CN216654539U - A new type of salt-forming reaction tank - Google Patents

A new type of salt-forming reaction tank Download PDF

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CN216654539U
CN216654539U CN202122973225.3U CN202122973225U CN216654539U CN 216654539 U CN216654539 U CN 216654539U CN 202122973225 U CN202122973225 U CN 202122973225U CN 216654539 U CN216654539 U CN 216654539U
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tank
inner tank
salt
mounting plate
support frame
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钱晨
倪峰
吴圣曦
王艳明
常艳玲
李辉
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Shanghai Shyndec Pharmaceutical Co Ltd
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Shanghai Shyndec Pharmaceutical Co Ltd
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Abstract

The utility model discloses a novel salifying reaction tank which comprises an outer tank, wherein an inner tank is arranged in the outer tank, an electric heating tube is arranged between the outer tank and the inner tank, a support frame is arranged in the middle of the upper portion of the inner tank, a motor is arranged above the support frame, a motor rotating shaft penetrates through the support frame and is fixedly connected with a coupler, the other end of the coupler is fixedly connected with a stirring rod, the stirring rod penetrates through the inner tank and extends to the bottom of the inner tank to be fixedly connected with a mounting plate, a plurality of stirring blades which are arranged in a matrix mode are arranged on the stirring rod above the mounting plate, scraping rods are arranged on two sides of the mounting plate, a material distributing structure is arranged below the mounting plate, and a temperature sensor is arranged at the upper end in the inner tank. This kind of retort simple structure, convenient operation, stirring effect is good, has avoided the phenomenon of salt caking to take place, the effectual efficiency that improves salt and produce.

Description

一种新型成盐反应罐A new type of salt-forming reaction tank

技术领域technical field

本实用新型涉及盐加工技术领域,具体为一种新型成盐反应罐。The utility model relates to the technical field of salt processing, in particular to a novel salt-forming reaction tank.

背景技术Background technique

中和反应、酯化反应和水洗反应是精细化工反应过程中的重要环节,化工工艺中常常需要用到中和反应的步骤,而中和反应往往生成固体和液体,因此对于中和反应的装置,应当考虑到对反应生成物的处理,同时也要注意尽量使得反应完全。反应成盐装置,酸和碱反应过程中会产生大量气体,因为大量气体的产生,所需的反应装置体积必须足够大,所以对搅拌桨的要求比较高,以达到充分搅拌的目的,由于反应装置是底部下凹的弧形,且底部造成搅拌桨的桨叶无法设计成贴近反应装置底部,会造成搅拌桨凌空于反应溶液之上,不能保证反应完全。为此,我们提出了一种新型成盐反应罐。Neutralization reaction, esterification reaction and water washing reaction are important links in the reaction process of fine chemical industry. The steps of neutralization reaction are often used in chemical process, and the neutralization reaction often generates solid and liquid. , the treatment of the reaction product should be considered, and attention should be paid to make the reaction as complete as possible. In the reaction salt-forming device, a large amount of gas will be generated during the reaction of acid and alkali. Because of the production of a large amount of gas, the required volume of the reaction device must be large enough, so the requirements for the stirring paddle are relatively high to achieve the purpose of full stirring. The device is a concave arc at the bottom, and the blades of the stirring paddle at the bottom cannot be designed to be close to the bottom of the reaction device, which will cause the stirring paddle to float above the reaction solution, which cannot guarantee the complete reaction. To this end, we propose a new type of salt-forming reactor.

实用新型内容Utility model content

本实用新型的目的在于提供一种新型成盐反应罐,以解决上述背景技术中提出的问题。The purpose of this utility model is to provide a new type of salt-forming reaction tank to solve the problems raised in the above background technology.

