CN210495300U - Crystallization kettle for valine synthesis - Google Patents
Crystallization kettle for valine synthesis Download PDFInfo
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- CN210495300U CN210495300U CN201920988490.9U CN201920988490U CN210495300U CN 210495300 U CN210495300 U CN 210495300U CN 201920988490 U CN201920988490 U CN 201920988490U CN 210495300 U CN210495300 U CN 210495300U
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- 238000002425 crystallisation Methods 0.000 title claims abstract description 55
- 230000008025 crystallization Effects 0.000 title claims abstract description 55
- KZSNJWFQEVHDMF-BYPYZUCNSA-N L-valine Chemical compound CC(C)[C@H](N)C(O)=O KZSNJWFQEVHDMF-BYPYZUCNSA-N 0.000 title claims abstract description 27
- KZSNJWFQEVHDMF-UHFFFAOYSA-N Valine Natural products CC(C)C(N)C(O)=O KZSNJWFQEVHDMF-UHFFFAOYSA-N 0.000 title claims abstract description 26
- 239000004474 valine Substances 0.000 title claims abstract description 26
- 230000015572 biosynthetic process Effects 0.000 title claims abstract description 21
- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 47
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- 235000015334 Phyllostachys viridis Nutrition 0.000 claims description 7
- 239000011425 bamboo Substances 0.000 claims description 7
- 238000009434 installation Methods 0.000 claims description 6
- 238000012856 packing Methods 0.000 claims description 6
- 229910001220 stainless steel Inorganic materials 0.000 claims description 6
- 239000010935 stainless steel Substances 0.000 claims description 6
- 238000009833 condensation Methods 0.000 claims description 5
- 230000005494 condensation Effects 0.000 claims description 5
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 3
- 229910052802 copper Inorganic materials 0.000 claims description 3
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- 238000005859 coupling reaction Methods 0.000 claims description 3
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- 239000011229 interlayer Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- AGPKZVBTJJNPAG-WHFBIAKZSA-N L-isoleucine Chemical compound CC[C@H](C)[C@H](N)C(O)=O AGPKZVBTJJNPAG-WHFBIAKZSA-N 0.000 description 1
- ROHFNLRQFUQHCH-YFKPBYRVSA-N L-leucine Chemical compound CC(C)C[C@H](N)C(O)=O ROHFNLRQFUQHCH-YFKPBYRVSA-N 0.000 description 1
- ROHFNLRQFUQHCH-UHFFFAOYSA-N Leucine Natural products CC(C)CC(N)C(O)=O ROHFNLRQFUQHCH-UHFFFAOYSA-N 0.000 description 1
- 208000010428 Muscle Weakness Diseases 0.000 description 1
- 206010028372 Muscular weakness Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 150000005693 branched-chain amino acids Chemical class 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000020776 essential amino acid Nutrition 0.000 description 1
- 239000003797 essential amino acid Substances 0.000 description 1
- 230000002394 glycogenic effect Effects 0.000 description 1
- 229960000310 isoleucine Drugs 0.000 description 1
- AGPKZVBTJJNPAG-UHFFFAOYSA-N isoleucine Natural products CCC(C)C(N)C(O)=O AGPKZVBTJJNPAG-UHFFFAOYSA-N 0.000 description 1
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- 238000000034 method Methods 0.000 description 1
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- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
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- 231100000765 toxin Toxicity 0.000 description 1
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Abstract
The utility model discloses a crystallization kettle for valine synthesis, which comprises a kettle body, wherein a crystallization device is arranged at the lower part of the kettle body, the crystallization device comprises a crystallization cylinder, a temperature control device and a crystal making rolling frame, the temperature control device comprises a heater, a circulating pump, a water tank and a condensing pipe, one side of the kettle body is provided with a case, the inside of the case is provided with the water tank, one side of the water tank is provided with the heater, one side of the heater is provided with the circulating pump, and a water outlet of the case is connected with a water inlet of the heater through a water pipe; this crystallization kettle for valine synthesis has realized the integration of system crystal and ejection of compact structure through crystallization device, temperature control device and the discharging device who sets up, not only makes the structure simpler, convenient to use moreover, and system crystal efficiency is higher, especially adopts the system crystal to roll the mode that frame and temperature control device combine, through the centrifugation to the material with higher speed and accurate temperature control, not only makes system crystal control more convenient, makes system crystal speed faster moreover.
