CN214716640U - Continuous flow tubular reactor - Google Patents
Continuous flow tubular reactor Download PDFInfo
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- CN214716640U CN214716640U CN202120970703.2U CN202120970703U CN214716640U CN 214716640 U CN214716640 U CN 214716640U CN 202120970703 U CN202120970703 U CN 202120970703U CN 214716640 U CN214716640 U CN 214716640U
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Abstract
The utility model provides a continuous flow tubular reactor, include: the stirring part is arranged at the top and inside the reactor body and comprises a servo motor, a stirring shaft and stirring blades; the heating part is arranged on the outer surface below the reactor body and comprises a heating oil outlet, a heating tank and a heating oil inlet; the feeding part is arranged at the bottom of the reactor body and comprises a first feeding pipe and a second feeding pipe; the reflux part is arranged on the right side of the reactor body and comprises a tee joint, an overflow port and a reflux port; and the gas-liquid separation part is arranged at the upper end of the right side of the reactor body and comprises a gas-liquid outlet pipe, a gas outlet pipe, a separation cylinder and a liquid outlet pipe. The utility model provides a current tubular reactor reaction mix the effect relatively poor, and reaction efficiency is lower, and the gas-liquid perhaps contains the relatively poor phenomenon of liquid-solid reaction effect, has the problem of the difficult operation of tubular reactor for the reaction type of gaseous production.
Description
Technical Field
The utility model relates to a tubular reactor technical field, concretely relates to continuous flow tubular reactor.
Background
The existing tubular reactor has the phenomena of poor reaction mixing effect, low reaction efficiency, poor gas-liquid or liquid-solid reaction effect, and difficult operation of the tubular reactor for the reaction type generated by gas.
SUMMERY OF THE UTILITY MODEL
In order to overcome the defects in the prior art, a continuous flow tubular reactor is provided so as to solve the problems that the existing tubular reactor has poor reaction mixing effect and low reaction efficiency, has poor gas-liquid or liquid-solid reaction effect and is difficult to operate in a reaction type tubular reactor with gas generation.
To achieve the above object, there is provided a continuous flow tubular reactor comprising:
the stirring part is arranged at the top and inside the reactor body and comprises a servo motor, a stirring shaft and stirring blades;
the heating part is arranged on the outer surface below the reactor body and comprises a heating oil outlet, a heating tank and a heating oil inlet;
the feeding part is arranged at the bottom of the reactor body and comprises a first feeding pipe and a second feeding pipe;
the reflux part is arranged on the right side of the reactor body and comprises a tee joint, an overflow port and a reflux port;
and the gas-liquid separation part is arranged at the upper end of the right side of the reactor body and comprises a gas-liquid outlet pipe, a gas outlet pipe, a separation cylinder and a liquid outlet pipe.
Further, the reactor body is the cylinder structure, reactor body top is provided with sealed lid, sealed lid left side is provided with temperature indicator, sealed lid right side is provided with pressure indicator, reactor body bottom is provided with the supporting seat, supporting seat top surface central point puts and is provided with the bearing frame, the inside equidistance in reactor body below is provided with the ultrasonic wave mixing section, the back correspondence of reactor body is provided with supersonic generator, the servo motor of stirring part installs in sealed lid top surface central point, shaft coupling and servo motor's output shaft fixed connection is passed through on the (mixing) shaft top, the outer end passes through dead lever fixedly connected with stirring leaf below the (mixing) shaft, the stirring leaf is the rectangular strip structure, bearing swing joint in (mixing) shaft bottom and the bearing frame.
Further, the heating jar cover of heating part is established at the surface of reactor body below, and heating jar left side upper end is provided with the heating oil export, and the offside of heating oil export is provided with the discharging pipe, and the discharging pipe passes the jar body and the reactor body intercommunication of heating jar, and heating jar right side bottom is provided with the heating oil import, and high temperature hot oil gets into the heating jar from the heating oil import and heats the reactor body inside.
Further, the first inlet pipe of feeding part passes the jar body and reactor body left side bottom intercommunication of heating jar left side bottom, and the second inlet pipe passes the jar body and reactor body front side bottom intercommunication of heating jar front side bottom.
Further, the gas-liquid outlet pipe of the gas-liquid separation part is arranged at the upper end of the right side of the reactor body, the gas-liquid outlet pipe is communicated with the gas-liquid separation cylinder, the gas outlet pipe is arranged at the top of the gas-liquid separation cylinder, the lower end of the gas outlet pipe extends into the gas-liquid separation cylinder, the lower end of the gas outlet pipe is of a cylindrical filter screen structure, and the liquid outlet pipe is arranged at the bottom end of the gas-liquid separation cylinder.
