CN214680082U - Short-range distiller for organic silicon - Google Patents

Short-range distiller for organic silicon Download PDF

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Publication number
CN214680082U
CN214680082U CN202120868788.3U CN202120868788U CN214680082U CN 214680082 U CN214680082 U CN 214680082U CN 202120868788 U CN202120868788 U CN 202120868788U CN 214680082 U CN214680082 U CN 214680082U
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short
cylinder
barrel
communicated
conduction oil
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周伟良
钱立冬
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Wuxi Sufu Equipment Technology Co ltd
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Wuxi Sufu Equipment Technology Co ltd
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Abstract

The utility model discloses a short distance distiller for organosilicon, its technical scheme main points are: the heat exchange tube type heat exchanger comprises a tube body, wherein a short section tube body is arranged at the lower part of the tube body, a lower tube body is arranged at the bottom of the short section tube body, a light component outlet and a circulating water outlet are arranged at the lower part of a bottom plate, one side of the lower tube body is communicated with a circulating water inlet, one side of the short section tube body is communicated with a heavy component outlet, an inclined baffle is arranged inside the short section tube body, one side of the short section tube body is communicated with a vacuum port, the side edge of the tube body is communicated with a first heat conduction oil inlet, a first heat conduction oil outlet, a second heat conduction oil inlet, a first vent, a sealing plate, a second heat conduction oil outlet and a second vent, tube boxes are respectively arranged at the upper end and the lower end of the tube body, and heat exchange tubes are communicated among the tube boxes; the device has the advantages of high working efficiency, high reliability, visual display, easy operation and maintenance, strong separation capability, good effect and the like.