为实现上述目的,本实用新型提供如下技术方案:一种新型成盐反应罐,包括外罐,所述外罐内设有内罐,所述外罐与内罐同轴设置,所述外罐和内罐之间设有电热管,所述内罐上方中部设有支撑架,所述支撑架上方设有电机,所述电机旋转轴贯穿支撑架与联轴器固定连接,所述联轴器另一端与搅拌杆固定连接,所述搅拌杆贯穿内罐并延伸至内罐底部与安装板固定连接,所述搅拌杆位于安装板上方设有多个矩阵排布的搅拌叶,所述安装板两侧均设有刮杆,所述安装板下方设有分料结构,所述分料结构包括刮板,所述刮板设有两个,两个所述刮板之间垂直设置,所述刮板上开设有有个通孔,所述内罐内上端设有温度传感器。In order to achieve the above purpose, the present utility model provides the following technical solutions: a novel salt-forming reaction tank, comprising an outer tank, the outer tank is provided with an inner tank, the outer tank and the inner tank are arranged coaxially, and the outer tank An electric heating pipe is arranged between the inner tank and the inner tank, a support frame is arranged in the upper and middle part of the inner tank, a motor is arranged above the support frame, and the rotating shaft of the motor runs through the support frame and is fixedly connected with a coupling, and the coupling The other end is fixedly connected with the stirring rod. The stirring rod penetrates the inner tank and extends to the bottom of the inner tank and is fixedly connected with the mounting plate. The stirring rod is located above the mounting plate and is provided with a plurality of stirring blades arranged in a matrix. Scraper bars are arranged on both sides, a material distribution structure is arranged under the mounting plate, and the material distribution structure includes a scraper, and two scrapers are arranged vertically between the two scrapers. A through hole is opened on the scraper, and a temperature sensor is arranged on the upper end of the inner tank.

优选的,所述内罐上方一侧设有出气管,所述出气管上设有过滤盒,所述过滤盒内设有活性炭过滤层。Preferably, an air outlet pipe is arranged on the upper side of the inner tank, a filter box is arranged on the air outlet pipe, and an activated carbon filter layer is arranged in the filter box.

优选的,所述内罐远离出气管一侧上端设有进液管,所述进液管上设有第一阀门。Preferably, the upper end of the inner tank away from the air outlet pipe is provided with a liquid inlet pipe, and the liquid inlet pipe is provided with a first valve.

优选的,所述外罐上端设有控制面板,所述控制面板上端设有显示屏,所述显示屏下方设有控制按钮。Preferably, the upper end of the outer tank is provided with a control panel, the upper end of the control panel is provided with a display screen, and a control button is provided below the display screen.

优选的,所述内罐下方中部设有出料管,所述出料管下端延伸至外罐下方,所述出料管下端设有第二阀门。Preferably, a discharge pipe is provided in the lower middle part of the inner tank, the lower end of the discharge pipe extends to the bottom of the outer tank, and the lower end of the discharge pipe is provided with a second valve.

与现有技术相比,本实用新型的有益效果是:该种新型成盐反应罐,电热管发出的热量对内罐进行供热,从而滑块内罐内部的酸和碱中和效率,使搅拌叶对内罐内部原料进行搅拌,搅拌杆在进行转动的同时,通过安装板的带动,使刮杆特随之转动,从而使刮杆将内罐内壁附着的固定刮下,刮板可对沉淀在内罐底部的盐颗粒进行搅拌,通孔的设置,使沉淀的盐颗粒可以自用的通过,避免了盐颗粒结块的现象发生。该种反应罐结构简单,操作方便,搅拌效果好,避免了盐结块的现象发生,有效的提高了盐生成的效率。Compared with the prior art, the beneficial effect of the present utility model is that in this new type of salt-forming reaction tank, the heat emitted by the electric heating tube supplies heat to the inner tank, so that the acid and alkali inside the inner tank of the slider are neutralized efficiently, and the inner tank is neutralized. The stirring blade stirs the raw materials inside the inner tank. When the stirring rod rotates, it is driven by the mounting plate to make the scraper rod rotate along with it, so that the scraper rod scrapes off the fixed adhered to the inner wall of the inner tank, and the scraper can remove The salt particles precipitated at the bottom of the inner tank are stirred, and the arrangement of the through holes allows the precipitated salt particles to pass through for their own use, avoiding the phenomenon of agglomeration of the salt particles. The reaction tank has simple structure, convenient operation and good stirring effect, avoids the phenomenon of salt agglomeration, and effectively improves the efficiency of salt generation.

附图说明Description of drawings

图1为本实用新型的结构示意图;Fig. 1 is the structural representation of the utility model;

图2为本实用新型的剖视图;Fig. 2 is the sectional view of the utility model;

图3为本实用新型的分料结构结构示意图;Fig. 3 is the structural schematic diagram of the material distribution structure of the present invention;

图中:1外罐、2内罐、3电热管、4支撑架、5电机、6搅拌杆、7搅拌叶、8安装板、9刮杆、10分料结构、101刮板、102通孔、11温度传感器、12联轴器、13出气管、14过滤盒、15活性炭过滤层、16进液管、17第一阀门、18控制面板、19显示屏、20控制按钮、21出料管、22第二阀门。In the picture: 1 outer tank, 2 inner tank, 3 electric heating tube, 4 support frame, 5 motor, 6 stirring rod, 7 stirring blade, 8 mounting plate, 9 scraper rod, 10 material distribution structure, 101 scraper, 102 through hole , 11 temperature sensor, 12 coupling, 13 outlet pipe, 14 filter box, 15 activated carbon filter layer, 16 liquid inlet pipe, 17 first valve, 18 control panel, 19 display screen, 20 control button, 21 discharge pipe, 22 second valve.

