CN215353458U - Reaction device for synthesizing R-tetrahydrobase hydrochloride - Google Patents

Reaction device for synthesizing R-tetrahydrobase hydrochloride Download PDF

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Publication number
CN215353458U
CN215353458U CN202121768176.3U CN202121768176U CN215353458U CN 215353458 U CN215353458 U CN 215353458U CN 202121768176 U CN202121768176 U CN 202121768176U CN 215353458 U CN215353458 U CN 215353458U
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wall
reaction tank
fixedly connected
reaction
synthesizing
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CN202121768176.3U
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张久彦
张皓翔
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LIANYUNGANG SHENGHE BIOTECHNOLOGY CO Ltd
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LIANYUNGANG SHENGHE BIOTECHNOLOGY CO Ltd
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Abstract

The utility model discloses a reaction device for synthesizing R-tetrahydrobase hydrochloride, which belongs to the technical field of reaction devices and comprises a reaction tank, wherein a motor is installed at the top of the reaction tank, an output shaft of the motor is fixedly connected with the top end of a connecting shaft, the bottom end of the connecting shaft penetrates into the reaction tank and is fixedly connected with a rotating plate, the outer wall of the connecting shaft is rotatably connected with a fixed block fixedly arranged at the top of the inner side of the reaction tank, the rotating plate is in an equilateral triangle shape, three corners of the rotating plate are rotatably connected with rotating shafts, gears are fixedly connected to the top ends of the rotating shafts, two side walls of the fixed block are fixedly connected to an inner gear ring through a fixed rod, and the inner gear ring is meshed with the three gears; this device can improve the mixed effect of material thing, improves reaction rate, also can carry out the separation work of reactant, perfect functional diversity, retort self possesses heating and rapid cooling function, but the normal clear of reaction process is guaranteed to the inside temperature conditions of real-time supervision retort.

