CN213726451U - Morphology-controllable double-sided polymer particle synthesis device - Google Patents

Abstract

The utility model discloses a synthesizing device for shape-controlled double-sided polymer particles, comprising a stirring and mixing device, a rinsing device and a filtering device. One end of the rinsing device is connected with a stirring and mixing device, and the other end of the rinsing device is connected with a filtering device , The inner cavity of the reaction tank is equipped with a double-shaft stirring mechanism, which has a compact structure and is conducive to promotion and use. At the same time, the stirring and dissolving of the polymer are more sufficient, and the stirring efficiency is improved. The heating resistance wire is made of material and has a simple structure, which reduces the time required for polymer synthesis. A brush is installed on the edge of the blade, and the blade drives the brushes arranged on the edges of both sides of the blade to rotate, so that the brush is brushed to rinse the box. The residue on the inner wall saves manpower and is fully rinsed, so that the polymer particles are evenly contacted, and the polymer is filtered through the filter tank, so as to reduce the environmental pollution caused by harmful solvents generated during the polymer synthesis process, and improve the practicability of the device.

Description

Morphology-controllable double-sided polymer particle synthesis device

Technical Field

The utility model relates to a controllable two-sided polymer particle equipment technical field of appearance specifically is a synthesizer of controllable two-sided polymer particle of appearance.

Background

A double-sided microparticle refers to a type of microparticle in which the two spherical surfaces of the particle have different compositions, properties, or structures. This anisotropic and asymmetric structure makes it very versatile, but also makes its preparation difficult. The environment-responsive amphiphilic polymer particles as the solid surfactant not only have stronger interfacial adsorption capacity and more efficient emulsification performance than homogeneous polymer particles, but also can realize the rapid phase transition of emulsion through the rapid response to environmental stimuli (pH value, temperature, ionic strength and the like). The latex particles with carboxylate radicals or amine radicals on the surface are also a good high molecular material, can be used for preparing novel organic-inorganic composite materials with excellent performance by compounding surface functional groups and inorganic nano particles, and have wide application in the fields of solid surfactants, drug controlled release, intelligent coatings, interface catalysis and the like.

The existing synthesis device of the double-sided polymer particles with controllable shapes occupies a large area, wastes space, has overlong polymer reaction time and insufficient reaction, and is attached with a solvent harmful to the environment.

This synthesizer of controllable two-sided polymer particle of appearance, biax rabbling mechanism is installed to the inner chamber of retort, compact structure, be favorable to promoting and use, make the stirring of polymer more abundant with dissolving simultaneously, the efficiency of stirring is improved, the zone of heating is installed in the outside of retort, the required time of polymer synthesis has been reduced, the brush is installed at the edge of blade, the blade drives the brush rotation that sets up at blade both sides edge, make the brush remove the residue on the rinsing box inner wall, abundant rinsing, make polymer particle even contact, filter the polymer through filtering the jar, alleviate the pollution of the harmful solvent that produces to the environment among the polymer synthesis process.

SUMMERY OF THE UTILITY MODEL

The utility model aims to provide a synthesis device of double-sided polymer particles with controllable appearance, a double-shaft stirring mechanism is arranged in the inner cavity of a reaction tank, the structure is compact, the popularization and the use are facilitated, meanwhile, the stirring and dissolving of the polymer are more sufficient, the stirring efficiency is improved, the heating layer is arranged on the outer side of the reaction tank, the time required by the synthesis of the polymer is reduced, the hairbrushes are arranged on the edges of the blades, the blades drive the hairbrushes arranged on the edges of the two sides of the blades to rotate, so that the hairbrushes brush residues on the inner wall of the rinsing tank body, the rinsing is performed fully, and polymer particles are in uniform contact, the polymer is filtered by the filter tank, so that the pollution of harmful solvents to the environment in the polymer synthesis process is reduced, and the problems that in the prior art, the occupied area of equipment is large, the space is wasted, the polymer reaction time is too long, the reaction is insufficient, and the solvents harmful to the environment are attached to the synthesized polymer particles are solved.

