CN211189761U - A nanofiltration device for the recovery of amikacin waste ammonia water - Google Patents

A nanofiltration device for the recovery of amikacin waste ammonia water Download PDF

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CN211189761U
CN211189761U CN201922090004.4U CN201922090004U CN211189761U CN 211189761 U CN211189761 U CN 211189761U CN 201922090004 U CN201922090004 U CN 201922090004U CN 211189761 U CN211189761 U CN 211189761U
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ammonia water
waste
nanofiltration
liquid outlet
waste ammonia
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张茂华
蒋永飞
倪行辉
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Fujian Kanghong Biotechnology Co ltd
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Abstract

本实用新型公开了一种用于阿米卡星废氨水回收的纳滤装置,包括废氨水罐、输送泵、纳滤系统、饮用水管、脱氨废水管和氨水回收罐,废氨水罐出液口连接输送泵进液口,输送泵出液口连接纳滤系统进液口,纳滤系统出液口分别与废氨水罐和氨水回收罐的进液口连接,饮用水管与纳滤系统进液口连接,纳滤系统出液口与脱氨废水管连接,本实用新型能够回收氨水的同时,最低限度地向污水处理系统排放污水,并且设备简单、能耗小、运行维护成本低。

Figure 201922090004

The utility model discloses a nanofiltration device for recycling amikacin waste ammonia water. The liquid port is connected to the liquid inlet of the transfer pump, the liquid outlet of the transfer pump is connected to the liquid inlet of the nanofiltration system, the liquid outlet of the nanofiltration system is respectively connected to the liquid inlet of the waste ammonia water tank and the ammonia water recovery tank, and the drinking water pipe is connected to the nanofiltration system The liquid inlet is connected, and the liquid outlet of the nanofiltration system is connected with the deamination waste water pipe. The utility model can recycle ammonia water and discharge sewage to the sewage treatment system at a minimum, and has simple equipment, low energy consumption and low operation and maintenance cost.

Figure 201922090004

Description

一种用于阿米卡星废氨水回收的纳滤装置A nanofiltration device for the recovery of amikacin waste ammonia water

技术领域:Technical field:

本实用新型涉及生物医药技术领域,尤其涉及一种用于阿米卡星废氨水回收的纳滤装置。The utility model relates to the technical field of biomedicine, in particular to a nanofiltration device for recycling amikacin waste ammonia water.

背景技术:Background technique:

在生物医药行业中,离子交换树脂应用广泛。离子交换树脂是一类具有离子交换功能的高分子材料,在溶液中它能将本身的离子与溶液中的同号离子进行交换。离子交换树脂吸附各种离子的能力不一,有些离子易被交换树脂吸附,但吸着后要把它置换下来就比较困难;而另一些离子很难被吸着,但被置换下来却比较容易,这种性能称为离子交换的选择性。In the biomedical industry, ion exchange resins are widely used. Ion exchange resin is a kind of polymer material with ion exchange function, which can exchange its own ions with the same ions in the solution in solution. The ability of ion exchange resin to adsorb various ions varies. Some ions are easily adsorbed by the exchange resin, but it is more difficult to replace them after adsorption; while other ions are difficult to be adsorbed, but it is easier to be replaced. This property is called the selectivity of ion exchange.

阿米卡星在合成过程中会产生大量结构相近的杂质,常规分离方法无法进行有效分离,离子交换树脂对不同物质的基团的有着不同的的吸附能力,利用不同浓度的氨水对各组分实现洗脱分离。Amikacin will produce a large number of impurities with similar structures during the synthesis process, which cannot be effectively separated by conventional separation methods. Elution separation is achieved.

在洗脱前期、不同组分切换间隙、洗脱之后用水清洗树脂柱这三个阶段均有大量废氨水产生,若让这部分废氨水进入污水处理系统,则会产生大量的处理费用。由于这部分废氨水含有其他大分子杂质如色素等,不能直接在生产上使用。目前常规氨回收系统的主设备为蒸氨塔,其缺点是系统复杂、设备多、能耗大、运行维护成本高,且蒸氨塔只是回收氨气用于重新配制,蒸氨后产生的大量废水还是要进入污水系统处理。A large amount of waste ammonia water is produced in the three stages of pre-elution, switching between different components, and washing the resin column with water after elution. If this part of waste ammonia is allowed to enter the sewage treatment system, a large amount of treatment costs will be incurred. Since this part of waste ammonia contains other macromolecular impurities such as pigments, it cannot be used directly in production. At present, the main equipment of the conventional ammonia recovery system is the ammonia distillation tower. Wastewater still has to go into the sewage system for treatment.

