CN215996686U - Reaction unit is used in synthesis of difluoro benzophenone - Google Patents
Reaction unit is used in synthesis of difluoro benzophenone Download PDFInfo
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- CN215996686U CN215996686U CN202122116247.8U CN202122116247U CN215996686U CN 215996686 U CN215996686 U CN 215996686U CN 202122116247 U CN202122116247 U CN 202122116247U CN 215996686 U CN215996686 U CN 215996686U
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- difluorobenzophenone
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 24
- BWQOPMJTQPWHOZ-UHFFFAOYSA-N (2,3-difluorophenyl)-phenylmethanone Chemical compound FC1=CC=CC(C(=O)C=2C=CC=CC=2)=C1F BWQOPMJTQPWHOZ-UHFFFAOYSA-N 0.000 title claims abstract description 23
- 230000015572 biosynthetic process Effects 0.000 title claims description 11
- 238000003786 synthesis reaction Methods 0.000 title claims description 11
- 238000003756 stirring Methods 0.000 claims abstract description 27
- 230000005540 biological transmission Effects 0.000 claims description 26
- 230000008878 coupling Effects 0.000 claims description 6
- 238000010168 coupling process Methods 0.000 claims description 6
- 238000005859 coupling reaction Methods 0.000 claims description 6
- 239000000463 material Substances 0.000 abstract description 7
- 239000002994 raw material Substances 0.000 abstract description 6
- 239000000126 substance Substances 0.000 abstract description 2
- -1 base and roof Chemical compound 0.000 abstract 1
- 230000002194 synthesizing effect Effects 0.000 description 4
- 244000309464 bull Species 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- 239000004696 Poly ether ether ketone Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007123 defense Effects 0.000 description 1
- 229920006351 engineering plastic Polymers 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229920002530 polyetherether ketone Polymers 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model relates to a chemical industry raw materials produces technical field, and discloses a synthetic reaction unit that uses of difluorobenzophenone, including base and roof, the upper surface both sides of base are the fixed bracing piece that is provided with all, the roof is fixed set up in two the top of bracing piece, the upper surface of base rotates and is provided with the rotor plate, the inside of rotor plate is rotated and is provided with a plurality of rotary disks, and is a plurality of the equal fixed jar body that is provided with of upper surface of rotary disk is a plurality of the upper surface of the jar body all is provided with the upper cover, and is a plurality of the inside of upper cover all rotates and is provided with the puddler, the lower fixed surface of roof is provided with interior ring gear, and is a plurality of the first gear has all been fixed the cover in the upper end of puddler, be provided with the transfer line between base and the roof, the upper surface of roof is provided with the motor. The utility model discloses can carry out quick and abundant stirring to raw and other materials, and can stir convenient to use to a plurality of reation kettle insidely through single drive arrangement.
Description
Technical Field
The utility model relates to a chemical industry raw materials production technical field especially relates to a synthetic reaction unit that uses of difluorobenzophenone.
Background
Difluorobenzophenone is a very important organic fluorine intermediate, is mainly used for synthesizing an important strategic national defense military material, namely novel aromatic thermoplastic engineering plastic polyether ether ketone, and needs to mix and stir a plurality of raw materials during alignment and synthetic processing.
Traditional synthetic reaction unit for difluorobenzophenone simple structure only stirs through single puddler, forms the vortex during stirring, and raw and other materials follow the puddler and rotate, and mixing efficiency is low, and every reation kettle all needs solitary drive arrangement drive moreover, extravagant energy very much.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the problem that the synthetic reaction unit of using of difluorobenzophenone among the prior art is difficult to carry out even stirring and every reation kettle all need solitary drive arrangement drive to raw and other materials, extravagant energy very much, and the synthetic reaction unit of using of difluorobenzophenone who provides.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
a reaction device for synthesizing difluorobenzophenone, which comprises a base and a top plate, wherein two sides of the upper surface of the base are both fixedly provided with a support rod, the top plate is fixedly arranged at the top ends of the two support rods, the upper surface of the base is rotatably provided with a rotating plate, a plurality of rotating disks are rotatably arranged in the rotating plate, tank bodies are fixedly arranged on the upper surfaces of the rotating disks, upper covers are arranged on the upper surfaces of the tank bodies, stirring rods are rotatably arranged in the upper covers, the lower surface of the top plate is fixedly provided with an inner gear ring, the upper ends of the stirring rods are fixedly sleeved with a first gear, a transmission rod is arranged between the base and the top plate, the upper surface of the top plate is provided with a motor, the upper surface of the base is provided with a cavity, a transmission mechanism is arranged in the cavity, and a connecting mechanism is arranged between the upper cover and the tank body.