Description

Reaction device for synthesizing R-tetrahydrobase hydrochloride
Technical Field
The utility model belongs to the technical field of reaction devices, and particularly relates to a reaction device for synthesizing R-tetrahydrobase hydrochloride.
Background
The compound is a pure substance composed of two or more different elements, and the compound has certain characteristics, is different from the elements or ions contained in the compound, is different from other compounds, and generally has certain composition, and the R-tetrahydrochysene hydrochloride is a compound.
At present, a reaction device is needed to be used in the synthesis of R-tetrahydrobase hydrochloride, but the existing part of the reaction device has a simple structure and is lack of a stirring function, so that the reaction synthesis time is long, crystals can be separated out in the synthesis of the R-tetrahydrobase hydrochloride, a filtering component is lacked in the subsequent discharging process, the separated crystals are difficult to separate and process, and meanwhile, the heating and rapid cooling functions are lacked, so that certain disadvantages exist in the use.
SUMMERY OF THE UTILITY MODEL
The present invention is directed to a reaction apparatus for synthesizing an R-tetrahydrochysene hydrochloride, which solves the problems of the prior art.
In order to achieve the purpose, the utility model provides the following technical scheme: the utility model provides a synthetic reaction unit that uses of R-tetrahydrobase hydrochloride, including the retort, the motor is installed at the top of retort, the output shaft and the connecting axle top rigid coupling of motor, the bottom of connecting axle is run through in to the retort and the rigid coupling has the rotor plate, the outer wall of connecting axle rotates with the fixed block that the retort inboard top set firmly and is connected, the shape of rotor plate is equilateral triangle, the three corner of rotor plate all rotates and is connected with the rotation axis, the top rigid coupling of rotation axis has the gear, the both sides wall of fixed block all is at the ring gear through a dead lever rigid coupling, the ring gear meshes with three gear mutually, the outer wall of rotation axis has stirring vane through two rigid couplings of a plurality of dead levers, the retort is equipped with the inlet pipe near inlaying on the outer wall at top, the bottom of retort is hourglass hopper-shaped and is connected with the discharging pipe, the bottom of retort has set firmly filtering component.
The scheme is as follows:
the type of the temperature sensor can be JC-1000-WF-HSM;
the motor is a common component in the prior art, and the adopted models and the like can be customized according to actual use requirements.
As a preferred embodiment, the outer wall of the reaction tank close to the bottom is provided with two containing cavities, an electric heater and a heat conduction pipe are respectively arranged in the two containing cavities, the heat conduction pipe is in a snake shape, two ends of the heat conduction pipe respectively extend to the outer side of the reaction tank and are connected with a water inlet pipe and a water outlet pipe, and a valve is arranged on the water inlet pipe.
In a preferred embodiment, a temperature sensor is installed on the inner wall of the reaction tank, a temperature display is installed on the outer wall of the reaction tank, and the temperature sensor is electrically connected with the temperature display.
In a preferred embodiment, the stirring blade has a spiral shape.
As a preferred embodiment, filtering component includes the fixed column of rigid coupling in the retort bottom, and the rigid coupling has solid fixed ring on the outer wall of fixed column, still overlaps on the outer wall of fixed column to be equipped with activity ring and spring, and the activity ring passes through spring and solid fixed ring elastic connection, and the rigid coupling has the fixture block of card notch on solid fixed ring's the outer wall, rotates on the outer wall that the fixed column is close to the bottom to be connected with and rotates the cover, and the outer wall that rotates the cover passes through the connecting rod rigid coupling and is having the filtration fill, filters the fill and is in under the discharging pipe.
As a preferred embodiment, the inner wall of the movable ring is fixedly connected with a limiting slide block, and the limiting slide block is slidably connected in a limiting hole formed in the outer wall of the fixed column.
Compared with the prior art, the reaction device for synthesizing the R-tetrahydrobase hydrochloride provided by the utility model at least has the following beneficial effects:
(1) the device can improve the mixing effect of materials and materials, improve the reaction rate, separate reactants and perfect functional diversity;
(2) through the setting of electric heater and heat pipe, electric heater can carry out heating work to the retort, and lets in the heat pipe through the inlet tube with the cooling water to can carry out quick cooling work to the retort, make retort self possess heating and rapid cooling function, and under the effect of temperature sensor and temperature display ware, but the normal clear of reaction process is guaranteed to the inside temperature condition of real-time supervision retort.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a side view of the present invention;
FIG. 3 is a schematic sectional view of the reaction tank of the present invention;
FIG. 4 is a schematic view of the connection of the components of the rotating plate according to the present invention;
FIG. 5 is a schematic view of the filter assembly of the present invention;
fig. 6 is a schematic structural view of the fixing post of the present invention.
In the figure: 1. a reaction tank; 2. a motor; 3. a connecting shaft; 4. a fixed block; 5. a rotating plate; 6. a rotating shaft; 7. a gear; 8. an inner gear ring; 9. fixing a rod I; 10. a second fixing rod; 11. a stirring blade; 12. an electric heater; 13. a heat conducting pipe; 14. a water inlet pipe; 15. a water outlet pipe; 16. a temperature sensor; 17. a temperature display device; 18. a feed pipe; 19. a discharge pipe; 20. a filter assembly; 2001. fixing a column; 2002. a fixing ring; 2003. a movable ring; 20031. a limiting slide block; 2004. a spring; 2005. a clamping block; 2006. rotating the sleeve; 2007. a connecting rod; 2008. and (4) filtering the funnel.