In order to achieve the above object, the utility model provides a following technical scheme: a synthesis device of morphology-controllable double-sided polymer particles comprises a stirring and mixing device, a rinsing device and a filtering device, wherein one end of the rinsing device is connected with the stirring and mixing device, the other end of the rinsing device is connected with the filtering device, the stirring and mixing device comprises a reaction tank, a first stirring mechanism, a second stirring mechanism, a first feeding hole, a heat preservation box body, a first discharging hole and a first electromagnetic valve, the reaction tank is installed in the inner cavity of the heat preservation box body, the first feeding hole is formed in the upper end of the reaction tank, the first stirring mechanism and the second stirring mechanism are installed in the inner cavity of the reaction tank, the first discharging hole is formed in the lower end of the reaction tank, and the first electromagnetic valve is installed at the lower end of the first discharging hole;

the rinsing device comprises a rinsing box body, a second feeding hole, a rinsing mechanism, a first connecting pipe, a second electromagnetic valve and a water pump, wherein the first connecting pipe is connected to one side, close to the stirring and mixing device, of the rinsing mechanism, the second connecting pipe is connected to one side, close to the filtering device, of the rinsing mechanism, the second electromagnetic valve and the water pump are installed on the second connecting pipe, the second feeding hole is formed in the upper end of the rinsing box body, and the rinsing mechanism is installed in the inner cavity of the rinsing box body;

the filter device comprises a feeding pipeline, a supporting pipeline, a filter tank, a collecting box body, a discharge pipeline and a third electromagnetic valve, wherein the lower end of the feeding pipeline is connected with the supporting pipeline, the support pipeline is connected with the filter tank, the lower end of the supporting pipeline is connected with the collecting box body, the side end of the collecting box body is connected with the discharge pipeline, and the third electromagnetic valve is installed on the discharge pipeline.

Further, a heating layer is installed on the outer side of the reaction tank, and the heating layer is made of a material of a heating resistance wire.

Further, rinsing mechanism includes driving motor, axis of rotation, blade and brush, driving motor's lower extreme is connected with the axis of rotation, installs the blade in the axis of rotation, and the brush is installed at the edge of blade.

Further, the filter tank comprises an upper filter pipeline, a tank body and a lower filter pipeline, the upper end of the tank body is connected with the upper filter pipeline, and the lower end of the tank body is connected with the lower filter pipeline.

Further, the jar body is including jar body, filter layer and litter are installed to the inner chamber of jar body, the upper end of filter layer is provided with the litter.

Compared with the prior art, the beneficial effects of the utility model are as follows:

1. the utility model provides a synthesizer of controllable two-sided polymer particle of appearance, first rabbling mechanism and second rabbling mechanism are installed to the inner chamber of retort, biax stirring compact structure has reduced the equipment volume, practice thrift the space, be favorable to promoting and using, make the stirring of polymer more abundant with dissolving simultaneously, the efficiency of stirring has been improved, the zone of heating is installed in the outside of retort, the zone of heating chooses the material of heating resistor silk for use to make, moreover, the steam generator is simple in structure, high durability and convenient use, the required time of polymer synthesis has been reduced.

2. The utility model provides a synthesizer of controllable two-sided polymer particle of appearance, driving motor's lower extreme is connected with the axis of rotation, installs the blade in the axis of rotation, and the brush is installed at the edge of blade, and the blade drives the brush that sets up at blade both sides edge and rotates, makes the brush remove the residue on the rinsing box inner wall, practices thrift the manpower, and abundant rinsing makes polymer particle evenly contact.

3. The utility model provides a synthesizer of controllable two-sided polymer particle of appearance filters the polymer through filtering the jar, alleviates the harmful solvent that produces in the polymer synthesis process to the pollution of environment, improves the practicality of device.

Drawings

FIG. 1 is an overall cross-sectional view of the present invention;

FIG. 2 is a cross-sectional view of the stirring and mixing device of the present invention;

FIG. 3 is a cross-sectional view of the rinsing apparatus of the present invention;

FIG. 4 is a cross-sectional view of the rinsing mechanism of the present invention;

FIG. 5 is a cross-sectional view of the filter assembly of the present invention;

fig. 6 is a cross-sectional view of the filter tank of the present invention.

In the figure: 1. a stirring and mixing device; 11. a reaction tank; 111. a heating layer; 12. a first stirring mechanism; 13. a second stirring mechanism; 14. a first feed port; 15. a heat preservation box body; 16. a first discharge port; 17. a first solenoid valve; 2. a rinsing device; 21. rinsing the box body; 22. a second feed port; 23. a rinsing mechanism; 231. a drive motor; 232. a rotating shaft; 233. a blade; 234. a brush; 24. a first connecting pipe; 25. a second connecting pipe; 26. a second solenoid valve; 27. a water pump; 3. a filtration device; 31. a feed conduit; 32. supporting the pipeline; 33. a filter tank; 331. an upper filtering pipe; 332. a tank body; 3321. a tank body; 3322. a filter layer; 3323. a floating rod; 333. a lower filter conduit; 34. a collection box body; 35. a discharge conduit; 36. and a third solenoid valve.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.