Description

Short-range distiller for organic silicon
Technical Field
The utility model relates to a distillation technical field, in particular to short distance distiller for organosilicon.
Background
The organic silicon industrialization direction should tightly hold the development trend of the organic silicon technology in the world, a novel organic silicon or modified organic silicon material which has high reliability, energy conservation, green environmental protection and flame retardance is taken as a key development object, meanwhile, the organic silicon is an additive and a modified material of various high-tech composite materials, and can promote the research and development of new materials in related fields, and a new material industrial chain with wide application is derived, so that the continuous development of organic silicon products can play a positive role in saving energy, protecting the environment and promoting the sustainable development of economy and society in the whole society.
Referring to the prior Chinese patent publication No. CN111318039A, it discloses a short path distiller, which comprises an upper tank body, the top of the upper tank body is fixedly provided with a sealing cover, the top end of the sealing cover is fixedly provided with a feeding pipe, the bottom end of the feed pipe penetrates through and extends into the upper tank body, the inner wall of the upper tank body is fixedly provided with an annular shell, a heating liquid inlet pipe is fixedly arranged on the right side of the upper tank body, a heating liquid outlet pipe is fixedly arranged on the left side of the upper tank body, the bottom of the upper tank body is movably connected with a lower tank body, the left side and the right side of the lower tank body are both fixedly connected with fixed blocks, the tops of the two fixed blocks are both provided with limiting holes, go up the equal fixedly connected with gag lever post in the left and right sides of jar body and corresponding spacing hole department, the gag lever post is located the inside in spacing hole, two the through-hole has all been seted up to the inside of gag lever post.
The short-path distiller is convenient to clean, maintain and replace, and distillation quality is improved. However, the short path distiller of the above type still has some disadvantages, such as: firstly, the distillation and condensation efficiency is low, and the distillation operation cannot be realized quickly; and secondly, the function of a vacuum port cannot be realized, part of formed medium flows out from the light component outlet, and the rest medium flows out from the heavy component outlet through the inclined baffle.
SUMMERY OF THE UTILITY MODEL
In view of the problems mentioned in the background art, the utility model aims to provide a short-path distiller for organic silicon to solve the problems mentioned in the background art.
The above technical purpose of the present invention can be achieved by the following technical solutions:
a short-path distiller for organic silicon comprises a barrel, wherein a short section barrel is arranged at the lower part of the barrel, a lower barrel is fixedly arranged at the bottom of the short section barrel, a bottom plate is fixedly arranged at the bottom of the lower barrel, a light component outlet and a circulating water outlet are fixedly arranged at the lower part of the bottom plate, a circulating water inlet is fixedly communicated with one side of the lower barrel, a heavy component outlet is fixedly communicated with one side of the short section barrel, an inclined baffle is fixedly arranged inside the short section barrel, a vacuum port is fixedly communicated with one side of the short section barrel, a first heat conduction oil inlet is fixedly communicated with the lower end of one side of the barrel, a first heat conduction oil outlet is fixedly communicated with the upper end of one side of the barrel, a second heat conduction oil inlet is fixedly communicated with the upper end of one side of the barrel, a first vent port is communicated with the lower part of the second heat conduction oil inlet, and a sealing plate is fixedly arranged at the upper part of the first heat conduction oil outlet, the improved heat exchanger is characterized in that a second heat conduction oil outlet is fixedly communicated with the upper end of one side of the barrel, pipe boxes are fixedly mounted at the upper end and the lower end of the barrel respectively, a heat exchange pipe is fixedly communicated between the pipe boxes, a second vent is fixedly communicated with one side of the upper end of the barrel, a flat cover is fixedly arranged on the upper portion of the barrel, a feed inlet is fixedly communicated with the flat cover, and a scraper mechanism is fixedly mounted on the flat cover.
By adopting the technical scheme, be equipped with the feed inlet above the short distance distiller flat cover for organosilicon, the medium sprays scraper blade system, flow down along the barrel inner wall, there is the clamp cover outside the barrel, the conduction oil gets into the heating barrel through first conduction oil import and second conduction oil import, flow out by first conduction oil export and second conduction oil export, cooling water gets into by the circulating water import, flow into one side heat exchange tube through lower part pipe case, reach the upper portion pipe incasement, rethread opposite side heat exchange tube flows back to lower part pipe case, flow out by the circulating water export, reach the effect that reduces equipment internal temperature, through the vacuum mouth effect, some mediums are exported by the light component and flow out, the rest mediums are exported by the heavy component through the oblique baffle and flow out.
