CN215886427U - Alcohol recovery device for sodium hyaluronate preparation - Google Patents
Alcohol recovery device for sodium hyaluronate preparation Download PDFInfo
- Publication number
- CN215886427U CN215886427U CN202121708158.6U CN202121708158U CN215886427U CN 215886427 U CN215886427 U CN 215886427U CN 202121708158 U CN202121708158 U CN 202121708158U CN 215886427 U CN215886427 U CN 215886427U
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- CN
- China
- Prior art keywords
- heating coil
- sodium hyaluronate
- communicated
- liquid
- recovery device
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title claims abstract description 41
- 238000011084 recovery Methods 0.000 title claims abstract description 30
- 229920002385 Sodium hyaluronate Polymers 0.000 title claims abstract description 16
- 229940010747 sodium hyaluronate Drugs 0.000 title claims abstract description 16
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 238000010438 heat treatment Methods 0.000 claims abstract description 135
- 239000007788 liquid Substances 0.000 claims abstract description 67
- 239000000178 monomer Substances 0.000 claims abstract description 5
- 230000008676 import Effects 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 7
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 239000002699 waste material Substances 0.000 description 8
- 238000010586 diagram Methods 0.000 description 3
- 238000007599 discharging Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
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Abstract
The utility model relates to an alcohol recovery device for sodium hyaluronate preparation, which comprises a barrel body with an upper cover and a lower cover, wherein supporting legs are installed on the side wall of the barrel body, a recovery cavity is arranged inside the barrel body, a feed inlet communicated with a recovery cavity is formed in the side wall, a discharge outlet communicated with the recovery cavity is formed in the lower cover, a steam outlet communicated with the recovery cavity is formed in the upper cover, a heating coil assembly is arranged in the recovery cavity, the upper end of the heating coil assembly is communicated with an upper circulating liquid outlet installed on the upper cover, the lower end of the heating coil assembly is communicated with a bottom circulating liquid inlet installed on the lower cover, and the heating coil assembly comprises at least two coaxially arranged heating coil monomers. The utility model has the following beneficial effects: the heat exchange area is enlarged, the heat transfer effect is further optimized, and the recovery efficiency and the recovery effect are accelerated. In order to better utilize heat, save energy and reduce consumption; the temperature sensor measures the temperature and controls the liquid supply speed of the pump to ensure the recovery effect.
Description
Technical Field
The utility model relates to an alcohol recovery device for sodium hyaluronate preparation, and belongs to the technical field of alcohol recovery devices.
Background
At present, in the process of producing sodium hyaluronate, one step is alcohol (ethanol) purification, ethanol waste liquid is often generated, and an ethanol recovery device is generally required to recover the ethanol waste liquid. However, when the existing ethanol waste liquid recovery device recovers the ethanol waste liquid, the recovery effect on the ethanol is poor, and the ethanol waste liquid cannot be rapidly recovered.
SUMMERY OF THE UTILITY MODEL
According to the defects in the prior art, the technical problems to be solved by the utility model are as follows: in order to solve one of the problems, the alcohol recovery device for preparing the sodium hyaluronate is provided.
The utility model relates to an alcohol recovery device for sodium hyaluronate preparation, which is characterized in that: including the barrel that has upper cover and lower cover, install the landing leg on the lateral wall of barrel, the barrel is inside for retrieving the cavity, be provided with on the lateral wall and retrieve the feed inlet that the chamber is linked together, cover down and be provided with and retrieve the discharge gate that the chamber is linked together, cover up and be provided with and retrieve the steam outlet that the chamber is linked together, retrieve the intracavity and be provided with heating coil assembly, heating coil assembly's upper end and the upper portion circulation liquid export intercommunication of installing on covering, heating coil assembly's lower extreme and the bottom circulation liquid import intercommunication of installing on covering down, heating coil assembly includes the heating coil monomer of two at least coaxial settings.