Referring to fig. 1-2, a morphology-controllable double-sided polymer particle synthesizer comprises a stirring and mixing device 1, a rinsing device 2 and a filtering device 3, wherein one end of the rinsing device 2 is connected with the stirring and mixing device 1, the other end of the rinsing device 2 is connected with the filtering device 3, the stirring and mixing device 1 comprises a reaction tank 11, a first stirring mechanism 12, a second stirring mechanism 13, a first feed inlet 14, a heat preservation box body 15, a first discharge outlet 16 and a first electromagnetic valve 17, a reaction tank 11 is installed in the inner cavity of the heat preservation box body 15, a heating layer 111 is installed on the outer side of the reaction tank 11, the heating layer 111 is made of a heating resistance wire, the structure is simple, the use is convenient, the time required by polymer synthesis is reduced, the first feed inlet 14 is formed in the upper end of the reaction tank 11, the first stirring mechanism 12 and the second stirring mechanism 13 are installed in the inner cavity of the reaction tank 11, the double-shaft stirring structure is compact, the equipment volume is reduced, the space is saved, the popularization and the use are facilitated, the stirring and the dissolution of the polymer are more sufficient, the stirring efficiency is improved, the lower end of the reaction tank 11 is provided with the first discharge port 16, and the lower end of the first discharge port 16 is provided with the first electromagnetic valve 17.

Referring to fig. 3-4, a morphology-controllable double-sided polymer particle synthesizer, a rinsing device 2 includes a rinsing tank 21, a second feed inlet 22, a rinsing mechanism 23, a first connection pipe 24, a second connection pipe 25, a second electromagnetic valve 26 and a water pump 27, the first connection pipe 24 is connected to one side of the rinsing mechanism 23 close to the stirring and mixing device 1, the second connection pipe 25 is connected to one side of the rinsing mechanism 23 close to the filtering device 3, the second electromagnetic valve 26 and the water pump 27 are installed on the second connection pipe 25, the rinsing mechanism 23 includes a driving motor 231, a rotating shaft 232, a blade 233 and a brush 234, the lower end of the driving motor 231 is connected to the rotating shaft 232, the blade 233 is installed on the rotating shaft 232, a brush 234 is installed on the edge of the blade 233, the blade 233 drives the brushes 234 installed on the edges of the two sides of the blade 233 to rotate, so that the brushes 234 brush off residues on the inner wall of the rinsing tank 21, the manpower is saved, the rinsing is fully carried out, the polymer particles are uniformly contacted, the second feeding hole 22 is formed in the upper end of the rinsing box body 21, and the rinsing mechanism 23 is installed in the inner cavity of the rinsing box body 21.

Referring to fig. 5-6, a morphology-controllable double-sided polymer particle synthesis device, a filter device 3 includes a feeding pipe 31, a supporting pipe 32, a filter tank 33, a collection box 34, a discharge pipe 35 and a third electromagnetic valve 36, the lower end of the feeding pipe 31 is connected with the supporting pipe 32, the supporting pipe 32 is connected with the filter tank 33, the filter tank 33 includes an upper filter pipe 331, a tank body 332 and a lower filter pipe 333, the upper end of the tank body 332 is connected with the upper filter pipe 331, the lower end of the tank body 332 is connected with the lower filter pipe 333, the tank body 332 includes a tank body 3321, a filter layer 3322 and a float rod 3323, the inner cavity of the tank body 3321 is provided with the filter layer 3322 and the float rod 3323, the upper end of the filter layer 3322 is provided with the float rod 3323 for filtering polymer, thereby reducing the pollution of harmful solvent generated in the polymer synthesis process to the environment, improving the practicability of the device, the lower end of the supporting pipe 32 is connected with the collection box 34, a discharge pipe 35 is connected to a side end of the collection tank 34, and a third electromagnetic valve 36 is installed on the discharge pipe 35.