Preferably, including servo motor in the scraper blade mechanism, servo motor's output fixedly connected with axostylus axostyle, be connected with the reduction gear on the axostylus axostyle, still including the frame in the scraper blade mechanism, servo motor fixed mounting is in inside the frame, the output fixedly connected with scraper blade of reduction gear.
By adopting the technical scheme, the inner wall of the cylinder body can be cleaned through the scraper mechanism.
Preferably, the flat cover and the cylinder are fixedly connected through a first connecting flange.
Through adopting above-mentioned technical scheme, first connection flange can realize carrying out stable connection to flat lid and barrel.
Preferably, the two sides of the cylinder body are respectively and fixedly provided with an ear seat.
Through adopting above-mentioned technical scheme, the setting of ear seat can realize carrying out fixed mounting to the barrel.
Preferably, a jacket is fixedly adhered to the outer side of the cylinder.
Through adopting above-mentioned technical scheme, the setting of pressing from both sides the cover can realize heat preservation and protection.
Preferably, the cylinder body is fixedly connected with the short section cylinder body through a second connecting flange, and the short section cylinder body is fixedly connected with the lower cylinder body through a third connecting flange.
Through adopting above-mentioned technical scheme, second flange and third flange can realize carrying out fixed mounting to between barrel, nipple joint barrel and the lower barrel and be connected.
Preferably, the heat exchange tubes are provided with a plurality of groups, the first heat conduction oil inlet is fixedly communicated with the first heat conduction oil outlet, and the second heat conduction oil inlet is fixedly communicated with the second heat conduction oil outlet.
Through adopting above-mentioned technical scheme, the heat exchange tube can realize condensing the distillation, and the connection of heat conduction hydraulic fluid port can realize the circular transport.
To sum up, the utility model discloses mainly have following beneficial effect:
this short distance distiller flat cover top for organosilicon is equipped with the feed inlet, the medium sprays scraper blade system, flow down along the barrel, there is the clamp cover the barrel outside, the conduction oil passes through the conduction oil import and gets into the heating barrel, flow out by the conduction oil export, the cooling water gets into by the circulating water import, flow into the heat transfer pipe through lower tube case, reach the last pipe case, the rethread heat transfer pipe flows back to lower tube case, flow out by the circulating water export, reach the effect that reduces the inside temperature of equipment, through the vacuum mouth effect, some medium is exported by the light component and is flowed, the surplus medium is exported by the heavy component through the oblique baffle and is flowed. The advantages of high working efficiency, high reliability, visual display, easy operation and maintenance, strong separation capability, good effect and the like are realized.
Drawings
Fig. 1 is a schematic structural diagram of the present invention;
fig. 2 is a sectional view of the top view structure of the present invention.
Reference numerals: 1. a barrel; 2. a short section cylinder; 3. a lower cylinder body; 4. a base plate; 5. a light component outlet; 6. a circulating water outlet; 7. a circulating water inlet; 8. a heavy component outlet; 9. an inclined baffle plate; 10. a vacuum port; 11. a first conduction oil inlet; 12. a first heat transfer oil outlet; 13. a second heat transfer oil inlet; 14. a first vent; 15. closing the plate; 16. a second heat transfer oil outlet; 17. a pipe box; 18. a heat exchange pipe; 19. a second vent; 20. a feed inlet; 21. a scraping plate mechanism; 22. a servo motor; 23. a shaft lever; 24. a speed reducer; 25. flattening the cover; 26. a first connecting flange; 27. an ear mount; 28. a jacket; 29. a second connecting flange; 30. and a third connecting flange.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Example 1
Referring to fig. 1-2, a short-path distiller for organic silicon comprises a barrel 1, wherein a short section barrel 2 is arranged at the lower part of the barrel 1, a lower barrel 3 is fixedly arranged at the bottom of the short section barrel 2, a bottom plate 4 is fixedly arranged at the bottom of the lower barrel 3, a light component outlet 5 and a circulating water outlet 6 are fixedly arranged at the lower part of the bottom plate 4, a circulating water inlet 7 is fixedly communicated with one side of the lower barrel 3, a heavy component outlet 8 is fixedly communicated with one side of the short section barrel 2, an inclined baffle 9 is fixedly arranged in the short section barrel 2, a vacuum port 10 is fixedly communicated with one side of the short section barrel 2, a first heat conduction oil inlet 11 is