Preferably, the heating coil assembly comprises an inner heating coil, a middle heating coil and an outer heating coil which are coaxially arranged, the middle heating coil is located between the inner heating coil and the outer heating coil, the upper ends of the inner heating coil, the middle heating coil and the outer heating coil are communicated with an upper circulating liquid outlet, and the lower ends of the inner heating coil, the middle heating coil and the outer heating coil are communicated with a bottom circulating liquid inlet.
Preferably, the upper portion circulation liquid outlet includes the body, the one end that the body inserted the barrel has the tip, the outer end and the back flow of body are linked together, bottom circulation liquid import is through sending liquid pipe and liquid pump intercommunication, the upper end of inlayer heating coil, middle level heating coil and skin heating coil is fixed on the lateral wall of body.
Preferably, the heating coil assembly comprises a first heating coil, a second heating coil, a third heating coil and a fourth heating coil, the first heating coil, the second heating coil, the third heating coil and the fourth heating coil are coaxially arranged from inside to outside, the upper ends of the first heating coil, the second heating coil, the third heating coil and the fourth heating coil are connected with an upper circulating liquid outlet, the bottom ends of the first heating coil, the second heating coil, the third heating coil and the fourth heating coil are connected with a bottom circulating liquid inlet, and the radiuses of the two adjacent heating coils are equal.
Preferably, the steam outlet is a jacketed pipe, the steam outlet is externally connected with a condenser, the jacketed pipe is provided with an inlet and an outlet, the outlet is connected with a bottom circulating liquid inlet through a liquid feeding pipe, and the inlet is connected with a liquid feeding pump.
Preferably, the cylinder, the steam outlet and the liquid conveying pipe are externally provided with heat insulation sleeves.
Preferably, the inner wall of the cylinder body is provided with a temperature sensor, the cylinder body further comprises a controller electrically connected with the temperature sensor, and an electrical output end of the controller is electrically connected with the liquid feeding pump.
Compared with the prior art, the utility model has the following beneficial effects:
according to the alcohol recovery device for preparing sodium hyaluronate, the lower end of the heating coil assembly is communicated with the bottom circulating liquid inlet arranged on the lower cover, and the heating coil assembly comprises at least two heating coil monomers which are coaxially arranged, so that the heat exchange area is enlarged, the heat transfer effect is further optimized, and the recovery efficiency and effect are accelerated;
in order to better utilize heat, save energy and reduce consumption, in the embodiment, the circulating heating liquid heat passes through the sleeve, the heating coil assembly and the bottom circulating liquid inlet and is recycled;
the temperature sensor measures the temperature and controls the liquid supply speed of the pump to ensure the recovery effect.
Drawings
In order to more clearly illustrate the detailed description of the utility model or the technical solutions in the prior art, the drawings that are needed in the detailed description of the utility model or the prior art will be briefly described below. Throughout the drawings, like elements or portions are generally identified by like reference numerals. In the drawings, elements or portions are not necessarily drawn to scale.
FIG. 1 is a schematic structural diagram according to a first embodiment of the present invention;
FIG. 2 is a schematic structural diagram according to a second embodiment of the present invention;
FIG. 3 is a schematic structural diagram of a heating coil assembly according to the first and second embodiments;
in the figure: 1. the heating device comprises a barrel body 2, supporting legs 3, a feeding hole 4, a discharging hole 5, a steam outlet 6, a bottom circulating liquid inlet 7, an upper circulating liquid outlet 7.1, a pipe body 7.2, an end part 8, a heating coil assembly 8.1, an inner-layer heating coil 8.2, a middle-layer heating coil 8.3, an outer-layer heating coil 9, a temperature sensor 10 and a controller.
Detailed Description
The utility model is further described below with reference to the accompanying drawings:
the present invention is further illustrated by the following specific examples, which are not intended to limit the scope of the utility model, and any modifications, equivalents, improvements, etc. made within the spirit and principle of the present invention should be included in the scope of the present invention.