实用新型内容:Utility model content:

针对上述问题,本实用新型要解决的技术问题是提供一种用于阿米卡星废氨水回收的纳滤装置,包括废氨水罐、输送泵、纳滤系统、饮用水管、脱氨废水管和氨水回收罐,所述废氨水罐出液口连接输送泵进液口,所述输送泵出液口连接纳滤系统进液口,所述纳滤系统出液口分别与废氨水罐和氨水回收罐的进液口连接,所述饮用水管与纳滤系统进液口连接,所述纳滤系统出液口与脱氨废水管连接,所述纳滤系统内设置有纳滤膜。In view of the above problems, the technical problem to be solved by this utility model is to provide a nanofiltration device for recycling amikacin waste ammonia water, including a waste ammonia water tank, a transfer pump, a nanofiltration system, a drinking water pipe, and a deamination waste water pipe and the ammonia water recovery tank, the liquid outlet of the waste ammonia water tank is connected to the liquid inlet of the transfer pump, the liquid outlet of the transfer pump is connected to the liquid inlet of the nanofiltration system, and the liquid outlet of the nanofiltration system is respectively connected with the waste ammonia water tank and the ammonia water. The liquid inlet of the recovery tank is connected, the drinking water pipe is connected with the liquid inlet of the nanofiltration system, the liquid outlet of the nanofiltration system is connected with the deamination waste water pipe, and the nanofiltration system is provided with a nanofiltration membrane.

优选的,所述脱氨废水管连接至污水处理系统。Preferably, the deamination waste water pipe is connected to a sewage treatment system.

优选的,所述纳滤系统出液口通过管线与废氨水罐进液口连接。Preferably, the liquid outlet of the nanofiltration system is connected to the liquid inlet of the waste ammonia water tank through a pipeline.

本实用新型有益效果:本实用新型中废氨水罐内废氨水通过输送泵进入纳滤系统,其中绝大部分氨和水能透过纳滤膜,并流入氨水回收罐,色素等大分子杂质随少量水回流至废氨水罐内;经过一段时间的纳滤浓缩,废氨水罐内剩余色素等大分子组分、少量水和氨,由于浓度过高无法再透过纳滤膜,此时开启纳滤系统饮用水进管,利用饮用水将剩余的少量氨透过纳滤膜,并进入氨水回收罐。本实用新型装置同时回收了氨和水,最大限度地减少了污水系统压力和处理成本。Beneficial effects of the utility model: In the utility model, the waste ammonia water in the waste ammonia water tank enters the nanofiltration system through the conveying pump, and most of the ammonia and water can pass through the nanofiltration membrane and flow into the ammonia water recovery tank. A small amount of water is returned to the waste ammonia water tank; after a period of nanofiltration concentration, the remaining macromolecular components such as pigments, a small amount of water and ammonia in the waste ammonia water tank can no longer pass through the nanofiltration membrane due to the high concentration, and the nanofiltration membrane is turned on at this time. Filter system drinking water into the pipe, use drinking water to pass the remaining small amount of ammonia through the nanofiltration membrane, and enter the ammonia water recovery tank. The device of the utility model recycles ammonia and water at the same time, and minimizes the pressure of the sewage system and the treatment cost.

附图说明:Description of drawings:

为了易于说明,本实用新型由下述的具体实施及附图作以详细描述。For ease of description, the present invention is described in detail by the following specific implementation and accompanying drawings.

图1为本实用新型整体结构示意图。Figure 1 is a schematic diagram of the overall structure of the utility model.

图中:1-废氨水罐;2-输送泵;3-纳滤系统;4-管线;5-饮用水管;6-脱氨废水管;7-氨水回收罐。In the figure: 1-waste ammonia water tank; 2-transport pump; 3-nanofiltration system; 4-pipeline; 5-drinking water pipe; 6-deamination waste water pipe; 7-ammonia water recovery tank.

具体实施方式:Detailed ways:

为使本实用新型的目的、技术方案和优点更加清楚明了,下面通过附图中示出的具体实施例来描述本实用新型。但是应该理解,这些描述只是示例性的,而并非要限制本实用新型的范围。此外,在以下说明中,省略了对公知结构和技术的描述,以避免不必要地混淆本实用新型的概念。In order to make the objectives, technical solutions and advantages of the present utility model more clear, the present utility model will be described below through the specific embodiments shown in the accompanying drawings. It should be understood, however, that these descriptions are only exemplary and are not intended to limit the scope of the present invention. Also, in the following description, descriptions of well-known structures and techniques are omitted to avoid unnecessarily obscuring the concepts of the present invention.