Description
Technical Field
The utility model relates to a crystallization kettle field is used in the valine synthesis, specifically is a crystallization kettle is used in the valine synthesis.
Background
Valine is one of eight essential amino acids in human body, and can be synthesized by using isobutyraldehyde as raw material. Is white crystal or crystalline powder, is soluble in water, and is hardly soluble in ethanol. Valine, one of the 20 amino acids constituting proteins, has the chemical name of 2-amino-3-methylbutyric acid, belongs to a branched chain amino acid, and is also an essential 8 amino acids and a glycogenic amino acid for the human body, and works with other two high-concentration amino acids (isoleucine and leucine) to promote the normal growth of the body, repair tissues, regulate blood glucose, and supply required energy. Valine can provide additional energy to the muscle to produce glucose when engaged in strenuous physical activity to prevent muscle weakness. It also helps to clear excess nitrogen (potential toxins) from the liver and to transport the body's required nitrogen to various sites.
The crystallization kettle is a crystallization device which needs chilled water or refrigerant water to be rapidly cooled in an interlayer after material mixing reaction, and the key links of the crystallization kettle are the size of the area of the interlayer, the structural form and the material outlet form of a stirrer, high-precision polishing in a tank body and the requirement of no dead angle in cleaning in the tank body so as to meet the use conditions of the process.
The crystallization kettle for valine synthesis is an important device in the production process of valine, and the existing crystallization kettle for valine synthesis usually has the problems of low crystallization efficiency, complex equipment and inconvenience in use, so that the new crystallization kettle for valine synthesis is needed.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a crystallization kettle is used in valine synthesis to solve the problem that proposes in the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme:
a crystallization kettle for valine synthesis comprises a kettle body, wherein a crystallization device is arranged at the lower part of the kettle body and comprises a crystallization cylinder, a temperature control device and a crystal making rolling frame, the temperature control device comprises a heater, a circulating pump, a water tank and a condenser pipe, a machine box is arranged at one side of the kettle body, the water tank is arranged in the machine box, the heater is arranged at one side of the water tank, the circulating pump is arranged at one side of the heater, a water outlet of the machine box is connected with a water inlet of the heater through a water pipe, a water outlet of the heater is connected with a water inlet of the circulating pump through a water pipe, the condenser pipe is arranged at the outer side of the front part of the crystallization cylinder, and; a crystal making rolling frame is arranged in the front part of the crystallization cylinder and at a position corresponding to the condensing pipe; the rear portion of a crystallization section of thick bamboo is provided with discharging device, and discharging device includes ejection of compact motor, discharge gate, discharging pipe, auger and connecting axle, ejection of compact motor passes through bolt and nut to be fixed at the rear portion of a crystallization section of thick bamboo, and the front side of ejection of compact motor is provided with the auger, and the center of auger is provided with the connecting axle, and the rear portion of a crystallization section of thick bamboo is provided with the installation through-hole, and the rear end of connecting axle passes the installation through-hole and passes through the pivot of shaft coupling and ejection of compact motor and connect, the bottom position of the crystallization section of.
As a further aspect of the present invention: the water tank, the heater and the circulating pump are fixed in the case through bolts and nuts; the condenser pipe is made of copper.
As a further aspect of the present invention: the crystal making rolling frame is made of stainless steel, the crystal making rolling frame is of a cylindrical brush structure and comprises a shaft sleeve and a crystal needle, and the crystal needle is welded on the shaft sleeve along the radial direction.
As a further aspect of the present invention: the packing auger is a stainless steel packing auger.
As a further aspect of the present invention: the front end of the connecting shaft is fixedly connected with the crystal manufacturing rolling frame through a screw; the upper end of the discharge pipe is welded with the discharge hole.