Furthermore, the top end of a three-way joint of the backflow part is communicated with the liquid outlet pipe, the three-way joint is communicated with an overflow port at the upper end of the right side of the reactor body through an overflow pipe, and the bottom end of the three-way joint is communicated with a backflow port at the bottom end of the right side of the reactor body through a backflow pipe.
The beneficial effects of the utility model reside in that, the utility model discloses a continuous flow tubular reactor utilizes the servo motor of stirring part to drive the ultrasonic wave that stirring leaf cooperation supersonic generator sent and carries out intensive mixing to the material, thereby improve mixed effect, the mode that the reverse transport high temperature that utilizes the heating part hot oil makes the material heating effect better, the reaction efficiency is improved, utilize the gas-liquid separation part to separate the gas and the liquid that the reaction produced, liquid reflux after the separation continues the reaction to the reactor body, thereby improve reaction efficiency, it is relatively poor to have solved current tubular reactor reaction mixing effect, reaction efficiency is lower, gas-liquid perhaps contains the relatively poor phenomenon of liquid-solid reaction effect, the problem of the difficult operation of tubular reactor for the reaction type that has gas to produce.
Drawings
Fig. 1 is a schematic front sectional view of an embodiment of the present invention;
fig. 2 is a schematic front view of the embodiment of the present invention;
FIG. 3 is a schematic top sectional view of the bottom end of the reactor body according to an embodiment of the present invention;
fig. 4 is a schematic rear view of the embodiment of the present invention.
1. A reactor body; 2. a pressure indicator; 3. a temperature indicator; 4. a stirring section; 41. a servo motor; 42. a stirring shaft; 43. stirring blades; 5. a heating section; 51. a heating oil outlet; 52. a heating tank; 53. a heating oil inlet; 6. an ultrasonic wave mixing section; 61. an ultrasonic generator; 7. a feed portion; 71. a first feed tube; 72. a second feed tube; 8. a supporting seat; 9. a reflux part; 91. a three-way joint; 92. an overflow port; 93. a return port; 10. a gas-liquid separation section; 101. a gas-liquid outlet pipe; 102. a gas outlet pipe; 103. a separation cylinder; 104. a liquid outlet pipe; 11. and (4) discharging the pipe.
Detailed Description
The following description of the embodiments of the present invention is provided for illustrative purposes, and other advantages and effects of the present invention will be readily apparent to those skilled in the art from the disclosure herein. The present invention can also be implemented or applied through other different specific embodiments, and various details in the present specification can be modified or changed based on different viewpoints and applications without departing from the spirit of the present invention.
Referring to fig. 1 to 4, the present invention provides a continuous flow tubular reactor comprising: stirring section 4, heating section 5, feed section 7, reflux section 9 and gas-liquid separation section 10.
Specifically, the stirring section 4 is provided at the top and inside of the reactor body 1, and the stirring section 4 includes a servo motor 41, a stirring shaft 42, and stirring blades 43.
The heating part 5 is provided at an outer surface below the reactor body 1, and the heating part 5 includes a heating oil outlet 51, a heating tank 52, and a heating oil inlet 53.
The feeding portion 7 is provided at the bottom of the reactor body 1, and the feeding portion 7 includes a first feeding pipe 71 and a second feeding pipe 72.
The reflux portion 9 is provided on the right side of the reactor body 1, and the reflux portion 9 includes a three-way joint 91, an overflow port 92, and a reflux port 93.
And a gas-liquid separation part 10 disposed at the upper end of the right side of the reactor body 1, the gas-liquid separation part 10 including a gas-liquid outlet pipe 101, a gas outlet pipe 102, a separation cylinder 103, and a liquid outlet pipe 104.
The existing tubular reactor has the phenomena of poor reaction mixing effect, low reaction efficiency, poor gas-liquid or liquid-solid reaction effect, and difficult operation of the tubular reactor for the reaction type generated by gas. Therefore, the utility model discloses a continuous flow tubular reactor utilizes servo motor 41 of stirring part 4 to drive the ultrasonic wave that stirring leaf 43 cooperation supersonic generator 61 sent and carries out the intensive mixing to the material, thereby improve the mixed effect, the mode that utilizes the reverse transport high temperature hot oil of heating part 5 makes material heating effect better, improve reaction efficiency, utilize gas-liquid separation part 10 to separate the gas and the liquid that the reaction produced, liquid reflux after the separation continues the reaction to reactor body 1, thereby improve reaction efficiency, it is relatively poor to have solved current tubular reactor reaction mixing effect, reaction efficiency is lower, gas-liquid perhaps contains the relatively poor phenomenon of liquid-solid reaction effect, the problem of the difficult operation of tubular reactor for the reaction type that has gas to produce.