如图1所示,本实用新型的一种用于阿米卡星废氨水回收的纳滤装置,包括废氨水罐1、输送泵2、纳滤系统3、饮用水管5、脱氨废水管6和氨水回收罐7,所述废氨水罐1出液口连接输送泵2进液口,所述输送泵2出液口连接纳滤系统3进液口,所述纳滤系统3出液口分别与废氨水罐1和氨水回收罐7的进液口连接,所述饮用水管5与纳滤系统3进液口连接,所述纳滤系统3出液口与脱氨废水管6连接,所述纳滤系统3内设置有纳滤膜。As shown in Figure 1, a kind of nanofiltration device for amikacin waste ammonia water recycling of the present utility model comprises waste ammonia water tank 1, delivery pump 2, nanofiltration system 3, drinking water pipe 5, deamination waste water pipe 6 and the ammonia water recovery tank 7, the liquid outlet of the waste ammonia water tank 1 is connected to the liquid inlet of the delivery pump 2, the liquid outlet of the delivery pump 2 is connected to the liquid inlet of the nanofiltration system 3, and the liquid outlet of the nanofiltration system 3 are respectively connected with the liquid inlets of the waste ammonia water tank 1 and the ammonia water recovery tank 7, the drinking water pipe 5 is connected with the liquid inlet of the nanofiltration system 3, and the liquid outlet of the nanofiltration system 3 is connected with the deamination waste water pipe 6, The nanofiltration system 3 is provided with a nanofiltration membrane.

具体地,脱氨废水管6连接至污水处理系统,纳滤系统3出液口通过管线与废氨水罐1进液口连接。Specifically, the deamination waste water pipe 6 is connected to the sewage treatment system, and the liquid outlet of the nanofiltration system 3 is connected to the liquid inlet of the waste ammonia water tank 1 through a pipeline.

其工作原理:使用时,废氨水罐1内料液通过输送泵2进入纳滤系统3,绝大部分氨和水透过纳滤膜进入氨水回收罐7,色素等大分子组分随着少量的水和氨通过管线4回流至废氨水罐1,经过一段时间纳滤浓缩后,废氨水罐1内剩余高浓度的色素等大分子组分,以及少量的水和氨,由于浓度过高已经无法再透过纳滤膜。此时开启纳滤系统3进液口的的饮用水管5,利用饮用水的稀释作用将剩余的少量氨透过纳滤膜,并进入氨水回收罐7。完成氨水回收后,将剩余含有色素等大分子杂质的少量废水通过脱氨废水管6排放至污水处理系统。Its working principle: When in use, the feed liquid in the waste ammonia water tank 1 enters the nanofiltration system 3 through the conveying pump 2, and most of the ammonia and water enter the ammonia water recovery tank 7 through the nanofiltration membrane, and the macromolecular components such as pigments flow with a small amount. The water and ammonia returned to the waste ammonia water tank 1 through the pipeline 4, after a period of nanofiltration concentration, the remaining high concentration of pigments and other macromolecular components in the waste ammonia water tank 1, as well as a small amount of water and ammonia, due to the high concentration. can no longer pass through the nanofiltration membrane. At this time, open the drinking water pipe 5 of the liquid inlet of the nanofiltration system 3, and use the dilution effect of drinking water to pass the remaining small amount of ammonia through the nanofiltration membrane and enter the ammonia water recovery tank 7. After the recovery of ammonia water is completed, the remaining small amount of waste water containing macromolecular impurities such as pigments is discharged to the sewage treatment system through the deamination waste water pipe 6 .

以上显示和描述了本实用新型的基本原理和主要特征和本实用新型的优点。本行业的技术人员应该了解,本实用新型不受上述实施例的限制,上述实施例和说明书中描述的只是说明本实用新型的原理,在不脱离本实用新型精神和范围的前提下,本实用新型还会有各种变化和改进,这些变化和改进都落入要求保护的本实用新型范围内。本实用新型要求保护范围由所附的权利要求书及其等效物界定。The basic principles and main features of the present invention and the advantages of the present invention are shown and described above. It should be understood by those skilled in the art that the present invention is not limited by the above-mentioned embodiments. The above-mentioned embodiments and descriptions only illustrate the principle of the present invention. Without departing from the spirit and scope of the present invention, the present invention There will also be various changes and improvements in the new model, which all fall within the scope of the claimed invention. The claimed scope of the present invention is defined by the appended claims and their equivalents.

Claims (3)

1. The utility model provides a receive filter equipment for amikacin waste ammonia water retrieves, its characterized in that, include waste ammonia water jar, delivery pump, receive filtration system, drinking water pipe, deamination waste water pipe and ammonia recovery tank, the delivery pump inlet is connected to waste ammonia water jar liquid outlet, the delivery pump outlet is connected and is received the filtration system inlet, receive the filtration system liquid outlet and be connected with waste ammonia water jar and ammonia recovery tank's inlet respectively, the drinking water pipe is connected with the nanofiltration system inlet, receive the filtration system liquid outlet and be connected with the deamination waste water pipe, be provided with in the nanofiltration system and receive the filter membrane.
2. The nanofiltration device for recycling amikacin waste ammonia water according to claim 1, wherein the nanofiltration device comprises: the deamination wastewater pipe is connected to a sewage treatment system.
3. The nanofiltration device for recycling amikacin waste ammonia water according to claim 1, wherein the nanofiltration device comprises: and the liquid outlet of the nanofiltration system is connected with the liquid inlet of the waste ammonia water tank through a pipeline.
CN201922090004.4U 2019-11-28 2019-11-28 A nanofiltration device for the recovery of amikacin waste ammonia water Active CN211189761U (en)

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