具体实施方式Detailed ways

下面将结合本实用新型实施例中的附图,对本实用新型实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本实用新型一部分实施例,而不是全部的实施例。基于本实用新型中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本实用新型保护的范围。The technical solutions in the embodiments of the present utility model will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model. Obviously, the described embodiments are only a part of the embodiments of the present utility model, rather than all the implementations. example. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative work fall within the protection scope of the present invention.

请参阅图1-3,本实用新型提供一种技术方案:一种新型成盐反应罐,包括外罐1,其特征在于:所述外罐1内设有内罐2,所述外罐1与内罐2同轴设置,所述外罐1和内罐2之间设有电热管3,电热管3在进行工作时,电热管3发出的热量对内罐2进行供热,从而滑块内罐2内部的酸和碱中和效率,所述内罐2上方中部设有支撑架4,所述支撑架4上方设有电机5,所述电机5旋转轴贯穿支撑架4与联轴器12固定连接,所述联轴器12另一端与搅拌杆6固定连接,所述搅拌杆6贯穿内罐2并延伸至内罐2底部与安装板8固定连接,所述搅拌杆6位于安装板8上方设有多个矩阵排布的搅拌叶7,所述安装板8两侧均设有刮杆9,电机5在进行工作时,电机5通过联轴器12带动搅拌杆6以及搅拌叶7进行转动,从而使搅拌叶7对内罐2内部原料进行搅拌,搅拌杆6在进行转动的同时,通过安装板8的带动,使刮杆9特随之转动,从而使刮杆9将内罐2内壁附着的固定刮下,联轴器12的设置,提高了搅拌杆6的转动稳定性,所述安装板8下方设有分料结构10,所述分料结构10包括刮板101,所述刮板101设有两个,两个所述刮板101之间垂直设置,所述刮板101上开设有有个通孔102,刮板101可对沉淀在内罐2底部的盐颗粒进行搅拌,通孔102的设置,使沉淀的盐颗粒可以自用的通过,避免了盐颗粒结块的现象发生,所述内罐2内上端设有温度传感器11,温度传感器11可对内罐2内部温度进行监测。Please refer to FIGS. 1-3, the present utility model provides a technical solution: a novel salt-forming reaction tank, comprising an outer tank 1, characterized in that: the outer tank 1 is provided with an inner tank 2, and the outer tank 1 Coaxially arranged with the inner tank 2, an electric heating pipe 3 is arranged between the outer tank 1 and the inner tank 2. When the electric heating pipe 3 is working, the heat emitted by the electric heating pipe 3 supplies heat to the inner tank 2, so that the slider The acid and alkali neutralization efficiency inside the inner tank 2, the upper middle of the inner tank 2 is provided with a support frame 4, the upper part of the support frame 4 is provided with a motor 5, and the rotating shaft of the motor 5 runs through the support frame 4 and the coupling 12 is fixedly connected, the other end of the coupling 12 is fixedly connected with the stirring rod 6, the stirring rod 6 penetrates the inner tank 2 and extends to the bottom of the inner tank 2 and is fixedly connected with the mounting plate 8, and the stirring rod 6 is located on the mounting plate. 8 is provided with a plurality of stirring blades 7 arranged in a matrix, and both sides of the mounting plate 8 are provided with scrapers 9. When the motor 5 is working, the motor 5 drives the stirring rod 6 and the stirring blade 7 through the coupling 12. It rotates, so that the stirring blade 7 stirs the raw materials in the inner tank 2. When the stirring rod 6 rotates, it is driven by the mounting plate 8 to make the scraper rod 9 rotate along with it, so that the scraper rod 9 rotates the inner tank. 2. The fixed scraping attached to the inner wall, the setting of the coupling 12 improves the rotational stability of the stirring rod 6, and the material distribution structure 10 is provided under the mounting plate 8, and the material distribution structure 10 includes a scraper 101, so The scraper 101 is provided with two, and the two scrapers 101 are arranged vertically. The scraper 101 is provided with a through hole 102. Stirring, the setting of the through hole 102 allows the precipitated salt particles to pass through for their own use, and avoids the phenomenon of salt particles agglomerating. temperature is monitored.

