CN216259196U - High-efficient reation kettle is used in ammonium chloride purification - Google Patents
High-efficient reation kettle is used in ammonium chloride purification Download PDFInfo
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- CN216259196U CN216259196U CN202122620316.9U CN202122620316U CN216259196U CN 216259196 U CN216259196 U CN 216259196U CN 202122620316 U CN202122620316 U CN 202122620316U CN 216259196 U CN216259196 U CN 216259196U
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- Prior art keywords
- reaction kettle
- ammonium chloride
- kettle body
- discharge pipe
- liquid discharge
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- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 title claims abstract description 31
- 235000019270 ammonium chloride Nutrition 0.000 title claims abstract description 31
- QDHHCQZDFGDHMP-UHFFFAOYSA-N monochloramine Chemical compound ClN QDHHCQZDFGDHMP-UHFFFAOYSA-N 0.000 title claims abstract description 31
- 238000000746 purification Methods 0.000 title claims description 7
- 238000006243 chemical reaction Methods 0.000 claims abstract description 58
- 238000003756 stirring Methods 0.000 claims abstract description 32
- 239000007788 liquid Substances 0.000 claims abstract description 24
- 238000003780 insertion Methods 0.000 claims abstract description 8
- 230000000875 corresponding Effects 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 238000005485 electric heating Methods 0.000 claims description 12
- 239000011248 coating agent Substances 0.000 claims description 7
- 238000000576 coating method Methods 0.000 claims description 7
- 230000003028 elevating Effects 0.000 claims description 4
- 238000009434 installation Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000004090 dissolution Methods 0.000 description 3
- -1 chemical industry Substances 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 229910000617 Mangalloy Inorganic materials 0.000 description 1
- 238000005804 alkylation reaction Methods 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- REDXJYDRNCIFBQ-UHFFFAOYSA-N aluminium(3+) Chemical class [Al+3] REDXJYDRNCIFBQ-UHFFFAOYSA-N 0.000 description 1
- 238000005039 chemical industry Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000005712 crystallization Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 238000006396 nitration reaction Methods 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000000630 rising Effects 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 238000005987 sulfurization reaction Methods 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
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Abstract
The utility model discloses a high-efficiency reaction kettle for purifying ammonium chloride, which comprises a working frame, wherein an insertion groove is formed in the upper end of the working frame, a reaction kettle body is inserted in the insertion groove, a kettle cover is fixed at the upper end of the reaction kettle body, a reaction tank is also arranged in the reaction kettle body through a lifting mechanism, a stirring mechanism is also arranged at the lower end of the kettle cover, the lower end of the stirring mechanism extends into the reaction tank, a discharge hole is formed in the bottom of the reaction tank, a filter screen is arranged at the discharge hole, a first liquid discharge pipe is fixed at the lower end of the discharge hole, a second liquid discharge pipe is arranged at the corresponding position of the lower end of the reaction kettle body, the lower end of the second liquid discharge pipe penetrates through the reaction kettle body, the first liquid discharge pipe is slidably sleeved in the second liquid discharge pipe, and a solenoid valve is further arranged on the first liquid discharge pipe. Can bring convenience to the technical field of ammonium chloride production and processing.
Description
Technical Field
The utility model relates to the technical field of ammonium chloride processing, in particular to a high-efficiency reaction kettle for ammonium chloride purification.
Background
The ammonium chloride is colorless crystal or white crystalline powder; no odor, good taste and cool; it has hygroscopicity. The product is soluble in water and slightly soluble in ethanol. The broad understanding of the reaction kettle is that the reaction kettle is a container for physical or chemical reaction, and the heating, evaporation, cooling and low-speed mixing functions required by the process are realized through the structural design and parameter configuration of the container. The reaction kettle is a pressure vessel widely used in petroleum, chemical industry, rubber, pesticide, dye, medicine and food for completing the technological processes of sulfuration, nitration, hydrogenation, alkylation, polymerization, condensation and the like, such as a reactor, a reaction kettle, a decomposition kettle, a polymerization kettle and the like; the material is carbon manganese steel, stainless steel, zirconium, nickel-based alloy and other composite materials. The existing ammonium chloride reaction kettle is easy to corrode after being used for a long time, cannot purify ammonium chloride efficiently, and is not beneficial to production and development of enterprises.