fixedly communicated with the lower end of one side of the barrel 1, a first heat conduction oil outlet 12 is fixedly communicated with the upper end of one side of the barrel 1, a second heat conduction oil inlet 13 is fixedly communicated with the upper end of one side of the barrel 1, the lower part of the second heat conduction oil inlet 13 is communicated with a first vent 14, the upper part of the first heat conduction oil outlet 12 is fixedly provided with a sealing plate 15, the upper end of one side of the barrel 1 is fixedly communicated with a second heat conduction oil outlet 16, the upper end and the lower end of the barrel 1 are respectively fixedly provided with a pipe box 17, heat exchange pipes 18 are fixedly communicated between the pipe boxes 17, one side of the upper end of the barrel 1 is fixedly communicated with a second vent 19, the upper part of the barrel 1 is fixedly provided with a flat cover 25, the flat cover 25 is fixedly communicated with a feed inlet 20, and the flat cover 25 is fixedly provided with a scraper mechanism 21.
By adopting the technical scheme, a feed inlet 20 is arranged above a flat cover 25 of the short-distance distiller for organic silicon, a medium is sprayed to a scraper system 21 and flows downwards along the inner wall of a cylinder 1, a jacket 28 is arranged on the outer side of the cylinder 1, heat conduction oil enters a heating cylinder through a first heat conduction oil inlet 11 and a second heat conduction oil inlet 13 and flows out from a first heat conduction oil outlet 12 and a second heat conduction oil outlet 16, cooling water enters from a circulating water inlet 7 and flows into a heat exchange pipe 18 on one side through a lower pipe box 17 to reach the inside of the upper pipe box 17 and then flows back to the lower pipe box 17 through the heat exchange pipe 18 on the other side and flows out from a circulating water outlet 6, the effect of reducing the internal temperature of equipment is achieved, part of the medium flows out from a light component outlet 8 under the action of a vacuum port 10, and the rest of the medium flows out from a heavy component outlet 5 through an inclined baffle 9.
In this embodiment, preferably, the scraper mechanism 21 includes a servo motor 22 therein, an output end of the servo motor 22 is fixedly connected with a shaft rod 23, the shaft rod 23 is connected with a speed reducer 24, the scraper mechanism 21 further includes a frame, the servo motor 22 is fixedly mounted inside the frame, and an output end of the speed reducer 24 is fixedly connected with a scraper. The effect is that the inner wall of the cylinder 1 can be cleaned by the scraper mechanism 21.
In this embodiment, preferably, the flat cover 25 and the cylinder 1 are fixedly connected by a first connecting flange 26. The effect is that the first connecting flange 26 can achieve a stable connection of the flat cover 25 and the cylinder 1.
In this embodiment, preferably, ear seats 27 are respectively fixedly disposed on two sides of the cylinder 1. The effect is that the setting of the ear mount 27 enables a fixed mounting of the cartridge 1.
In this embodiment, preferably, a jacket 28 is fixedly adhered to the outer side of the cylinder 1. The effect is that the jacket 28 is designed to provide both thermal insulation and protection.
In this embodiment, preferably, the cylinder 1 and the nipple cylinder 2 are fixedly connected through a second connecting flange 29, and the nipple cylinder 2 and the lower cylinder 3 are fixedly connected through a third connecting flange 30. The effect does, and second flange 29 and third flange 30 can realize carrying out fixed mounting to connecting between barrel 1, nipple joint barrel 2 and the lower barrel 3.
In this embodiment, preferably, the heat exchange tubes 18 are provided with a plurality of groups, the first heat transfer oil inlet 11 is fixedly communicated with the first heat transfer oil outlet 12, and the second heat transfer oil inlet 13 is fixedly communicated with the second heat transfer oil outlet 16. The effect is that the heat exchange tube 18 can realize condensing distillation, and the connection of the heat conduction oil port can realize circular conveying.
The use principle and the advantages are as follows:
a feed inlet 20 is arranged above a flat cover 25 of the short-path distiller for organic silicon, a medium is sprayed to a scraper system 21 and flows downwards along the inner wall of a cylinder 1, a jacket 28 is arranged on the outer side of the cylinder 1, heat conduction oil enters a heating cylinder through a first heat conduction oil inlet 11 and a second heat conduction oil inlet 13 and flows out from a first heat conduction oil outlet 12 and a second heat conduction oil outlet 16, cooling water enters from a circulating water inlet 7, flows into a heat exchange pipe 18 on one side through a lower pipe box 17 and reaches the inside of the upper pipe box 17, and then flows back to the lower pipe box 17 through the heat exchange pipe 18 on the other side and flows out from a circulating water outlet 6, so that the effect of reducing the internal temperature of equipment is achieved, part of the medium flows out from a light component outlet 8 under the action of a vacuum port 10, and the rest of the medium flows out from a heavy component outlet 5 through an inclined baffle 9.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (8)