Examples
As shown in fig. 1 and 3, alcohol recovery unit is used in sodium hyaluronate preparation, including barrel 1 that has upper cover and lower cover, install landing leg 2 on the lateral wall of barrel 1, the inside cavity that is retrieved of barrel 1, be provided with on the lateral wall and retrieve the feed inlet 3 that the chamber is linked together, be provided with the discharge gate 4 that is linked together with retrieving the chamber on the lower cover, be provided with the steam outlet 5 that is linked together with retrieving the chamber on the upper cover, retrieve the intracavity and be provided with heating coil assembly 8, heating coil assembly 8's upper end and the upper portion circulation liquid export 7 intercommunication of installing on the upper cover, heating coil assembly 8's lower extreme and the bottom circulation liquid import 6 intercommunication of installing on the lower cover, heating coil assembly 8 includes the heating coil monomer of two at least coaxial settings.
In this embodiment, the heating coil assembly 8 includes an inner heating coil 8.1, a middle heating coil 8.2 and an outer heating coil 8.3 which are coaxially arranged, the middle heating coil 8.2 is located between the inner heating coil 8.1 and the outer heating coil 8.3, the upper ends of the inner heating coil 8.1, the middle heating coil 8.2 and the outer heating coil 8.3 are all communicated with an upper circulating liquid outlet 7, and the lower ends of the inner heating coil 8.1, the middle heating coil 8.2 and the outer heating coil 8.3 are all communicated with a bottom circulating liquid inlet 6; upper portion circulation liquid export 7 includes body 7.1, the one end that body 7.1 inserted barrel 1 has tip 7.2, the outer end and the back flow of body 7.1 are linked together, bottom circulation liquid import 6 is through sending liquid pipe and liquid pump intercommunication, the upper end of inlayer heating coil 8.1, middle level heating coil 8.2 and outer heating coil 8.3 is fixed on the lateral wall of body 7.1.
In the second embodiment, referring to fig. 2 and 3, the difference from the first embodiment is that the steam outlet 5 is a jacketed pipe, the steam outlet 5 is externally connected with a condenser, the jacketed pipe has an inlet and an outlet, the outlet is connected with a bottom circulating liquid inlet 6 through a liquid sending pipe, and the inlet is connected with a liquid sending pump; the cylinder body 1, the steam outlet 5 and the liquid conveying pipe are externally provided with heat insulation sleeves; the inner wall of the cylinder body 1 is provided with a temperature sensor 9, the cylinder body further comprises a controller 10 electrically connected with the temperature sensor 9, and the electrical output end of the controller 10 is electrically connected with the liquid feeding pump.
The ethanol waste liquid is injected into the barrel body 1 through the feed port 3, the pump is connected with a liquid storage tank with a heating device, circulating liquid is pumped into a sleeve of the steam outlet 5, flows out of the sleeve and then enters the heating coil assembly 8 through the bottom circulating liquid inlet 6, and flows back to the liquid storage tank through the upper circulating liquid outlet 7, the ethanol waste liquid in the barrel body 1 is heated, and the difference of boiling points is utilized. Distilling off ethanol, discharging the distilled ethanol through a steam outlet 5, condensing and recovering.
After the recovery, the waste liquid is discharged through the discharge port 4.
In the third embodiment, the heating coil assembly 8 includes a first heating coil, a second heating coil, a third heating coil and a fourth heating coil, the first heating coil, the second heating coil, the third heating coil and the fourth heating coil are coaxially arranged from inside to outside, the upper ends of the first heating coil, the second heating coil, the third heating coil and the fourth heating coil are all connected with the upper circulating liquid outlet 7, the bottom ends of the first heating coil, the second heating coil, the third heating coil and the fourth heating coil are all connected with the bottom circulating liquid inlet 6, and the radii of the two adjacent heating coils are equal.
The foregoing shows and describes the general principles, essential features, and advantages of the utility model. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the utility model as claimed. The scope of the utility model is defined by the appended claims and equivalents thereof.