Compared with the prior art, the beneficial effects of the utility model are that: this crystallization kettle for valine synthesis has realized the integration of system crystal and ejection of compact structure through crystallization device, temperature control device and the discharging device who sets up, not only makes the structure simpler, convenient to use moreover, and system crystal efficiency is higher, especially adopts the system crystal to roll the mode that frame and temperature control device combine, through the centrifugation to the material with higher speed and accurate temperature control, not only makes system crystal control more convenient, makes system crystal speed faster moreover.
Drawings
FIG. 1 is a schematic view of a crystallization vessel for valine synthesis.
FIG. 2 is a schematic view showing a structure of a crystallizing device in a crystallizing tank for valine synthesis.
FIG. 3 is a schematic view of the structure of a discharge apparatus in a crystallizing tank for valine synthesis.
In the figure: the device comprises a kettle body 1, a crystallization cylinder 2, a crystallization device 3, a temperature control device 4, a condenser pipe 5, a water tank 7, a circulating pump 8, a case 9, a discharge pipe 10, a discharge device 11, a discharge motor 12, an auger 13, a discharge port 14, a crystal-making rolling frame 15, a connecting shaft 16 and a heater 17.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-2, in an embodiment of the present invention, a crystallization kettle for valine synthesis comprises a kettle body 1, the lower part of the kettle body 1 is provided with a crystallizing device 3, the crystallizing device 3 comprises a crystallizing cylinder 2, a temperature control device 4 and a crystal-making rolling frame 15, the temperature control device 4 comprises a heater 17, a circulating pump 8, a water tank 7 and a condenser pipe 5, a cabinet 9 is arranged on one side of the kettle body 1, the water tank 7 is arranged in the cabinet 9, the heater 17 is arranged on one side of the water tank 7, the circulating pump 8 is arranged on one side of the heater 17, the water tank 7, the heater 17 and the circulating pump 8 are fixed in the cabinet 9 through bolts and nuts, a water outlet of the case 9 is connected with a water inlet of a heater 17 through a water pipe, a water outlet of the heater 17 is connected with a water inlet of a circulating pump 8 through a water pipe, a condensing pipe 5 is arranged on the outer side of the front part of the crystallization cylinder 2, and the condensing pipe 5 is made of copper; the water inlet and the water outlet of the condenser pipe 5 are connected with the water outlet of the circulating pump 8; the temperature control device 4 is used for controlling the temperature of the crystallization cylinder 2, so that the crystallization effect of valine can be conveniently controlled;
referring to fig. 3, in the embodiment of the present invention, a crystal-making rolling frame 15 is disposed in a position corresponding to the condenser tube 5 inside the front portion of the crystallization cylinder 2, the crystal-making rolling frame 15 is made of stainless steel, the crystal-making rolling frame 15 is a cylindrical brush structure, the crystal-making rolling frame 15 includes a shaft sleeve and crystal needles, and the crystal needles are radially welded on the shaft sleeve; the crystal-making rolling frame 15 is used for driving materials to rotate, and is matched with the temperature control device 4, so that the materials are centrifugally accelerated, and the proper temperature is matched, so that efficient and rapid crystal making is realized;
referring to fig. 3, in the embodiment of the present invention, a discharging device 11 is disposed at the rear portion of the crystallization cylinder 2, the discharging device 11 includes a discharging motor 12, a discharging port 14, a discharging pipe 10, an auger 13 and a connecting shaft 16, the discharging motor 12 is fixed at the rear portion of the crystallization cylinder 2 through a bolt and a nut, the auger 13 is disposed at the front side of the discharging motor 12, the auger 13 is a stainless steel auger 13, the connecting shaft 16 is disposed at the center of the auger 13, an installation through hole is disposed at the rear portion of the crystallization cylinder 2, the rear end of the connecting shaft 16 passes through the installation through hole and is connected with the rotating shaft of the discharging motor 12 through a coupling, and the front end of the connecting shaft 16 is; a discharge port 14 is arranged at the bottom of the crystallization barrel 2 corresponding to the rear part of the auger 13, a discharge pipe 10 is arranged at the lower side of the discharge port 14, and the upper end of the discharge pipe 10 is welded with the discharge port 14; the discharging device 11 is used for discharging the crystallized finished product;
when the device is used, reaction materials enter the crystallization cylinder 2, rapid crystal preparation is realized by matching the rotation of the crystal preparation rack through the temperature control device 4, and the reaction materials are driven to centrifugally accelerate by the rotation of the crystal preparation rolling rack 15; when the temperature control device 4 works, water is heated by the heater 17, and is guided into the condensation pipe 5 by the circulating pump 8, so that the temperature of reaction materials is controlled; the blanking device drives the crystal making roller frame 15 to rotate and simultaneously drives the packing auger 13 to rotate, and the packing auger 13 rotates to guide the material out through the discharge hole 14 and the discharge pipe 10.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments or portions thereof without departing from the spirit and scope of the invention.