SUMMERY OF THE UTILITY MODEL
The utility model aims to provide an efficient reaction kettle for purifying ammonium chloride, which aims to solve the problems in the background technology.
In order to achieve the purpose, the utility model provides the following technical scheme:
an efficient reaction kettle for purifying ammonium chloride comprises a working frame, wherein the upper end of the working frame is provided with an insertion groove, a reaction kettle body is inserted in the insertion groove, a kettle cover is fixed at the upper end of the reaction kettle body, a reaction tank is also arranged in the reaction kettle body through a lifting mechanism, the lower end of the kettle cover is also provided with a stirring mechanism, the lower end of the stirring mechanism extends into the reaction tank, the bottom of the reaction tank is provided with a discharge hole, a filter screen is arranged at the discharge port, a first liquid discharge pipe is fixed at the lower end of the discharge port, a second liquid discharge pipe is arranged at the corresponding position at the lower end of the reaction kettle body, the lower end of the second liquid discharge pipe penetrates through the reaction kettle body, the first liquid discharge pipe is sleeved in the second liquid discharge pipe in a sliding manner, still be provided with the solenoid valve on the first drain pipe, still cartridge has feed hopper in kettle cover upper end, feed hopper's lower extreme stretches into in the retort.
Preferably, elevating system is including installing the multiunit lift slide rail at the inside lateral wall of reation kettle body, the lift lead screw is installed to the lift slide rail internal rotation, lift motor is installed to lift slide rail upper end, lift motor's output is connected with the axle head drive of lift lead screw, and the edgewise screw suit of retort is provided with waterproof coating outside the lift lead screw on the lift lead screw.
Preferably, a waterproof cover is arranged on the outer side of the lifting motor.
Preferably, the stirring mechanism includes that kettle cover lower extreme intermediate position rotates the stirring axis of rotation of installation, the multiunit stirring leaf is installed to stirring axis of rotation lower extreme, agitator motor is still installed to the upper end of kettle cover, agitator motor's output is connected with the axle head drive of stirring axis of rotation.
Preferably, the retort is multilayer structure, including the anticorrosive coating of inlayer, the electric heating layer in intermediate level and outer waterproof layer, the anticorrosive coating external fixation has the electric heating layer, the electric heating layer external fixation has the waterproof layer.
Preferably, the left side of reation kettle body still is provided with the water inlet, the right side of reation kettle body is provided with the delivery port, the delivery port is located the water inlet top.
Compared with the prior art, the utility model has the beneficial effects that: the speed of purification can be improved by arranging the stirring mechanism to be matched with the lifting mechanism; through setting up the anticorrosive coating, can prolong the life of device. The device has a simple structure, is convenient to operate, can purify ammonium chloride efficiently, and can bring convenience to the technical field of ammonium chloride production and processing.
Drawings
FIG. 1 is a schematic diagram of a cross-sectional front view of a high-efficiency reaction kettle for purifying ammonium chloride;
FIG. 2 is an enlarged schematic view of the point A of the high-efficiency reaction kettle for ammonium chloride purification.