In the present embodiment, the stirring part 4 is disposed at the top and inside of the reactor body 1, the stirring part 4 includes the servo motor 41, the stirring shaft 42 and the stirring blade 43, the heating part 5 is disposed at the outer surface below the reactor body 1, the heating part 5 includes the heating oil outlet 51, the heating tank 52 and the heating oil inlet 53, the feeding part 7 is disposed at the bottom of the reactor body 1, and the feeding part 7 includes the first feeding pipe 71 and the second feeding pipe 72.
As a better embodiment, the reactor body 1 is a cylindrical structure, the top of the reactor body 1 is provided with a sealing cover, the left side of the sealing cover is provided with a temperature indicator 3, the temperature between-50 ℃ and 300 ℃ can be set according to the temperature required by the reaction, the temperature control precision is 0.1 ℃, the right side of the sealing cover is provided with a pressure indicator 2, the bottom end of the reactor body 1 is provided with a supporting seat 8, the central position of the top surface of the supporting seat 8 is provided with a bearing seat, the inside of the lower part of the reactor body 1 is equidistantly provided with ultrasonic mixing sections 6, the back of the reactor body 1 is correspondingly provided with an ultrasonic generator 61, a servo motor 41 of a stirring part 4 is arranged at the central position of the top surface of the sealing cover, the top end of a stirring shaft 42 is fixedly connected with an output shaft of the servo motor 41 through a coupler, the outer end of the lower part of the stirring shaft 42 is fixedly connected with stirring blades 43 through fixing rods, the stirring blades 43 are rectangular structures, the bottom end of the stirring shaft 42 is movably connected with a bearing in a bearing seat, a heating tank 52 of the heating part 5 is sleeved on the outer surface below the reactor body 1, a heating oil outlet 51 is arranged at the upper end of the left side of the heating tank 52, a discharging pipe 11 is arranged at the opposite side of the heating oil outlet 51, the discharging pipe 11 penetrates through a tank body of the heating tank 52 to be communicated with the reactor body 1, a heating oil inlet 53 is arranged at the bottom end of the right side of the heating tank 52, a first feeding pipe 71 of the feeding part 7 penetrates through the tank body at the bottom end of the left side of the heating tank 52 to be communicated with the bottom end of the left side of the reactor body 1, a second feeding pipe 72 penetrates through the tank body at the bottom end of the front side of the heating tank 52 to be communicated with the bottom end of the front side of the reactor body 1, high-temperature hot oil enters into the heating tank 52 from the heating oil inlet 53 to heat the reactor body 1, the materials are fully and uniformly mixed by the high-speed mixer and then enter into the reactor body 1 to react, the material makes progress the in-process through twice ultrasonic wave intensive mixing reaction again and flows out through discharging pipe 11, 41 servo motor drive 43 stirring leaf cooperation ultrasonic generator 61 ultrasonic wave that send carry out intensive mixing to the material to improve mixed effect, the mode of the reverse transport high temperature hot oil of utilizing heating part 5 makes material heating effect better, improves reaction efficiency.
In this embodiment, the reflux portion 9 is disposed at the right side of the reactor body 1, the reflux portion 9 includes a three-way joint 91, an overflow port 92 and a reflux port 93, the gas-liquid separation portion 10 is disposed at the upper end of the right side of the reactor body 1, and the gas-liquid separation portion 10 includes a gas-liquid outlet pipe 101, a gas outlet pipe 102, a separation cylinder 103 and a liquid outlet pipe 104.
As a preferred embodiment, the gas-liquid outlet 101 of the gas-liquid separation part 10 is arranged at the upper right end of the reactor body 1, the gas-liquid outlet 101 is communicated with the gas-liquid separation cylinder 103, the gas outlet 102 is arranged at the top of the gas-liquid separation cylinder 103, the lower end of the gas outlet 102 extends into the gas-liquid separation cylinder 103, the lower end of the gas outlet 102 is in a cylindrical filter screen structure, the liquid outlet 104 is arranged at the bottom end of the gas-liquid separation cylinder 103, the top end of the tee joint 91 of the reflux part 9 is communicated with the liquid outlet 104, the tee joint 91 is communicated with the overflow port 92 at the upper right end of the reactor body 1 through an overflow pipe, the bottom end of the tee joint 91 is communicated with the reflux port 93 at the bottom right end of the reactor body 1 through a reflux pipe, when gas or reflux is generated during the reaction process, the reacted material can reflux to the inside the reactor body 1 for continuous reaction through the tee joint 91 and the overflow port 92 and the liquid outlet 104, thereby improving the reaction efficiency and being convenient to operate.
The utility model discloses a continuous flow tubular reactor can effectively solve current tubular reactor reaction mixing effect relatively poor, and reaction efficiency is lower, and the gas-liquid perhaps contains the relatively poor phenomenon of liquid-solid reaction effect, has the problem of the difficult operation of tubular reactor for the reaction type of gaseous production, is applicable to the mixing reaction of material.