Preferably, drive mechanism includes second gear and third gear, the second gear is fixed to be cup jointed in the lower extreme of transfer line, the inside of cavity is rotated and is provided with a plurality of bull sticks, and is a plurality of the third gear is all fixed to be cup jointed in the pole wall of the bull stick that corresponds, and is a plurality of the lower surface of rotary disk all passes through connecting rod fixedly connected with fourth gear, and is a plurality of second gear, third gear and fourth gear all match.
Preferably, the connecting mechanism comprises a plurality of connecting plates which are respectively fixedly arranged on two side walls of the corresponding tank body and the corresponding upper cover, and the two adjacent sides of the connecting plates are fastened and connected through bolt threads.
Preferably, coupling mechanism includes L template and set casing, and is a plurality of the L template is fixed respectively and sets up in the both sides wall of the jar body that corresponds, and is a plurality of the jack has all been seted up to the upper end of L template, and is a plurality of the set casing is fixed respectively and sets up in the both sides wall of the upper cover that corresponds, and is a plurality of the inside of set casing all slides and is provided with the slider, and is a plurality of the outside of slider is all fixed and is provided with the inserted bar, and is a plurality of the outside one end of inserted bar all extends to the outside of the set casing that corresponds and all pegs graft with the jack that corresponds, and is a plurality of equal fixedly connected with spring between the inboard of slider and the inner wall of set casing.
Preferably, the output end of the motor is fixedly connected with the upper end of the transmission rod.
Preferably, a feeding hopper is fixedly arranged on the upper surface of the upper cover.
Preferably, the motor is fixedly connected with the top plate through a support frame.
Compared with the prior art, the utility model provides a synthetic reaction unit that uses of difluorobenzophenone possesses following beneficial effect:
1. this synthetic reaction unit that uses of difluoro benzophenone drives the transfer line through the motor and rotates, drives the rotor plate promptly and rotates, drives a plurality of jar bodies promptly around the transfer line revolution, even the relative inner ring of tooth of a plurality of first gears rotates, even a plurality of first gears drive the puddler and rotate, can stir convenient to use inside a plurality of reation kettle through single drive arrangement promptly.
2. This synthetic reaction unit that uses of difluoro benzophenone drives second gear through the transfer line and rotates, and the second gear drives a plurality of third gear rotations, and a plurality of third gear drive a plurality of fourth gear rotations, even rotation and opposite with the direction of rotation of puddler when a plurality of jar body revolution, can carry out quick and abundant stirring to raw and other materials promptly.
The part that does not relate to in the device all is the same with prior art or can adopt prior art to realize, the utility model discloses can carry out quick and abundant stirring to raw and other materials, and can stir convenient to use to a plurality of reation kettle insidely through single drive arrangement.
Drawings
Fig. 1 is a schematic structural diagram of a reaction apparatus for synthesizing difluorobenzophenone, which is provided by the present invention;
fig. 2 is a schematic structural diagram of another embodiment of a reaction apparatus for synthesizing difluorobenzophenone, according to the present invention;
fig. 3 is an enlarged view of a portion a of fig. 2.
In the figure: the automatic stirring device comprises a base 1, a supporting rod 2, a top plate 3, a rotating plate 4, a rotating disk 5, a tank body 6, an upper cover 7, a stirring rod 8, an inner toothed ring 9, a first gear 10, a transmission rod 11, a motor 12, a second gear 13, a rotating rod 14, a third gear 15, a connecting rod 16, a fourth gear 17, a connecting plate 18, bolts 19, a 20L-shaped plate, a fixed shell 21, a sliding plate 22, an inserted rod 23 and a spring 24.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
In the description of the present invention, it is to be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplicity of description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore, should not be construed as limiting the present invention.