In summary, the following steps: the utility model provides a controllable two-sided polymer particle's of appearance synthesizer, including stirring mixing arrangement 1, rinsing device 2 and filter equipment 3, the one end of rinsing device 2 is connected with stirring mixing arrangement 1, the other end of rinsing device 2 is connected with filter equipment 3, first rabbling mechanism 12 and second rabbling mechanism 13 are installed to the inner chamber of retort 11, the biax stirring compact structure, the equipment volume has been reduced, save space, be favorable to promoting and using, make the stirring and the dissolution of polymer more abundant simultaneously, the efficiency of stirring is improved, the outside of retort 11 is installed heating layer 111, heating layer 111 chooses for use the material of heating resistor silk to make, simple structure, high durability and convenient use, the required time of polymer synthesis has been reduced, the lower extreme of driving motor 231 is connected with axis of rotation 232, install blade 233 on the axis of rotation 232, the brush 234 is installed to the edge of blade 233, the blade 233 drives the brush 234 arranged at the edges of both sides of the blade 233 to rotate, so that the brush 234 brushes away the residues on the inner wall of the rinsing box 21, manpower is saved, the rinsing is sufficient, polymer particles are uniformly contacted, the polymer is filtered through the filtering tank 33, the pollution of harmful solvents generated in the polymer synthesis process to the environment is reduced, and the practicability of the device is improved.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (5)

1. A device for synthesizing double-sided polymer particles with controllable morphology, comprising a stirring and mixing device (1), a rinsing device (2) and a filtering device (3), wherein one end of the rinsing device (2) is connected with a stirring and mixing device Device (1), the other end of the rinsing device (2) is connected with a filtering device (3), characterized in that: the stirring and mixing device (1) comprises a reaction tank (11), a first stirring mechanism (12), The second stirring mechanism (13), the first feed port (14), the heat preservation box (15), the first discharge port (16) and the first solenoid valve (17), the heat preservation box (15) A reaction tank (11) is installed in the inner cavity, the upper end of the reaction tank (11) is provided with a first feeding port (14), and the inner cavity of the reaction tank (11) is equipped with a first stirring mechanism (12) and a second stirring mechanism (12) a stirring mechanism (13), the lower end of the reaction tank (11) is provided with a first discharge port (16), and the lower end of the first discharge port (16) is provided with a first solenoid valve (17); The rinsing device (2) comprises a rinsing box (21), a second feeding port (22), a rinsing mechanism (23), a first connecting pipe (24), a second connecting pipe (25), and a second solenoid valve (26) and a water pump (27), a first connecting pipe (24) is connected to the side of the rinsing mechanism (23) close to the stirring and mixing device (1), and the rinsing mechanism (23) is close to the filter device (3). One side is connected with a second connecting pipe (25), a second solenoid valve (26) and a water pump (27) are installed on the second connecting pipe (25), and a second inlet is provided on the upper end of the rinsing box (21). a material port (22), a rinsing mechanism (23) is installed in the inner cavity of the rinsing box (21); The filtering device (3) includes a feed pipe (31), a support pipe (32), a filter tank (33), a collection box (34), a discharge pipe (35) and a third solenoid valve (36), the A support pipe (32) is connected to the lower end of the feed pipe (31), a filter tank (33) is connected to the support pipe (32), and a collection box (34) is connected to the lower end of the support pipe (32). A discharge pipe (35) is connected to the side end of the body (34), and a third solenoid valve (36) is installed on the discharge pipe (35). 2. The apparatus for synthesizing double-sided polymer particles with controllable morphology according to claim 1, characterized in that: a heating layer (111) is installed on the outside of the reaction tank (11), and the heating layer (111) It is a component made of the material of a heating resistance wire. 3 . The apparatus for synthesizing double-sided polymer particles with controllable morphology according to claim 1 , wherein the rinsing mechanism ( 23 ) comprises a driving motor ( 231 ), a rotating shaft ( 232 ), a blade ( 233) and a brush (234), a rotating shaft (232) is connected to the lower end of the drive motor (231), a blade (233) is installed on the rotating shaft (232), and a brush (233) is installed on the edge of the blade (233). 234). 4. The apparatus for synthesizing double-sided polymer particles with controllable morphology according to claim 1, characterized in that: the filter tank (33) comprises an upper filter pipe (331), a tank body (332) and a lower filter tank (332). A filter pipe (333), an upper filter pipe (331) is connected to the upper end of the tank body (332), and a lower filter pipe (333) is connected to the lower end of the tank body (332). 5 . The apparatus for synthesizing double-sided polymer particles with controllable morphology according to claim 4 , wherein the tank body ( 332 ) comprises a tank body ( 3321 ), a filter layer ( 3322 ) and a floating A rod (3323), a filter layer (3322) and a floating rod (3323) are installed in the inner cavity of the tank body (3321), and a floating rod (3323) is provided on the upper end of the filter layer (3322).

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