1. A short-range distiller for organic silicon comprises a barrel body (1), and is characterized in that: the heat-conducting oil recovery device is characterized in that a short section cylinder (2) is arranged at the lower part of the cylinder (1), a lower cylinder (3) is fixedly arranged at the bottom of the short section cylinder (2), a bottom plate (4) is fixedly arranged at the bottom of the lower cylinder (3), a light component outlet (5) and a circulating water outlet (6) are fixedly arranged at the lower part of the bottom plate (4), a circulating water inlet (7) is fixedly communicated with one side of the lower cylinder (3), a heavy component outlet (8) is fixedly communicated with one side of the short section cylinder (2), an inclined baffle (9) is fixedly arranged in the short section cylinder (2), a vacuum port (10) is fixedly communicated with one side of the short section cylinder (2), a first heat-conducting oil inlet (11) is fixedly communicated with the lower end of one side of the cylinder (1), a first heat-conducting oil outlet (12) is fixedly communicated with the upper end of one side of the cylinder (1), a second heat-conducting oil inlet (13) is fixedly communicated with the upper end of one side of the cylinder (1), the lower part intercommunication of second conduction oil import (13) is equipped with first drain (14), the fixed shrouding (15) that is equipped with in upper portion of first conduction oil export (12), the fixed intercommunication in one side upper end of barrel (1) has second conduction oil export (16), the upper and lower both ends of barrel (1) are fixed mounting respectively have pipe case (17), fixed intercommunication has heat exchange tube (18) between pipe case (17), the fixed intercommunication in upper end one side of barrel (1) has second drain (19), the upper portion of barrel (1) is fixed and is equipped with flat lid (25), fixed intercommunication has feed inlet (20) on flat lid (25), fixed mounting has scraper blade mechanism (21) on flat lid (25).
2. The short path distiller for organosilicon according to claim 1, wherein: the scraper mechanism (21) comprises a servo motor (22), the output end of the servo motor (22) is fixedly connected with a shaft lever (23), and a speed reducer (24) is connected onto the shaft lever (23).
3. A short path distiller for organosilicon according to claim 2, characterized in that: still including the frame in scraper blade mechanism (21), servo motor (22) fixed mounting is in inside the frame, the output fixedly connected with scraper blade of reduction gear (24).
4. The short path distiller for organosilicon according to claim 1, wherein: the flat cover (25) is fixedly connected with the cylinder body (1) through a first connecting flange (26).
5. The short path distiller for organosilicon according to claim 1, wherein: the two sides of the cylinder body (1) are respectively and fixedly provided with an ear seat (27).
6. The short path distiller for organosilicon according to claim 1, wherein: the outer side of the cylinder body (1) is fixedly adhered with a clamping sleeve (28).
7. The short path distiller for organosilicon according to claim 1, wherein: the barrel (1) is fixedly connected with the short section barrel (2) through a second connecting flange (29), and the short section barrel (2) is fixedly connected with the lower barrel (3) through a third connecting flange (30).
8. The short path distiller for organosilicon according to claim 1, wherein: the heat exchange tubes (18) are provided with a plurality of groups, the first heat conduction oil inlet (11) is fixedly communicated with the first heat conduction oil outlet (12), and the second heat conduction oil inlet (13) is fixedly communicated with the second heat conduction oil outlet (16).
CN202120868788.3U 2021-04-26 2021-04-26 Short-range distiller for organic silicon Active CN214680082U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202120868788.3U CN214680082U (en) 2021-04-26 2021-04-26 Short-range distiller for organic silicon

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202120868788.3U CN214680082U (en) 2021-04-26 2021-04-26 Short-range distiller for organic silicon

Publications (1)

Publication Number Publication Date
CN214680082U true CN214680082U (en) 2021-11-12

Family

ID=78533960

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202120868788.3U Active CN214680082U (en) 2021-04-26 2021-04-26 Short-range distiller for organic silicon

Country Status (1)

Country Link
CN (1) CN214680082U (en)

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