In the figure: 1-a working frame, 2-a reaction kettle body, 3-a kettle cover, 4-a stirring mechanism, 41-a stirring motor, 42-a stirring rotating shaft, 43-a stirring blade, 5-a feeding funnel, 6-a lifting mechanism, 61-a lifting motor, 62-a lifting slide rail, 63-a lifting screw rod, 7-a reaction tank, 71-an anticorrosive layer, 72-an electric heating layer, 73-a waterproof layer, 8-a filter screen, 9-an electromagnetic valve, 10-a first liquid discharge pipe, 11-a second liquid discharge pipe, 12-a water inlet and 13-a water outlet.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-2, the present invention provides a technical solution: a high-efficiency reaction kettle for purifying ammonium chloride comprises a working frame 1, wherein an insertion groove is formed in the upper end of the working frame 1, a reaction kettle body 2 is inserted in the insertion groove, a kettle cover 3 is fixed at the upper end of the reaction kettle body 2, a reaction tank 7 is further arranged in the reaction kettle body 2 through a lifting mechanism 6, a stirring mechanism 4 is further arranged at the lower end of the kettle cover 3, the lower end of the stirring mechanism 4 extends into the reaction tank 7, a discharge port is formed in the bottom of the reaction tank 7, a filter screen 8 is mounted at the discharge port, a first liquid discharge pipe 10 is fixed at the lower end of the discharge port, a second liquid discharge pipe 11 is mounted at the corresponding position of the lower end of the reaction kettle body 2, the lower end of the second liquid discharge pipe 11 penetrates through the reaction kettle body 2, the first liquid discharge pipe 10 is slidably sleeved in the second liquid discharge pipe 11, and an electromagnetic valve 9 is further arranged on the first liquid discharge pipe 10, still the cartridge has charging hopper 5 in the 3 upper ends of kettle cover, charging hopper 5's lower extreme stretches into in the retort 7.
The electromagnetic valve 9 is arranged, so that the discharging can be controlled conveniently, and the filter screen 8 can filter.
Through setting up elevating system 6, be convenient for realize retort 7's lift, be convenient for remove retort 7 to the condensate in, the cooling crystallization of solution in retort 7 with higher speed.
And a waterproof cover is arranged on the outer side of the lifting motor 61.
Through setting up the buckler, can protect elevator motor 61 normal work.
Through setting up rabbling mechanism 4, can accelerate the dissolution of ammonium chloride to improve the purification efficiency of ammonium chloride, during the use, open agitator motor 41, make it drive stirring axis of rotation 42 and rotate, make stirring leaf 43 stir, accelerate the dissolution of ammonium chloride.
The reaction tank 7 is of a multilayer structure and comprises an inner anti-corrosion layer 71, an intermediate electric heating layer 72 and an outer waterproof layer 73, wherein the electric heating layer 72 is fixed outside the anti-corrosion layer 71, and the waterproof layer 73 is fixed outside the electric heating layer 72. Through setting up anticorrosive coating 71, can prolong the life of device, electric heating layer 72 can the rising temperature, improves the solubility of ammonium chloride.
The left side of reation kettle body 2 still is provided with water inlet 12, the right side of reation kettle body is provided with delivery port 13, delivery port 13 is located water inlet 12 top.
Through setting up highly inconsistent delivery port 13 and water inlet 12, can improve the condensation effect, during the use, from water inlet 12 input condensate, delivery port 13 run-on water pipe makes the condensate discharge by the drain pipe.
The working principle of the utility model is as follows: when the device is used, firstly, ammonium chloride is added into the reaction tank 7 through the feeding funnel 5, then, water is added, then, the reaction tank 7 is heated through the electric heating layer 72, meanwhile, the stirring motor 41 is turned on to drive the stirring rotating shaft 42 to rotate, the stirring blades 43 are stirred to accelerate the dissolution of the ammonium chloride, after the ammonium chloride is completely dissolved, condensate is input from the water inlet 12, then, the lifting motor 61 is turned on to drive the reaction tank 7 to move downwards to enter the condensate in the reaction kettle body 2, so that the ammonium chloride is crystallized and separated out, then, the electromagnetic valve 8 is turned on, filtering is performed through the filter screen 8, the electromagnetic valve 9 is turned off after the filtering is completed, the reaction tank 7 is reset, then, the water is heated to dissolve crystals, the steps are repeated, and after multiple operations, the obtained crystals are air-dried, so that high-purity ammonium chloride crystals can be obtained.
