1) has inlet pipe (2) and row material pipe (3), the interior roof of box (1) rotates and is connected with rotor plate (4), two electric putter (5) of the bottom fixedly connected with of rotor plate (4), the inner wall sliding connection of box (1) has clamp plate (6), the top of clamp plate (6) respectively with two electric putter (5) fixed connection, the top fixedly connected with motor (7) of box (1), the output shaft fixedly connected with actuating lever (8) of motor (7), the bottom of actuating lever (8) runs through box (1), rotor plate (4) and clamp plate (6) in proper order and extends to the below of clamp plate (6), the front and the equal fixedly connected with puddler in the back (9) of actuating lever (8), set up logical groove (10) with puddler (9) looks adaptation on clamp plate (6), drain (11) have all been seted up to the left and right sides of box (1), the inner wall sliding connection of box (1) has drain (12), the outside of closing plate (12) respectively with the inner wall of two closing plate (10) fixed connection have two springs (14).
2. The neutralization treatment system for trifluoromethanesulfonic acid production according to claim 1, characterized in that: the inner wall of the box body (1) is embedded with a support ring (15) which is connected with the support ring in a rotating mode, the inner side of the support ring (15) is fixedly connected with two scraping plates (16), and the tops of the two scraping plates (16) are inserted into the pressing plate (6) in a penetrating mode and are connected with the pressing plate in a sliding mode.
3. The neutralization treatment system for trifluoromethanesulfonic acid production according to claim 1, characterized in that: the bottom fixedly connected with two cleaning plates (17) of clamp plate (6), two the relative one side of cleaning plate (17) all contacts with actuating lever (8).
4. The neutralization treatment system for trifluoromethanesulfonic acid production according to claim 1, characterized in that: the box is characterized in that mounting boxes (18) are fixedly connected to the left side and the right side of the box body (1), through openings (19) are formed in one sides of the two mounting boxes (18), and waste material boxes (20) which are connected with the mounting boxes in a sliding mode are inserted into the tops of the two mounting boxes (18).
5. The neutralization treatment system for trifluoromethanesulfonic acid production according to claim 1, characterized in that: the top fixed mounting of box (1) has controller (13), the output of controller (13) respectively with electric putter (5) and motor (7) signal connection.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221121109.7U CN217614728U (en) | 2022-05-11 | 2022-05-11 | Neutralization treatment system is used in trifluoromethanesulfonic acid production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221121109.7U CN217614728U (en) | 2022-05-11 | 2022-05-11 | Neutralization treatment system is used in trifluoromethanesulfonic acid production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN217614728U true CN217614728U (en) | 2022-10-21 |
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ID=83652191
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202221121109.7U Active CN217614728U (en) | 2022-05-11 | 2022-05-11 | Neutralization treatment system is used in trifluoromethanesulfonic acid production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN217614728U (en) |
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2022
- 2022-05-11 CN CN202221121109.7U patent/CN217614728U/en active Active
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