进一步的说,所述内罐2上方一侧设有出气管13,所述出气管13上设有过滤盒14,所述过滤盒14内设有活性炭过滤层15,通过出气管可将中和反应中产生的气体排出,并通过活性炭过滤层15对气体进行过滤,避免排出的气体对大气造成污染。Further, an air outlet pipe 13 is arranged on the upper side of the inner tank 2, a filter box 14 is arranged on the air outlet pipe 13, and an activated carbon filter layer 15 is arranged in the filter box 14, and the neutralization can be neutralized through the air outlet pipe. The gas generated in the reaction is discharged, and the gas is filtered through the activated carbon filter layer 15 to prevent the discharged gas from polluting the atmosphere.

进一步的说,所述内罐2远离出气管13一侧上端设有进液管16,所述进液管16上设有第一阀门17,通过进液管16可向内罐2内部加入待反应的酸碱溶液。Further, the upper end of the inner tank 2 away from the air outlet pipe 13 is provided with a liquid inlet pipe 16, and the liquid inlet pipe 16 is provided with a first valve 17, through which the liquid inlet pipe 16 can be added to the inner tank 2. Reaction acid-base solution.

进一步的说,所述外罐1上端设有控制面板18,所述控制面板18上端设有显示屏19,所述显示屏19下方设有控制按钮20,显示屏19可对反应罐的工作状态进行显示,从而更便于操作人员了解到内罐2内部情况,通过控制按钮20可对反应罐的工作流程进行操控。Further, a control panel 18 is arranged on the upper end of the outer tank 1, a display screen 19 is arranged on the upper end of the control panel 18, and a control button 20 is arranged below the display screen 19. The display screen 19 can monitor the working state of the reaction tank. It is displayed, so that it is more convenient for the operator to know the internal situation of the inner tank 2 , and the working process of the reaction tank can be controlled through the control button 20 .

进一步的说,所述内罐2下方中部设有出料管21,所述出料管21下端延伸至外罐1下方,所述出料管21下端设有第二阀门22,通过出料管21可将反应完成的盐排出。Further, a discharge pipe 21 is provided in the lower middle part of the inner tank 2, the lower end of the discharge pipe 21 extends to the bottom of the outer tank 1, and a second valve 22 is provided at the lower end of the discharge pipe 21. 21 The salt after the reaction is completed can be discharged.

具体的,本实用新型中,首先,通过进液管向内罐2内部加入待反应的酸碱溶液,启动电热管3以及电机5,电热管3发出的热量对内罐2进行供热,从而滑块内罐2内部的酸和碱中和效率,电机5通过联轴器12带动搅拌杆6以及搅拌叶7进行转动,从而使搅拌叶7对内罐2内部原料进行搅拌,搅拌杆6在进行转动的同时,通过安装板8的带动,使刮杆9特随之转动,从而使刮杆9将内罐2内壁附着的固定刮下,同时,安装板8带动分料结构10转动,刮板101可对沉淀在内罐2底部的盐颗粒进行搅拌,通孔102的设置,使沉淀的盐颗粒可以自用的通过,避免了盐颗粒结块的现象发生。Specifically, in the present invention, firstly, the acid-base solution to be reacted is added into the inner tank 2 through the liquid inlet pipe, the electric heating pipe 3 and the motor 5 are started, and the heat emitted by the electric heating pipe 3 supplies heat to the inner tank 2, thereby The neutralization efficiency of acid and alkali inside the inner tank 2 of the slider, the motor 5 drives the stirring rod 6 and the stirring blade 7 to rotate through the coupling 12, so that the stirring blade 7 stirs the raw materials in the inner tank 2, and the stirring rod 6 is in At the same time of rotation, driven by the mounting plate 8, the scraper rod 9 is rotated along with it, so that the scraper rod 9 scrapes off the fixation attached to the inner wall of the inner tank 2. At the same time, the mounting plate 8 drives the material distribution structure 10 to rotate, scraping The plate 101 can agitate the salt particles deposited at the bottom of the inner tank 2. The arrangement of the through holes 102 enables the deposited salt particles to pass through for their own use, thereby avoiding the occurrence of agglomeration of the salt particles.

尽管已经示出和描述了本实用新型的实施例,对于本领域的普通技术人员而言,可以理解在不脱离本实用新型的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型,本实用新型的范围由所附权利要求及其等同物限定。Although the embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes and modifications can be made to these embodiments without departing from the principles and spirit of the present invention , alternatives and modifications, the scope of the present invention is defined by the appended claims and their equivalents.