Claims (6)
1. A continuous flow tubular reactor, comprising:
the stirring part (4) is arranged at the top and inside of the reactor body (1), and the stirring part (4) comprises a servo motor (41), a stirring shaft (42) and a stirring blade (43);
the heating part (5) is arranged on the outer surface below the reactor body (1), and the heating part (5) comprises a heating oil outlet (51), a heating tank (52) and a heating oil inlet (53);
a feeding portion (7) provided at the bottom of the reactor body (1), the feeding portion (7) including a first feeding pipe (71) and a second feeding pipe (72);
the backflow part (9) is arranged on the right side of the reactor body (1), and the backflow part (9) comprises a three-way joint (91), an overflow port (92) and a backflow port (93);
the gas-liquid separation part (10) is arranged at the upper end of the right side of the reactor body (1), and the gas-liquid separation part (10) comprises a gas-liquid outlet pipe (101), a gas outlet pipe (102), a separation cylinder (103) and a liquid outlet pipe (104).
2. The continuous flow tubular reactor according to claim 1, wherein the reactor body (1) is cylindrical, a sealing cover is disposed on the top of the reactor body (1), a temperature indicator (3) is disposed on the left side of the sealing cover, a pressure indicator (2) is disposed on the right side of the sealing cover, a supporting seat (8) is disposed at the bottom end of the reactor body (1), a bearing seat is disposed at the center of the top surface of the supporting seat (8), ultrasonic mixing sections (6) are equidistantly disposed in the lower portion of the reactor body (1), an ultrasonic generator (61) is correspondingly disposed on the back surface of the reactor body (1), a servo motor (41) of the stirring portion (4) is mounted at the center of the top surface of the sealing cover, the top end of the stirring shaft (42) is fixedly connected with an output shaft of the servo motor (41) through a shaft coupling, and the outer end of the lower portion of the stirring shaft (42) is fixedly connected with a stirring blade (43) through a fixing rod, the stirring blades (43) are in a rectangular strip structure, and the bottom end of the stirring shaft (42) is movably connected with a bearing in the bearing seat.
3. The continuous flow-tube reactor according to claim 2, wherein the heating tank (52) of the heating part (5) is sleeved on the outer surface of the lower part of the reactor body (1), the upper end of the left side of the heating tank (52) is provided with a heating oil outlet (51), the opposite side of the heating oil outlet (51) is provided with a discharge pipe (11), the discharge pipe (11) passes through the tank body of the heating tank (52) to be communicated with the reactor body (1), the bottom end of the right side of the heating tank (52) is provided with a heating oil inlet (53), and high-temperature hot oil enters the heating tank (52) from the heating oil inlet (53) to heat the reactor body (1).
4. The continuous flow-tube reactor according to claim 3, wherein the first feeding tube (71) of the feeding portion (7) is communicated with the left bottom end of the reactor body (1) through the tank body at the left bottom end of the heating tank (52), and the second feeding tube (72) is communicated with the front bottom end of the reactor body (1) through the tank body at the front bottom end of the heating tank (52).
5. The continuous flow tubular reactor according to claim 1, wherein the gas-liquid outlet pipe (101) of the gas-liquid separation part (10) is arranged at the upper right end of the reactor body (1), the gas-liquid outlet pipe (101) is communicated with the gas-liquid separation cylinder (103), the gas outlet pipe (102) is arranged at the top of the gas-liquid separation cylinder (103), the lower end of the gas outlet pipe (102) extends into the gas-liquid separation cylinder (103), the lower end of the gas outlet pipe (102) is of a cylindrical filter screen structure, and the liquid outlet pipe (104) is arranged at the bottom end of the gas-liquid separation cylinder (103).
6. The continuous flow-tube reactor according to claim 5, wherein the top end of the tee joint (91) of the return portion (9) is connected to the liquid outlet tube (104), the tee joint (91) is connected to the overflow port (92) at the upper right end of the reactor body (1) via an overflow tube, and the bottom end of the tee joint (91) is connected to the return port (93) at the bottom right end of the reactor body (1) via a return tube.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120970703.2U CN214716640U (en) | 2021-05-08 | 2021-05-08 | Continuous flow tubular reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202120970703.2U CN214716640U (en) | 2021-05-08 | 2021-05-08 | Continuous flow tubular reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN214716640U true CN214716640U (en) | 2021-11-16 |
Family
ID=78619854
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202120970703.2U Active CN214716640U (en) | 2021-05-08 | 2021-05-08 | Continuous flow tubular reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN214716640U (en) |
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2021
- 2021-05-08 CN CN202120970703.2U patent/CN214716640U/en active Active
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