Claims (7)
1. The utility model provides a sodium hyaluronate preparation is with alcohol recovery unit which characterized in that: including the barrel that has upper cover and lower cover, install the landing leg on the lateral wall of barrel, the barrel is inside for retrieving the cavity, be provided with on the lateral wall and retrieve the feed inlet that the chamber is linked together, cover down and be provided with and retrieve the discharge gate that the chamber is linked together, cover up and be provided with and retrieve the steam outlet that the chamber is linked together, retrieve the intracavity and be provided with heating coil assembly, heating coil assembly's upper end and the upper portion circulation liquid export intercommunication of installing on covering, heating coil assembly's lower extreme and the bottom circulation liquid import intercommunication of installing on covering down, heating coil assembly includes the heating coil monomer of two at least coaxial settings.
2. The alcohol recovery device for sodium hyaluronate preparation according to claim 1, characterized in that: the heating coil assembly comprises an inner heating coil, a middle heating coil and an outer heating coil which are coaxially arranged, the middle heating coil is located between the inner heating coil and the outer heating coil, the upper ends of the inner heating coil, the middle heating coil and the outer heating coil are communicated with an upper circulating liquid outlet, and the lower ends of the inner heating coil, the middle heating coil and the outer heating coil are communicated with a bottom circulating liquid inlet.
3. The alcohol recovery device for sodium hyaluronate preparation according to claim 2, characterized in that: the upper portion circulation liquid outlet comprises a pipe body, an end portion is arranged at one end, inserted into the barrel, of the pipe body, the outer end of the pipe body is communicated with the return pipe, the bottom circulation liquid inlet is communicated with the liquid feeding pump through a liquid feeding pipe, and the upper ends of the inner heating coil, the middle heating coil and the outer heating coil are fixed on the side wall of the pipe body.
4. The alcohol recovery device for sodium hyaluronate preparation according to claim 1, characterized in that: the heating coil assembly comprises a first heating coil, a second heating coil, a third heating coil and a fourth heating coil, the first heating coil, the second heating coil, the third heating coil and the fourth heating coil are coaxially arranged from inside to outside, the upper ends of the first heating coil, the second heating coil, the third heating coil and the fourth heating coil are all connected with an upper circulating liquid outlet, the bottom ends of the first heating coil, the second heating coil, the third heating coil and the fourth heating coil are all connected with a bottom circulating liquid inlet, and the radiuses of the adjacent two heating coils are equal.
5. The alcohol recovery device for sodium hyaluronate preparation according to any one of claims 1 to 4, characterized in that: the steam outlet is a jacketed pipe, the steam outlet is externally connected with a condenser, the jacketed pipe is provided with an inlet and an outlet, the outlet is connected with a bottom circulating liquid inlet through a liquid feeding pipe, and the inlet is connected with a liquid feeding pump.
6. The alcohol recovery device for sodium hyaluronate preparation according to claim 5, characterized in that: and the cylinder, the steam outlet and the liquid conveying pipe are externally provided with heat insulation sleeves.
7. The alcohol recovery device for sodium hyaluronate preparation according to claim 6, characterized in that: the inner wall of the barrel is provided with a temperature sensor, the barrel further comprises a controller electrically connected with the temperature sensor, and the electrical output end of the controller is electrically connected with the liquid feeding pump.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202121708158.6U CN215886427U (en) | 2021-07-27 | 2021-07-27 | Alcohol recovery device for sodium hyaluronate preparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202121708158.6U CN215886427U (en) | 2021-07-27 | 2021-07-27 | Alcohol recovery device for sodium hyaluronate preparation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN215886427U true CN215886427U (en) | 2022-02-22 |
Family
ID=80344559
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202121708158.6U Active CN215886427U (en) | 2021-07-27 | 2021-07-27 | Alcohol recovery device for sodium hyaluronate preparation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN215886427U (en) |
-
2021
- 2021-07-27 CN CN202121708158.6U patent/CN215886427U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Sodium hyaluronate preparation and backup alcohol recovery device Granted publication date: 20220222 Pledgee: Qufu sub branch of Postal Savings Bank of China Ltd. Pledgor: SHANDONG RUNXIN BIOTECHNOLOGY Co.,Ltd. Registration number: Y2024980006159 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right |