Detailed Description
The present invention will be further described with reference to the following examples.
The following examples are intended to illustrate the utility model but are not intended to limit the scope of the utility model. The conditions in the embodiments can be further adjusted according to specific conditions, and simple modifications of the method of the present invention based on the concept of the present invention are within the scope of the claimed invention.
Referring to fig. 1-6, the utility model provides a reaction device for synthesizing R-tetrahydrochysene hydrochloride, which comprises a reaction tank 1, wherein a motor 2 is installed at the top of the reaction tank 1, an output shaft of the motor 2 is fixedly connected with the top end of a connecting shaft 3, the bottom end of the connecting shaft 3 penetrates into the reaction tank 1 and is fixedly connected with a rotating plate 5, the outer wall of the connecting shaft 3 is rotatably connected with a fixed block 4 fixedly arranged at the top of the inner side of the reaction tank 1, the rotating plate 5 is in an equilateral triangle shape, three corners of the rotating plate 5 are rotatably connected with a rotating shaft 6, the top end of the rotating shaft 6 is fixedly connected with a gear 7, two side walls of the fixed block 4 are fixedly connected with an inner gear ring 8 through a fixed rod one 9, the inner gear ring 8 is meshed with three gears 7, the outer wall of the rotating shaft 6 is fixedly connected with stirring blades 11 through a plurality of fixed rods two 10, a feeding pipe 18 is embedded on the outer wall of the reaction tank 1 close to the top, the bottom of retort 1 is hopper-shaped and is connected with discharging pipe 19, and the bottom of retort 1 has set firmly filtering component 20.
As further shown in fig. 3, two cavities are provided on the outer wall of the reaction tank 1 near the bottom, an electric heater 12 and a heat conduction pipe 13 are respectively installed in the two cavities, the heat conduction pipe 13 is serpentine, two ends of the heat conduction pipe 13 respectively extend to the outer side of the reaction tank 1 and are connected with a water inlet pipe 14 and a water outlet pipe 15, and a valve is installed on the water inlet pipe 14; the electric heater 12 can heat the reaction tank 1, and the cooling water is introduced into the heat pipe 13 through the water inlet pipe 14, so that the reaction tank 1 can be rapidly cooled, and the reaction tank 1 can be heated and rapidly cooled.
As further shown in fig. 1 and 3, a temperature sensor 16 is installed on the inner wall of the reaction tank 1, a temperature display 17 is installed on the outer wall of the reaction tank 1, and the temperature sensor 16 is electrically connected with the temperature display 17; the temperature condition in the reaction tank 1 can be monitored in real time, and the normal operation of the reaction process is ensured.
As further shown in fig. 3 and 4, the stirring blade 11 is helical; the stirring effect of the stirring vanes 11 is improved.
As further shown in fig. 1 and 5, the filtering assembly 20 includes a fixed column 2001 fixedly connected to the bottom of the reaction tank 1, a fixed ring 2002 is fixedly connected to an outer wall of the fixed column 2001, a movable ring 2003 and a spring 2004 are further sleeved on an outer wall of the fixed column 2001, the movable ring 2003 is elastically connected to the fixed ring 2002 through the spring 2004, a fixture block 2005 with a fixture notch is fixedly connected to an outer wall of the fixed column 2002, the outer wall of the fixed column 2001 near the bottom end is rotatably connected to a rotating sleeve 2006, an outer wall of the rotating sleeve 2006 is fixedly connected to a filtering funnel 2008 through a connecting rod 2007, and the filtering funnel 2008 is located right below the discharge pipe 19; the filter hopper 2008 is rotated to the lower side of the discharge pipe, and the reactant discharged through the discharge pipe 19 can be filtered to intercept the precipitated crystals.
Further as shown in fig. 6, a limiting slide block 20031 is fixedly connected to the inner wall of the movable ring 2003, and the limiting slide block 20031 is slidably connected to a limiting hole formed in the outer wall of the fixed column 2001; the movable ring 2003 is restricted from rotating.
When the device is used, materials are poured into the reaction tank 1 through the feeding pipe 18, the motor 2 is started to work and drives the rotating plate 5 to rotate through the connecting shaft 3, under the action of the gear 7 and the inner gear ring 8, the rotating plate 5 drives the stirring blades 11 on the three rotating shafts 6 to revolve and rotate, through the arrangement of the electric heater 12 and the heat conduction pipe 13, the electric heater 12 can heat the reaction tank 1, cooling water is introduced into the heat conduction pipe 13 through the water inlet pipe 14, so that the reaction tank 1 can be rapidly cooled, the reaction tank 1 has the heating and rapid cooling functions, under the action of the temperature sensor 16 and the temperature display 17, the temperature condition in the reaction tank 1 can be monitored in real time, the normal operation of the reaction process is ensured, finally, through the arrangement of the filtering component 20, the filtering hopper is rotated to the lower part of the discharging 2008, the movable ring 2003 is pushed to move under the action of the spring 2004, the movable ring 2003 drives the clamping block 2005 to clamp the connecting pipe, so that the rotation of the filter bucket 2008 is limited, the reactant discharged through the discharge pipe 19 can be filtered, the separated crystal is intercepted, and after the filtration is finished, the movable ring 2003 is pushed upwards and the filter bucket 2008 is rotated to one side.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the utility model, the scope of which is defined in the appended claims and their equivalents.