Example 1
Referring to fig. 1, a reaction device for synthesis of difluorobenzophenone, comprising a base 1 and a top plate 3, wherein two sides of the upper surface of the base 1 are fixedly provided with support rods 2, the top plate 3 is fixedly arranged at the top ends of the two support rods 2, the upper surface of the base 1 is rotatably provided with a rotating plate 4, the rotating plate 4 is rotatably provided with a plurality of rotating disks 5, the upper surfaces of the rotating disks 5 are fixedly provided with tank bodies 6, the upper surfaces of the tank bodies 6 are provided with upper covers 7, the inner parts of the upper covers 7 are rotatably provided with stirring rods 8, the lower surface of the top plate 3 is fixedly provided with an inner toothed ring 9, the upper ends of the stirring rods 8 are fixedly sleeved with first gears 10, the first gears 10 are engaged with the inner toothed ring 9, a transmission rod 11 is arranged between the base 1 and the top plate 3, the upper end of the transmission rod 11 is rotatably connected with the top plate 3, and the lower end of the transmission rod 11 is fixedly connected with the rotating plate 4, the upper surface of roof 3 is provided with motor 12, and the cavity has been seted up to the upper surface of base 1, and the inside of cavity is provided with drive mechanism, is provided with coupling mechanism between upper cover 7 and the jar body 6.
The transmission mechanism comprises a second gear 13 and a third gear 15, the second gear 13 is fixedly sleeved at the lower end of the transmission rod 11, a plurality of rotating rods 14 are arranged in the cavity in a rotating mode, the third gears 15 are fixedly sleeved on the rod walls of the corresponding rotating rods 14, the lower surfaces of the rotating disks 5 are fixedly connected with fourth gears 17 through connecting rods 16, and the second gears 13, the third gears 15 and the fourth gears 17 are matched.
The connecting mechanism comprises connecting plates 18, the connecting plates 18 are respectively and fixedly arranged on two side walls of the corresponding tank body 6 and the corresponding upper cover 7, and the adjacent connecting plates 18 on the two sides are in threaded fastening connection through bolts 19.
The output end of the motor 12 is fixedly connected with the upper end of the transmission rod 11 to provide rotating power for the transmission rod 11.
The fixed feeding hopper that is provided with of upper cover 7's upper surface conveniently feeds in raw material.
The motor 12 is fixedly connected with the top plate 3 through the support frame, so that the motor 12 is more stably connected with the top plate 3.
In the utility model, when in use, the worker switches on the power supply of the motor 12, the motor 12 drives the transmission rod 11 to rotate, namely, the rotation plate 4 is driven to rotate, the rotation plate 4 drives the plurality of the tank bodies 6 to revolve around the transmission rod 11, namely, the plurality of the first gears 10 rotate relative to the inner ring gear 9, because the inner ring gear 9 is fixedly arranged, the plurality of the first gears 10 rotate, the plurality of the first gears 10 drive the corresponding stirring rods 8 to rotate, namely, the interiors of the plurality of reaction kettles can be stirred by a single driving device, the use is convenient, meanwhile, the transmission rod 11 drives the second gear 13 to rotate, the second gear 13 drives the plurality of the third gears 15 to rotate, namely, the plurality of the fourth gears 17 rotate along with the revolution of the rotation plate 5, and the rotation directions of the plurality of the fourth gears 17 are opposite to the rotation direction of the first gears 10, namely, the plurality of the tank bodies 6 are driven to rotate, and the rotation directions of the stirring rods 8 are opposite to the corresponding directions, can carry out quick and abundant stirring to raw and other materials, twist off both sides bolt 19 after the stirring, can separate upper cover 7 and jar body 6, can take out the article of jar body 6.