It will be evident to those skilled in the art that the utility model is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the utility model being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (6)
1. The utility model provides an ammonium chloride purification is with high-efficient reation kettle, includes work frame (1), its characterized in that: the upper end of the working frame (1) is provided with an insertion groove, a reaction kettle body (2) is inserted in the insertion groove, the upper end of the reaction kettle body (2) is fixed with a kettle cover (3), a reaction tank (7) is further installed in the reaction kettle body (2) through a lifting mechanism (6), the lower end of the kettle cover (3) is further provided with a stirring mechanism (4), the lower end of the stirring mechanism (4) extends into the reaction tank (7), the bottom of the reaction tank (7) is provided with a discharge port, a filter screen (8) is installed at the discharge port, a first liquid discharge pipe (10) is fixed at the lower end of the discharge port, a second liquid discharge pipe (11) is installed at the corresponding position of the lower end of the reaction kettle body (2), the lower end of the second liquid discharge pipe (11) penetrates through the reaction kettle body (2), and the first liquid discharge pipe (10) is slidably sleeved in the second liquid discharge pipe (11), still be provided with solenoid valve (9) on first drain pipe (10), still cartridge has feed hopper (5) on kettle cover (3), the lower extreme of feed hopper (5) stretches into in retort (7).
2. The high-efficiency reaction kettle for purifying ammonium chloride as claimed in claim 1, wherein: elevating system (6) are including installing multiunit lift slide rail (62) at the inside lateral wall of reation kettle body (2), lift lead screw (63) are installed to lift slide rail (62) internal rotation, elevator motor (61) are installed to lift slide rail (62) upper end, the output of elevator motor (61) is connected with the axle head drive of lift lead screw (63), and the edgewise screw suit of retort (7) is on lift lead screw (63).
3. The high-efficiency reaction kettle for purifying ammonium chloride as claimed in claim 2, wherein: and a waterproof cover is arranged on the outer side of the lifting motor (61).
4. The high-efficiency reaction kettle for purifying ammonium chloride as claimed in claim 1, wherein: rabbling mechanism (4) include that kettle cover (3) lower extreme intermediate position rotates stirring axis of rotation (42) of installation, multiunit stirring leaf (43) are installed to stirring axis of rotation (42) lower extreme, agitator motor (41) are still installed to the upper end of kettle cover (3), the output of agitator motor (41) is connected with the axle head drive of stirring axis of rotation (42).
5. The high-efficiency reaction kettle for purifying ammonium chloride as claimed in claim 1, wherein: retort (7) are multilayer structure, including anticorrosive coating (71) of inlayer, electric heating layer (72) and outer waterproof layer (73) in intermediate level, anticorrosive coating (71) external fixation has electric heating layer (72), electric heating layer (72) external fixation has waterproof layer (73).
6. The high-efficiency reaction kettle for purifying ammonium chloride as claimed in claim 1, wherein: the left side of reation kettle body (2) still is provided with water inlet (12), the right side of reation kettle body is provided with delivery port (13), delivery port (13) are located water inlet (12) top.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202122620316.9U CN216259196U (en) | 2021-10-29 | 2021-10-29 | High-efficient reation kettle is used in ammonium chloride purification |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202122620316.9U CN216259196U (en) | 2021-10-29 | 2021-10-29 | High-efficient reation kettle is used in ammonium chloride purification |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN216259196U true CN216259196U (en) | 2022-04-12 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202122620316.9U Active CN216259196U (en) | 2021-10-29 | 2021-10-29 | High-efficient reation kettle is used in ammonium chloride purification |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN216259196U (en) |
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2021
- 2021-10-29 CN CN202122620316.9U patent/CN216259196U/en active Active
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