Claims (5)

1.一种新型成盐反应罐,包括外罐(1),其特征在于:所述外罐(1)内设有内罐(2),所述外罐(1)与内罐(2)同轴设置,所述外罐(1)和内罐(2)之间设有电热管(3),所述内罐(2)上方中部设有支撑架(4),所述支撑架(4)上方设有电机(5),所述电机(5)旋转轴贯穿支撑架(4)与联轴器(12)固定连接,所述联轴器(12)另一端与搅拌杆(6)固定连接,所述搅拌杆(6)贯穿内罐(2)并延伸至内罐(2)底部与安装板(8)固定连接,所述搅拌杆(6)位于安装板(8)上方设有多个矩阵排布的搅拌叶(7),所述安装板(8)两侧均设有刮杆(9),所述安装板(8)下方设有分料结构(10),所述分料结构(10)包括刮板(101),所述刮板(101)设有两个,两个所述刮板(101)之间垂直设置,所述刮板(101)上开设有有个通孔(102),所述内罐(2)内上端设有温度传感器(11)。1. a novel salt-forming reaction tank, comprising an outer tank (1), characterized in that: the outer tank (1) is provided with an inner tank (2), the outer tank (1) and the inner tank (2) Coaxial arrangement, an electric heating pipe (3) is arranged between the outer tank (1) and the inner tank (2), a support frame (4) is arranged in the upper middle of the inner tank (2), and the support frame (4) ) above is provided with a motor (5), the rotating shaft of the motor (5) penetrates the support frame (4) and is fixedly connected with the coupling (12), and the other end of the coupling (12) is fixed with the stirring rod (6) connection, the stirring rod (6) penetrates through the inner tank (2) and extends to the bottom of the inner tank (2) and is fixedly connected to the mounting plate (8), the stirring rod (6) is located above the mounting plate (8) with multiple stirring blades (7) arranged in a matrix, scraper bars (9) are provided on both sides of the mounting plate (8), and a material distributing structure (10) is arranged under the mounting plate (8), the material distributing The structure (10) includes a scraper (101), two scrapers (101) are provided, the two scrapers (101) are vertically arranged, and a through hole is opened on the scraper (101). The hole (102) is provided with a temperature sensor (11) at the inner upper end of the inner tank (2). 2.根据权利要求1所述的一种新型成盐反应罐,其特征在于:所述内罐(2)上方一侧设有出气管(13),所述出气管(13)上设有过滤盒(14),所述过滤盒(14)内设有活性炭过滤层(15)。2. A new type of salt-forming reaction tank according to claim 1, characterized in that: an air outlet pipe (13) is provided on the upper side of the inner tank (2), and a filter is provided on the air outlet pipe (13). A box (14) is provided with an activated carbon filter layer (15) in the filter box (14). 3.根据权利要求1所述的一种新型成盐反应罐,其特征在于:所述内罐(2)远离出气管(13)一侧上端设有进液管(16),所述进液管(16)上设有第一阀门(17)。3. A new type of salt-forming reaction tank according to claim 1, characterized in that: the upper end of the inner tank (2) away from the gas outlet pipe (13) is provided with a liquid inlet pipe (16), the liquid inlet pipe A first valve (17) is provided on the pipe (16). 4.根据权利要求1所述的一种新型成盐反应罐,其特征在于:所述外罐(1)上端设有控制面板(18),所述控制面板(18)上端设有显示屏(19),所述显示屏(19)下方设有控制按钮(20)。4. A new type of salt-forming reaction tank according to claim 1, characterized in that: the upper end of the outer tank (1) is provided with a control panel (18), and the upper end of the control panel (18) is provided with a display screen ( 19), a control button (20) is provided below the display screen (19). 5.根据权利要求1所述的一种新型成盐反应罐,其特征在于:所述内罐(2)下方中部设有出料管(21),所述出料管(21)下端延伸至外罐(1)下方,所述出料管(21)下端设有第二阀门(22)。5. A new type of salt-forming reaction tank according to claim 1, characterized in that: a discharge pipe (21) is provided in the lower middle of the inner tank (2), and the lower end of the discharge pipe (21) extends to Below the outer tank (1), the lower end of the discharge pipe (21) is provided with a second valve (22).
CN202122973225.3U 2021-11-30 2021-11-30 A new type of salt-forming reaction tank Active CN216654539U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118420184A (en) * 2024-06-17 2024-08-02 无锡雪浪环境科技股份有限公司 A method and system for resource utilization of deacidified salty wastewater by neutralization

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118420184A (en) * 2024-06-17 2024-08-02 无锡雪浪环境科技股份有限公司 A method and system for resource utilization of deacidified salty wastewater by neutralization

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