Example 2
Referring to fig. 2-3, a reaction device for synthesis of difluorobenzophenone, comprising a base 1 and a top plate 3, wherein two sides of the upper surface of the base 1 are fixedly provided with support rods 2, the top plate 3 is fixedly arranged at the top ends of the two support rods 2, the upper surface of the base 1 is rotatably provided with a rotating plate 4, the rotating plate 4 is rotatably provided with a plurality of rotating disks 5, the upper surfaces of the rotating disks 5 are fixedly provided with tank bodies 6, the upper surfaces of the tank bodies 6 are provided with upper covers 7, the interiors of the upper covers 7 are rotatably provided with stirring rods 8, the lower surface of the top plate 3 is fixedly provided with an inner toothed ring 9, the upper ends of the stirring rods 8 are fixedly sleeved with first gears 10, the first gears 10 are engaged with the inner toothed ring 9, a transmission rod 11 is arranged between the base 1 and the top plate 3, the upper end of the transmission rod 11 is rotatably connected with the top plate 3, and the lower end of the transmission rod 11 is fixedly connected with the rotating plate 4, the upper surface of roof 3 is provided with motor 12, and the cavity has been seted up to the upper surface of base 1, and the inside of cavity is provided with drive mechanism, is provided with coupling mechanism between upper cover 7 and the jar body 6.
The transmission mechanism comprises a second gear 13 and a third gear 15, the second gear 13 is fixedly sleeved at the lower end of the transmission rod 11, a plurality of rotating rods 14 are arranged in the cavity in a rotating mode, the third gears 15 are fixedly sleeved on the rod walls of the corresponding rotating rods 14, the lower surfaces of the rotating disks 5 are fixedly connected with fourth gears 17 through connecting rods 16, and the second gears 13, the third gears 15 and the fourth gears 17 are matched.
Coupling mechanism includes L template 20 and set casing 21, a plurality of L templates 20 are fixed respectively and are set up in the both sides wall of the jar body 6 that corresponds, the jack has all been seted up to the upper end of a plurality of L templates 20, a plurality of set casings 21 are fixed respectively and are set up in the both sides wall of the upper cover 7 that corresponds, the inside of a plurality of set casings 21 all slides and is provided with slider 22, the outside of a plurality of sliders 22 is all fixed and is provided with inserted bar 23, the outside one end of a plurality of inserted bars 23 all extends to the outside of the set casing 21 that corresponds and all pegs graft with the jack that corresponds, equal fixedly connected with spring 24 between the inboard of a plurality of sliders 22 and the inner wall of set casing 21.
The output end of the motor 12 is fixedly connected with the upper end of the transmission rod 11 to provide rotating power for the transmission rod 11.
The fixed feeding hopper that is provided with of upper cover 7's upper surface conveniently feeds in raw material.
The motor 12 is fixedly connected with the top plate 3 through the support frame, so that the motor 12 is more stably connected with the top plate 3
In the utility model, when in use, the worker switches on the power supply of the motor 12, the motor 12 drives the transmission rod 11 to rotate, namely, the rotation plate 4 is driven to rotate, the rotation plate 4 drives the plurality of the tank bodies 6 to revolve around the transmission rod 11, namely, the plurality of the first gears 10 rotate relative to the inner ring gear 9, because the inner ring gear 9 is fixedly arranged, the plurality of the first gears 10 rotate, the plurality of the first gears 10 drive the corresponding stirring rods 8 to rotate, namely, the interiors of the plurality of reaction kettles can be stirred by a single driving device, the use is convenient, meanwhile, the transmission rod 11 drives the second gear 13 to rotate, the second gear 13 drives the plurality of the third gears 15 to rotate, namely, the plurality of the fourth gears 17 rotate along with the revolution of the rotation plate 5, and the rotation directions of the plurality of the fourth gears 17 are opposite to the rotation direction of the first gears 10, namely, the plurality of the tank bodies 6 are driven to rotate, and the rotation directions of the stirring rods 8 are opposite to the corresponding directions, namely, the raw materials can be rapidly and fully stirred, the inserted rods 23 at the two sides are pushed towards the corresponding inner parts of the fixed shells 21 after the stirring is finished, the inserted rods are separated from the corresponding L-shaped plates 20, the upper cover 7 and the tank body 6 can be separated, and the articles in the tank body 6 can be taken out.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.