Claims (6)

1. A reaction device for synthesizing R-tetrahydrochysene hydrochloride comprises a reaction tank (1), and is characterized in that: the top of the reaction tank (1) is provided with a motor (2), an output shaft of the motor (2) is fixedly connected with the top end of a connecting shaft (3), the bottom end of the connecting shaft (3) penetrates into the reaction tank (1) and is fixedly connected with a rotating plate (5), the outer wall of the connecting shaft (3) is rotatably connected with a fixed block (4) fixedly arranged at the top of the inner side of the reaction tank (1), the rotating plate (5) is in an equilateral triangle shape, three corners of the rotating plate (5) are rotatably connected with a rotating shaft (6), the top end of the rotating shaft (6) is fixedly connected with a gear (7), two side walls of the fixed block (4) are fixedly connected with an inner gear ring (8) through a first fixed rod (9), the inner gear ring (8) is meshed with three gears (7), the outer wall of the rotating shaft (6) is fixedly connected with stirring blades (11) through a plurality of second fixed rods (10), a feeding pipe (18) is embedded on the outer wall of the reaction tank (1) close to the top, the bottom of the reaction tank (1) is funnel-shaped and is connected with a discharge pipe (19), and the bottom of the reaction tank (1) is fixedly provided with a filtering component (20).
2. The reaction apparatus for synthesizing R-tetrahydrochysene hydrochloride according to claim 1, wherein: the reaction tank is characterized in that two containing cavities are formed in the outer wall, close to the bottom, of the reaction tank (1), electric heaters (12) and heat conducting pipes (13) are installed in the two containing cavities respectively, the heat conducting pipes (13) are S-shaped, the two ends of the heat conducting pipes (13) extend to the outer side of the reaction tank (1) respectively and are connected with a water inlet pipe (14) and a water outlet pipe (15), and valves are installed on the water inlet pipe (14).
3. The reaction apparatus for synthesizing R-tetrahydrochysene hydrochloride according to claim 1, wherein: install temperature sensor (16) on retort (1) inner wall, install temperature display ware (17) on the outer wall of retort (1), temperature sensor (16) and temperature display ware (17) electric connection.
4. The reaction apparatus for synthesizing R-tetrahydrochysene hydrochloride according to claim 1, wherein: the stirring blade (11) is spiral.
5. The reaction apparatus for synthesizing R-tetrahydrochysene hydrochloride according to claim 1, wherein: the filtering assembly (20) comprises a fixed column (2001) fixedly connected to the bottom of the reaction tank (1), a fixed ring (2002) is fixedly connected to the outer wall of the fixed column (2001), a movable ring (2003) and a spring (2004) are further sleeved on the outer wall of the fixed column (2001), the movable ring (2003) is elastically connected with the fixed ring (2002) through the spring (2004), a clamping block (2005) with a clamping groove opening is fixedly connected to the outer wall of the fixed column (2001) close to the bottom end, a rotating sleeve (2006) is rotatably connected to the outer wall of the rotating sleeve (2006) through a connecting rod (2007), a filtering hopper (2008) is fixedly connected to the outer wall of the rotating sleeve (2006), and the filtering hopper (2008) is located right below the discharge pipe (19).
6. The reaction apparatus for synthesizing R-tetrahydrochysene hydrochloride according to claim 5, wherein: the inner wall of the movable ring (2003) is fixedly connected with a limiting sliding block (20031), and the limiting sliding block (20031) is connected in a limiting hole formed in the outer wall of the fixed column (2001) in a sliding mode.
CN202121768176.3U 2021-07-31 2021-07-31 Reaction device for synthesizing R-tetrahydrobase hydrochloride Active CN215353458U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202121768176.3U CN215353458U (en) 2021-07-31 2021-07-31 Reaction device for synthesizing R-tetrahydrobase hydrochloride

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202121768176.3U CN215353458U (en) 2021-07-31 2021-07-31 Reaction device for synthesizing R-tetrahydrobase hydrochloride

Publications (1)

Publication Number Publication Date
CN215353458U true CN215353458U (en) 2021-12-31

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN202121768176.3U Active CN215353458U (en) 2021-07-31 2021-07-31 Reaction device for synthesizing R-tetrahydrobase hydrochloride

Country Status (1)

Country Link
CN (1) CN215353458U (en)

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