Claims (5)
1. The crystallization kettle for valine synthesis comprises a kettle body (1) and is characterized in that a crystallization device (3) is arranged at the lower part of the kettle body (1), the crystallization device (3) comprises a crystallization cylinder (2), a temperature control device (4) and a crystal making rolling frame (15), the temperature control device (4) comprises a heater (17), a circulating pump (8), a water tank (7) and a condensation pipe (5), a cabinet (9) is arranged at one side of the kettle body (1), the water tank (7) is arranged inside the cabinet (9), the heater (17) is arranged at one side of the water tank (7), the circulating pump (8) is arranged at one side of the heater (17), a water outlet of the cabinet (9) is connected with a water inlet of the heater (17) through a water pipe, a water outlet of the heater (17) is connected with a water inlet of the circulating pump (8) through a water pipe, the condensation pipe (5) is arranged at the outer side of, the water inlet and the water outlet of the condensation pipe (5) are connected with the water outlet of the circulating pump (8); a crystal making rolling frame (15) is arranged in the front part of the crystallization cylinder (2) and at a position corresponding to the condensing pipe (5); the rear portion of crystallization section of thick bamboo (2) is provided with discharging device (11), and discharging device (11) are including ejection of compact motor (12), discharge gate (14), discharging pipe (10), auger (13) and connecting axle (16), ejection of compact motor (12) are fixed at the rear portion of crystallization section of thick bamboo (2) through bolt and nut, and the front side of ejection of compact motor (12) is provided with auger (13), and the center of auger (13) is provided with connecting axle (16), and the rear portion of crystallization section of thick bamboo (2) is provided with the installation through-hole, and the rear end of connecting axle (16) is passed the installation through-hole and is connected through the pivot of shaft coupling and ejection of compact motor (12), the bottom position of crystallization section of thick bamboo (2) that the rear portion of auger (13) corresponds is provided with discharge gate (.
2. The crystallization kettle for valine synthesis according to claim 1, wherein the water tank (7), the heater (17) and the circulating pump (8) are fixed in the cabinet (9) through bolts and nuts; the condensation pipe (5) is made of copper.
3. The crystallization kettle for valine synthesis according to claim 1, wherein the crystal-making roller frame (15) is made of stainless steel, the crystal-making roller frame (15) is of a cylindrical brush type structure, the crystal-making roller frame (15) comprises a shaft sleeve and crystal needles, and the crystal needles are radially welded on the shaft sleeve.
4. The crystallization kettle for valine synthesis according to claim 1, wherein the packing auger (13) is a stainless steel packing auger (13).
5. The crystallization kettle for valine synthesis according to claim 1, wherein the front end of the connecting shaft (16) is fixedly connected with the crystal making roller frame (15) through a screw; the upper end of the discharge pipe (10) is welded with the discharge hole (14).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920988490.9U CN210495300U (en) | 2019-06-28 | 2019-06-28 | Crystallization kettle for valine synthesis |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201920988490.9U CN210495300U (en) | 2019-06-28 | 2019-06-28 | Crystallization kettle for valine synthesis |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN210495300U true CN210495300U (en) | 2020-05-12 |
Family
ID=70581742
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201920988490.9U Active CN210495300U (en) | 2019-06-28 | 2019-06-28 | Crystallization kettle for valine synthesis |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN210495300U (en) |
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2019
- 2019-06-28 CN CN201920988490.9U patent/CN210495300U/en active Active
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