Claims (7)
1. The reaction device for synthesis of difluorobenzophenone comprises a base (1) and a top plate (3), and is characterized in that supporting rods (2) are fixedly arranged on two sides of the upper surface of the base (1), the top plate (3) is fixedly arranged on the top ends of the two supporting rods (2), a rotating plate (4) is rotatably arranged on the upper surface of the base (1), a plurality of rotating disks (5) are rotatably arranged in the rotating plate (4), a plurality of tank bodies (6) are fixedly arranged on the upper surface of each rotating disk (5), an upper cover (7) is fixedly arranged on the upper surface of each tank body (6), a plurality of stirring rods (8) are rotatably arranged in the upper cover (7), an inner toothed ring (9) is fixedly arranged on the lower surface of the top plate (3), and a first gear (10) is fixedly sleeved on the upper end of each stirring rod (8), be provided with transfer line (11) between base (1) and roof (3), the upper surface of roof (3) is provided with motor (12), the cavity has been seted up to the upper surface of base (1), the inside of cavity is provided with drive mechanism, be provided with coupling mechanism between upper cover (7) and the jar body (6).
2. The reaction device for difluorobenzophenone synthesis according to claim 1, wherein the transmission mechanism comprises a second gear (13) and a third gear (15), the second gear (13) is fixedly sleeved on the lower end of a transmission rod (11), a plurality of rotating rods (14) are rotatably arranged in the cavity, the plurality of third gears (15) are fixedly sleeved on the rod walls of the corresponding rotating rods (14), a fourth gear (17) is fixedly connected to the lower surfaces of the plurality of rotating disks (5) through a connecting rod (16), and the plurality of second gears (13), the plurality of third gears (15) and the plurality of fourth gears (17) are matched.
3. The reaction device for synthesis of difluorobenzophenone as claimed in claim 1, wherein said connecting mechanism comprises a plurality of connecting plates (18), said plurality of connecting plates (18) are respectively fixed on two side walls of the corresponding tank (6) and upper cover (7), and said connecting plates (18) adjacent to each other on two sides are fastened and connected by bolts (19) through screw threads.
4. The reaction apparatus for the synthesis of difluorobenzophenone as recited in claim 1, coupling mechanism includes L template (20) and set casing (21), and is a plurality of L template (20) is fixed respectively and sets up in the both sides wall of the jar body (6) that corresponds, and is a plurality of the jack has all been seted up to the upper end of L template (20), and is a plurality of set casing (21) is fixed respectively and sets up in the both sides wall of the upper cover (7) that corresponds, and is a plurality of the inside of set casing (21) all slides and is provided with slider (22), and is a plurality of the outside of slider (22) is all fixed and is provided with inserted bar (23), and is a plurality of the outside one end of inserted bar (23) all extends to the outside of the set casing (21) that corresponds and all pegs graft with the jack that corresponds, and is a plurality of equal fixedly connected with spring (24) between the inboard of slider (22) and the inner wall of set casing (21).
5. A reaction device for synthesis of difluorobenzophenone as in claim 1, wherein the output of the motor (12) is fixedly connected to the upper end of the driving rod (11).
6. The reaction device for the synthesis of difluorobenzophenone as claimed in claim 1, wherein a hopper is fixedly arranged on the upper surface of the upper cover (7).
7. The reaction device for the synthesis of difluorobenzophenone as claimed in claim 1, wherein said motor (12) is fixedly connected with said top plate (3) by means of a support frame.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202122116247.8U CN215996686U (en) | 2021-09-03 | 2021-09-03 | Reaction unit is used in synthesis of difluoro benzophenone |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202122116247.8U CN215996686U (en) | 2021-09-03 | 2021-09-03 | Reaction unit is used in synthesis of difluoro benzophenone |
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| Publication Number | Publication Date |
|---|---|
| CN215996686U true CN215996686U (en) | 2022-03-11 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116196870A (en) * | 2023-01-10 | 2023-06-02 | 江苏万隆化学有限公司 | Reaction equipment for synthesizing difluorobenzophenone |
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2021
- 2021-09-03 CN CN202122116247.8U patent/CN215996686U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116196870A (en) * | 2023-01-10 | 2023-06-02 | 江苏万隆化学有限公司 | Reaction equipment for synthesizing difluorobenzophenone |
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